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Predicting the Uniaxial Compressive and Tensile Strengths of Gypsum Rock by


Point Load Testing

Article  in  Rock Mechanics and Rock Engineering · March 2011


DOI: 10.1007/s00603-011-0196-8

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Rock Mech Rock Eng
DOI 10.1007/s00603-011-0196-8

TECHNICAL NOTE

Predicting the Uniaxial Compressive and Tensile Strengths


of Gypsum Rock by Point Load Testing
M. Heidari • G. R. Khanlari • Mehdi Torabi Kaveh •

S. Kargarian

Received: 25 October 2010 / Accepted: 17 October 2011


Ó Springer-Verlag 2011

Keywords Gypsum rock  Uniaxial compressive strength  measurements (Sonmez et al. 2004, 2006) are often used to
Brazilian tensile strength  Point load strength index predict the uniaxial compressive strength (UCS). Tensile
strength may be measured directly, but in practice it is
difficult to do so. Instead, the indirect method of Brazilian
1 Introduction testing can be used, as recommended by ISRM (1978).
The Brazilian test measures tensile strength indirectly by
Uniaxial compressive and tensile strengths are considered developing tension across the diameter of a rock disc that is
key properties for characterising rock material in engi- subjected to compression through a vertical load. In prac-
neering practice. They are determined, directly and indi- tice, however, the test has limitations, and more experi-
rectly, as described by the International Society for Rock mental data are needed to substantiate the correlation
Mechanics (ISRM) (1985) and the American Society for between the point load index and the UCS.
Testing Materials (ASTM) (1986). The point load strength The objective of this paper is to compare all of the PLT
index (PLSI), an indirect strength test, has been correlated methods and their usefulness in practical applications. This
empirically with both the compressive and tensile strengths study presents the PLSI (Is(50)) (air-dried and saturated
of rock. The point load test (PLT) may be applied to states) obtained by three methods (axial, diametral, and
cylindrical specimens, either along the axis, or the diam- irregular), and establishes the relationships between them.
eter, but as noted by Chau (1998), the diametral PLT is We then develop empirical equations relating UCS and
preferred (Bieniawski 1975). In the PLT, rock specimens Brazilian tensile strength (BTS) to Is(50) with the aim of
(of cylindrical, prismatic, or irregular form) are loaded obtaining simple, fast, practical and economical estimates
between two platen contact points, and they fail by the of the UCS and BTS of gypsum rocks.
development of one or more extensional planes containing
the line of loading. According to recommendations by
ISRM (1985) and the standards of ASTM (1986), these 2 Geological Setting
types of failure mode are regarded as valid, whereas
deviations from them are treated as invalid. The Gachsaran Formation (Early Miocene) of Zagros
Although relatively simple, the uniaxial compressive Basin, Iran, is an evaporitic interval comprising interbeds
test is time-consuming and expensive, and it requires well- of marl, salt, anhydrite, gypsum, and very thin beds of
prepared cores. For these reasons, indirect tests such as the dolomitic limestone. Based on lithological variations, the
PLT, the Schmidt hammer rebound test, and sound velocity formation is divided into seven members (Slinger and
Crichton 1959; James and Wynd 1965). The formation was
named in Iran after the Gachsaran oil field, where it is best
M. Heidari (&)  G. R. Khanlari  M. Torabi Kaveh  developed (Fig. 1). The properties of the rocks of the for-
S. Kargarian
mation are influenced by mineral composition, texture
Department of Geology, Faculty of Sciences, Bu-Ali Sina
University, Mahdieh Ave., 65175-38695 Hamedan, Iran (grain-size and shape), fabric, mineral distribution, voids,
e-mail: Heidari_Enggeol@Yahoo.com and the state of weathering (Irfan 1996). The evaporites

123
M. Heidari et al.

Fig. 1 Geological map of study area (modified Gachsaran geological map, 1:100,000, Iranian Oil Operating Companies (IOOC), 1966)

