Designation: C1580-15, ‘Standard Test Method for Water-Soluble Sulfate in Soil! ‘ea te in C80 ees ny ie tin ae a 1, Scope 1 This est mated 6 forte deteminion of war sole ste noi 1.2 Tis ot method was develop for connie of arabe safc sos bacon 0.02 and 329 mali tyme 13 This test meth doe ot rine sulin ay form exc ae 14 Sone goveing bade reuse te move of sis ‘rom oe rea ane Is sp the sre sn berate ta comply with leptons 15 The vas sain Sune at be repaid andor. No othe is of ment aloe is rd 1.6 This standard does no purpon 1 abies lof he sefety concer fa. asocoed ith ete te ‘sprain of he wer of thi andar eth eppes rte sry and heath pracces and to determin he plea of replay ltt prir to se 2 Referenced Documents 21 ASTM Siondande™ (i Terminology Relating to Conrete and Cone Ag ‘gees cies Meds for Chemical Analysis of Hyde Cones DIDS pete fn Reagent Weer ag mdchars npr nd Set penne bet grate ek pv lin pe now C0)“ DOE Bio Pratce for Analysis of Meal, Ores, and Reed Materals by Spectoptaony 1275 Prac for Desabing and Metaing Peformance of ‘Urwilt nd Visible Spctopomesre ‘3. Terminalogy 1. For tensors ed in thet mato fro ‘ernaaogy C128 4 Siguleance and Use 4.1 This st mtb can be ed to stein if si cold have an adver reaction with hy coment cont Apparatus 5. Phaomcer-One ofthe flowing given in oer of pcre ‘SLT Nephlonster or ubiimee, 51.2 Speophaamete To eset 20m with igh ph of Ato Semand 5:13 Fler planter wih vl er having & max ‘mum ner €20 nm and ight pa of 419 3m. Fer Pomel and potmetic paces preside hi et fthod ull confor to Practise B40, wecpotomect ates tl olor to Pacis EIS 52 Stopwatch, esse 0. mie 53 Measuring Spoon capicy 021903 mb. 34 Dring ven, cpl of coninuusy heing a se 55 Bone, shal be eagle of reproducing res widhin (90002 gh an acuaty of #00002 Dine icaig Tulane shall hae a senviy not excsting 0.0001 CConetioel tropa balances shal have smi ily eit of OOS Any pid weighing device tat ‘may be provides, suchas chain, dumped to hey ‘ier sal nt ies the Ba lcency by ee tha at any reting ad Wi ay ond wii th ed ‘pect he ane A Sm Chaps eo ope hea std ‘Sony AST wt pram Tce Tae ie Ady Mc Ws Ay pm A fi a inGp crs00-15 56 Sirer, magnetic viable speed, with a, THE- ‘torcaton costed mga ving oan overhear win propel. (6, Reagents and Materials ‘61 Party of Reagnte—AB renga sal confor to te specieaons the Commits on Aas Reagents of he ‘eensan Chemie! Sos 162 Paty of Weer—Unles eerie nde, reference to et shal Seu oman agent ecto te Speieson DI, Type Oder ape waer pe (See Nowe 1 my bens prove fist scene Ua the ‘we of suet ign yy to pits ose woe ‘Uherslyalfting the pit sd tes te tet etd “REN geet 163 Borin. Clorde—Coysals of baium chloride (ac 2,0) serene to AN 0 600 ym To pear te Ahora. seal spt oe 2 luge wach pus, dese {34h een feore ay esas Ul a ot 80 0 600 fi se ore, ‘4 Conditioning Reapet-Plce 30 mL of cocetacd Anrochone nit CL sp p19). 200 reagent wate, 10 IRL 884% hale propel an 5 gsm chide {SGCD i aso Add 30 ma perl a 165 Siete Sain, Sand (tm. = 0100 my SO, Dinatoe © 187 g of anys soi site (0,50. ‘te ud die wth aero Lina volume sk. 166 pH poper adil to eat 5p ws. 67 Sod Hyde, (OIN)—Dislve 4 of sium hone (N2OH) i rae nd te with wat fo HL 168 Hydrochloric Acid (218) 8.6m of concen trad ioc a O41 sp 1-19) tT with wae 17, Permit Variations 111 Both the ile meted snd quid methods as derived Tet Mets Cee permissible as aeratves tote tiie rose. 1, Callpraton and Standariization 1.1 Pepe sandr by dling 00,20, $0,100,150, 200,300 nd f0.0 mL of sada sli slion with wae ib Tod volume ie volume ass These soon wil vests coneatns of 00,2150, 10,130,200, 300, an 