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  • Nama: Erinna Putri D - 201FF04037 NIM: 201FF04048 Kelas: Ekstensi FA1

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    siti nurjanah
    6 views2 pages
    analisis spektrum

    Original Title

    Phenobarbital

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    analisis spektrum

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    6 views2 pages

    Nama: Erinna Putri D - 201FF04037 NIM: 201FF04048 Kelas: Ekstensi FA1

    Uploaded by

    siti nurjanah
    analisis spektrum

    Copyright:

    © All Rights Reserved
    Download as DOCX, PDF, TXT or read online from Scribd
    Flag for inappropriate content
    of 2

    Nama : Erinna Putri D_201FF04037

    NIM : 201FF04048
    Kelas : Ekstensi FA1

    Inteprestasi data spektrum IR, Massa, dan NMR

    1. Phenobarbital

    No Molekul/gugus fungsi Bilangan gelombang


    1 N-H stretching 3080 - 3220/cm
    2 C=O stretching 1710 -1770/cm
    3 Vibrasi cincin aromatik 1500 -1590/cm
    4 C-N stretching (Ikatan 1250 - 1450/cm
    Amide III)
    5 N – H wagging 830/cm
    6 C-H 720 – 770 /cm

    No Fragmen Massa m/z


    1 M+ 232
    2 M-(CH3) 217
    3 M-(CO) 204
    4 M-(HNCO) 189
    5 M-(HNCONH) 174
    6 M-(CONHCO) 161
    7 M-(CONHCONH) 146
    8 M-(C2H5) -(CONHCONH) 117
    9 C6H5+ 77

    No Proton (H) Geseran Kimia (ppm)


    1 - CH3 0.8
    2 - CH2 - 2.2
    3 - C6H5 - 7.3
    4 2 > (NH) 11.6

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