include a wide range of rock types that vary in mineralogy, Ninety cores (perpendicular to stratification) and irreg-
petrography, and engineering properties. Large variations ular specimens were prepared from the gypsum rocks, and
in mechanical properties have been attributed to variations each sample was subjected to three types of point load
in the petrographic characteristics of the evaporites. testing (axial, diametral, and irregular). For each test
Petrographical studies using thin sections of the method, 15 drill cores or irregular samples were prepared
Gachsaran gypsum rocks indicate that the principal mineral and samples were then subjected to the test. Air-dried and
gypsum is cut by veins of micrite, scattered through the saturated samples were numbered randomly from G1 to
rocks (Fig. 2b), but mainly developed parallel to stratifi- G15 for each method. Irregular gypsum specimens were
cation (Fig. 2a). Most of the rocks are relatively fresh, used for point load tests, whilst the preparation steps
although some show a slight discoloration on their surfaces described below were followed for specimens undergoing
due to minor weathering. the compression and Brazilian tests.
Laboratory core drill and saw machines were used to
prepare cylindrical specimens with diameters of 56.70 mm,
3 Experimental Procedures but with variable length-to-diameter ratios (L/D). The ends
of the cores were smoothed to within 0.02 mm and per-
Many rock block samples (40 numbers) were collected pendicularity was kept within 0.05 mm. The UCS tests for
from various locations throughout the study area (southeast fresh rocks were carried out on cylindrical specimens
of Gachsaran City, southwest of Iran) (Fig. 1). Tests on the (L/D = 2.5) under dry and saturated conditions following
samples were performed at the Rock Mechanics Labora- the recommendations of ISRM (1981). For the Brazilian
tory of the Engineering Geology Department of Bu-Ali- tests, additional cylindrical core specimens were obtained
Sina University in Hamedan, Iran. Sample preparation, test by drilling. Disc specimens for the Brazilian test were
methods, and calculations followed the standard practices obtained from cylindrical cores using the saw. Sample
described by ASTM (2001a, b, 2010). preparation and test procedures followed the standards

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Predicting the Uniaxial Compressive and Tensile Strengths of Gypsum Rock

Fig. 2 a Orientation of micrite veins parallel to the stratification. b Photomicrograph of gypsum rock (XPL)

Table 1 Calculated values of


Specimen Is(50) Is(50) Is(50) UCS BTS
Is(50), UCS and BTS for
no. (MPa, axial) (MPa, diametral) (MPa, irregular) (MPa) (MPa)
gypsum rocks (air-dried state)
G1 1.88 0.92 2.24 31.24 5.47
G2 2.10 1.07 1.64 29.03 5.00
G3 1.91 1.29 3.15 29.63 4.39
G4 1.85 0.76 2.70 31.92 3.78
G5 1.34 1.14 1.02 37.36 4.68
G6 1.87 1.84 1.60 35.54 4.12
G7 1.63 1.34 2.07 32.19 4.68
G8 1.52 1.17 2.58 33.69 3.80
G9 2.01 1.16 2.21 31.71 4.86
G10 1.94 1.02 2.42 31.00 5.14
G11 1.30 0.67 1.83 31.04 4.24
G12 2.47 1.03 2.80 32.41 4.00
G13 2.54 0.86 1.58 31.20 3.99
G14 1.53 1.30 1.62 30.22 4.76
G15 1.39 1.04 1.56 33.13 5.09

proposed by ASTM (2001a, b). The loading rate was 1996), the methods suggested by ASTM (2001a, b) for
controlled at approximately 200 N/S. determining Is(50) comply completely with the following
equation for the index:
 
P
4 Results and Discussion IS ð50Þ ¼ F 2 ; ð1Þ
De
The results of the uniaxial compression tests under dry and where P = peak load and De = equivalent core diameter
saturated conditions are presented in Tables 1 and 2. The for diametral and other states (D2e = 4A/p where A = WD,
values of dry and saturated uniaxial compressive strengths and W = the smallest specimen width perpendicular to the
vary from 31.00 to 33.69 MPa and from 17.44 to loading direction). If the sides of samples are not parallel,
29.84 MPa, respectively. Therefore, according to the ISRM W is calculated as (W1 ? W2)/2, as shown in Fig. 3, and
classification (1981), these rocks belong to the low order of D = distance between the platens at failure for axial point
strength. In axial, diametral, and irregular test methods, the load testing, and F = size correction factor, (De/50)0.45
load was steadily increased until failure occurred, and the (Fig. 3).
failure load was then recorded. Although the actual stress All the data used in this paper were obtained from valid
distribution under point loading is poorly understood (Irfan failure modes. Generally, the PLT is the most commonly

123
M. Heidari et al.

Table 2 Calculated values of


Specimen Is(50) Is(50) Is(50) UCS BTS
Is(50), UCS and BTS for
no. (MPa, axial) (MPa, diametral) (MPa, irregular) (MPa) (MPa)
gypsum rocks (saturated state)
G1 1.55 1.68 1.18 23.48 3.31
G2 1.55 0.84 1.72 18.66 4.61
G3 1.97 0.97 1.42 17.44 4.20
G4 1.24 0.98 1.30 26.95 3.43
G5 1.62 0.52 1.02 18.02 2.66
G6 1.11 0.97 0.94 17.46 4.55
G7 1.42 0.85 1.60 29.84 3.61
G8 1.23 0.65 1.02 22.69 3.85
G9 1.26 0.65 1.20 23.37 4.22
G10 1.10 0.96 1.21 21.46 5.08
G11 0.76 0.87 1.04 22.82 5.02
G12 1.25 0.84 1.18 24.13 2.34
G13 1.37 0.94 1.14 21.40 5.06
G14 1.14 1.29 1.23 20.93 2.52
G15 1.76 1.14 1.69 21.11 3.32