00 mg rrp Fallow the poste gen in Stcton9 wing sppopnte motto he andar sae Binion repr. tcteaee ah 5nd prepare first cave showing suf on cota it mg loti ‘inte canespontng plone rang oon Shige ropa i seein ro bes Ua etn Se Pr oat AST eed eM} RODENT 9 2A separ clraton carve must be prepare foreach ior nd ane curve rb prepa seca, {Dchange te sl arp or ter, oe any oe abn of Inorument or reagnts ne made. Chek he eave wih e2 ce fib roming two of more slatons of Known Shit snc nt range Yo 40mg SOL Non 2M spot cane my mea Ww rahe 0 ne soAtearase nae 1 Colt test 10 gf representative slo anal ‘ye simple for 18028 110°. Cra pas 600 Jimena 409m bela bled Sample A put ample sining of spose 30 p Tn a second 00 mesh IneledSupleB place ssl of spreaiatl 3p Record thems of ech ple to threat 0.001 g Add 280 ml of ‘Sooo wate fo ac Beste and ton & magnet ier forte 0 bb 0 more than 12h Pere extn through to ry sou etre er apr ude sein. Do fo wah the reside. Repeat te ato soln is not ou Chest the pi of te eae wing pH per and ode aul each leet pH of 7 = singer 0.18 Het or.N NaOH ‘92 Adj the temper of he solution in the veut task to Between 39 ted 25°C (55 1077 93 Use an alqut of 10 mL for specimen Al, 20 mL for spesimen a, 1m forpcinen BI, and 20m fr spimen Bite 6 wae of 100ml na volute Has od fan th poate tow or To Matode Cts, Por the Too mts a 280 ml boa, Ad 5.0m condoning tengo Ma by eg wih ss bat and apc ati. [Rad 3g of te pop BoC ess using meting {pon and act 94 Sir exacly 1.0 min athe same cons speed or all 195 Remove the beste rom th sie, poor sition ino tte col and pt te ell no the pometer. Record the tary at #0 ar poring the slain mt the oll ‘96 Determine the mg of $0, fom he ean curve 10, Caleaatin o Interpretation of Results 10 Cake the mt coment (% by mas) for ech posinen a flows 1 50, a died si Imo 950, scl fom eration carve tar fsa me 00m eae ue of alga specie. ns 102 Limits of vals fore ob va. See Note 3) on on neate =| PES ay a osname Ant Nf in sinWp c1500-15 1 Deemine which res fl within he above limits 2 Disa tone a et 4. Argel ie hat comply erSteW mph mda of ince sple pe when aon ieee rect pena 1 Report 1 Report the average oid 8% sue by mas of samp. Ilias alate mops of me SO hg Sei sea, many Salty 10 OM Repo ae ‘are: 001 o 10 mph 121 Prcson—Te standard devon was fou 0 vy ith concent, eee cuenta iain wt Sep th i. AST et ng ‘eet cos eco ‘sod fr the poke. The ingle operator cece 1 varation Wa oun be 8. Teer ol fo rope cndated es by the sae operate the ste Final shouldnt fer by more tan [24% of he verge The mullabortay cots fw was food tobe 212% Therefore esi of two dirt ibs dene sper of» tel shoslé no die fro ech ‘ter by ore tha 60 5 of tl averse 122 BiesSive tere & 90 scape reference male suinble for deteminng Bis, bas an 20 be dried, 13, Keywords 13. hyde coment si Sue; mite ANNEX ‘taney Information) ‘A, REDUCING THLE NUMUER OF SUD-SAMPLES AND SAMPLES OUT OF COMPLIANCE. AL. This proofre was wie to sccommote aon ‘itt are ot familar wit the a aoder tet per Toop caval alse number of sub sampe, nor ‘uns many be we AL2 If sample fils above 3.3 ali, hn iit ‘mpi mise dor itn canbe ued I is proce 'S flowed han he mg SO, rom the tins ead ‘all be manne win to 40 mgt saber procodare i usd, then vation wal be povided showing hat tbe ‘sls re win he nea geo he eabraon SUMMARY OF CHANGES Commiase C19 hs idee the loeation of selected changes w this et method soe the Int ae, (SH00F", ut may input he ue af Bs med. (Approved Ox |, 2013) 1) Ries Sesion So AST ard Ta 21 EDT NE ‘Seemahy AST ti eed Mr KBEDTIIS Parry te ts Annet Aran er pti ian‘Standard Test Method