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This certificate verifies that part number K2337X, Constant Temperature Kinematic
Viscosity Bath, was manufactured in conformance with the applicable standards set
forth in this certification.
This unit is tested before it leaves the factory, to ensure total functionality and
compliance to the above specifications and ASTM standards. Test and inspection
records are on file for verification.
Jesse Kelly
Application Engineer
Koehler Instrument Company
KV1000 Kinematic Viscosity Bath
Operation and Instruction Manual
Table of Contents
1. Introduction _______________________________________________________ 3
1.2 Recommended Resources and Publications _____________________________________________ 3
1.3 Instrument Specifications ______________________________________________________________ 4
1.4 Environmental Conditions _____________________________________________________________ 4
4. Descriptions ______________________________________________________ 5
4.1 Instrument Controls ___________________________________________________________________ 5
4.2 Temperature Controller ________________________________________________________________ 6
4.3 Accessories for Running Tests _________________________________________________________ 6
4.4 Recommended Accessories ___________________________________________________________ 8
5 Operation _________________________________________________________ 8
5.1 Bath ________________________________________________________________________________ 8
5.2 Power ______________________________________________________________________________ 8
5.3 Circulator Pump ______________________________________________________________________ 9
5.4 Temperature Controller Operation ______________________________________________________ 9
7 Maintenance _____________________________________________________ 12
7.3 Routine Maintenance ________________________________________________________________ 12
7.4 Replacement Parts __________________________________________________________________ 13
8 Troubleshooting __________________________________________________ 13
8.1 Unit Will Not Operate (no heat, cooling, or pumping) _______________________________________ 13
8.2 No Pumping ________________________________________________________________________ 13
8.3 Slow or Insufficient Pumping __________________________________________________________ 13
9 Service __________________________________________________________ 13
KV1000-Manual -1-
KV1000 Kinematic Viscosity Bath
Operation and Instruction Manual
10 Storage _________________________________________________________ 13
11 Warranty ________________________________________________________ 13
Notes ______________________________________________________________ 15
KV1000-Manual -2-
KV1000 Kinematic Viscosity Bath
Operation and Instruction Manual
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KV1000 Kinematic Viscosity Bath
Operation and Instruction Manual
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KV1000 Kinematic Viscosity Bath
Operation and Instruction Manual
3.2 Unpacking
Carefully unpack and place the instrument and
accessories in a secure location. Use extra care
while unpacking the Pyrex® glass jar. Ensure
that all parts listed on the packing list are
present. Inspect the unit and all accessories for
damage. If any damage is found, keep all
packing materials and immediately report the
damage to the carrier. We will assist you with
your claim, if requested. When submitting a
claim for shipping damage, request that the
carrier inspect the shipping container and
equipment. Do not return goods to Koehler
without written authorization. 1. Temperature Controller (See section 4.2
for detailed operation)
3.3 Setup
2. Coolant Outlet/Inlet (Sold Separately)
Equipment Placement. Place the instrument on
a firm, level table in an area with adequate 3. Temperature Sensor
ventilation or in a hood. Please note that
Koehler does not supply a level with this 4. Pyrex Glass Bath
equipment.
5. Cooling Coil (Sold Separately)
Ventilation. A fume hood or exhaust system is
required when operating the unit. Flammable 6. Heating Coil
vapors and/or steam are generated during
operation and must not be permitted to 7. Viscometer Port
accumulate. A canopy-style hood may be used if
the height from the top of the unit to the canopy 8. Thermometer/Thermocouple Port
is 5 feet or less. The exhaust blower should
have a rating of 1000 C.F.M or greater. All wetted parts are corrosion resistant 300
series stainless steel.
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KV1000 Kinematic Viscosity Bath
Operation and Instruction Manual
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KV1000 Kinematic Viscosity Bath
Operation and Instruction Manual
Catalog No. Size Approximate Kinematic Viscosity 378-650-C02 650 45 9,000 To 45,000
Constant, c Range, c St 378-700-C02 700 100 20,000 To 100,000
St/s
378-025-C01 25 0.002 0.5 To 2.0 Ubbelohde Viscometers
378-050-C01 50 0.004 0.8 To 4.0 Ubbelohde viscometers measure transparent
378-075-C01 75 0.008 1.6 To 8.0 liquids, and unlike the Cannon®-Fenske Routine
378-100-C01 100 0.015 3 To 15 viscometers, they maintain the same viscometer
378-150-C01 150 0.035 7 To 35 constant at all temperatures. This is
378-200-C01 200 0.1 20 To 100 advantageous when samples are to be
378-300-C01 300 0.25 50 To 250 measured at different temperatures.
