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  • jf500909h Si 001

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    ToddCrahan
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    jf500909h_si_001

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    11 views1 page

    jf500909h Si 001

    Uploaded by

    ToddCrahan

    Copyright:

    © All Rights Reserved
    Download as PDF, TXT or read online from Scribd
    Flag for inappropriate content
    of 1

    Pecan Kernels

    Soxhlet extraction with


    C6H14

    Pecan Lipids Defatted Pecan Meal

    Extraction with
    (CH3)2CO/H2O/CH3COOH

    Acetonic Phenolic Extract

    Separation via
    Sephadex LH-20
    95% ethanol 50% aqueous acetone

    Low-Molecular-Weight High-Molecular-Weight
    (LMW) Fractions (HMW) Fractions

    RP-HPLC Diol Phase HPLC


    RP-HPLC-ESI-MS/MS DP-HPLC-ESI-MS/MS

    Flow diagram for the preparation of pecan LMW and HMW fractions from a Sephadex LH-20 column
    and their characterization.

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