Kurva Kalibrasi

X ethanol VS Indeks Bias

1.365

1.36

1.355
f(x) = − 0.020306118268412 x² + 0.005129374734859 x + 1.35423748150859
1.35

1.345

1.34

1.335

1.33
0 0.2 0.4 0.6 0.8 1 1.2

X ethanol Indeks Bias

1 1.3418
0.739 1.3453
0.558 1.3461
0.422 1.3483
0.321 1.3528
0.2 1.3594
0.174 1.3603
0.118 1.3626
0.072 1.3603
0.032 1.3522
0 1.3409
Kurva X Ethanol VS 1/(y-x)
3.5
3.098
3

2.5

2
1/(y-x)

1.5

1
0.431
0.5

0
0 0.5 1 1.5 2 2.5 3 3.5
X ethanol
 sampling

Volume (ml) Indeks bias X ethanol

Waktu (menit)
Distilat Residu Distilat Residu Distilat
0 25 2975 1.3496 - 0.6179
15 25 2950 1.3462 1.3502 0.7658
30 24 2926 1.341 1.3505 0.8756
45 23 2903 1.3428 1.3516 0.8854
60 23 2880 1.3421 1.3526 0.9078
75 23 2857 1.3419 1.353 0.914
90 22 2835 1.3415 1.3534 0.9264
rata2: 0.8418428571

Keterangan Volume (ml) Indeks bias X ethanol

umpan 30 1.3524 0.4488
boil 17 1.3537 0.3266

Waktu VS Volume Distilat

Reyleigh
25.5
X ethanol 1/(y-x) 25 25
25
0.4488 3.232
24.5
0.431 3.098 24
24
23.5
23 23 23
23
22.5
22
22
21.5
3.098
21
20.5
0 10 20 30 40 50 60 70 80 90

5 2 2.5 3 3.5
X ethanol
 t Xd t Xr t
X ethanol 0 0.6179 0
Residu 15 0.7658 15 0.5869 15
- 30 0.8756 30 0.57 30
0.5869 45 0.8854 45 0.5049 45
0.57 60 0.9078 60 0.4331 60
0.5049 75 0.914 75 0.3992 75
0.4331 90 0.9264 90 0.3605 90
0.3992
0.3605
0.475766666666667

u VS Volume Distilat Waktu VS X Ethanol Res

0.7
0.5869 0.57
0.6
0.5049
0.5
0.4331
0.4
23 23 23
0.3
22
0.2

0.1

0
40 50 60 70 80 90 100 10 20 30 40 50 60 7
 Vd
25
25
24
23
23
23
22

Penentuan Koefisien Distribusi

X ethanol Feed X ethanol distilat Waktu VS X Ethanol Distilat
Koef distribusi
0.4488 0.95 0.8418 1.87566844919786 0.914 0.9264
0.9078
0.8756 0.8854
0.9
0.85
0.8
Waktu VS X Ethanol Residu 0.7658
0.75
0.7
0.65
0.6179
0.5049
0.4331 0.6
0.3992
0.3605 0.55
0.5
0 10 20 30 40 50 60 70 80 90 100

40 50 60 70 80 90 100
0.914 0.9264

80 90 100
Tabel 1.1
Data
kesetimb
angan
untuk
system
Etanol -
Air
(Geankop
lis, 1997)

Temperatur Temperatur
xA yA xA yA
O
C O
F O
C O
F
100 212 0 0 81.0 177.8 0.600 0.794
98.1 208.5 0.020 0.192 80.1 176.2 0.700 0.822
95.2 203.4 0.050 0.377 79.1 174.3 0.800 0.858
91.8 197.2 0.100 0.527 78.3 173.0 0.900 0.912
87.3 189.2 0.200 0.656 78.2 172.8 0.940 0.942
84.7 184.5 0.300 0.713 78.1 172.7 0.960 0.959
83.2 181.7 0.400 0.746 78.2 172.8 0.980 0.978
82.0 179.6 0.500 0.771 78.3 173.0 1,000 1,000