for Rapid Determination of Carbonate Content of Soils" “hs nen deri D7: ie ty vi nin ne po 1. Soper This teat mead cover he determination of carbone viet of sis ad at ock wich canbe realy broken ‘downy mshi efi asa mathd tha ses Sipe poral appr, Rete sould be ary aed ‘Ge ene eqn percent because ere erbonste species coer ane age of cent cle equalea as ‘own below fr 2 mur of eon mate ™ For example, 1004 dolomite woul be expected yield 1086 8 ale equ while 100% sere would eld ly 864 aie equale Cale and aragonite actos Sl pslly compl within stout 0 mists. Ts eed tes not dsingith mee the cane spc a ‘Atcoinaion must be nade sing qenaive emia analy ‘Stood sucha ami aero, 1.2 Unls—The vals sed in ST unis art be eared 153 All observed ance ales al conform oe uns for Sit digs sed rounding established in 131 The poceduesust oc how date cota scone or eles, nth Handa! sre ropa 38 De {ndusey standard In aiion, hey ae representative of te signi cigs dat gral shold be eine. The pose ‘airs wd donee coma fal vara, purpono for ‘heainng techn spr pupos ste, ay come tron forthe ees obec and common prc fneeae rece signe age of repo dna to Be ‘pattie eben Denys omens with hte onions ibeyond the sop is standard wo consider sian ised aay Iethds fr enineing desi 14 This stad doesnot po 10 ars ll of the safety concern, ny. sso with ie att the eypnsiy of the at of headed fo eal apres rae sry and els practice and deemine he sptios= bitty of mutton Hntations par to we. For Spee cco sateen, see Sect 8 2 Referenced Documents 21 ASTM Sendak seat Mets for Chemical Analysis of Limexone, Qulekline, nd Hydted Line ‘gS Terminclogy Relig to Sol, Rock, ad Cnuined HOA? Tet Metal for Isle Rese ia Catente Ages DEMO Pactoe foe Misimar Regiments fr Apecies Engaged in Tsing ane Inspection of ol and Rock a5 Used Egieeie Design and Canstucon ‘DATS Gade for Ealing Seletng. a Speriyng Bak tices and Sandud Naser for Us in Sl, Rock, 28 Conuton Mitel Testing ‘eons Pate fe Using Sgt Digs in Gotti Date II Speciation fr Woven Wie Text Sieve Cloth an Test ‘eres aS Seifeaton for Gaviy-Cemecton and Foret 2 Terminology 31 DeftionsFoe dinions of common tn ems se ns standard flr to Tero D638 4. Summary f Test Method 4.1 The carte conten clit equivalent) of sil is “deerined by treing 3 I ed sol specimen wth yo ‘hoo acd (CD ian erlsed eto einer (eat, hommes Cha in ott a of ard Soom pn mag eT Ph ey A Way ute Ae fate tinQp ossrs—14 Carbon sionde (CO, gu i evolved ding te ention eeen the acid ad arent ton fhe specimen. The resulting pressure peered in te cel reac Is propor: tonal Gee lg 1 ote ele equivalent of he specie ‘ih agen ga atm coma S. Signifcance and Use ‘5.1 This tet mtd is to dtrine he pesene and nity of carbonate sil pines ne fhe ele Suivlene. Te met x general iene for wen index of approxi carbone cata 1 wi with care ang marine ss. Ot st eto ei (ch ss Meo (C25 and Test Mad D301) to eve ctu exbnaie evivalney fr purpose of chrcering we of cles ‘terials ssl mete: or actual ing materia SL Calcium eutomts (CACO) ae known eeting age sie pt <7, and a Be 52.1 1 low carbonate coments clit eqivaeats) ae mesure te wae dees not know wher the sla fn ‘abort cote acon couse, wir, ad thee, ‘care carbo specs whone eas wi hye eid re eer vary lwo he. ‘522 Tsing ties maybe enlesve Gong tan 1 hou?) for some catonte pels (uch a dolore) cle ‘sven win abort 1% ae eed, 1523 The ees of pcinen gin sa, drain of tng i and specimen mas ae diated ne Hasire Non 1—The git tah pnd by hi tad it sept Eom he ets eran ‘SEs of ceo a alr es Age a ee ‘Sa af eee Bt we ply et pti ong Shel sci Bsus bio cs nt ae ‘iro pee oi Spend nr