"his international sand
= (Gy
Se
—
Standard Test Methods for
Specimens’
Sper epsn Ce)
E_NOTE— Changes were edraly mae fn June 2018
oa a a a wt
1. Scope
1.1 These test methods deseribe two ways of determining
the total/moist and dry densities (unit weights) of intact,
isturbed. remolded. and reconstituted (compacted) soil spec
‘mens. Density (unit weight) as used in this standard means the
Fame as “hulk density” of soil as defined by the Soil Science
Society of America. Intact specimens may be obtained fr
hin-walled sampling tubes. block samples, oF clods. Spec
mens that are remolded by dynamic or static. compaction
FBrocedures may also be measured by these methods. These
methods apply to sols that will retain their shape during the
Mreasurement process and may also apply to other materials
a) ‘as. soil-cement. soil-lime, soil-bentonite or solidified
roil-bentonite-cement slurries. Tt is common for the density
Hit weight) of specimens ater remmoval from sampling tubes
tnd compaction molds to be less than the value based on tube
A nold volumes, or of in sity conditions. This is due tothe
ag ecimensweling flr remoal of era presses
I 11 Method A covers the procedure for measuring the
gy tune of wan etl spesimers by dernning he quant
by water displaced.
FT tps method only applies to specimens in which the
I sit nor pensrate the outer surface ofthe specimen.
athe B covers the procedure by means ofthe diet
ca oe eof the dimensions and. ass of a specimen,
tM cylindrical shape Tat a reconstitute
Aj trecimens may be tested by this method in onjune-
emolded ssh, permeability (awatr) and compressibility
AB terminations
vo ie values sated in SI units ae toe repr as
|
Bird. ‘The values given in parentheses after SI units are
sander fama ol ane not considered sanded
Tse ea methods ar unde th json of ASTM Connie D8 ua Soil
A Pee Ih eine det espns of Sticonmitee ISOS on Tex
asaya Dey Charset Sih an
icy dyson apponcd Feb 13.2018, Pubsed Mah 2018. Origialy
car in) me 268-7. Ln evi con approved 20 as
Hrresepo, DO 10.1S20/D7 26.40 REDD
co maby ASTM Ital ighsseseset, Tae Aig ID 13123 EDT2019
rnlaaded/printed bY
Hi oi gre th oti
a: iii.
seas developed in accordance with internationally eecognied princpeg
Development of International Stand, Guest Recommeadatons ised hy fhe Mord Tra
Gopanirtion Teale Barrer ora
‘stalahcd inthe cio on Principles for the
‘Cnty Commie
Designation: D7263 - 09 (Reapproved 2018)'?
Laboratory Determination of Density (Unit Weight) of Soil
‘This standard i sued under the fed designation 1726%; the number immediately following the designation indicts the year of
‘orginal adoption om the case of eson the year of ls! revision. number in preneses indicates he year of ast rp
eal. A
heer cage snc the hat ev son oF EANPRVA
NOTE—Iatoriliy updated unis of measoremen statement In Ail 2018
1.3 All observed and calculated values shall conform to the
‘guidelines for significant digits and rounding established
Practice D6026.
13.1 The method used to specify how data are collected,
calculated, or recorded in this standard is not directly related to
the accuracy with which the data can be applied in design or
other uses, or both. How one applies the results obtained using
this standard is beyond its scope.
14 This standard does not purport to address all of the
safety concerns, if any, associated with its use. It is the
responsibility of the user of this standard to establish appro
priate safety, health, and environmental practices and deter~
‘mine the applicabiliey of regulatory limitations prior to use.
1.5 This international standard was developed in accor
dance with internationally recognized principles on standard-
ization established in the Decision on Principles for the
Development of International Standards, Guides and Recom-
mendations issued by the World Trade Organization Technical
Barriers to Trade (TBT) Commitee.