used test for estimating the UCS of rock specimens in the pronounced in the axial and irregular methods. Therefore,
field. Although the PLSI (Is(50)) is not easily correlated we can conclude that the diametral method of point load
with UCS, it is the quickest and cheapest way of deter- testing is the most convenient for practical purposes.
mining strength parameters in the laboratory and in the Many studies, for all rock types, have shown that there is
field. no single factor relating PLSI to UCS (Palchik and Hatzor
The Brazilian test methods, as described by ISRM 2004; Barla et al. 2006). Most studies found a linear rela-
(1978), were developed to overcome the difficulties asso- tionship between the two mechanical parameters, though
ciated with performing direct uniaxial tensile tests, and we power functions were sometimes observed. All of them
calculated Brazilian tensile strengths for each specimen showed an increase in UCS as PLSI increases.
using these methods and Eq. 2:
2P
rt ¼ ; ð2Þ
pDt
where rt = BTS, P = peak load, D = diameter of the
disc, and t = thickness of the disc. The results for the
gypsum rock specimens are presented in Tables 1 and 2.
The results were analysed using the method of least-
squares regression. The equation of the best-fit line and the
correlation coefficient were determined for each regression.
First, Is(50) values were correlated with the corresponding
UCS values for all methods in the air-dried and saturated
states, yielding a significant relationship (Figs. 4, 5).
As shown in Tables 1 and 2, in both the air-dried and
saturated states for axial, diametral, and irregular PLT
methods, Is(50) shows a good correlation with UCS. The
equations and regressions of these lines are presented in
Table 3. The irregular method shows the weakest correla-
tion (R2 = 0.89) among the three methods, but it is close to
that of the other methods.
Our work also demonstrates that the diametral method is
more convenient and simpler to use than the other two
Fig. 3 Suggested methods for determining equivalent core diameter
methods. Previous work by Broch and Franklin (1972) also in three methods of point load test, a axial method, b diametral
revealed that the size and shape effects are very method, and c irregular method

123
Predicting the Uniaxial Compressive and Tensile Strengths of Gypsum Rock

Fig. 4 Uniaxial compressive strength versus point load strength index (air-dried state). a Axial method, b diametral method, and c irregular
method

Fig. 5 Uniaxial compressive strength versus point load strength index (saturated state). a Axial method, b diametral method, and c irregular
method

Figures 6 and 7 show Is(50) values plotted against The plots indicate a significant correlation between
BTS for all PLT methods in the air-dried and saturated Is(50) and BTS, and the equations and regressions of the
states. linear trends are presented in Table 4.

123
M. Heidari et al.

Table 3 Regression equations and determination coefficient (R2)


Parameters to be related Regression equations R2

Uniaxial compressive (Axial) UCS = 5.58 Is(50) ? 21.92 0.93


Strength and point load (Diametral) UCS = 7.56 Is(50) ? 23.68 0.94
Strength index (air-dried state) (Irregular) UCS = 3.49 Is(50) ? 24.84 0.89
Uniaxial compressive (Axial) UCS = 10.99 Is(50) ? 7.04 0.92
Strength and point load (Diametral) UCS = 11.96 Is(50) ?10.64 0.94
Strength index (saturated state) (Irregular) UCS = 13.92 Is(50) ? 5.25 0.90

Fig. 6 Brazilian tensile strength versus point load strength index (air-dried state). a Axial method, b diametral method, and c irregular method

