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    9 views35 pages

    Norma Composicion Quimica de Metales ISO 19272

    Uploaded by

    Carol Centeno

    Copyright:

    © All Rights Reserved
    Download as PDF or read online from Scribd
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    BS ISO 19272:2015 BSI Standards Publication Low alloyed steel — Determination of C, Si, Mn, P, S, Cr, Ni, Al, Ti and Cu - Glow discharge optical emission spectrometry (routine method) Sena 9230-DE-721 ry BS ISO 19272:2016 Low alloyed steel — REGIONAL VALE! Determination of C, Si, Mn, P, S, Cr, Ni, Al, Ti ‘and Cu - Glow discharge optical emission spectrometry (routine method) e bsi. ..making excellence a habit” BS ISO 19272:2015 BRITISH STANDARg, ih standard is the UK implementation of 150 19272:2015. ion in it .d to Technical ‘The UK participation in its preparation was entrustes Connie Ist/100, Methods of Chemical Analysis for Iron and Steel {A list of organizations represented on this committee can be ‘obtained on request to its secretary. This publication does not purport to incl provisions of a contract. Users are respons application. ‘© The British Standards Institution 2015. Published by BSI Standards Limited 2015 {ISBN 978 0 580 66322 2 cs. 77.140.20 Compliance with a British Standard cannot confer immunity from legal obligations. This British Standard was published under the authority of the Standards Policy and Strategy Committee on 31 August 2015. ‘Amendments issued since publication Date Text affected lude all the necessary ible for its correct & Bs 1SO 19272:2015 INTERNATIONAL Iso STANDARD 19272 irstedition 2015-08-15 ———$$_ $$ Low alloyed steel — Determination of C, Si, Mn, P, S, Cr, Ni, Al, Tiand Cu - Glow discharge optical emission spectrometry (routine method) { 1 ' i i ' i i t i a F i 5 i Aciers faiblement alliés — Détermination de C, Si, Mn, B.S, Cr, Ni, Al, : Teeth spectromttriedemisionopiqueddécharge luminescente (méthode de routine) & : i i : i : a i ‘ i it i i : i ; sive) Detection Minit Additional taformation on | p of precision data. Reference number 180 19272:2015(6) ©1580 2015, Bs 1SO 19272:2015 ISO 19272:2015(E) Contents ee ForeWOrd arbscopel a ies 2 Normative references. 3 Principle. m ne 4 giperetns— a aide Glow discharge opal emision spectrometer 411 General 4.12 Shortterm stability 4.13 Detection limit nn... 4.14 Data acquisition and processing system. 415 Others... be iz 5 Sampling... 6 Procedure... 6.1 Sample preparation 62 Selection of spectral lines 63 Optimization ofthe instrument 631 Geman 63.2 _ Setting the discharge parameters ofa direct current (DG) source. 63.3 Setting the discharge parameters of radiofrequency (RF) source... 634 Optimization of the detection system... 63.5 _Pre-burning time and integration time... 6.3.6 Validation of the instrumental parameters. 64 Calibration. a 65 Checking ofthe trueness ofthe method 66 Driftcorrection... 67 Analysis ofthe samples 7 Expression of results... 71 Method of calculation... 72 Precision 8 Test report... Annex A (informative) Detection limit... Annex B (informative) Additional information on international interlaboratory test... Annex C (informative) Graphical representation of precision data.. BS ISO 19272:2015, 1S0 19272:2015(E) Foreword ofnational standards {50 (the International Organization fr Standardization) isa worlwide federation of nations Soe Mt bodies (ISO member bodies), The work of preparing International Standards fs normal Stray ay through ISO technical committees. Each member body interested in a subject for which 1 Eee a Committee has been established has the right to be represented on that committee. INtTN organizations, governmental and non-governmental, in aison with ISO, also take part in the work 1SO collaborates closely with the International Electrotechnical Commission (IEC) on lectrotechnical standardization. tenance are The procedures used to develop this document and those intended for its further maintenance are described inthe 1S0/1EC Directives, Part 1, In particular the different approval criteria needed for the Aifferent types of 180 documents should be noted. This document was drafted in accordance wit editorial rules ofthe ISO/IEC Directives, Part 2 (see www.iso.arg/directives). Attention is drawn tothe possibilty that some ofthe elements of this document may be the subject of Patent rights 80 shall not be held responsible fr identifying any oral such patent rights. Details of any patent rights identified during the development ofthe document will be in the Introduction and/or on the 150 lis of patent declarations received (see wwivisoorg/patents) Any trade name used in this document is information given for the convenience of users and does not constitute an endorsement. For an explanation on the meaning of 1S specific terms and expressions related to conformity assessment, as well as information about 1S0's adherence to the WTO principles in the Technical Barriers to Trade (TBT) see the following URL: = ‘The committee responsible for this document is 1S0/TC 17, Steel, Subcommittee SC 1, Method of determination of chemical composition. 3e30 (roivodat ote Healt malioase (wientwin') A oan eee oe f se Bs 150 19272:2015 INTERNATIONAL STANDARD 10 19272:2015(E) Low alloyed steel — Determination of C, Si, Mn, P, S, Cr, Ni, Al, Ti and Cu - Glow discharge optical emission spectrometry (routine method) 1 Scope This International Standard “ic iD-OES] nal Standard specifies a glow discharge optical emission spectrometric (GD-OES) ‘The content ranges to which the method is applicable are shown in Table 1 Table 1 — Content ranges ‘Content ranges Element mass fraction, % c 0.060t0035 s 0,14 10 150 Mn 0,090 00,70 P 0,010t0 0,070 s 0,005 t0 0,050 cr (0,008 to 0,65 Ni 0,050.0 0,50) Al 0,006 t0 0.90 T 0.01410 0,13 wu (0,005 to 1,00) 2. Normative references The following documents, in whole or in part, are normatively referenced in this document and are indispensable to its application. For dated references, only the edition cited applies. For wndated references, the latest edition ofthe referenced document (including any amendments) applice ISO 5725-1, Accuracy (trueness and precision) of measurement methods and results — Part 1: Gener principles and definitions Part 1: General ISO 5725-2, Accuracy (trueness and precision) of measurement methods and results — Part 2: Basic ‘method {for the determination of repeatability and reproducibility ofa standard measurement noth 1S0 5725-3, Accuracy (trueness and precision) of measurement methods and results — Part 3: Intermedi ‘measures of the precision ofa standard measurement method eee ations 150 14284, Steel and iron — Sampling and preparation of samples for the determination of chemical composition 1S0 14707, Surface chemical analysis — Glow discharge optical emission spectrometry (GD-OES) — Introduction to use (© 150 2015 Allrights reserved 1 i i i i : t t i i i i t i i u ' : i i i i i i i i BS ISO 19272:2015 ISO 19272:2015(E) 3 Principle ‘The method used involves the following steps: orradio frequency 2) asample witha fat and smooth surface used asthe cathode of2 re Sue! glow discharge device; nd ions from the ¥) cathodic sputtering of the sample surface, atomization of the sputtered

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