2. Referenced Documents
2.1 ASTM Standards:*
D653 Terminology Relating to Soi
Fluids
1698 Test Methods for Laboratory Compaction Character
isties of Soil Using Standard Effort (12,400 ft-Ibi/t* (600
kN-nvm’))
D854 Test Methods for Specific Gravity of Soil Solids by
Water Pycnometer
11557 Test Methods for Laboratory Compaction Character-
istics of Soil Using Modified Elfort (56,000 f-tbi/a*
(2,700 kN-nvm'))
1D1587/D1587M Practice for Thin-Walled Tube Sampling of
Fine-Grained Soils for Geotechnical Purposes
1D2166/D2166M Test Method for Unconlined Compressive
and Contained
Fewer ASTM stirs, vb the ASTM website, wasn or. ot
ntact ASTAT Cosomer Service a ervielasim org. For Anal Book of (STAY
Standards volun infomation few te ands Document Sunary page on
the ASTM web
cpa asrt baton 02S th Ort, PO Box 7 Ve Gone Bsa Ue ne
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trength of Cohesive Soil
12216 Test Methods for Laboratory Determination of Water
(Moisture) Content of Soil and Rock by Mass
2487 Practice for Chissificaion of Soils for
Purposes (Unified Soil Classification System)
D24RK Practice for Description and Identification of Soils
(Visual-Manual Procedures)
D3SS0/D3SSUM Practice for Thick Wall, Rin
Barrel, Drive Sampling of Soils ~
D3740 Practice for Minimum Requit
Eng
ne
ring
Lined, Split
ments for Agencies
ed in Testing and/or Inspection of Soil and Rock as
in Engineering Design and Construction
vD4220M Practices for Preserving and Transport
mples
4818 Test Methods for Liquid Limit,
Plasticity Index of Soils
D4753 Guide for Evaluating, Selecting, and Specifying Bal-
ances and Standard Masses for Use in Soil, Rock, and
Construction Materials ‘Testing
16026 Practice for Using Significam Digit
Dat
lastie Limit, and
n Geotechnical
Specification for Liquid-in-Glass ASTM Thermom-
‘eters with Low-Hazard Precision Liquids
2.2 Other Reference:
Soil Science Society of Ameriva Glossary of Soil Science
Terms*
3.1 For definitions of common technical terms used in this
standard, refer to Terminology D653.
4. Signitcance and Use
1.1 Day density. as defined “Sensi of si or rok" in
“Teninlogy DOSS and "bulk density” by so scents, canbe
Ufhumse basi and vise-versa, When part density that
eee gravity (Test Methads DRS!) fs alo known, oy
BReaiy cine wed to calelate porosity and void ratio (
sy Xt) Dry density measurements are aso ws for
vent ol density provide ite wel infomation
Except to xnte the ht of sl pert vlumes fr
seein suis with dying of sweling oi, bak density
Sir ay with moisture content. Hence, the water content of
The so Ehould he determined at the cme oF sampling
“L2 Densities (unit weighs) of remoldedesonsttuted
caumonly aned to evaluate the degree of
J mbankments, ete, Dry density
specimens al
compaction of earthen il
Values are usually used in conjunction
values (Test Methods D698 and D1S57).
43 Density (unit weight) is one of the key components in
determining, the mass composition/phase relations of soil, se
Appendix X!
TNoit The quality of the result produced by this standard is
~ pill online: we sie publcatonsiusary
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dependent on the compete
Sunanility oF the equipment and facilities used. Agencies that meet the
Gites of Practice D3740 are generally considered eapable of competent
find ebjective lesting/samplinginspestiondetc, Users of this standard are
‘Guitoned that compliance with Practice D3740 does notin itself assure
{ella esl, Reliable results depend an several factors: Practice D3740
feane of evaluating some of these factors,
provides a
Apparatus
5.1 For Method A the following apparatus are required
5.1.1 Batance—All balances must meet the requirements of
Specification D$753 and this section. A Class GP! balance of
0.01 g readability is required for specimens having a mass up
to 200 grams and a Class GP2 balance of 0.1 g readability is
required for specimens having a mass over 200 grams. For
method A, the balance must be capable of measuring the mass
Of the specimen suspended in water. This is usually accom-
plished by a weighing hook built into the balance for that
purpose, or a yoke assemblage is placed upon the pan which
Suspends thin, non-absorbent string or wire, that is, a nylon
line, etc., below the balance into the water reservoir,
5.1.2 Drving Oven—A thermostatically controlled, pref
ably of the Forced-draft type, capable of maintaining a uniform
temperature of 110 = 5°C throughout the drying chamber.
