TOCT 22692—77 MEXKXTOCYRAPCTBEHHHU CTAHRAPT MATEPHAJIBI YTIEPOXHbIE METOX ONPEJEIEHMA 30JIbBHOCTH Hsaanne odpunnamnoe B3 7-99 MINK H3ATEJIBCTBO CTAHJIAPTOB MocxsaYINK 661.66:543.822:006.354 Tpynna 139 MEXTrOCYRAPCTBEHH HH CTAHMAPT —_— Sees MATEPHAJIbI YTIEPOXHBIE Merog onpegeazenus 302580CTH rocr Carbon materials. 22692—77 Method for determination of ash OKCTY 1909 Hava sseneuns 01.07.78 Hacrosuyti cranapr pacnpoctpatiseres Ha yreponvicrbte marepHaril (Heiprarble KOKCbI, YTOBHEIE M rpadHTosble MaTepHalbl) M YCTAHABIMBaeT MeTOL OFIpeseeHMA 301bHOCTH. Cyutocts Metouia sakmouaeTon B O207eHHK HaBeCKH HcMbTTyeMoro MaTepHama B MycpembHOlt nest i MIpoKaNHBAHHM 3onbHOTO OCTATKa fo TOcTOAHHO# MacceI MPH TeMmepatype (850+20) °C. 1. ATITIAPATYPA Wf PEAKTHBbI LL. Jaa onpesetenus sonsHoctn npumensor: lesb MycbebHyi0 ¢ 9NeKTPHYeCKHM OGOTPeBOM H TepMoperynaTOpoM, oGecrIeHBAIOUIYIO HATpeB sO remmeparypbt (850:20) °C; Tepmonapy mo TOCT 6616, oecreymeaiomyio usMepeHe Temmepatypsi 10 900 °C ¢ noMoutbi0 aueKTpOHHOTO AUcKoBoro HoTeHtWoMerpa Tuma ITDJ{-250 WAM SMeKTPOHHOTO aBTOMATHTYecKOTO HloTeHUH- ometpa Tuna STITI-09 no FOCT 7164, wim MasuiMponstwerpa Tuna MITILIMp-54 M no TOCT 9736, wan Mpyroro peryaupyioulero yerpolicrea TakoTo Xe Ktacca TOYHOCTH; slonoxKu dapipopossie Turta JI3 Ne 3 u 4 mo FOCT 9147; ‘Tura Kopyrmonsre Ne 6; Taran daphopossie HHakne Ne 4 no TOCT 9147; Bechi AAGopaTopHibie ¢ HAaMOOMBILMM MpeneNOM BsBeuIMBAHUA 200 r 2-ro KNacca TOUHOCTH 110 TOCT 24104; ‘oKxeukatop 0 TOCT 25336; TORKY aptoponyio; umatesb; LHTTUBE THTeNLBHEBIe; KAISUMIL XIOPMCTBI TpaHyAMpoBaHHBI WIM TiaBNeHBIt no HL. (Mamenennas penaxnua, ism. Ne 1, 2). 2. MIOJTOTOBKA K ACIIBITAHHIO 2.1. THEM H TOMONKH ROWKHBI GbITb MIPOHYMePOBAHB!, BbICyHIeHbI H BaBeWeHBI. Maccy THrvelt 1 JOMOYeK MpoRepHIOT NepeL KAXAKIM ONPeENEHHEM SOMHOCTH. 2.2, Tpobsi Hedranbix KOKCOB OTGHpaIoT M ToToBAT no TOCT 16799, yronbubix H rpaduToppx Marepnanos — no TOCT 23083. (Hmenenuas pexaxwa, sm. Ne 2). 2.3. TMpo6y ucnuiryemoro marepuaa c pasMepamnt YacrHit He Goxee 0,25 MM nepeMeuimpaior uima~ TemeM WIK TOKKOIE HC paIHOit FYOHHBI HS WBYX-TpeX MecT GepyT B NpeMBApHTeNbHO MpOKAIeHHY!O H BaBELICHHYlO TONONKY HIM THTEN’ HaBeCKY Maccoll, yKAIaHHOH B TaGa. 1. Vinanne odummamnoe Tlepenesarxa socmpeniena © Visnareaserno craxmapros, 1977 © MINK Mazareascrno crannaptos, 2001TOCT 22692—77 C, 2 Ta6anua | Macca naneck, r Or 0,01 20 0,10 | 5 Cn. 010 » 10 | 2 Ce. 1.0 1 2.4, Tpo6y saneummparor c rorpenmoctsio He Gore 0,0002 r. 2.5. Harpenaior mycbensiyio mew» 10 Temmeparypst (850420) °C. 3. TIPOBEJEHHE MCIBITAHHA 3.1, Jlonouky Wm THrenb © HaReCKO MoMeWIaIOT Ha mepeaHHit Kpaii Mycbens. Tloctenentio mepe- ABHTAIOT AOMOUKY B IOHY TlOMHOTO HaKalla My‘heuA, SAKPLIBAIOT ABEKY M MPOKANBAOT AOLONKY ¢ HaBecKOHt pu (850420) ‘C go nomHoro osonenHs, HO He MeHee 1,54. 