Cy MEDCOENERGI Oil &Gas GUIDELINE QA QC STIMULATIONNo. Dokumen : COP-PED-GL-02-PE-PE4231400 MEDCOENERGI Oil &Gas Tingkat Dokumen : 2 Judul Dokumen —_: GUIDELINE QA QC STIMULATION Pemilik Dokumen _: PETROLEUM ENGINEERING DIVISION (PED) Nama Jabatan TTanggal_| Tanda Tangan jj _| Senior Production Disiapkan | Ahmad Sujai Engineer 20.0 dei oleh: ‘maxi y | Technical Support Meru TrisektiH# | feo Diperiksa Technical Support beh, | ae Manager Manager Production Noviadi Istono Engineering PutiPermata | EOR Manager Producing Assets 7, hore Sonny Andrianto | Reservoir Engineering | (3 'f } uk | Manager Ss Exploration and Ahmad Toha | Development assets foo‘ Reservoir Engineering | 7o% J Manager Disetujul Petroleum Engineering oleh: __| Herman Sanitioso | conior anager has me =[ No. Dok: COP-PED-GL-02-PE-PE4231400 Rev. 01 | Him ii dariv GUIDELINE Tanggal: 20 Januari 2016 QA QC STIMULATION & Tidak ada bagian dari panduan ini yang boleh direproduksi, disebarluaskan, dan/atau disalin dalam bentuk apapun atau dengan cara apapun, termasuk dengan cara memfotocopi tanpa Persetujuan tertulis dari Medco E&P Diterbitkan oleh Medco E&P Jakarta, IndonesiaNo. Dok: COP-PED-GL-02-PE-PE4231400 GUIDELINE Rev. 01 | Himiv dariv Tanggal: 20 Januari 2016 GA OC STRUCTION MeocoFena LEMBAR REVIS! No.Dokumen — : COP-PED-GL-02-PE-PE4231400 Rev: 04 Tingkat Dokumen: 2 Judul Dokumen : GUIDELINE QA QC STIMULATION PemilikDokumen : PETROLEUM ENGINEERING DIVISION (PED) CATATAN REVISI INISIASI OLEH | TANGGAL Semua Format template guideline Ahmad Sujai BAB VIII Di tambahkan BAB IX Di tambahkanNo. Dok: COP-PED-GL-02-PE-PE4231400 GUIDELINE Rev.01 | Him dariv Tanggal: 20 Januari 2016 QA QC STIMULATION Vil vil, DAFTAR ISI PURPOSE s.:cctcnirseicsesstocerrrcsan SCOPE... DEFINITIONS. RESPONSIBLE.......... TECHNICAL GUIDELINE Introduction. Stimulation strategy ............. Objective of Stimulation .......... Type of Stimulation technique. ‘Stimulation technique selection guide Acid Stimulation Quality Control Guide ... Acid Stimulation Safety Fracturing Stimulation Quality Control guide KNOWLEDGE) TRAINING/ REFERENCES: REVIEW AND UPDATE.......... REFERENCE ATTACHMENT... Stimulation Decision Tree : Safety and Safety Checklist for Acid Jobs. Fracturing Treatment supervision and quality control guide Zo™moom> O MencoENeRe!No. Dok: COP-PED-GL-02-PE-PE4231400 GUIDELINE = Rev.01 | Him1 dari 50 2 TION Tanggal: 20-Januari-2016 oh oceans MepcoExera! 1. PURPOSE This document will provide stimulation guidelines to obtain optimum production and overcome the negative effects of each productive layer. IL, SCOPE This document will provide stimulation guidelines with more focus on quality control and assurance including safety guide to be used before, during and after stimulation treatment. The details of stimulation design, knowledge and technology are outside this document and that should be obtained by independent study, attending course/ workshop, attached to stimulation projects and/ or mentoring program, II]. DEFINITIONS Completion Strategy — A well completion is usually defined as the final string of casing, the production tubing and associated downhole equipment, and the specific arrangement of these components. IV. RESPONSIBLE A. Senior Manager of PED Division (L3) 1, Reviewing documents of the guideline. 2. Ensuring that the guidelines and supporting documents approved, distributed and updated. 3. Evaluate management system completion strategy guidelines. 4. Review and revise the guidelines, B. Manager of PED Division (L4) Identify the need for the in operations, Initiating document creation according to the requirements guidelines. Reviewing guidelines to its operations. Ensuring the implementation of the guideline in operations. Ensure that guidelines in its operations are reviewed and revised in accordance with these guidelines, 6. Ensuring that the control in strategy operations are the latest guidelines (update). 7. Assign qualified personnel to design / modify / update guidelines. €. Lead of PED Division (L5) ye ene 1, Creating a guideline document to its operations. 2. Completing and updating guidelines strategy.No. Dok: COP-PED-GL-02-PE-PE4231400 GUIDELINE Rev. 01 Him2 dari 60 CF Tanggal: 20-Januari-2016 QA QC STIMULATION eocoberc ve 3. Checking whether guideline documents used in the field is still valid and is the latest revision. 4. Verify field activities carried out in accordance with guidelines. 5. Overseeing the implementation of the guideline, 6. Review periodically and revise the guidelines in the department. D. Engineer of PED Di sion 1. Create a draft and revise the document. TECHNICAL GUIDELINE A Introduction This document will provide stimulation guidelines with more focus on quality control and assurance including safety guide to be used before, during and after stimulation treatment. The details of stimulation design, knowledge and technology are outside this document and that should be obtained by independent study, attending course/ workshop, attached to stimulation projects and/ or mentoring program. Stimulation strategy The application of a stimulation treatment: © When the well is declining in production or injection and it is concluded through an analysis that the declining is because of formation damage around wellbore then a stimulation should be considered. © When the formation will not produce at a rate equal to the expectations for the project and it is concluded through an analysis that the formation will not produce because of low permeability and/or severely damaging while the reservoir pressure is still high, then a stimulation should be considered. If elther of the conditions are met and there are sufficient reserves remaining so that the increase in production or injection will pay for the total cost of the. stimulation, then the treatment can be justified. Objective of Stimulation ‘The primary objective of well stimulation is to increase the productivity or to restore the flow capacity of a well by removing the near wellbore damage or by superimposing a highly conductive structure onto the formation. Type of Stimulation technique 1. If the objective is to restore flow capacity of the well due to formation damage, the stimulation technique could be: a. Wellbore clean-up Wellbore cleanup is commonly used to remove scale, paraffin, bacteria or other materials from the tubing, casing or gravel-pack screen,No. Dok: COP-PED-GL-02-PE-PE4231400 GUIDELINE Rev. 01 | Him3 dari 50 CF QA QC STIMULATION Tanggal: 20-Januari-2016 MeocoENenat ‘These treatments normally use acid or solvent systems that are placed in the wellbore area to soak. There is no injection to formation, * Sandstone: Flow acid to the bottom of the tubing and flowback underbalanced treatment * Carbonate: Bullhead of fluids to bottom of perfs and flow back underbalanced treatment Key parameters in treatment design are the placement technique, chemical selection and soak time. b. Matrix treatment acidizing Matrix stimulation is a technique in which a solvent is injected into the formation to dissolve some of the materials present and hence recover or increase the permeability in the near-wellbore region. Matrix acidizing has application in both carbonate and sandstone formations. In sandstone formation, matrix acidizing treatment should be designed to remove or dissolve “acid removal” damage or plugging in the perforation and in the formation pore network near the wellbore. In carbonate formations, matrix acidizing works by forming conductive channel, called “wormholes,” through the formation rock. These penetration beyond the near-wellbore region, or extend from perforations. The