tne Pe ross mm of sng seo eh 6 Apparatus (61 Rapid Crbmae Arter schematic rong ofthe api exboete aly Is shown i Fp. 2. The We omens of he spars blue "SL Reaction Chnder (Reactor) with tae cap a ‘sting sea Yo enone the evince clear plac eye allows vag oellervesceat ection (612 Prature Gage (Bauder Tube-pe oF Electronic Pretre Trader) 70 Xs (10 pl wah an ey OF (033 and a ean of 03 3a i ps. “613 aed oral Conlon or Both of cla pai wih 2 tall hande to hold20 ma ld Opty nao a, of ‘place of the adenine, use ssl ona feet nso ol theo peimen Ac aed ody sft fs consceabt sping and we ofa comme rede ‘psig before ractor wld 1711 ype abrton Cur for 0374 Test Cal an 74Pa (1p PrenreGnge Sent AS wt re ee 820 ‘Rea ty hc Was Ay put Le Aye te pi tin‘F,2 Senate Drawing of Rapid Caton raat 6.14 Pram Relief Ve, for ele rl of CO, gs pee 62 Balnce—The balance mest met the eles of Specieaton D473 a ths soto A Chats GP bance ‘ha niu caty of 00 gan a edaity of O01 [srequrel to este te Sl mas {63 Dong Over trermstaelly-comzle, pet of the fret type, mating th regener Splice ton E148 ahd expat maining t wf epee ot 19 "5° troupe! the dying chant. {64 Sieve—No. 40 (25 yon) Fieve at confers to ihe eguiement of Specfeaon Et. 65 Mortar and Rubber-Coveed Pestle (Optional) Apr sal for belig op agent nr ‘epics without being ini paris. {6 Mechanical Aton Dec (Optienall~A plato, est ston osm pe sake bang» yay. otal, "eipoeatg or sr min tt he cto res By coninotlyapating the soking sa, 67 Graduated Cinder Fas, Piet, or the Ute—A hs of equivalent ne device its eough capac fo ld 20°" 2a hyo ald and real 1 the ate (68 Mscelaneous mses ich spa, 00, amen ay Be afl 7 Reagenis 1 Parity of Rengens—Reagent ue cial alte sed inal tes, Unless teri nes, i tended that tegen sl color othe pein fhe Commit tee on Alva Regent fhe American Chem Sosy ‘thr suc peietone ae aaa 12 Cale Carbonate (CACO). Reagent prado (8 100°) fer eateaon of easton ender, 13 Hydrochloric Aeid (HC, Gn abot 1 sluon — pare 1 L of aboot | N aston by pacing #0 mk of once, eaent rie HCl shew $00 mf ded far (p= ina HL volute fs. Die the mark ‘tt commer grade dtd water: Ste pebene oul: Fate reaction tines my achieve by Instsig the ncenaion fo higher normal slons (upto about 3 ‘elton, Hysreclone elds alo commensal stale in STN eon. 74 Water—Diailod or deminer water iste oly pecmisble ws uid ‘gen ny tanga, Sr guar sag sg ot ty Piet at ats uy pene ge he pi iQy vaste 14 Hazards 1.1 Use cae in hing the hdc wid 0 at n0 cid i spilled one skin coin. Ifa eons he ‘Sin or en medal sh with age qenin of we Process connie byte aid beeah abortry oud or in welled env ede he inblaion f 182 The prewar re valve of the caboose alae should be oad folowing each tt sia as restr fo tht he eap cat be afly removed 9. Test Speciens 221 Slot $10 10g peimens rn coe o suze gab sample Oven dy a 102 5° fora period o 121028 hes. Puwesie the enue simple with = morte and pes of ames vat ll fe pars ps a No, 40 (045mm) or fice seve Sai als react Caster tan lage prices ‘when eed with 98 10, Caltraton 1041 Calton is ascomplited by aring regen rade ‘¢xC0, oabin the rato etn temas of CACO, Sth prs ene int cnsant ome ee Each ‘Some oar ar press pge xual arate. Prepare ve ses of cape specimens wi he following 10.12 Ser 20 specimens at 04 £ 001g TOLLS SerThwespecnens at 6 = 001 & 10.1 Ser4we specimen at 8 ¥ OO 10.13 Ser5—Twempesimen at LD = O01 102 Price the spcinen ino the rector (sng sil come taine wv) h8 30 © 2 ma of el salu I e stor atng deiner avaiable) Sal te ect Wi {lpeop and Cont per ee valve Tk erator 1 Inka ration tetveen the and specie. Mi te ‘hates by ering or