For gypsum rocks, the correlation between Is(50) and and they show exceptionally low values of Is(50) compared
BTS values, obtained using the axial and irregular meth- with the axial method.
ods, is significant (R2 [ 0.89). On the other hand, the To index the rock strength of relatively homogeneous
diametral method for the air-dried and saturated states rock material, the diametral PLT is a credible method, but
shows lower correlation coefficients (R2 = 0.87 and it has been shown that diametral point load testing is often
R2 = 0.77, respectively). not reliable in the case of inhomogeneous rocks with non-
Inhomogeneities in rocks are due to: (1) mechanical uniform strength characteristics. Read et al. (1980) and
contrasts between the mineral components, (2) variable Pells (1975) reported that diametral testing on bedded
grain shapes and sizes, and (3) the presence of micro- rocks, in which failure occurs along bedding planes and not
fractures. The presence of one or more of these factors through the rock fabric, gives an unreasonably low estimate
almost always ensures that rocks are inhomogeneous of UCS normal to bedding. This is very clear in the case of
(Valley et al. 2010). In the case of the gypsum rock sam- inhomogeneous rocks where the results of diametral tests
ples, the first and second factors clearly play a part. Het- show a scattered distribution because of the planes of
erogeneities in strength and deformation properties are weakness. We found this same situation applied to our tests
thought to play important roles in the failure of rocks. In when using the diametral method. We conclude, therefore,
the present study, samples failed along micrite veins that the remarkable reduction in diametral method regres-
(diametral method) (Fig. 8a), not as a result of the rock sion can be attributed to the role of micrite veins in the
fabric (as occurs when using the axial method) (Fig. 8b), failure of the gypsum samples.

123
Predicting the Uniaxial Compressive and Tensile Strengths of Gypsum Rock

Fig. 7 Brazilian tensile strength versus point load strength index (saturated state). a Axial method, b diametral method, and c irregular method

Table 4 Regression equations


Parameters to be related Regression equations R2
and determination coefficients
(R2) Brazilian tensile strength (Axial) BTS = 1.36 Is(50) ? 2.06 0.93
and point load strength (Diametral) BTS = 1.77 Is(50) ? 2.57 0.87
index (air-dried stat)
(Irregular) BTS = 0.88 Is(50) ? 2.70 0.95
Brazilian tensile strength and (Axial) BTS = 2.88 Is(50) - 0.07 0.88
point load strength (Diametral) BTS = 2.90 Is(50) ? 1.10 0.77
index (saturated stat)
(Irregular) BTS = 3.47 Is(50) - 0.52 0.86

Test results show that for the diametral method, Is(50) 1. Point load testing on specimens of the Gachsaran
decreases with an increase of (L/D) for short cylindrical gypsum rocks using all three methods (diametral,
specimens. Figure 9 shows the relation between Is(50) and axial, and irregular) yield significant and strong linear
the shape factor (L/D). The earlier numerical and exper- correlations between Is(50) and UCS.
imental studies of Chau and Wei (2001) also showed that 2. Based on these test results, we conclude that values of
uniaxial tensile strength decreases drastically with an UCS can be obtained with a high degree of confidence
increase in L/D for short cylinders (L/D \ 0.4), but using any of these point load testing methods. Since
remains roughly constant when L/D is sufficiently long the irregular method can be applied in the field and is
(L/D [ 0.7), and these experimental observations are, simple, fast, and low cost, this is the most useful
therefore, consistent and in agreement with the predicted method for determining UCS in practice. However,
effects of specimen size and shape on the diametral obtaining reliable results with the irregular method
method. requires a high degree of precision.
3. Although the diametral method is commonly used for
determining BTS, the results of this study show a
5 Conclusions weaker correlation (R2 = 0.87 and R2 = 0.77 for air-
dried and saturated states, respectively) than for other
We have studied the relationships between UCS, BTS, and methods (Figs. 6, 7). The irregular method, given its
Is(50) for 150 gypsum rock specimens, and our conclusions advantages detailed above, is, therefore, more suitable
can be summarised as follows: for a preliminary estimation of BTS.

123
M. Heidari et al.

Fig. 8 Failure types in the


diametral (a) and axial
(b) methods; a the failure plane
followed the micrite vein in
gypsum rock, b the micrite vein
has not any role in the failure
type

Fig. 9 The experimental PLSI (Is(50)) versus the geometric ratio L/D for the gypsum specimen (D = 56.70 mm), a air-dried state, b saturated
state

4. We obtained a predictable relationship between Is(50) represented by these equations. It is particularly


and (L/D). The diametral method is therefore sensitive important to note that the equations used are valid
to the shape of specimens, and the difficulties of only for gypsum rocks from the Gachsaran Formation,
sample preparation mean that this method is imprac- and they are not recommended for gypsum rocks from
ticable for field applications. other regions.
5. The weak correlation obtained for the diametral
method, compared with the other methods, reflects Acknowledgments The authors gratefully acknowledge the anon-
loading along inhomogeneities in the rock that are ymous reviewers for the constructive comments and suggestions
parallel to the diameter of rock cores. which have significantly improved the quality of the paper. The
6. Is(50) shows a strong correlation with UCS authors are grateful Mr. Mirmohammad Miri and Mr. Mehdi Amiri
for the edition of paper language.
(R2 = 0.94) for both air-dried and saturated samples
using the diametral method, but under the same
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Predicting the Uniaxial Compressive and Tensile Strengths of Gypsum Rock

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