nature of wormholes created depend on injection rate, temperature, and formation reaction characteristic as well, In carbonate formation, matrix acidizing is principally a “damage bypass” treatment. If a carbonate formation is undamaged, matrix acidizing treatment probably cannot be expected to do more than double the production rate. 2, If the objective is to improve permeability or to create new flow capacity from the reservoir to the well, the stimulation technique could be by fracturing the rock and leaving very highly permeable fractures by the use of proppants or acid etched wralls. a. Acid fracturing ‘Acid fracturing are generally confined to carbonate formations. Acid fracturing treatments of carbonates are conducted either to bypass formation damage or to stimulate undamaged formation. This can be include vugular and naturally fractured chalks, limestones, and dolomites. Acid fracturing is an alternate to hydraulic fracturing with proppant. ‘The acid fracture main principles: + The downhole injection pressure must be higher than the * Formation fract pressure.No. Dok: . a a COP-PED-GL-02-PE-PE4231400 GUIDELINE = Rev.01 | Him4 dari 50 ee Q \C STIMULATI Tanggal: 20-Januari-2016 oo ION MeocoEnenct © The acid must be reactive with the formation. © This will lead to etched walls. * The formation to be fractured must always keep integrity, in order to not collapse the fracture. b. Hydraulic (propping) fracturing The objectives are the same; the creation of a long, open, conductive channel from the wellbore, extending deep into formation. The basic principles of fracture propagation and geometry are also the same. The difference between the two fracturing is in how fracture conductivity is created and maintained, Hydraulic fracturing uses Proppant (e.g. sand) to hold the fracture open. Fracture acidizing does not use proppant. Fracture acidizing relies on the etching of fracture faces with acid to provide the required conductivity. Acid is injected into a fracture created by viscous fluid (pad) or itself used to create the fracture. As acid travels down the fracture, acid is transforted to the fracture wells, resulting in dissolution etching. If the etching is nonuniform (differential), then the fracture may close with conductivity retained, as there will be low and high spots — voids and points of support — holding the channel open. E. Stimulation technique selection guide There are many factors that may influence selection of the stimulation technique. Attachment-1 provides a decision tree to help the process of stimulation selection. The selection is begun with a valid well for stimulation, As for identification of a valid well for stimulation will refer to COP-PED-GL- 02-RESENG-007 "Guideline for formation well damage evaluation, prevention and remedial work", Rev 01. ‘As shown in the figure, the productivity target, lithology, operational limitations and various other considerations dictates the stimulation technique. Normally the productivity target dictates the stimulation technique. For example, if 2 90% reduction in skin effect in a sandstone yields the target production, then matrix stimulation will probably be the most Cost-effective technique. If matrix stimulation cannot be accomplished, then the feasibility of using propped fracturing should be evaluated. 1. Matrix Acidizing Treatment If the productivity target can be reached with a skin effect of 10% of the original damage skin effect in sandstones and -2 to -3 in carbonates, matrix stimulation will be adequate and probably cost effective. In sandstone reservoirs the only stimulation alternative is hydraulic fracturing. In general, high damage skin effect and a large reservoir permeability (K-10 md) would indicate matrix acidizing.No. Dok: (COP-PED-GL-02-PE-PE4231400 GUIDELINE Rev.01 | Him5 dari 50 — Cy marr aoc STIMULATION Tenggal: 20-Januari-2016 aA.08) i MencoEvenat In unconsolidated or friable sands, it is advisable to examine the maximum pressure drawdown allowed before formation production. This drawdown limit may lead to the selection of fracture stimulation to allow obtaining target rates at a lower drawdown. On the other hand, concern about zonal isolation may preclude fracture stimulation. If vertical fracture growth into an aquifer or gas cap cannot be controlled, matrix stimulation may be indicated. 2. Propped Fracturing treatment The following factors may suggest consideration of a propped fracturing treatment: © HCI solubility is low (< 65-75%) * The carbonate formation is homogeneous (pure limestone) © Acid reactivity is low (low-temperature dolomites; <150°F) * The rock is weak and/or it has a very high closure pressure, resulting in poor retention of acid-etched fractures Permeability is very low (k<1 md), requiring very long fracture length Propped fracturing has an advantages for many carbonates. The leak-off coefficient, fracture shape, and proppant conductivity can be estimated or measured with a greater degree of confidence than for an acid fracture. This because the fiuid is nonreactive. A pretreatment data data measurement frac (mini-frac analysis) is an established technique used to generate appropriate design parameters for propped fracturing, In deep formation with high closure pressure, proppant may create a more conductive fracture than can be retained after closure of an acid- etched fracture. This is also true in shallow, soft carbonates. A propped fracturing treatment may create a longer effective fracture length because fluid properties, especially leak-off, are not compromised by reactivity. In naturally fracture carbonates, propped fracturing may not be appropriate because of difficulty of placing necessary amount of proppant. The tortuous paths often present, and the complex stress properties, can result in fracture geometry that is so complex that is become impossible to maintain proppant injection, 3, Acid Fracturing Treatment Factors that may suggest consideration of an acid fracturing treatment are: * The carbonate formation is predominantly naturally fractured, which could lead to propped fracture complications * The formation is heterogeneous, with porosity and permeability streaks that are conducive to a higher degree of differential acid- etching of the fracture wallsNo. Dok: | COP-PED-GL-02-PE-PE4231400 | GUIDELINE S Rev. 01 | Himé dari 50 Qy = STiM Tanggal: 20-Januari-2016 Ae aE ATON MencoEnenat + Formation permeability is good, but formation damage is exists + The well will not mechanically accept proppant * Hard (not soft) carbonate formation with > 95% soluble in acid system. Advantage + In general, acid fracturing is the more conservative treatment design because proppant is not pumped. * The risk of failing to complete the treatment is also much lower. © There is no risk of premature screen-out, which can leave the fracturing tubing string full of proppant. © There is no risk of the consequences of proppant flowback. * Quite often less expensive that propped fracturing, especially in deep wells, * Therefore, acid fracturing should probably be considered first and ruled out before choosing propped fracturing. * Acid fracturing can create conductivity to, but not within, an undesirable sand stone or shale interval. * Furthermore, if effective etched conductivity can be imparted, flow turbulence in the fracture would be expected to be less in an open acid fracture than in a fracture containing proppant. Disadvantage: * A disadvantage of acid fracturing is that controlling the leak-off rate of reactive acid in a fracture is very difficult. Without benefit of field experience in a particular formation, predicting etched conductivity and fracture length with a higher degree of confidence is not possible. This is due to unknown leak-off characteristics. F. Acid Stimulation Quality Control Guide Incorporating quality control measures during all aspects of an acid job can make the difference success and failure. Quality control monitoring only during the actual pumping of the treatment is not sufficient. In addition to the pumping stages, quality control steps must also be planned and executed during rig-up of equipment, before pumping, and after pumping. 