5.1.3 Wax—Non-shrinking, paraffin and/or microcrystalline
wax that has a known and constant density, Pye to. four
significant figures and that does not change after repeated
‘melting and cooling cycles.
Non: 2—The waxes generally used are commercially available and
ave dens values n the range of O87 0 0.91 gfem of Mem
5.14 War-Melting Container—Used to melt the wax, but
should not allow the wax to overheat. A container heated by hot
water, preferably thermostatically controlled. is satisfactory.
“The vax should be heated 10 only slightly above the melting
point to avoid flashing ofthe wax vapors and to permit quickly
forming & uniform surface coating of wax. Warning—Vapors
given off by molten wax ignite spontaneously above 205°C
(400°F) and should not be allowed to come in contact with the
heating element or open Mame.
5.15 Wire Basket—A wire basket of 3.35 mm or finer mesh
‘of approximately equal width and height of sufficient size to
contain the specimen. ‘The basket shall be constructed to
prevent trapping air when it is submerged. The basket is
suspended from the balance by a fine thread or string. A hairnet
may also be used in liew of the basket for smaller soil
specimens.
Container—A container or tank of sufficient size to
contain the submerged hasket and specimen.
Specimen Container—A corrosion-resistant container
ficient size to contain the specimen for water content
Thermometer—Capable of measuring the temperature
range within which the test is being performed graduated in a
0.1 degree C division scale and meeting the requirements of
Specification F225
5.19 Container Handling Apparatus—Gloves or suitable
holder for moving and handling hot containers.
5.1.10 Miscellaneous—Paintbrush, trimming tools, speci-
men containers, and data sheets provided as required.
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5.2 For Method B the follow
5.2.1 Bulunce—See $11
5.2.2 Drving Oven—Sce 8.1
5.2.3 Specimen-Sice Measurement Devices
determine the height and width or diameter of the specimen
shall measure the respective dimensions to four sipnificant
its and shall be constructed so that their use wall not indent
‘oF penetrate into the specimen,
appa
Devices used
Non
aliens
2—Crreumferential messining tapes are te
rmeasining the diameter eh
al specimens
5.2.4 Apparatus for Preparing Reconstituted or Remolded
Spa Orion) Such apr
Kies af specimens are being tested
yg 525 Mivetencons Anparatus—Specinen rimming and
arving tools including a wire saw, steel straightedge, miter
pox and vertical tnmming lathe. specimen containers, and data
beets shall he provided as required
1s only required if these
BE. Samples and Test Specimens
6.1. Samples—Intact samples shall he preserved and transe
Whhried in accordance with Practice D4220/D4220M Groups C
and D_ soil, Cory mens. shall be
reserved
‘cordance with Practice D4220/D4220M Group,
B soil, Man
in the samples that are stored prior to testing in
pion-corradible aitight containers ata temperatu
ied oF remolded 9p
hetween
ents direct
approximately 3° and 30°C and in an area that pre
sontact with sunlight
6.2 SpecimensSpecimens for testing shall e sallicintly
Mohcsive and firm to maintain shape during the measuring
rocedure if Method A is used, sce 11-11. Specimens shall
Swe ee simure dimension of 0 mm (nan the ages
article contained within the test specimen shull be smaller
= i ‘one-tenth of the specimen's smallest dimension. For
specimens having a dimension of 72 nm (2.8 in.) or larger the
St parucle sie shall be smaller than one-sixth of the
en's smallest dimension I after completion ofa test on
Visual observations indicate Uh anger
spe
in intact specimen.
particles than permitted are present, indicate this information in
Ate rem jon of the feport of test dati
ap Procedure
7.1 Record all identifying information for the speci
Luch as project, boring number, depth, sample type (hat is,
Tube, trimmed, etc) Visual soil classitication (Practice D2488),
ars se
ay rer pertinent dat.
