Scribd Logo
Upload

Welcome to Scribd!

  • Purification, Analysis. (Density 1.70g/mL) - . Until The Benzanilide Dissolves. Solution Will Then Be Added

    Uploaded by

    Samantha Lau
    48 views1 page
    This document outlines the steps for a chemistry practicum on bromination. It instructs the student to outline a pre-lab with details on reactants, solvents, reaction conditions, work-up and analysis. It also provides specifics on the bromine solution used, the amount of bromine needed, and the steps of heating the mixture and adding the bromine solution. The goal is to brominate benzanilide using 1.5 equivalents of bromine in acetic acid at 55-60 degrees Celsius.

    Original Description:

    Original Title

    practicum_202_bromination

    Copyright

    © © All Rights Reserved

    Available Formats

    PDF, TXT or read online from Scribd

    Did you find this document useful?

    Is this content inappropriate?

    Report this Document
    This document outlines the steps for a chemistry practicum on bromination. It instructs the student to outline a pre-lab with details on reactants, solvents, reaction conditions, work-up and analysis. It also provides specifics on the bromine solution used, the amount of bromine needed, and the steps of heating the mixture and adding the bromine solution. The goal is to brominate benzanilide using 1.5 equivalents of bromine in acetic acid at 55-60 degrees Celsius.

    Copyright:

    © All Rights Reserved
    Download as PDF, TXT or read online from Scribd
    Flag for inappropriate content
    48 views1 page

    Purification, Analysis. (Density 1.70g/mL) - . Until The Benzanilide Dissolves. Solution Will Then Be Added

    Uploaded by

    Samantha Lau
    This document outlines the steps for a chemistry practicum on bromination. It instructs the student to outline a pre-lab with details on reactants, solvents, reaction conditions, work-up and analysis. It also provides specifics on the bromine solution used, the amount of bromine needed, and the steps of heating the mixture and adding the bromine solution. The goal is to brominate benzanilide using 1.5 equivalents of bromine in acetic acid at 55-60 degrees Celsius.

    Copyright:

    © All Rights Reserved
    Download as PDF, TXT or read online from Scribd
    Flag for inappropriate content
    of 1

    Chemistry 202L

    Practicum

    Name: Bromination

    Mol. Wt.
    Volume solid
    Density -----
    % 100%
    Grams .098g
    Moles

    1. Using your laboratory textbook and your write-up of a similar experiment, outline a
    pre-lab: grams of reactants and solvents, reaction conditions, quenching, work- up,
    purification, analysis.
    2. Bromine comes as a 24% by weight bromine solution in conc HBr
    (density=1.70g/mL).
    3. You will need to use 1.5 equivalents of Br2.
    4. You will need to heat the benzanilide/acetic acid mixture in a 55-60 C water bath
    until the benzanilide dissolves.
    5. You will then turn off the heat and remove the water bath. The Br2 solution will then
    be added.

    You might also like