1. Quality Control During Rig Up Inspect all tanks which will be used to hold acid or water. The tanks must be clean. Small amount of dirt, mud, or other debris can easily ruin an acid job. b. Make sure the service company has the equipment to circulate the acid tank prior to pumping.GUIDELINE © Rev.01 | Him7 dari 50 Gy IN ‘Tanggal: 20-Januari-2016 ere MeocoEnenst c. The line to the fit or tank should be laid and ready to connect to the wellhead so the acid can be backflow immediately after the end of the ‘overflush. 2. Quality control before pumping a. Check service company ticket to be sure all additives for the job are ‘on location. b. Circulate the acid storage tank(s) just before the a the well. cc. Check the concentration of acid with a test kit. is injected into d. Make sure the service company personnel know the maximum surface pressure and stay below that pressure. e. Check the pressure-time recorder, or any other on-site treatment monitoring or evaluation mechanism for proper operation. f. Acid-clean (pickle) the tubing. 3. Quality control during pumping @. Control injection rate. Maintain surface annulus pressure at or below 500 psi during treatment. b. Watch the pressure response when acid reaches the formation. c. Note the pressure response when the diverting agent reaches the formation. d. Never exceed breakdown pressure of the formation in a sandstone acidizing treatment, unless absolutely necessary intially to breakdown the perfs (with a perforation wash tool), or to bypass severe damage to initiate injectivity. e. In the final flush, make sure acid is displaced from the wellbore. 4. Quality control after pumping/ during flowback a, Do not shut the well in after acid injection. Flow the well back to the tank or pit as soon as the flowiine is connected, b. Collect at least three one-quart samples of backflow acid for analysis. ‘Sample the acid backflow at the beginning, middle, and near the end of the flow. If on swab, get a sample from every other swab run, c. Take the treatment report and the pressure charts to the office for evaluation and placement into well file. G. Acid Stimulation Safety Attachment-2 provides a copy of safety and safety check list for acid stimulation job. ‘a. Consider all safety rules. b. Designate a gathering area in the event of disaster.No. Dok COP-PED-GL-02-PE-PE4231400 GUIDELINE : Rev.01 | Him8 dari 50 Gy = LATI Tanggal: 20-Januar-2016 ee ea TON MeocoExenct VI. KNOWLEDGE/ TRAINING/ REFERENCE: . Production test analysis H. Fracturing Stimulation Quality Control gi . Establish a maximum treating pressure. d. Each person should be assigned a specific responsibility. fe. Assign leadership (one person in charge from the oil company and one from the service company). f. The oil company representative should designate the persons responsible for each task. g. Make sure a good communication network is set up. Have alternative visual commands. h. Have a fire extinguisher placed on ground for ease access. 1. Have two individuals given the responsibility of transporting injured persons to the nearest clinic/ hospital. J. Have designated vehicle set aside for transporting injured personnel, k. Do.a complete head count of all personnel on location, |. Set up a gathering area in case an accident occurs. ‘Attachment-3 provides treatment supervision and quality control guide including the checklist and tables. This attachment including safety guidelines, in the appendix A is to assist the engineer in planning, executing and collaborating with the service company in providing a quality fracturing treatment. The quality control will cover the following: © Pre-Treatment Preparation = Prior to Arriving on Location ~ Day Before Treatment - Immediately Before Treatment * Monitoring Treatment Procedure © Post-Treatment By employing this quality control procedure in all aspects of the fracturing process, a quality fracture treatment will result maximizing the production increase, 1 2. Logs analysis and interpretation 3 4. COP-PED-GL-02-RESENG-007 “Guideline for formation well damage Economides, M. and Boney, C, - Reservoir Stimulation evaluation, prevention and remedial work", Rev 01. Kalfayan, Leonard “Production Enhancement with Acid Stimulation”No. Dok COP-PED-GL-02-PE-PE4231400 Rev.01 | Him9 dari 50 GUIDELINE a Tanggal: 20-Januari-2016 QA QC STIMULATION \VIII.REVIEW AND UPDATE The QA QC Stimulation guideline should be reviewed every three years or whenever there is change in the system or organization, to ensure the document management procedure can be applied in accordance with actual conditions in the company. Senior manager PED is responsible for reviewing and revising this guideline if deemed necessary. Audit of safety, occupational health, environmental protection and quality should include checks on this guideline and are conducted regularly for the effectiveness of implementation of this checklist can be known and then can be repaired, TX. REFERENCE A, SHEQ Management System manual / PRIME Dok. No. SHEQMS-001 B. Panduan Sistem Pengelolaan Dokumen & Records / COP-SHE-GL-02-SYS-01 C. Well Production Practical Handbook D. “Well Stimulation”, Schlumberger E. “Matrix Acidizing”, PetroWikiNo. Dok COP-PED-GL-02-PE-PE4231400 GUIDELINE Rev.01 | Him 10 dari 50 QA QC STIMULATION Tanggal: 20-Januari-2016 X. ATTACHMENT Attachment — 1 Stimulation Decision Tree mmcoerNo, Dok e | COP-PED-GL-02-PE-PE4231400 GiDEr NE - STIMULATION Tanggal: 20-Januari-2016 ax ac 1} MeocoEneRGt Attachment — 2 Safety and Safety Checklist for Acid Jobs SAFETY Personal protective equipment mast be worn by everyone handling and mixing chemical sand by nearby observers. Equipment needed for adequate protection will depend on the chemicals and the potential exposure. At the pre job meeting, make certain everyone knows what equipment is to be used and understands the procedures to be followed always refer to the HSDS for specifics, but generally, the following will apply: PROTECTIVE CLOTHING The basic rule is to avoid direct contact of any chemical with any body part. Al persons on site should wear safety glosses. When handling or mixing any chemical, wear safety goggles. When handling or mixing acids, wear rubber boots and rubber gloves. When handling or mixing powdered chemicals, wear a fitter mask over the nose and mouth to avoid inhaling powder. In a warm or hot environment, a face shield may be needed. For example, when mixed with water ammonium bifluoride forms hydrofluoric acid (HF), an extremely dangerous acid. If the powder is inhaled or ingested, it may be converted to HF in the body. If mixed with sweat, it may form HF on the skin, EXPOSURE TO CHEMICALS When handling or mixing any chemical, stay upwind. If any part of the body is contacted with any chemical, immediately remove all contaminated clothing and thoroughly flush the contacted area with large amounts of clean water. Avoid contaminating other parts of the body during the flushing process. ‘SEEK EMERGENCY MEDICAL TREATMENT IMMEDIATELY. If acid is ingested, do NOT induce vomiting Drink