378-350-C01 350 0.5 100 To 500
378-400-C01 400 1.2 240 To 1,200
Suspended-level type viscometers are for
378-450-C01 450 2.5 500 To 2,500
transparent liquids of up to 100,000cSt
378-500-C01 500 8 1,600 To 8,000
378-600-C01 600 20 4,000 To 20,000
Requires a sample volume of approximately
378-650-C01 650 45 9,000 To 45,000
11mL.
378-700-C01 700 100 20,000 To 100,000
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KV1000 Kinematic Viscosity Bath
Operation and Instruction Manual
ASTM Thermometers fluid based upon the testing temperature. Fill the
bath with the medium to 2" (5 cm) from the top
ASTM Designation Catalog No. Range of the bath to allow room for fluid expansion.
28C Kinematic Viscosity 250-000-28C This will provide the proper depth for immersing
at 37.8°C 36.6 To the viscometers and allow for thermal
39.4°C expansion.
28C CERTIFIED at 250-004-28C
ASTM specified test
points of 0, 37.8, Testing Recommended Fluid
39°C Temperature
28F Kinematic 250-000-28F Below 4°C Koehler recommends a suitable medium that
Viscosity at 100C 97.5 To will not freeze like ethylene glycol. Do NOT use
103.5°F distilled water. Use of a coolant may be
28F CERTIFIED at 250-004-28F
necessary, See
ASTM specified
test points 32, 100,
Section 4.4, Recommended
102°F Accessories.
29C Kinematic 250-000-29C
Viscosity at 54.4C 52.6 To 4 - 50°C Distilled water will be suitable
55.4°C
29C CERTIFIED at 250-004-29C Above 50°C Koehler supplies highly refined white technical
ASTM specified oil (part # 355-001-001) that contains an
test points 0, 54.4, oxidation inhibitor to limit
55°C clouding at higher temperatures.
29F Kinematic 250-000-29F
Viscosity at 130F 127.5 To Above 110°C Koehler supplies a clear silicone heat transfer
132.5°F fluid (part # 355-001-002) with high oxidation
29F CERTIFIED at 250-004-29F resistance and low
ASTM specified volatility.
test points 32, 130,
132°F
32F Kinematic 250-000-30F
Viscosity at 210F 207.5 To
212.5°F 5.2 Power
30F CERTIFIED at 250-004-30F
ASTM specified WARNING: Do NOT turn the power on unless
test points 32, 210, the bath is filled with the proper medium;
212°F otherwise, damage may occur to the unit and
the warranty would be void.
4.4 Recommended Accessories An IEC power cord is provided with the KV1000
Withdrawal Bulb (K22090) Bath. This power cord should be plugged into
Used to pull sample into viscometer tube the IEC receptacle on the rear of the controller
and then plugged into a properly grounded
Rubber Stopper, pk/12 (K23311) outlet. Make sure that the power outlet is the
To hold sample after it is pulled through the same voltage and frequency indicated on the
viscometer prior to test identification label on the back of the Controller.
The use of an extension cord is not
Cooling Coil (K23377-01000) recommended. However, if one is necessary, it
Permits circulation of water or refrigerated must be properly grounded and capable of
coolant for operation at near ambient handling the total wattage of the unit. The
temperatures. Installs in top plate. Hose-barb extension cord must not cause more than a 10%
inlet and outlet connections for water or drop in voltage to the Circulator.
refrigerated coolant are located at the top of the Once the unit has been connected to an
bath. Secure with copper wire to prevent the appropriate electrical outlet, place the Circuit
tubing from disengaging from the connection. Breaker/Power Switch on the rear of the
Controller in the ON position. Four decimal
5 Operation points (….) will appear on the digital display. DO
NOT place the Power Switch on the front of the
5.1 Bath Controller ON until the Safety Set has been
NOTE: Ensure the Borosilicate glass jar is not adjusted to the desired temperature.
cracked or broken. DO NOT USE the jar if there
is any damage. Indicated Voltage
Fill the bath with the appropriate heat transfer
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KV1000 Kinematic Viscosity Bath
Operation and Instruction Manual
120/1/60 110 to 130V Single 60 1. Use a flat blade screwdriver to rotate the
Safety Set Indicator Knob to the desired
230/1/60 208 to 230V Single 60 temperature. Do NOT force the knob beyond
240/1/50 220 to 240V Single 50
the stops at either end of the temperature
value range.