3.2. Toaouky WAH THTeAS C SOTDHBIM OCTATKOM BHIHMMAIOT M3 TeNH, OWLaKIaIOT Ha acecroBOM aincte Ha Roayxe B TeveHHe 10 MuH AAA THETeI paphopossnx u 1S MUH — JUL KOPYHNOBLIX, a saTeM OMTAKAIOT B OKCHKATOPE [0 KOMHATHO!t TeMMepaTyPBI M BSBCILMBAIOT. (Hameneanas penaxmus, Ham. No 1). 3.3. TIpOKANHBAHWe, OXIAKNEHHE H BIBCLIMBAHME JONGHOTO OCTATKA TOBTOPsIOT, MOKA pasitocTb Mace /{ByX MOCTEMOBATENDHDIX BSBELUMBAHK OyzeT MeHee 0,001 r, MPH 9TOM MpoKAMHBAIOT OCTATOK No 30 mun. [Lia pactera NpHHMMaIOT MlocrenFiee MOKasaHMe B3BCLIMBAHHE. 4. OBPABOTKA PE3YJIbTATOB 4.1. 3onbkocts Memsryemoro Matepuaa (X) B mpoueHTax BEEMMCAALIOT Ho hbopMyuIe mile m — Macca 3obHOTO OCTaTKA, F; ‘m, — Macca HaBecKHM, F. 4.2. 3ombHocTb Ha cyxoit Marepwan (X;) B mpoueHTax BbIucHsOT 1 dopMy:e 100 x 00__ iy 100 ws’ re W* — conepxarine BIArH B HenITYeMOM MaTepHaTe, OMpeeMeHHO!t ro [OCT 27588, %. 4.3. 3a peasyibTaT MCIIBITAHMA NPHHUMAIOT cpemHee apMcMeTRYECKOE PesyAbTATOR BYX NapasLies- HBIX ONpexeNCHMt, TOMYCKAeMBIe PACKOATEHHA MEKIY KOTOPKIMH He AOIKHBI MpeBBULATD sHaxenutit, YxasaHHDIx 8 Ta67. 2, TaGauua 2 Honyckaemsie pacroxaenis, % diss Sonunoers, __ ee eee EE eee 4.4, Eon pacxoxueHHst MexTy pesysbTaTaMH ABYX MapAILICNBHBIX OnlpenenenHii MpeBbIUIAIOT 3Ha- YeHHs, yKaxaNHbIe B TAO. 2, TIPOBOAAT TpeTse ONpeTeMeHHe U 3a pesy!IBTAT HCMBITAHUA MPMHMMAIOT cpeittiee apudMeTuecKoe BYX HaNGoree GIHSKUX pesybTaTOR OMpesteMeHMit (B MIpemenax sOMYcKAeMBIX PACKOxMeHH).C. 3 FOCT 22692—77 HH®OPMAUMOHHBIE JAHHBIE 1. PASPABOTAH M BHECEH Munucrepcrsom upernoii meraxnypran CCCP 2. YIBEPXKJEH M1 BBEJIEH B JEMCTBUE Mocranonsenuem Tocyaapcrweutioro Komurera crannapros Conera Munucrpos CCCP or 13.09.77 Ne 2202 3. BBEJEH BITEPBBIE 4, CCbIIOUHBIE HOPMATHBHO-TEXHMYECKHE JOKYMEHTDI oie aoe a ea| = TOCT 6616—94 ll TOCT 7164—78 LL TOCT 9147—80 LL LOCT 9736—91 Li TOCT 16799—79 22 TOCT 23083—78 22 TOCT 24104—88 | Ld TOCT 25336—82 Lt TOCT 27588—91 42 5, Orpanusenne cpoKa seuicraua custo no npotoKony Ne 292 Mexrocyaapcrseunoro Cosera no crax- aaprusannn, Merposora, H cepraduxanmu (MYC 2-93) 6. H3AHME (mapr 2001 1.) c Hamenennamn Ne 1, 2, yreepxneumnima p mone 1983 r., xexabpe 1987 r. (AYC 7-83, 2—88) Penaxtop P.C. Dedoposa Texsutyeckui peaaxtop B.H. Mpyeaxooa Koppextop 4.C. Yepnoycoea Kommiotepnaa sepcrea AH. Soaomapesoit Hat. mm, Ne 02354 oF 14.07.2000, Cnano » iaGop 22.03.2001. Togmucano 8 newars 03.04.2001. Yen.nes.x. 0.47. Yo.-wan2. 0,37 Tupax 143 9x3. C 687. Sax. 372. UITIK Vonatemcrno craxinaptos, 107076, Mocksa, Koroaestustit nep., 14 ‘Ha6pano 8 Maaatemcree na T1I9BM Oaxnax HITK Vatetemcrno craiaptoa — nm. “Mockoscwri nevantik”, 103062, Mockpa, Jaan nep., 6. Thap Ne 080102