Large amounts of water end SEEK EMERGENCY MEDICAL TREATMENT IMMEDIATELY. NEUTRALIZATION AND DISPOSAL OF ACID Before using any acid, understand the procedure for neutralizing and disposing of that particular chemical. Arrange for neutralization and disposal of flow back spills, and/or excess acid prior to beginning the job. At the pre-jobmeeting clarify responsibilities and procedures for waste disposal of all chemicals to be used on the job. Make certain a Material Safety Data Sheet (MSDS) for each chemical on the site is on hard and easily accessible to everyone on the job.No. Dok: - 7 COP-PED-GL-02-PE-PE4231400 GUIDELINE Rev.01 | Him 12 dari 60 Tanggal: 20-Januari-2016 eer CF —TE SAFETY CHECKLIST FOR ACID JOBS Answer the following questions before beginning an acid job. If the answer to any question is "NO", correct the problem BEFORE starting the job. Keep these questions in mind. I f at any time during the job the answer to any question’ is "No", correct the pr roblem immediately. Yes | No 1. Has a pre job meeting been held with everyone who is to work on the job? 2. Were all applicable safety regulations discussed at the pre job meeting, ‘and does everyone understand all the requirements and their responsibilities? 3. Ts everyone on the site wearing safety glasses? 4. Is everyone who is mixing handling chemicals wearing safety goggles? 5, Is everyone who is mixing chemicals wearing rubber boots? 6. Is everyone working on the job wearing the proper protective clothing? 7. Does everyone on the job understand the safe procedures for mixing and handling all chemicals to be used on the job? 8. Is there a procedure for treating and transporting persons who have been directly exposed to any chemicals used? 9. Does everyone working on the job understand the procedures to follow when someone is contacted with any chemical? 10. Are an eye wash and an ample source of clean water readily accessible for washing in case of personal contamination by chemicals? 11. Has s safe and proper procedure been established for neutralizing and disposing of all chemical used? 12, Does everyone working on the job know and understand the proper procedure for disposing of all the chemicals used on the job? 13. Are all the chemicals property contained and stored? 14, Is there an MSDS on hand for all chemicals on site? 15. Do weather conditions permit safe mixing of chemicals and operation of equipment?Wo, Dok F COP-PED-GL-02-PE-PE4231400 GUIDELINE ie Rev. 01 | Him 13 dari 50 Qy Tanggal: 20-Januari-2016 Snore ow Mevcovenct QUALITY ASSURANCE DURING ACID TREATMENTS GENERAL GUIDELINES * Always hold a pre job meeting before every acid treatment. Be sure that all ARCO and contract personnel. Involved in the job attend. Verify that everyone knows the procedures to follow in case of leaks, spills, or other emergencies. * Verify that an adequate (not excessive) supply of each chemical specified for the jobs Is on site (with an MSDS) and all are properly contained and stored. * Verify the installation of a flow Line so the well can be returned to operation immediately following the treatment. * Determine the maximum surface treating pressure and check pressure ratings on all Lines and connections, pressure test the surface lines using brine, Ammonium chloride, etc. as the test fluid to at least 1000 psi greater than the maximum allowable treating pressure. Monitor the pressure during the treatment. © During the job.be certain all appropriate safety equipment is worn and/or used by persons on site. ® Check all tanks and equipment to be used during the job for c cleanliness. (Free of sludge, drilling mud, ail emulsions, dirt, etc.) + After- all the chemicals have been mixed, obtain a tank of fluid volumes. * Mix or circulate the acid before sampling and again just before pumping, * Titrate acid to verify concentration. HCL should be within +/- 1.5% and HF should be within +/- 0.5%. * In acid jobs return spent acid to the surface as & soon as possible. Long tumarounds increase the chances for precipitates to form, particularly in sandstones. A turnaround time of Less than 2 hours is ideal. © Cleans all spills and dispose of all spent chemicals promptly and safely Refer to the district safety and procedure manuals for Specific requirements, * Record all events and observations before during and after treatment * Save a pint sample of acid from each transport or tank for comparison and analysis. (Use plastic.) DURING PUMPING © If the pump time exceeds 30-60 minutes, agitate the fluid in the acid, Tanks during the treatment to ensure the acid and additives are uniformly mixed, * Establish injection with clean brine, NH4CL (ammonium chloride), water or nitrogen, and maintain a constant injection rate. * When treating sandstone formation, do not exceed the fracturing pressure when pumping the treatment.No. Dok: COP-PED-GL-02-PE-PE4231400 GUIDELINE Rev. 01 Him 14 dari 60 CF Tanggal: 20-Januari-2016 | MeocoENenct QA QC STIMULATION * When treating limestone or dolomite formations, it is acceptable to exceed the fracturing pressure. When acid contact the formation, a pressure decrease should occurs. * When diverters contact the formation, a pressure increase should occurs, If no pressure change occurs, the diverter concentration may be too low or the Particle size too small. If time allows, increase the diverter concentration during the next stage. * Alarge pressure decrease over the entire treatment may indicate the need for diverting, or in carbonate formations, may indicate the need for a fluid loss additive (Ex, OSRs, Polymers). * Ifa leak occurs, stop pumping bleed off the pressure, displace the acid in the surface lines with brine tighten or replace the leaking connection, retest the lines, and resume treatment. * Often when acid reaches the formation, wells will "go on a vacuum” and the fluid will be sucked out of the surface tanks faster than the recorded pump rate. If this occurs, use caution to insure the treatment and displacement volumes are not lost. AFTER PUMPING © Do not shut in the well a long time period unless specified in the procedure. * Return well to operation immediately after treatment. Dispose of all spent chemicals properly. If the well will flow, bring it on slowly over a period of 3-4 days to minimize fines movement. Avoid surging the well if possible. ‘An example of a flow increase may be as follows: Day 1: Set choke at % the original pre stimulation choke. Day 2: Increase choke ¥/2 original pre stimulation choke, Day 3: Increase choke % original pre stimulation choke. Day 4: Open choke to original pre stimulation choke * Collect fluid samples for analysis. © After the flow rate stabilizes, evaluate the well's productivity, ‘© Compare the design with the actual treatment. * Maintain a well file with copies of the treatment charts, reports, and notes.No. Dok: COP-PED-GL-02-PE-PE4231400 GUIDELINE Rev.01 | Him15 dari 50 Gy Tanggal: 20-Januari-2016 QA QC STIMULATION MeocoEweRsi Attachment - 3 Fracturing Treatment supervision and quality control guide (This attachment-3 is made available separately with two file name QA QC Stimulation and QA QC Stimulation Appendix) Attachment to Attachment-3: Fracturing Treatment Supervision and quality control guide Quality Control and Quality Assurance Guide Safety Guidelines Rigup Procedures Equations Tables Charts Table of ContentsNo. Dok: COP-PED-GL-02-PE-PE4231400 Rev. 01 | Him 16 dari 50 Tanggal: 20-Januari-2016 GUIDELINE CF QA QC STIMULATION MeocoEnenat APPENDIX A APPENDIX B Calculating Capacity of Pipe Slurry and Clean Volumes Stair-Step Schedule Ramp Schedule Density Calculations Surface