After filling the reservoir with fluid, you must set 2. Once the Safety Set temperature has been
the Safety Set and the Software High Limit as set, turn power to the Controller ON by
well as your desired control set point. pressing the Power Switch on the front of the
controller. The pump will begin operating, the
5.3 Circulator Pump display will flash the current temperature set
The HIGH or LOW speed selection switch on the point (tx.xx), the °C LED will light, and the
rear panel of the Controller is used to select current bath temperature will appear on this
pump speed. LOW is adequate for most display. Pump speed selection is made using
applications and provides quieter pumping. the Pump Speed Selection Switch on the rear
HIGH is recommended where temperature of the Controller.
varies frequently and there is a need for fast
recovery or when pumping to multiple external If power is disrupted because the Safety Set
units. temperature was exceeded, place the Circuit
Breaker/Power Switch in the OFF position,
press the Safety Set Reset Button, correct the
Speed Selection Maximum Pump problem (low liquid level, incorrect Safety Set
Outlet Ratings temperature, etc.), and then restore power.
HIGH 15 LPM / 2.6psi Activation of the Safety Set during normal
LOW 9 LPM / 1.5psi operation will display a fault (FLt 3) on the
readout.
Line Frequency= 50-60Hz
Selecting Temperature Units
The data in the table above are based on the
following criteria: The control set point and actual bath
temperatures may be displayed in either °C or
1. Maximum pump outlet flow rate is measured °F. The factory-default is °C.
in liters per minute (LPM) with no restriction on
the pump outlet To change from °C to °F, place the Circuit
Breaker/Power Switch on the rear of the
2. Maximum pump outlet pressure is measured Controller in the OFF position and then press
in pounds per square inch (PSI) at no flow. and hold the P2 Button while turning the power
back ON.
3. Water was used as the circulation fluid. Water
has a viscosity of one centistoke. High viscosity To change from °F to °C, place the Circuit
or low-density fluids will change these figures. Breaker/Power Switch in the OFF position and
then press and hold the P3 Button while turning
5.4 Temperature Controller Operation the power back ON.
Setting the Safety Set Point NOTE: When the temperature display units are
changed, the Software High Limit value and all
The Safety Set feature automatically temperature presets revert to the factory-default
disconnects Controller power to the heater and values. If a calibration value has been entered, the
pump in the event that the reservoir liquid level value will be retained.
drops too low or the Controller fails. The Safety
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KV1000 Kinematic Viscosity Bath
Operation and Instruction Manual
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KV1000 Kinematic Viscosity Bath
Operation and Instruction Manual
FLt 4 Heating Triac Error- Service required 3. Press the selected Preset Button a second
Failure time to enter the new set point. The new set
FLt 5 Probe Failure Error - Service required point temperature will not be saved unless the
Preset Button is pressed.
FLt 6 i2c error- Error- Service required
communication 4. The LED associated with Preset Button lights
(Appears only on
failure to continuously whenever that preset value is
Refrigerating/Heating
modulation controlling bath temperature. If more than one
Circulators)
board Preset Button is set at a given temperature set
point, the LED associated with all Preset
Buttons with that set point will light.
Setting the Set Point Temperature
Local Lockout Feature
1. Press and release the Select/Set Knob. The
decimal point flashes to indicate that the set
This feature enables the user to lock all controls
point temperature can be changed.
on the controller. While the feature is activated,
the unit will remain running at the current
2. Turn the Select/Set Knob until the desired
settings.
temperature set point is displayed. A
clockwise rotation increases the setting; a
To activate the local lockout feature:
counterclockwise rotation decreases the
setting.
