1.

METHOD

1.1 Date and Tim

Analysis of the quality of the fats in oil took place on April 28, 2021 online.

1.2 Tools and Materials

The tools and materials used are adjusted to the type of practicum being carried
out.

1.2.1. Asam lemak bebas

The tools used are a set of burettes, Erlenmeyer 250 ml, analytical scales. The
materials used are palm oil, olive oil, PP indicator, 95% ethanol, 0.1 N NaOH.

1.2.2. Bilangan saponifikasi

The tool used is a set of burette, Erlenmeyer 250 ml. The materials used are
palm oil, olive oil, PP indicator, KOH ethanol, 0.2 N NaOH.

1.2.3. Bilangan peroksida

The tools used are a set of burettes, Erlenmeyer 250 ml and an electric heater.
The ingredients used are palm oil, olive oil, 0.1 N sodium thiosulfate, saturated
potassium iodate, chloroform acetic acid (3: 2), 1% soluble fiber indicator.

1.2.4. Bilangan asam tiobarbiturat

The tools used were 250 ml Erlenmeyer, analytical scales, electric heating,
kjeltec, pH meter, spectophotometer, magnetic stirrer. The materials used are palm
oil, olive oil, distilled water, HCl 4 N, TBA 0.02 M.

1.3 Procedures
The tools and materials used are adjusted to the type of practicum being carried
out.

1.3.1 Asam lemak bebas

Weigh 5 grams of sample, add 100 ml of ethanol, shake until homogeneous,
add 3 drops of PP indicator, titrate using 0.1 N NaOh until pink.

1.3.2 Bilangan saponifikasi

Weigh 5 grams of sample, add 50 ml of ethanol-KOH, heated until
homogeneous, add 1 ml of indicator PP, titrate until it is white.
1.3.3 Bilangan peroksida
Weigh a sample of 5 grams, add 30 ml of chloroform acetic acid, homogenize,
add 0.5 ml of saturated KI, titrate using sodium thiosulfate until a light yellow color,
add 0.5 ml of soluble fiber indicator, titrate again using sodium thiosulfate until it is
white.

1.3.4 Bilangan asam tiobarbiturat

Weighed 10 grams of sample, added 50 ml of distilled water, homogenized
using a magnetic stirrer, adjusted the pH to 1.2 using HCl, carried out gestilation
using kjeltec, 5 l of distolate was taken into a test tube, and added 5 ml of TBA,
shaken using vortex, boiled for 35 minutes, the absorbance is read at the 538 nm
wave.