Wellhead Pressure ISIP Fracture Gradient Pipe Friction Pressure Perforation Friction Compressibility Hydrostatic Gradient API Gravity Conversion Hydraulic Horsepower Additive Rate Manifold Equipment Maximum Rates Rheology Equations Apparent Viscosity Fann Model 35 Fann Model 50 Bob Sizes Safety Guidelines A-2 Rigup Procedures A-4 Equations B2 B2 B2 B3 B3 B-4 B-4 BS B6 BG B6 B7 B7 B7 B7 B8 Bo BoNo. Dok: COP-PED-GL-02-PE-PE4231400 GUIDELINE Rev.01 | Him17 dari 50 PA QA QC STIMULATION Tanggal: 20-Januari-2016 APPENDIX C Typical Flange Connection Turbine Flow Meter Specifications Physical Properties of Proppants API Proppant Sizes Sand Setting Velocity (Based on Mesh Size) Service Company Proppant Storage Capabilities Acid Density Conversion Data for Carbon Dioxide Conversion Data for Nitrogen Frac Tank Capacity (Measuring From Bottom) Frac Tank Capacity (Measuring From Top) Frac Tank Capacity (Miser Flat Top) Horizontal Cylindrical Tank Capacity 55 Gallon Drum Base Fluid Viscosities BY (LFC-1, Guar) BY (LFC-2, HPG) Dowell (J-876, HPG) Dowell (J-877, Guar, Old) Dowell (J-877, Guar, New) Dowell (CMHPG) Halliburton (WG-11, HPG) Halliburton (WG-18, CMHPG) Halliburton (WG-19, Guar) Western (Guar, HPG, or CMHPG) TABLES C10 Cu C12 C13 14 C15 C16 Cl7 C18 C19 C20 cat C22 Cy MencoEnenctNo. Dok: (COP-PED-GL-02-PE-PE4231400 Rev. 01 | Him 18 dari 50 Tanggal: 20-Januari-2016 GUIDELINE Cy QA QC STIMULATION fe APPENDIX A SAFETY GUIDELINES A-2 RIGUP PROCEDURES A-4No. Dok: COP-PED-GL-02-PE-PE4231400 GUIDELINE Rev. 01 | Him 19 dari 50 QA QC STIMULATION ‘Tanggal: 20-Januari-2016 = Safety Guidelines Personnel 4. All personnel and equipment not necessary for the treatment operation should move to a point at least 150 feet from the well. 2. If flammable materials such as crude oil, diesel, xylene, methanol, etc, are to be pumped, all personnel within 150 feet from the well should remove matches, lighters, and cigarettes from their pockets. NO EXCEPTIONS! 3. Prior to pumping, all personnel on location should conduct a safety meeting to discuss treatment procedures and safety precautions. 4. An emergency assembly area should be designed in an upwind direction from the well. Also, a head count and buddy system should be established so all personnel can be accounted for. 5. Locate the nearest hospital and the vehicle and driver to perform the service if necessary. 6. Determine the person who will close the well in during an emergency situation, 7. No one should stand on or near discharge lines under pressure. Safety Equipment 1. Proper safety equipment will be worn by all personnel on location. This equipment includes safety hat, steel toe shoes, eye protection, and any other equipment dictated by well conditions. Before pumping any flammable material, all discharge hoses between the blender, manifold, and pump trucks should be wrapped with special covers designed to prevent spraying if a leak develops. 3. All equipment should be properly grounded when pumping flammable materials. 4. Ensure that adequate firefighting equipment is in good working condition, the Personnel are familiar with its operation, and itis strategically located. ment 1. Treatment monitoring equipment should be located as far as possible from the wellhead and high pressure lines, preferably upwind. 2, Mechanical pressure gauge should be in the discharge line independent of the frac van electronics. High Pressure Equipment 1. Position fracturing equipment and tanks crosswind and a safe practice distance from the wellhead, preferably 75 feet minimum, 2. Orient all vehicles away from well and keep access roads clear. 3. Do not run discharge lines or suction lines under any pump truck or service vehicle. 4. No rubber of steel wrapped hoses should be used in the discharge line.Wo, Dok : COP-PED-GL-02-PE-PE4231400 GUIDE IN: : Rev.01 | Him20 dari 50 Qy Tanggal: 20-Januari-2016 @A.Q6'STIMULATION MeocoEnenst Each discharge line should have a full flexible swing at the wellhead and at the truck manifold (no conditions) and staked down at each end. Additional staking may be required based on certain conditions. 6. Each discharge line should have a check valve and positive shutoff valve as near to the wellhead as possible. 7. Release lines and bleed-off lines should be staked down in a safe dirction away from the equipment to a tank battery, test tank, or pit. No swivel joints or bends should be in the line. Two 1-inch valves should be used, 8. Inspect wellhead for any low pressure connections that may have inadvertently been added during well servicing. 9. Pressure test discharge lines up to the last valve on the wellhead equipment. This Pressure test should be a minimum of 500 psi above the maximum allowable surface treating pressure and under no circumstances exceed the pressure rating of the equipment. 10. Never hammer on discharge (or any other) lines when they are under pressure. 11. Conduct pumping operations in daylight only. Do not pump during electrical or severe dust storms. 12. A casing release valve (popoff) should be used on fracture treatments performed via the tubing. 13. Do not shut in a line, high or low pressure, with carbon dioxide. The gas will heat and expand, raising the pressure. The pressure rise can rupture the lines, Proper Rig up Procedures Standby hydraulic power units for the proppant delivery system should be provided on larger treatments. 2. The proppant delivery system should be computerized to accurately blend the proppant. High Pressure Equipment 1, The equipment should be rigged up in an efficient and compact manner using a minimum amount of high pressure discharge line. This is a judgement situation that comes with experience. 2. Determine the amount of hydraulic horsepower and plunger size of each pump unit. This will confirm the amount of available standby horsepower during the treatment. The plunger size will dictate the rate and pressure rating of each pump unit. 3. The discharge lines should be large enough to accommodate the maximum. anticipated treating rate. Suggested rates are 8 BPM for a 2-inch lines, 20 BPM for a 3-inch line, and 37 BPM for a 4-inch line. Although rates can be achieved higher than this, it causes excessive friction and wear of the discharge lines. 4, The same rate criteria apply to the Mani folding equipment as well, whether it is called a discharge manifold or suction pig.No. Dok: COP-PED-GL-02-PE-PE4231400 GUIDELINE Rev.01 | Him21 dari 50 MULATION Tanggal: 20-Januari-2016 ano on QD 5. Determine the operating pressure of all the surface equipment. This pressure should be greater than the maximum allowable surface treating pressure. The pressure rating of the equipment should never be exceeded under any condition. 6. The tree saver or isolation tool should be carefully measured and spaced out such that the cup seal is well into the tubing. The wing valve should remain open and stay under visual inspection to ensure the tool is sealing properly and allow venting if the tool fails. Do not exceed the maximum recommended rate for the tool. Doing this will not harm the tool but will erode the tubing directly below the tool. jen Le 1. The standby blender should be primed up and running before and during the treatment. The same number of suction hoses should be rigged up to the standby blender that are required for the downhole blender. The proppant delivery system should be able to deliver sand to both blenders. A standby blender should be considered if the pump time is longer than one hour or the proppant volume is larger than 100,000 pounds. 