1. Press and hold the Select/Set Knob for 10
seconds. Once locked, the screen will read
3. Press the Select/Set Knob a second time to
LLo. When locked, the set point decimal point will
accept the displayed value. The decimal point
not flash as usual.
stops flashing and the display will indicate the
actual bath temperature. Allow sufficient time
2. Press and hold the Select/Set Knob again for
for the bath to stabilize at the desired
10 seconds to unlock the controls. Once
temperature before making any adjustments to
unlocked, the screen will read Can.
set point temperature.
Calibration
NOTE: The unit will automatically accept the
displayed set point after approximately 10
Calibration allows the user to match the
seconds of inactivity, even if the Select/Set Knob
Controller’s bath temperature display to an
was not pressed.
external reference thermometer. Calibration is
performed as follows:
The set point temperature may be checked at
any time by pressing the Select/Set Knob.
If the set point temperature cannot be raised, it 1. Set the desired operating fluid temperature
is possible that the Software High Limit value set point and allow temperature to stabilize.
is set lower than the desired control
temperature set point. Reset the Software 2. Press the P2 and P3 simultaneously and
High Limit value to 5°C or more above the release and repeat until the display reads
desired set point (oCx.x). Press P1 and hold until (Cal) is
temperature. displayed. This will take about 2 seconds.
User Defined Preset Temperatures 3. At one second intervals, the displayed value
will alternate between the actual bath fluid
1. With the unit on, press the desired Preset temperature and the current offset value,
Button — P1, P2, or P3. The LED associated which is the difference between the factory
with the selected Preset Button will begin to calibration setting and the user’s reference
flash. temperature sensor. The maximum offset is
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KV1000 Kinematic Viscosity Bath
Operation and Instruction Manual
4. To change the calibration offset value, rotate 3. Restart the unit. Monitor the operations to
the Select/Set Knob until the display matches ensure that the unit is operating properly.
the reading on the reference temperature If you are still experiencing trouble, please
sensor. The display will continue to alternate contact Koehler technical service for
between the offset value and the calibrated assistance.
display temperature.
6.2 Over Power Protection
5. Press the Select/Set Knob or the P1 Button to The KV1000 Kinematic Viscosity Bath
accept the entered value. When the new is equipped with Over-power Protection circuitry,
calibration is stored and the mode is exited, which prevents the unit from unsafe electrical
(DONE) will appear on the display. conditions. If power to the unit is lost, then turn
off the main power and turn it back on again.
NOTE: The displayed offset value will also be The main power switch also functions as a
accepted if there no activity for 20 seconds. circuit breaker.
Pump Motor
6 Safety Features
The pump bearings are permanently lubricated
The KV1000 Kinematic Viscosity Bath is with high-temperature silicone grease and do
equipped with several safety and protection not require additional lubrication. Should the
features, which are described in the following bearings become noisy, replacement of the
sections. entire pump motor is recommended. This will
reduce repair labor costs and retain fluid
pumping reliability. A replacement pump and
6.1 Over Temperature Protection
motor mounting kit is available (see Section 7.2-
The KV1000 Kinematic Viscosity Bath is Replacement Parts).
equipped with Over-temperature Protection
(OTP) circuitry, which prevents the unit from Cleaning
exceeding unsafe operating temperatures. If the Only mild detergents and water or an approved
unit cannot maintain the set point temperature cleaner should be used on the painted and
and begins to decline, the OTP circuitry may stainless steel surfaces of the Circulator. Do not
have been activated. Please follow these steps. allow cleaning liquids or sprays to enter the
Controller vents. A concentrated bath cleaner is
1. Turn off the unit power switch and available that can be used to remove mineral
disconnect the line cord. deposits from the reservoir (see Section 7.2-
Replacement Parts).
2. Determine the source of the problem and
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KV1000 Kinematic Viscosity Bath
Operation and Instruction Manual
- Check that the Safety Set temperature is This equipment was shipped from the factory
higher than the control temperature set point. in a corrugated cardboard container. If long term
storage is anticipated, re-packing the instrument
- Turn power off, press the Safety Set Reset in a water-resistant container is recommended
button and restore power. to ensure equipment safety and longevity.
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KV1000 Kinematic Viscosity Bath
Operation and Instruction Manual
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KV1000 Kinematic Viscosity Bath
Operation and Instruction Manual
Notes
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KV1000 Kinematic Viscosity Bath
Operation and Instruction Manual
Notes
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