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Split Disk Test-Photos
Split Disk Test-Photos
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Nicholas G. Tsouvalis
National Technical University of Athens
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ABSTRACT: In the present study, a series of material characterization tests is carried out on several car-
bon/epoxy filament wound ring shaped specimens. For the implementation of the tests a slightly modified and
improved version of the split-disk test method (ASTM D2290) is used. The modifications of the standardized
test method presented in this work have been applied in order to make it possible to measure not only the ap-
parent hoop strength of the specimens but also the Young’s modulus in the hoop direction. The experimental
procedure consists of testing specimens with various geometric characteristics in order to determine the effect
of the specimens’ geometry on the test results. Additionally, several manufacturing parameters of the filament
winding process are taken into account for the evaluation of their effect on the product quality, by comparing
the mechanical properties of the specimens.
Figure 4. General views of the 100 mm diameter split disk fix- Figure 6. General view of specimens of 100, 150 and 200 mm
ture with the ring mounted on it inner diameter
been decided to set the gap between the two disks fect of the diameter is studied by testing specimens
equal to 5 mm in all fixtures. The small value of this with inner diameter of 100, 150 and 200 mm. The
dimension has been applied in order to minimize the width and thickness of all these batches of speci-
effect of the local bending. mens is the same and equal to 10 mm and 2 mm, re-
spectively. In addition, in order to investigate the ef-
fect of the alteration of width and thickness for
2.2 Specimens constant diameter, one more batch of specimens has
The specimens tested in the present study have been been produced for the case of inner diameter of 150
manufactured with the filament winding method. mm, with width equal to 6.35 mm and thickness
They are all made from the same material (car- equal to 1.52 mm. It is worth noting that the last di-
bon/epoxy) and the winding in all cases is in the mensions are the ones proposed by the NOL proce-
hoop direction. The specimens were categorized ac- dure.
cording to the geometric and manufacturing charac-
teristics in 10 separate batches. Each batch consists 2.2.3 Manufacturing parameters
of 6 nominally identical ring specimens, leading to Another significant issue which was taken into
the testing of 60 specimens in total. General views account is the manufacturing process and its parame-
of the specimens are presented in Figures 5 and 6. ters, which potentially affect the quality of the pro-
duced specimens and therefore, the results of the
2.2.1 Materials present tests. Two of the most important manufac-
12K T700S Torayca carbon fibers have been used turing parameters in the filament winding method
for all specimens presented in this study. As far as are examined in the present work. The first one is
the resin is concerned, a three part epoxy resin sys- the tensioning force that is applied on the fibers dur-
tem has been applied, consisting of Voraforce TW ing the winding process. In addition, the number of
100 Epoxy Resin, Voraforce TW 150 hardener and fiber tows that are simultaneously used while the
Voraforce TC 3000 catalyst. winding is taking place is also investigated. Con-
cerning the last parameter, it is of high importance
2.2.2 Geometric characteristics during hoop winding as it determines the maximum
Several combinations of dimensions have been possible winding angle with respect to the cylinder’s
examined in the present study in order to investigate axis in order to avoid overlapping between sequen-
the effect of the geometric characteristics on the re- tial windings. As a result, the structural response of
sults of the split disk test. More specifically, the ef- the products can be significantly affected. By in-
creasing the number of tows, the bandwidth of the strains have been measured by only one strain gage
filament also increases and, as a result, the maxi- of 5 mm gage length which was installed on the out-
mum possible hoop winding angle decreases. In oth- er surface of the rings, at 45o position with respect to
er words, large filament bandwidth, which is desira- the loading axis. All the aforementioned magnitudes
ble since it accelerates production, constitutes at the have been measured with a sampling frequency of
same time an obstacle in obtaining winding angles 10 Hz.
near 90ο. In the case of 1 tow, the winding angle can In order to extract information not only about the
reach values even higher than 89ο, depending on the apparent hoop strength of the specimens but also
cylinder diameter. about their Young’s modulus, the procedure that is
In the present study three different tensioning proposed by Yoon et al. (1997) is adopted in this
force cases are studied, namely 8, 25 and 45 N. As study. As it is mentioned in the introduction of the
far as the number of tows is concerned, specimens present paper, Yoon et al. suggest that in order to
winded with only 1 tow are compared to specimens exclude the effect of friction from the extracted re-
winded with 8 tows, with all other characteristics sults of the tests, the Young’s modulus should be
remaining identical. calculated as the average value of the modulus de-
riving from loading the specimen up to a certain
2.2.4 Nomenclature strain level and that deriving from the respective un-
The specimens’ nomenclature used provides all loading phase. For this purpose, the present testing
geometric and manufacturing details. All the speci- procedure consists of an initial displacement con-
mens’ names start with the letter “C” which refers to trolled loading until a certain strain level, a subse-
the carbon material. Subsequently, three numbers quent unloading to the zero loading state and a final
follow, that correspond to the dimensions in mm of new loading until failure. The stress developed in the
the inner diameter, the width and the thickness, re- circumferential direction is calculated according to
spectively. The next part of the name consists of the ASTM D2290 with Equation 1 below, where Pb
information about the tensioning force, given with stands for the force that is measured by the testing
the letter “F” and followed by the force value in N. machine whereas Am stands for the specimens’ cross
Finally, the number of tows is described with the let- section.