2, The maximum delivery rate of the suction hoses should be evaluated in order to determine the number of hoses required. One 20 ft section of 4-inch hose should deliver a thin fluid at 10 BPM and a viscous fluid at 5 BPM. Evaluate the amount of removable fluid from the frac tanks and ensure an excess is on location. It is not unusual to leave up to 50 barrels in each frac tank. This is aggravated if the tanks are leaning back away from the suction header. Remove fluid from one tank at a time, two at higher rates. This will assist in tracking the fluid volumes. 4. The blender should have an automatic tub leveling valve. Instrumentation 1. The pressure transducers should be located as close to the wellhead as possible, This will result in accurately measuring the wellhead pressure by not measuring the friction pressure associated with the surface equipment, Test flow meters, densitometers, pressure transducers, and other monitoring equipment prior to the treatment to ensure all the electronics are functioning properly. The flow meters should be properly sized for the anticipated injection rates. 3. A computerized monitoring van should be used to calculate the bottom hole treating pressure during the treatment and provide the treatment data in ASCII format for post-frac analysis.No. Dok COP-PED-GL-02-PE-PE4231400 GUIDELINE Rev.01 | Him22 dari 50 ‘Tanggal: 20-Januari-2016 BAS ST ULATION APPENDIX B EQUATIONS Calculating Capacity of Pipe Slurry and Clean Volumes Stair-Step Schedule Ramp Schedule Density Calculations Surface Wellhead Pressure ISIP Fracture Gradient Pipe Friction Pressure Perforation Friction Compressibility Hydrostatic Gradient API Gravity Conversion Hydraulic Horsepower Additive Rate Manifold Equipment Maximum Rates Rheology Equations Apparent Viscosity Fann Model 35 Fann Model 50 Bob Sizes B-2 B-2 B3 B3 B-4 B-4 BS B-6 B6 B7 B-7 B7 B8 B9 CF MencoENeRatNo. Dok COP-PED-GL.02-PE-PE4231400 GUIDELINE = Rev.01 | Him23 dari 50 ce te eee JA QC STIMULATION Tanga 20-Januar-2016 a MeocoEvens! Capacity of Pipe gals/ft = 0.0408 x 1D2 bbls/ft = 0.0009714 x ID2 ID = Inside diameter of tubing or casing (inches) Capacity of Annulus gals/ft = 0.0408 (1D2 - 0D2) bbls/ft = 0.009714 (ID2 - OD2) ID = Inside diameter of casing (inches) OD = Outside diameter of tubing (inches) Estimate ID from OD ( Dif ) 2.667. ID = Inside diameter (inches) OD = Outside diameter (inches) lb/ft = Weight of tubing or casing HlNo. Dok COP-PED-GL-02-PE-PE4231400 GUIDELINE Rev.01 | Him24 dari 50 QA QC STIMULATION | Tanggal: 20-Januari-2016 Equations for Calculating Slurry and Clean Stage Volumes Stair-Step Schedules Slurry volume from clean volume Ve = Ve x[(S.* Vass) +1] ‘Clean volume from dirty volume Ramp Schedule Slurry volume from clean volume TAESC= SSC) Veg, » SC x Vy) +1 Vay) +1 Slurry volume from proppant volume ¥,(Ver) (ESC SSC) -_ T(escx rae] vy, (ESC SSC) Fag i (SSCxV,.,) +7 Cj MemcoR aeNo. Dok COP-PED-GL-02-PE-PE4231400 GUIDELINE Rev. 01 | Him25 dari 50 QA QC STIMULATION Tanggal: 20-Januari-2016 Clean volume from slurry volume : «i Be atl Proppant volume from clean and slurry volume y, oak Vass Cal Slurry density from clean density i De+ Pe * [(88C% Vass) +7 Proppant concentration from slurry and clean density P D,- De [1-(05 * Vats)] Clean density from slurry density De =[(Pe Vas) +1] Ds Pe Vg = Slurry volume or rate Ve = Clean volume or rate Pc = Proppant concentration (lb/gal) Vabs = Absolute volume of proppant (gal/lb) Vp = Proppant volume (Ibs) SC = Ending proppant concentration (Ib/gal) SSC = Starting proppant concentration (Ib/gal) Ds = Slurry density (\b/gal) 2 0 Clean density (Ib/gal) =No. Dok: (COP-PED-GL-02-PE-PE4231400 Rev. 01 | Him 26 dari 50 GUIDELINE QA QC STIMULATION ‘Tanggal: 20-Januari-2016 MeDcoENeRGi Py = BHTP ~ P,, + Py + Pry Py = Surface treating pressure (psi) HTP = Bottomhole treating pressure (psi) = FG X Depth Ph — = Hydrostatic pressure (psi) = Fluid Gradient x Depth Pf = Pipe friction pressure (psi) Pof = Perforation friction pressure (psi) Measuring __BHTP _ Surface ISIP +P DEPTH DEPTH Estimating FG=—"_(5, — Pp) + Pp imu FG = Fracture gradient (psi/ft) = Poisson's ratio Sz = _ Vertical stress (overburden) gradient (psi/ft) Pr = Pore pressure gradient (psi/ft)‘No. Dok: COP-PED-GL-02-PE-PE4231400_ GUIDELINE 5 Rev. 01 Him 27 dari 50 Q ‘Tanggal: 20-Januari-2016 Oe eee aL ATOM (MepcoENERat Pipe Friction Pressure ‘SPE Paper No. 15367 0.40429 p*80"8 i mee 7) (suze ? EXP| 2.38-| 2408 DY) _) 0.01579.G . ( Q Q PS } 0.1639 In G 0.05266 Py oa(2)| ‘otal friction pressure (psi) D of tubing or casing (inches) Rate (BPM) epth (Feet) =Gel concentration (Ib/1000 gal) =Proppant conentration (Ib/gal) VHrOOR 8 nian Flui nt FI 518 p079QHT9 40.207 PSI = 3 Equivalent diameter for annulus ID-oOD)?”*(ID+ OD)? riction pressure gradient (psi/1000 ft) Specific gravity of fluid iscosity of fluid (cp) side diameter of pipe or equivalent (in) ID__ =Inside diameter of casing (inches) OD =Outside diameter of tubing (inches)No. Dok: ] COP-PED-GL.02-PE-PE4231400 GUIDELINE - Tanggal: 20-Januari-2016 eee non MeocoENenat lating Publi ipe Friction 2 (APi) Di AP, = D; Py =Unknown pressure gradient (psi/100 ft) Px. =Known pressure gradient (psi/100 ft) Arvo mm. Hr POZO ipe diameter of known friction (inches) ipe diameter of unknown friction (inches) .85 - Extrapolating to larger diameter pipe .17 - Extrapolating to smaller diameter pipe Perforation F1 ion Rate per Perforation ir Z Pe, fp 9 x0. 23688 0867 pats jow rate per perforation (BPM) rforation diameter (inches) rforation friction (psi) nsity of fluid (Ib/gal) erforation coefficient 0.56 to 0.65 before proppant 0.85 to 0.90 after proppant Total Rate ? px0.23688 P= w2 pact =Total flow rate, bbl/min =Number of perforations erforation diameter, inches foration friction, psi ensity of fluid, Ib/gal rforation coefficient 0.56 to 0.65 before proppant 0.85 to 0.90 after proppantWo, Dok COP.PED.GL-02-PE-PE4231400 GOELINE = Tanggal: 20-Januari-2016 OA OG STRRULATION MencoEyeRat Near Wellbore Pressure (FRACPROPT) P= KQ%p Total Friction Pos = Kivb{0 Tortuosity Friction Prot = KooiQ"2 Perforation Friction ‘otal friction, psi otal friction coefficient Q =Flow rate, bbl/min ‘otal friction exponent rortuosity friction, psi Koo =Total friction coefficient Poo = Perforation friction, psi ‘otal friction coefficient C_— =Compressibility (water = E-6 ps v Av 4p -4 E-6 psi: Oil = 5-100 E-6 psit: Gas = 50-1300 ‘otal volume of system Change in volume Change in pressure Hydrostatic Gradient Density (ib / gal )x0,052 = Hydrostatic Gradient (psi / ft)No. Dok: COP-PED-GL-02-PE-PE4231400 GUIDELINE 5 Rev. 01 Him 30 dari 50 Gy Tanggal: 20-Januari-2016 GA OCIS TRAUCATION MencoENerst API Gradient 1s Specific Gravity = 131.5 + APIGravity HLS API Gravity ———_ 131.5 Specific Gravity __Rate (BPM) Pressure(psi) a 40.8 Additive Rate Concentration (gal/ 1000 gal) x Clean Rate 2381 High Pressure Discharge Line Maximum Velocity = 35 ft/sec Rate (BPM) = 2 x ID2 HHP Rate(G 1D Maximum Rate (inches) BPM) 2 8 3 18 4 32 Note: Although higher rates can be achieved, it causes excessive wear of equipment.No. Dok: COP-PED-GL-02-PE-PE4231400 GUIDELINE Rev.01 | Him31 dari 50 TION Tanggal: 20-Januar-2016 an eer ee & ‘Suction Hoses Centrifugal pumps can only generate so much pressure drop. To maintain a supply of water or moderate gel, one 4'" hose can flow at 10 BPM for each 20 ft of length. Viscous or gaseous fluids require 50% more hoses to deliver the same rate. Suction Hoses Rate Number of 4" 20 ft Long BPM) Viscous Fluid 5 10 20 30 40 30, Apparent Viscosity Ina Fracture ‘Ata Known Shear Rate nid 3 40.469 ap yen ty 7880 al Ha = 47880 k'[y] 4g =Apparent viscosity (cp) ‘Shear rate (sec!) Viscosity Via Model 35 Vann