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Experiment Procedure Fix
Experiment Procedure Fix
By :
2016
Experiment Procedure
1. Title
Titration of an Acid and a Base.
2. Objectives
3. To determine the concentration H2SO4 through titration using phenolphtalein (pp)
indicator.
4. Basic Theory
Titration is an analytical procedure in which a solution of unknown
concentration is combined slowly and carefully with a standard solution until a color
change of some indicator or some other signal shows that equivalent quantities have
reacted. Either solution can be the titrant in a buret with the other solution being in a
receiving flask. End point of titration is the color change of titrant. Phenolphthalein is
a common indicator for titrations it changes from colorless to pink when a solution
changes from acidic to basic. This color change is very abrupt, and occurs with the
addition of only one final drop of the titrant just as the end of the reaction is reached.
When we observe the color change, the end point has been reached and the addition of
titrant is stopped.
Titration is can use to determate concentration of acid solutions or base
solution. By condition one of the concentration titrant is know. For example in this
reaction:
NaOH(aq) + HCl(aq) NaCl(aq) + H2O(l)
To determate concentration NaOH or HCl use the equition:
ekivalent titrant = ekivalent titrate
VNaOH . NNaOH = VHCl . NHCl
VNaOH . MNaOH = VHCl . MHCl
Information:
V is volume, N is normality, and M is molarity.
Equiptments
No
Name of Equipments Size Total
.
1 Burette 50 mL 1 piece
2 Erlenmeyer flask 250 mL 3 pieces
3 Drop pipette - 2 pieces
4 Graduated cylinder 25 mL 1 piece
5 Funnel - 1 piece
6 Beaker 250 mL 1 piece
6. Procedure
1. Plug the appliance as follows.
2. Rinse burette with distilled water and make sure the fauncet leaks.
3. Rinse burette with a solution that will be used as titrant.
4. Entering the titrant in the burette with a funnel until zero.
5. Add 10 mL titrant in to erlenmeyer.
6. Add 1 to 2 drops of indicator Phenolptalein.
7. Titration is stopped until the color changes are transparent to the titrate.
8. Record the volume of titrant.
9. Repeat steps five through eight for three times.
10. Average the volume of titrant used.
11. Calculate the concentration of the unknown.
7. Data Collection
Titrant volume ...
Titrant concentration
Calculation
8. References
Chang, R. 2005. Kimia Dasar Edisi Ketiga Jilid 2. Jakarta:Erlangga
Subagia, I Wayan dan Suheimi Sya’ban. 2004. “Materi Pratikum Kimia Dasar 1
Experiment Journal
1. Title
Titration of an Acid and a Base.
2. Objectives
To determate concentration of hidrochloric acid through titration with indicator
phenolphtalein (pp).
3. Data Collection.
Name of sudent
Singaraja, Mei 2016
(Name of Lecturer)