ter “T” which is followed by the respective number. Pb
“C-100-10-2-F25-T8” is a typical example of a spec- σ (1)
imen’s name and describes a ring with 100 mm inner 2 Am
diameter, 10 mm width and 2 mm thickness, which For both the loading and the unloading procedure,
has been manufactured by applying a tensioning the Young’s modulus is calculated according to the
force of 25 N and 8 tows simultaneously for each ASTM D3039 standard that refers to the material
winding. characterization of flat composite specimens under
tension. According to this standard, the Young’s
2.3 Test set-up and procedure modulus should be considered equal to the slope of
The testing procedure has been carried out with the the stress-strain curve part between 1000-3000 mi-
use of an MTS hydraulic testing machine with max- crostrains (με), as long as the strain to failure of the
imum loading capacity of 250 kN. All tests were specimen is higher than 6000 με. In the present case,
displacement controlled with a rate of 1 mm/min. prior experience (Papadakis & Tsouvalis, 2016) has
Before every test, the inner surface of the rings is shown that the strain to failure of similar specimens
covered with grease in order to minimize the friction is significantly higher than this threshold. As a re-
effects. A small magnitude preloading - unloading of sult, the first loading-unloading phase of the testing
the rings is initially applied in order to improve the procedure is controlled automatically by setting a
ring’s fitting on the fixture. This phase of the testing displacement limit which corresponds to a strain
procedure is not presented here since it has no im- level somewhat higher than 3000 με.
pact on the results and is only carried out for practi- Stress-strain curves are plotted for the whole pro-
cal reasons. cedure that is carried out for every specimen. A typ-
During the tests, the reaction force of the hydrau- ical stress-strain curve deriving from this study’s
lic machine and the actuator displacement were tests is presented in Figure 7, whereas Figure 8 pro-
measured. In addition, the circumferential strains vides a closer look to the hysteresis loop that is cre-
developed on the outer surface of the rings were ated by the loading and unloading of the specimen.
measured with the use of strain gages. Previous re- The fact that, as shown in Figure 7, the curve corre-
lated work (Papadakis & Tsouvalis, 2016) has sponding to the final loading to failure coincides
shown that hoop strain measurements are independ- with the curve of the first loading up to approx. 4000
ent of their position, as long as they are not taken at με indicates that, despite the initial pre-loading of
the unsupported part of the rings in-between the two the specimen, this remains in the linear area and has
half disc sectors. As a result, in the present study, the not been damaged at all during the procedure for the
Table 1. Effect of diameter for 10 mm width, 2 mm thickness,
8 N tensioning force and 1 tow
σu CV EH CV Wf
Specimen
MPa GPa
C_100_10_2_F8_T1 2392 4.5% 150.32 2.1% 77.3%
C_150_10_2_F8_T1 2453 4.5% 147.81 1.6% 84.7%
C_200_10_2_F8_T1 2662 4.2% 155.09 2.0% 82.3%
determination of the Young’s modulus. The hystere- 3.1 Geometric characteristics effect
sis loop for the determination of this modulus is In Tables 1-3 the effect of several geometric
shown in Figure 8. The curve with the larger slope characteristics is examined. Tables 1 and 2 present
(upper) corresponds to the loading phase while the the comparison between specimens with different
one with the smaller slope (lower), to the unloading inner diameter, whereas all the other characteristics
phase, respectively. Concerning the Young’s modu- remain the same. On the other hand, Table 3 pre-
lus calculation, it is achieved with the following sents two identical types of specimens regarding
Equation 2, in which EH corresponds to the finally their inner diameter, the tensioning force and the
calculated Young’s modulus in the hoop direction number of tows, in order to investigate the effect of
whereas El and Eu correspond to the values of the the width and thickness alteration.
Young’s moduli deriving from the loading and the
unloading phases, respectively.
E l E u 3.2 Manufacturing parameters effect
E H (2)
2 Tables 4-7 present the effect that some manufac-
turing characteristics of the filament winding meth-
od could have on the results of the testing procedure.
3 EXPERIMENTAL RESULTS More specifically, in Table 4 the results of three
types of specimens are examined in order to investi-
The results of the tests are presented in the following gate the effect of the tensioning force. These batches
Tables 1-7. The apparent hoop strength (σu) and the of specimens have inner diameter equal to 100 mm,
calculated mean Young’s modulus (EH) are the two width and thickness equal to 10 mm and 2 mm, re-
magnitudes that are presented, followed by the re- spectively, and have been winded with the use of
spective coefficients of variation (CV). The last col- one tow. The same parameter’s effect is presented in
umn of the following tables consists of the fiber Table 5 which contains the results of three more
weight fraction (Wf) for every type of specimen. The types of specimens. In this case, the rings’ inner di-
fiber weight fraction has been measured according to ameter is 200 mm and 8 tows have been used for
ASTM D3171 and is presented here for study com- their fabrication.
pleteness purposes. Finally, in Tables 6 and 7 the parameter which is
examined is the number of tows that are used for the
winding process, for 100 mm diameter specimens in
Table 6 and for 200 mm diameter specimens in Ta-
ble 7.
Table 4. Effect of tensioning force for specimens with inner di-
ameter 100 mm and 1 tow
Specimen σu CV EH CV Wf
MPa GPa
C_100_10_2_F8_T1 2392 4.5% 150.32 2.1% 77.3%
C_100_10_2_F25_T1 2293 7.8% 154.95 2.4% 77.7%
C_100_10_2_F45_T1 2332 4.6% 158.40 2.6% 83.0%
Table 7. Effect of number of tows for specimens with 200 mm Figure 10. Graphical representation of the effect of the tension-
inner diameter, 10 mm width, 2 mm thickness and 8 N tension- ing force on the mean Young’s modulus and the apparent hoop
ing force strength for the winding case of 1 tow
Specimen σu CV EH CV Wf
MPa GPa
C_200_10_2_F8_T1 2662 4.2% 155.09 2.0% 82.3%
C_200_10_2_F8_T8 1629 5.8% 131.13 2.6% 79.3%
4 DISCUSSION OF RESULTS