Meter n'= 3.32 Log (222) R300. R609= Dial reading at 600 RPM R309=Dial reading at 300 RPM IN =Spring factor (usually 1) Rj =Dial reading at i RPMNo. Dok: COP-PED-GL-02-PE-PE4231400 Rev. 01 | Him32 dari 50 GUIDELINE Tanggal: 20-Januari-2016 QA QC STIMULATION APPENDIX C TABLES CF MencoEnenatNo. Dok: COP-PED-GL-02-PE-PE4231400 GUIDELINE Rev. 01 Him 33 dari 0 Tanggal: 20-Januari-2016 QA QC STIMULATION Typical Flange Connection Turbine Flow Meter Specifications Physical Properties of Proppants ‘API Proppant Sizes Sand Settling Velocity (Based on Mesh Size) Service Company Proppant —_ Storage Capabilities Acid Density Conversion Data for Carbon Dioxide Conversion Data for Nitrogen Frac Tank Capacity (Measuring From Bottom) Frac Tank Capacity (Measuring From Top) Frac Tank Capacity (Miser Flat Top) Horizontal Cylindrical Tank Capacity 55 Gallon Drum Base Fluid Viscosities BY (LFC-1, Guar) B) (LFC-2, HPG) Dowell (J-876, HPG) Dowell (3-877, Guar, Old) Dowell (J-877, Guar, New) Dowell (CMHPG) Halliburton (WG-11, HPG) Halliburton (WG-18, CMHPG) Halliburton (WG-19, Guar) Western (Guar, HPG, or CMHPG) C10 Cit C12 C13 C14 1s C16 ci7 C18 C19 c-20 C21 22 CF MeocoEnenatNo. Dok: COP-PED-GL-02-PE-PE4231400 GUIDELINE = Rev.01 | Him34 dari 50 Gy 1A QC STIMULATION Tanggal 20-Januari-2016 cA cc sTa MeocoE nen Typical Flange Connections Typical Flange ‘Actual Size Working Pressure* | Connection Size inches (psi) (inches) R24) 2 5,000 23/8 R27, 29/16 5,000 27/8 BX153 29/16 10,000 27/8 BXI51 13/16 10,000 13/16 BX152 2 10,000 2 BX154 34/2 10,000 31/2 R46 71/16 5,000. 6" - 1500 Series BX156 71/16 10,000 6" = 1500 Series R45/46 7 WAG 3,000/5,000 6" = 1500 Series Combination Working pressures are minimum values with no safety factor. Verify age and previous service before using the listed pressure ratings. Turbine Flow Meters Size Flow Rate ‘Nominal Calibration inches) (GPM) (PM) (pulses/gal 12 0.75-7.5 0.02 = 0.18 13,000 3/4 2-15 0.05 = 0.36 3,000 1 5-50 O.12= 1.2 870 1172 15 - 180 0.4-4.3 330 2 40 - 400 1.0- 9.5 55 3 60 - 600, 14-143 57 4 100 - 1200 2.4- 28.6 29 6 200 - 2500 4.8 - 59.5 7 8 350 - 3500 83-83 3No. Dok: (COP-PED-GL-02-PE-PE4231400 GUIDELINE Rev.01 | Him35 dari 50 Tanggal: 20-Januari-2016 QA QC STIMULATION CF MeocoEnenat Physical Properties of Proppants Proppant Type Bulk Density* | Specific Gravity | Absolute Volume (Ibs/cuft) (gal/Ib) Ottawa Sand 100 2.63 0.0456 Resin-Coated Sand (2%) 99 2.56 0.0468 Resin-Coated Sand (4%) 98 25 0.0480 Lightweight Proppant (LWP) 101 2.72 0.0441 Intermediate Strength Proppant 113.5 3.25 0.0369 i) Sintered Bauxite 132.5 3.74 0.0321 *1 cuft is equal to one sack of proppant. Above values are for 20/40 mesh; other mesh sizes vary the bulk density. API Proppant Sizes Frac Sand Size 6/12 | 8/16 | 12/20 | 16/30 | 20/40 | 30/50 | 40/70 | 70/14 Designations 0 Nest of U.S.A. Sieves 4 | 6 [| 8 | i | ie | 2 | 30 | 50 Recommended for Testing | 6 | 8 | 12 | 16 | 20 | 30 | 40 | 70 8 | 12 | 16 | 20 | 30 | 40 | 50 | 100 to | 14 | 18 | 25 | 35 | 45 | 60 | 120 12 | 16 | 20 | 30 | 40 | 50 | 70 | 140 is | 20 | 30 | 40 | 50 | 70 | 100 | 200 Pan_| Pan_| Pan | Pan _| Pan_| Pan | Pan | Pan Minimum grain size, in Mamimum grain size, in ‘API Specifications: ‘over one percent (1%) should Minimum of Ninety Percent (90%) should fall between sieve sizes. Not fall into the Pan.No. Dok: COP-PED-GL-02-PE-PE4231400 | GUIDELINE Rev.01 | Him 36 dari 50 CF STIMULATION Tanggal: 20-Januari-2016 oo Meocobrenot Size Of API Mesh Proppant |Proppant] Proppant Diameter | Diamete| Diameter inches r microns mm 0.0937 2.380 2380 0.0787 2.000 2000 0.0661 1.680 1680 0.0555 1.410 1410 (0.0469 1.190 1190 0.0394 1.000 1000 0.0331 0.840 840 0.0280 0.710 710 0.0232 0.589 589, 0.0197, ‘0.500, 500, 0.0165 0.420 420 0.0138 0.351 351 0.0117 0.297, 297 (0.0098 0.250 250 (0.0083, 0.210 210 0.0070 0.177 177, 0.0059, 0.149 149 0.0049, 0.124 124 0.0041 0.104 104 0.0035 0.088 88 ‘0.0029 0.074 74 (0.0017 0.044 0.0015 0.037,No. Dok COP-PED.GL-02-PE-PE4231400 GUDHE - Rev.01 | Him37 dari 50 Gy ¢ STIM Tanggel: 20-Januar-2016 har ATION MeoconeRot Settling Velocity for Sand Settling Velocity, fin 8112~~AP| Mesh Size- 0.01 0.02 0.03 0.04 0.05 0.08 0.07 008 009 04 041 042 043 0.14 Proppant Diameter, in.No. Dok COP-PED-GL.02-PE-PE4231400 GUIDELINE = Rev.01 | Him 38 dari 50 Poe Tanggal: 20-Januar-2016 ee MeocoENeRs! BJ Services - SAND KING poe eae es 800 1,000 1,010 500. 1,010 800 1,250 750, 500 1,300 800. 750 1,100 800, 500. 1,010 500. 1,100 900 3,610 3,610 3,510 3,450 50 o}a}ao> Dowell Schlumberger - SAND CHIEF 1 2 1,210 1,300 1,385 1,180 ‘820 770 585, 490 Total 4,000 3,740 o)o}o|>: Halliburton Company - MOUNTAIN MOVER, 1 2 a 4 5 6 7 A 750 710 610 560 650, 460 710 B 575. 450. 450 460 420 460 470. iC. 575 450, 450 460 420 460 470. D E 575 450, 450 460 420 460 570 750 570. 570, 560 550, 560 = Total_| 3,225 | 2630 | 2,530 | 2,500 | 2,460 Western Company - SAND MASTER. 1 2 3 4 5 6 7 A 1,210 1,300 | 1,000 1,300_| 1,100 980, 830 B 1,385 |" 1,180 |" 1,000 ‘400 500, 420 900) Cc 820. 770. 750, “400 500 450 460, D 585, 490 500 1,100 900) 650. 300 Total_| 4000 | 3,740 | 3,250 | 3,200 | 3,000 | 2,500 | 2,490No. Dok COP-PED-GL-02-PE-PE4231400 GUIDELINE Rev. 01 | Him39 dari 50 QA QC STIMULATION ‘Tanggal: 20-Januari-2016 Acid Density Percent HCL Acid | Specific Gravity* 1 1.005 2 1.010 3 1.015 4 1.020 5 1.025 6 1.030 7 1.035 8 1.040 9 1.045 10 1.050 it 1.055 12 1.060 13 1.065 4 1.070 15 1.075 16 1.080 7 1.085 18 1.090 19 1.095 20 1.100 2t 1.105 22 1.110 23 1.116 24 1.122 25, 1.127 26 1.132 27. 1.136 28 1141 29 1.146 30, 1.153 31 1.158 31.45 (20 Be) 1.160 32 1.163 33 1.168 34 1.173 1.178 5. 1.179 *Density @ 60°F, 14.7 psia MeocoENersi toaNo. Dok: COP-PED-GL-02-PE-PE4231400 Rev.01 | Him40 dari 50 GUIDELINE QA QC STIMULATION ‘Tanggal: 20-Januari-2016 MencoENeRal Conversion Data for Carbon Dioxide Pounds ] Standard Cubic Feet Gallons (60°F, 14.7 psia! liquid, O°F; 1 Pound, 1.0 8.57 1Ton 2000 17,140 1 Gallon (liquid, 0°F) 8.51 72.93, 1.0 1 Cubic Foot (liquid, 0 °F) 63.65 545.5) 7.488 Critical Temperature 87.8°F Critical Pressure | 1071 psia Conversion Data for Nitrogen SCF Gas pounds | (60°F 14.7 | Liquid Liquid psia) 1 pound 1 13.8 0.1483 0.1982 1 ton 2000 27,600 296.6 39.65 1 gallon Liquid 6.743 93.05 1.0 0.1337 1 cubic foot 50.45 696.10 7.481 1.0 Liquid 1.0 0.01075 | 0.001436Wo, Dok = COP.PED.GL-02-PE-PE4231400 GUIDELINE 7 Rev. 01 | Him4t dari 60 Q) zy QA QC STIMULATION Tanggal: 20-Januari-2016 2 a MeocoEyenst Frac Tank Capacity (Fluid Remaining Measuring From Bottom) Inches | Barrels [Inches | Barrels | Inches Barrels [ Inches Barrels | Inches | Barrels o-1 | 3.57 | 25 [10357] 4-9 | 213.54 326.22 | 9-5 | 437.30 0-2 | 7.14 | 26 | 107.14 | 410 | 217.56 [7-2 [320.24 | 9-6 | 440.63 0-3 | 10.71 | 27 [110.71 | 411 | 221.59) 7-3 [334.27 | 9-7 | 443.86 0-4 | 14.28 | 2-8 | 114.28 [5-0 [225.61] 7-4 [338.30| 9-8 | 447.01 0-5 | 17.85 | 29 [i785] 5-1 [229.63] 7-5 [342.32] 9-9 | 450.01 0-6 | 21.42 | 2-10 | 121.42 | 5-2 [233.66 [7-6 [356.34 | 9-10 | 452.94 o-7 | 25.00 | 2-11 | 125.00} 5-3 | 237.68 | 7-7_| 350.37 [9-11 | 455.80 0-8 | 2857 | 30 [129.02] 5-4 | 241.71] 7-8 | 354.39 [10-0 [458.60 0-9 | 32.14 [3-4 [133.05 | 5-5 [245.73 | 7-9 [358.42 [10-1 | 461.34 0-10 | 35.71 | 3-2 [137.07 | 5-6 | 249.76 | 7-10 | 362.44 |_10-2_| 464.02 o-11_| 39.28 | 3-3 [141.10 | 5-7 | 253.78 |_7-11_| 366.46 |_10-3 | 466.58 1.0 | 42.85 | 3-4 [14512] 5-8 [257.817 8-0 [370.49] 104 | 469.10 di | 48.25 | 35 [149.15] 5-8 [261.83 | 8-1 [374.51] 10-5 | 471.60 12 | 50.00 | 3-6 | 153.17 | 5-10 [265.85 | 8-2 | 378.54] 10-6 | 475.00 13_| 53.57 | 3-7 | 157.20 | 5-11 [269.88 | 8-3 [382.56 | 10-7 | 476.95 14 | 57.14 | 38 | 161.22] 