2132020 TRC | CofA -51SU-41-4 CERTIFICATE OF ANALYSIS 20 Martin Ross Avenue, North York, ON, M3) 2K8, CANADA Tel: (416) 665-9696, Fax: (416) 665-4439 Email:orders@trc-canada.com Website: www.tre-canada.com anada 1. Identification Catalogue 279692 CAS Number: 1216764-05-4 2-hloro-13-opnedid (Heo) Smenym: —2.Gior1-dtydonpropane ts; ee DDDD vo HO OH a Cl D ‘Synthetic. Solubility: DMSO, Methanol Lot Number: sasuai-4 Purity: 8096 Shipping ‘This Product Is Stable To Be Shipped At Room Storage —_—_—Hygroscopic, -20°C Freezer, Under Inert Condition: Temperature Condition: atmosphere 2, Warning Warning 1: Warning 2: ‘Warning 3: 3. Analytical Information Specification: Results: Conforms to structure Conforms Conforms to Structure Conforms ‘Appearance Pale Yellow Oil TLC Conditions: Si02; Dichloromethane : Methanol = 9:1; Visualized with KMnO4; Single Spot, ‘Additional Information: RF= 0.35, 11H NMR and MS conform to structure. (Observed Intensity: 0 = 0.02%, dl = 0.10%, d2 = 0.34%, d3 = 0.00%, d4 = 2.64%, d5 = 94.82% Purity is based on the analytical results of the tests performed. NMR and TLC may have an accuracy +-2%. Isotopic purity is based on mass distribution observed, 4, Signatures Reviewed By Reviewed By CofAApproved By Test Date Retest Date Philip Chan an7pos 4ppspa022 n hitps:lwwuztre-canada comfr-erifcate-of- analysis