2 Method A—MWuter Displacement
T3 Determine, if not previunly established, the density
of tne wan te used 10 four sipmficant dips (sce 5.1.3)
413-2 Prepare specimens in an envionnvent th
any changes in wal or some soi, changes in waer
rent are minimized by trinwning specimens in contol
borironment, such as. conireled.high-humiity room
Enclosure
7.2.3 IF required, cut a specimen meeting the size requite
cents given in 62 from the sample tw be tested. If required
rim the specimen to a fairly repulur shape. Ke angles.
‘ould be avoided, and any cavities formed by large particles
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being pulled out should be patched with material
from the trimmings, Hanalle specimens carefully to minimize
disturbance. change in shape, or change in water content,
Typically. for most samples. changes in water content are
minimized by trimming specimens, controlled
environment, stich as a controlled high-humidity room/
enclosure.
7.24 Determine and record the moist mass of the soil
specimen (M,) to four significant figures ing or kg
7.25 Cover the specimen with a thin coat of melted wan,
cither with a paintbrush or by dipping the specimen in a
container of melted war, Apply a second coat of wax after the
first coat has hardened, The ax should be sufficiently warm to
yet it should not be so hot
flow when brushed on the spect
that it dries the veil
[Nou 4—If overheated wat comes im contaet wat the sei specimen. it
may cause the moisture 0 “an form air bubbles under the wa
ables may be tne! out al ile
7.2.6 Determine and record the mass of the wax-coated
specimen in air (M,) wo four significant figures in g oF kg.
7.2.7 Determine and record the submerged mass of the
war-coated specimen (M,,,) 10 four significant digits in g oF
kg. This is done by placing the specimen ina wire basket
hooked onto it balance and in ws the basket and specimen
in In order to directly measure the
submerged mass of the wet soil and war, the balanee must have
been previously balanced (tared to Zero) with the wire basket
completely submerged in the container of water. Make sure
e specimen sand basket is Tully submerged, and that the
basket is not touching th
7.2.8 Record the temperature of the water to 0.1 degrees C.
sides of bottom of the container.
in. Note inthe fpr if water content
¥s not tom the spin ssc
7.3 Method B—Divect Measurement:
TAA Intact Specimens—Prepare intact spec
lage block sample or trom samples secured in aecordance
with Prwctice DISS7/D1587M or other acceptable tube sam-
pling procedures, such as Practice D3SS0/DASSOM. Spe
‘can be obtained trom intact block samples using a sharp cutting
ing. Handle Sunples/specimens carefully Umi
disturbance, changes. in cross. section, or change in water
contents. Specimens re usally cubes or eylindrialin
shape.
ni T—Core sampling might he Util or impossible in gravelly or
hha dry soils. Wel soils tend to be more plastic and subject 10
compression,
7.3.1.1 Specimens obtained by tube sampling may be tested
without extrusion except for cutting the end surfaces plane and
perpendicular to the longitudinal axis of the sampling tube. The
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height and inner dimensions of the tube may be taken 10
represent specimen dimensions,
[Nore 8 Some solls may expand into the sampling tube witha resultant
change in volume from the original in situ condition,
7.3.1.2 Trim specimens in an environment that minimizes
any change in water content. see 7.2.2. Where removal of
gravel or crumbling resulting from trimming causes voids on
the surface of the specimen, carefully fill the voids with
remolded soil obtained from the trimmings. When the sample
condition permits. a vertical trimming lathe may be used to
reduce cylindrical specimens to 3
7.3.1.3 After obtaining uniform dimensions, place the speci-
men in a miter box or trimming collar (especially for friable
soils) and cut the specimen to a uniform height with a wire saw
or other suitable device, such as a sharpened steel straightedge
Perform one oF more water content determinations on material
oblained during the trimming of the specimen in accordance
with Test Method D2216 for the estimated water content(s),
Final water content shall be performed on the whole specimen
or representative slice (if other testing such as plasticity limits,
Test Methods D4318, are required) at the end of the test
Determine and record the mass (g) and dimensions (mm) of the,
specimen to four significant digits using the applicable appa-
ratus described in 5.2. A minimum of three height measure-
‘ments (approximately 120° apatt if three, 90” apart if four, ete.)