6-0 [273.90] 8-4 | 386.49] 10-8 | 478.55 15_ | 60.71 | 3-9 [165.24] 6-1 [277.93] 8-5 [390.61 16 | 64.28 | 310 | 169.27 | 6-2 | 281.95] 86 | 394.63, 1-7_| 67.85 | 311 [173.29 | 6-3 | 285.98 | 87 | 398.66 18 | 71.42 | 40 [177.31] 6-4 | 289.05] 88 | 402.68 | 11-0 | 486.77 1-9 | 75.00 | 41 [181.34 [6-5 | 290.00 | 8-9 | 406.71 |_11-1_ | 488.60 110 | 78.57 | 4-2 | 185.37 | 6-6 | 294.02 |_8-10 | 410.73 |_11-2_| 490.36 iit_| 62.14 | 4-3 [180.39 | 6-7 | 302.07 | 8-11 _| 414.76 | 11-3 | 492.06 2-0 | 85.71 | 44 | 193.41] 68 | 306.10 9-0 [41878] 11-4 [ 493.71 24 | 87.51 | 44 [197.44] 6-9 [310.127 9-1 [422.81 | 11-5 [495.29 22 | 92.85 | 46 | 201.46 | 6-10 [314.15] 9-2 [426.83] 11-6 | 496.69 23 | 96.42 | 47 | 205.00 | 6-11 [318.17 | 9-3 [430.36 | 11-7 | 497.99 24 | 100.0 | 48 | 209.51 [7-0 [322.20] 9-4 | 433.90] 11-8 | 499.09 11-9 [500.00No. Dok: (COP-PED-GL-02-PE-PE4231400 | Rev. 01 Him 42 dari 50 ‘Tanggal: 20-Januari-2016 GUIDELINE QA QC STIMULATION Frac Tank Capacity (Fluid Remaining Measuring From Top) “se a Inches | Barrels [inches | Barrels J Inches | Barrels | Inches | Barrels | Inches | Barrels 0- 500 | o-1 | 499.09 (2-5 433.90) 49 [322.20| 7-1 | 209.51] 9-5 | 100.00 o-2 [497.99 [2-6 | 430.36 | 4-10 [318.17] 7-2 | 205.00) 9-6 | 96.42 0-3 496.69 27 426.83 || 4-11 _| 314.15 7-3 201.46, 97 92.85, 0-4 | 495.29) 2-8 | 422.8150 [31012] 7-4 | 197.44 [ 98 | 87.51 o5 | 493.71 2-9 [418.78 | 5-1 [306.10 | 7-5 | 193.41] 9-9 | 85.71 0-6 | 492.06 | 2-10 [414.76 | 5-2 [302.07] 7-6 | 189.39 | 9-10 | 82.14 0-7 | 490.36 | 2-11_[ 410.73 | 5-3 [294.02 | 7-7_[ 185.37 | 9-11 _| 78.57 0-8 | 488.60 [3-0 [406.71 5-4 | 290.00] 7-8 | 181.34 [10-0 | 75.00 0-9 [486.77 | 3-1 | 402.68 | 5-5 [289.05] 7-9 [177.31] 10-1 | 71.42 0-10 | 484.87 398.66 | 5-6 | 285.98 | 7-10 | 173.29 | 10-2 | 67.85 o-11_| 482.87 394.63 | 5-7 | 281.95 | 7-11 | 169.27 | 10-3 | 64.28 1-0 _| 480.77 390.61 | 5-8 | 277.93 [8-0 [165.24] 10-4 | 60.71 i [478.55 396.49 | 5-8 | 273.90 | 81 | 161.22 | 10-5 | 57.14 1-2 _| 476.95 382.56 | 5-10 | 269.88 | 8-2 | 157.20 | 10-6 | 53.57 13_| 475.00 378.54 | 5-11 | 265.85] 8-3 | 153.17 | 10-7 | 50.00 1-4 | 471.60 37451 | 6-0 | 261.83] 84 | 149.15] 10-8 | 48.25 15 | 469.10 370.49 | 6-1_| 257.87 | 85 | 145.12 | 10-9 | 42.85 1-6 | 466.58 366.46 | 6-2 | 253.78 | 86 | 141.10] 10-10 | 39.28 1-7_| 464.02 362.44 | 6-3 | 249.76 | 8-7 | 137.07 | 10-11 | 35.71 18 | 46134[ 40 [35842 | 6-4 | 245,73] 88 | 133.05[ 11-0 | 32.14 1-9 [458.60 | 41 [35439 | 65 [241.71] €9 | 129.02) 11-1 | 28.57 ito [455.8042 [350.37] 6-6 | 237.68] 8-10 | 125.00] 11-2 | 25.00 ian] 452.7443 [356.34 | 6-7 [233.66] 6-11_| 121.42] 11-3 | 21.42 2-0 [450.01] 44 [34232 | 68 | 229.63 [9-0 [117.85] 11-4 | 17.85 21 [447.01 | 4-4 1338.30 [6-9 | 225.61 | 9-1 [114.28] 11-5 | 14.28 22 [443.86 | 4-6 | 334.27 | 6-10 | 221.59 | 9-2 [110.71] 11-6 | 10.71 23 | 440.63 | 4-7 | 320.24 |" 6-11 [217.56] 9-3 | 107.14] 11-7 | 7.14 24 | 437.30| 48 | 326.22 [77-0 [213.54] 9-4 | 103.57] 11-8 | 3.57 11-9 0.00No. Dok COP-PED-GL-02-PE-PE4231400 GUIDELINE = Rev.01 | Him43 dari 50 = STIMI ‘Tanggal: 20-Januari-2016 Seon MeocoEwens! Frac Tank Capacity (Miser, Flat Top) Inches _| Barrels _|__Inches_| Barrels [Inches | Barrels | Inches | Barrels O-1 45 23, 121.5 45 245, 7 375, 0-2, 9.0 24 126 4-6 250 68 380, 03 13.5 25) 130.5 47 255, 6-9 385, 0-4 18 26 135 48 260 6-10 390, 0-5 22.5 27, 139.5 4-9 265, 6-11 395, 0-6 27 28 144 4-10 270. 7-0 400 0-7 315 29) 148.5 ait 275 71 405) 0-8 36, 2:10 153 5-0 280 72 410 0-9) 40.5 211 157.5 5-1 285 73, 415 0-10 45, 3-0 162 5-2 290 74 420 O-ii 49.5 31 166.75 53 295 75 425) 1-0 54 3-2 171.5 5-4 300 7-6 430 11 58.5 3-3, 176.25, 55 305) 77 435) 122 63, 3-4 181 5-6 310 78 440, 1:3 67.5, 35 185.75, 57 315 79 445, 14 72. 3-6 190.5 5-8 320 7-10 450, 15 76.5 37, 195.25 5-9 325 FAL 455, 16 81 3-8 200 5-10 330 8-0 460 17 84.5 3-9 205; 5-11 335, BL 465 1-8 so | 3-10 210 6-0 340 8-2 470 19 94.5 3-11 215) G1 345, 83, 475 1-10 99, 40 220 6-2 350 8-4 480 111 103.5 41 225 63 355, 85) 485 2-0 108 42 230 6-4 360 8-6 490 2-1 112.5 43 235, 65, 365 8-7, 495 2:2 117 a4 240, 6-6 370 88 500No. Dok: COP-PED-GL-02-PE-PE4231400 GUIDELINE Rev. 01 | Him44 dari 50 1C STIMULATI Tanggal: 20-Januari-2016 a HON MencoEvensi Horizontal Cylindrical Tanks Ratio OF Ratio OF | Ratio Of Liquid Depth | Percent Of | Liquid Depth | Percent OF | Liquid Depth | Percent OF To Diameter_| Total Volume | To Diameter _| Total Volume | To Diameter _| Total Volume, 0.01 0.169 0.36 32.410 O71 76.929 0.02 0.447 0.37 33.636 0.72 77.079 0.03 0.875 0.38 34.869 0.73, 78.216 0.04 1.342 0.39) 36.108 0.74 79.340 0.05 1.869, 0.40 37.353 0.75 80.449 0.06 2.450 0.41 38.603 0.76 81.546 0.07 3.077 0.42 39.857 0.77 82.625 0.08 3.747 0.43 41.117 0.78 83.689, 0.09) 4.458 0.44 42.379 0.79 84.734 0.10 5.204 0.45 43.644 0.80 85.763 0.11 5.985 0.46 44.912 0.81 86.771 0.12 6.797 0.47 46.183 0.82 87.760 0.13 7.639 0.48 47.454 0.83 88.727 0.14 8.509 0.49) 48.727 0.84 89.673 0.15 9.405 0.50) '50.000 0.85 90.595 0.16 10.327 0.51 51.273 0.86 91.491 0.17 11.273, 0.52 52.546 0.87 92.361 0.18 12.240 0.53 53.817 0.88 93.203 0.19 13.229 0.54 55.088 0.89 94.015 0.20 14.237 0.55 56.356 0.90 94.796 0.21 15.266 0.56 57.621 0.91 95.542" 0.22 16.311 0.57 58.883 0.92 96.263, 0.23 17.375 0.58 60.143 0.93 96.923 0.24 18.454 0.59) 61.397 0.94 97.550 0.25 19.551 0.60 62.647 0.95 98.131 0.26 20.660 0.61 63.892 0.96 98.658 0.27 21.784 0.62. 65.131, 0.97 99.125 0.28 22.921 0.63 66.364 0.98 99.523 0.29) 24.071 0.64 67.590 0.99 99.831 0.30 25.232, 0.65 68.808 0.100 100.000 0.31 26.404 0.66 70.019 0.32 27.587 0.67 71.221 0.33 28.779 0.68 72.413 0.34 29.981 0.69 73.596 0.35, 31.192 [0.70 74,768No. Dok: COP-PED-GL-02-PE-PE4231400 Rev. 01 Him 45 dari 50 Tanggal: 20-Januari-2016 GUIDELINE QA QC STIMULATION 55 Gallon Drum a a 7 a ‘* Gallons Gallons Horizontal Vertical is i7 3.0 35 5.0 5.3 7.0 7.2 95 8.9 12.0 10.7 15.0 12.4 18.0 14.2 20.5 16.0 24.0 17.7 27.5 19.6 31.0 21.4 33.5 23.1 37.0 24.9 40.0 26.7 43.0 28.4 43.6 30.3 48.0 32.0 50.0 33.8 52.0 35.5 53.5, 37.3 54.0 39.1 55.0 40.8 42.7 MeocoEnerstNo. Dok: COP-PED-GL-02-PE-PE4231400 GUIDELINE Rev. 0 4 Him 46 dari 50 Tanggal: 20-Januari-2016 QA QC STIMULATION BJ Services LFC-1 Guar Meocoenent & 80 50 F- + + 60 Ib ae a 20 —_— 30 SE 1955 40 50 60 70 80 90 100 110 Temperature, F BJ Services LFC-2 HPG & 80 B70) —— Poet 8 eae tt ® Lee ee i 40) en ee ——_— som 20 a 2510 40 50 60 70 80 90 100 Temperature, F 110No. Dok COP-PED-GL-02-PE-PE4231400 GUIDELINE Rev. 01 | Him 47 dari 50 QA QC STIMULATION Tanggal: 20-Januari-2016 Dowell Schlumberger J-876 HPG 30 40 50 60 70 80 90 100 110 Temperature, F Dowell Schlumberger J-877 Guar ee ee ee ee) Temperature, FNo. Dok: COP-PED-GL-02-PE-PE4231400 GUIDELINE Rev. 01 | Him48 dari 50 ;->-—— Gy TIMULATI Tanggal: 20-Januari-2016 ee oN MeocoENexat Dowell Schlumberger CMHPG : 30 40 50 60 70 80 90 100 110 Temperature, F Halliburton Company WG-11 (LGC-5) HPG See Se oe ————See 40 50 60 70 80 90 100 110 120 130 Temperature, F oN 88 T @ 3 T y 3 T Apparent Viscosity @ 300 rpm, cp bh Oo & 8 ToT ge 6[No Dok : COP-PED-GL-02-PE-PE4231400 GUIDELINE = ILATION Tanggal: 20-vanuar-2016 eee MeDcoEnenat Halliburton Company WG-19 (LGC-4) Guar Apparent Viscosity @ 300 rpm, cp 0 i 30 40 50 60 70 80 90 100 110 Temperature, F Halliburton Company WG-18 (LGC-6) CMHPG 10 20 30 40 50 60 70 Polymer Concentration, Ib/1,000No. Dok: COP-PED-GL-02-PE-PE4231400 Rev. 01 | Him 0 dari 50 ‘Tanggal: 20-Januari-2016 GUIDELINE QA QC STIMULATION Western Company J-4, J-12, J-20 of J-20L (Guar, HPG or CMHPG) 190 |; ce 99 SEES oe 80 TY = 60 Ib. 20 a 20 1b 20 30 40 50 60 & i 8 8 fo — — es j 30 ee ee oe 70 80 90 Temperature, F 100 QO MencoEneRei once 110