ee shaking I aval, pace be feat on mechan apo device forthe ron of he 103 Ie rye hat hen ate pode wil completely reat in lee than 1 mito. Thor, Ss 6 Inenior the psu to vel hat the reaon comple (Gress li) a con ha eect popes ‘Saed ressre ene ot ders) Record te pressure ‘Rating oth earot 0 EPs (Lp o Bete. 104 Ope he prasar ease vale and renavethe ctr twp cap. poe othe cans and te te ete with 10S Repest 102 Hough 104 for renaising calibration 106 Data roc may ee anyon or al of the fooing {06,1 Make a gph of pereoncalte eulvalet (ne rs fel aed ese presse appropiate unit for the mge wed ty 457i Wy AINE 4 1062 Calton dats my brane the fice ofthe eestre gauge fore eng of prone eguvalet Tiaown Fe. 10:63 Ue a eat se erin ft of he elation ats arive tn equate for eling epee ate feels tom he pes da 1, Procedure 1st Selecta 00 gspcinen rom the plese x follow the procedures Sache i 102~ 10 obtain fact mexssrement of the ste egal. fee 180 esate renponse, butt ino eferesceat rect I ‘ered repeat experi wih 2= ODI g. 5 O01 g GrlO O01 g of ary sos Inte rece and vide i ‘Seton reading by 25 1, respectively oo the te ‘Slee eave 112 After mine reaction tne, real he pressure salto ohta be carbonae cone one wishes ovate ‘haber eter aoa sek ar preset skein Teanga show 113 113 Comin reading pease ute rection is com plete wing the flowing citer) Te Gnge In eae iva ee han 03 over a 1Omint ine pcod fe ‘Shing ime upto 190 mirror (The charge nee piven ss than 5 over a Smit ie pciod fo tein time peat ha 120 lots, 1A Take he pete ing abi shove an deter inne the comepending pect calc equivalent frm the (ha edcton mato chen 10. to un te Carona ‘Coment (percent cae eaaen. 12. Reports Text Daa Shiets/Foemis) 12.1 Te methodology sd to spec) tow un are re corde che et dt shor assed blow ‘over ia 13. 122 Record aa minim he following genera informa ona 221 Record the Caonte Coment (peceat alee piled oe teas 1 2.22 Lin sample sous, projet name and Jcaton GF 720.3 Recor he mass the ls specimen oe nearest 001 gums 12.4 Record he ecicnopetr name oii and 13, Precision an Blas 13.1 PreciiTest da on pesos int presented to the sue of the ol and ck mater ody AS teh I iter nt ese oo cae a hs ime ave {Gn or more boner erp in roun-0in fesing. [progr Als tetera feb cto calf produce ‘ape specimens at have for pyseal pees. Any ‘rion ‘bard in he ita Js ly to bed {pesinen vation 1 erator O boating va Rated at was Aan penn me Aye ere indMp 1070-14 1.11 Subcommitee DIB seeing ay it fom the ses fies mate ht might he a oe ied Stone on rection 132 Blas Thereo acoepa ference vale forth et mths hte, ie sat be smn. 133 Sone information o pertmance satin of is et Is povided inthe ere? naga eer Ger a ny ‘Karat ee sa fon Say A a 14, Keywords 141 ales sis nite eu’ atone cont ‘sana Bombe: arin is SUMMARY OF CHANGES 14 monde wits Commitee D8 poly ns seton Metis theocation of hanes this ana ice "he at tition 200 Reappeoved 2007) tt may nar ewe ol hs saad (1) Mino eral change in 1,133,102, Seton (2) Aated reteeace to Tet Method D082 and Speen Ein Sestee 3 (@)Renaved dimension eqemens of lop. a sive ‘and various miscellneoe appar ens n Seton 6 (@) Aad clasteions on reagent grader for CACO, and ‘ttled water in Seston 7, (5) Renamed Secon 86 Hazard, (@.Clunteaion on dtrmination of crore content in Seco I (7) Revision of Sect 12 for clay of Report requirement. (poe. on Prsion goa oto ty of tr i tn ce i em sR tae a a eosin fa Se ay ns waa Sent AS ag mere Wag OSES g i ‘a vs ype mL pent Nite pik137 ren: 1880 See re =o scmenmanmeamentens Beier serenemscatst Bm eeens SEESewe, 80 coyote by ee ts wed oot 34 925127 rent 10