and at least three diameter measurements at the quarter points
of the height shall be made to determine each the average
height and diameter of cylindrical specimens. A minimum of
three measurements each of length, width and height shall be
‘made to determine the volume of cubical specimens.
nilorm diameter
foseribes proce
sing
Nore 9—Test Method D2166D2166M, setion 6.2
dre for preparing intact est specimens for stengt
7.3.2 Remolded/Reconstituted (Compacted) Specimens—
Specimens shall be prepared as prescribed by the individual
assigning the test or as preseribed by the applicable related test
procedure. After a specimen is formed, (rim (if necessary) the
Ends perpendicular to the longitudinal axis, remove the mold,
fand detcrmine the mass and dimensions of the test specimens
in accordance with 7.3.].3. The height and inner dimensions of
the mold may be taken to represent specimen dimensions.
Nom» 10—I is common for the density (unit weight) of the specimen
after emoeal from the motd to be less than the value based on the volume
a epconold, This occurs asa result ofthe specimen swelling afer removal
fof the lateral confinement due 10 the mold
8, Calculations
8.1 Water Content, w—Calculate in wccordance with Test
Method D2216 to four significant digits
£.2 Calculate the moist density to four significant figures as
Follows:
8.2.1 Method A—Water Displacement:
n= MAM, ~ Mado.) = (MMe
mass of moisvtotal soil specimen, 8.
mass of wax-coated specimen, &
mass of submerged wax-coated specimen,
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density of wax, g/em* or Mg/n
Pp =
P= density of water attest temperature. giem’ or Mg/m,
(see Test Methods D854, Table 1), and
Pm = density of total (moist) soil specimen, gfem* or
Mey
8.2.2 Method B—Direct Measurement:
a= (MY) 2
where:
V_ = volume of moist soil specimen, em*.
8.2.2.1 Cylindrical Shape:
v= (x d° A)/4000 @
d_ = average specimen diameter, mm, and
hh = average specimen height,
2.2 Cubical Shape:
Lew xh
00 cy
average length, mm.
average width, mm, and
average height, mm.
8.3 Calculate the dry density for either method A or B as
follows:
h
y= pal(1 +0100) (3)
where:
pu = dry density of soil, gfem® ot Mg/m’, and
Ww = water content of soil specimen (in percent), to nearest
four significant digits.
84 Calculate the moisvtotal and dry unit weights to four
significant figures for either method A or B as follows:
52.428 p, inn’ (6)
62.428 pin It andy
Ya," 9.065 p, in Nim® and 74 = 9.806665 pn KN
wher
Ym = moisVtotal unit weight of specimen, and
31 = dry unit weight of soil specimen.
9, Report: Test Data Sheet(s)/Form(s)
9.1 The report (data sheet) shall contain the following (see
Appendix X2 andl Appendix X3):
91.1 Wentitication of the sample (material) being tested,
stich as project, boring number, simple number, test number,
container numb
9.1.2 Sample depth in met
elevation in meters (Feet) (if applicable),
9.1.3 Classilication of soil by Practice D2487, if
determined, oF visual classification of soil (group name and
symbol) as determined by Practice D2488,
9.1.4 Moisttotal and dry density (unit weigh), to four
significant digits,
‘9.1.5 Water content (in percent), to four signi
9.1.6 Method used (A or B), and
(feed below ground surface or
int digits,
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