(fly 407 - 07°" TABLE 2 Continued Cemooaten a 8 19 Foc, 8 precy Den HCl 59 FeCl, Tome He igcace 01 9Snci, 59 Foch, 160 mL hana! (95%) oF metanal (95%) 29%:0% 0) amen 80. “eps HC Saab 5-90 Immerse or swab few seconde at ame unt! dese resus ae obtanes Immerse or swab ow second to tow minutos Use carted and tested nod, Add he HC! us betre using. immerse 260s Og optic ammonium ORGS 06 rs water NH,OH "RG, OF To SEGA oe SAY alana. Tate SATs OA OF + g ammonium perstate eo nl water Tee omc A. OF 20-50 ml Hy Os (6) 19.000, 100 mt water 15m Nil OH 1S mLH.O, 8%) ‘Src water 4 pelts NaOH 5 a NACN or KCN 59 Nig $0, 109 Nac 39 FeSO, og nadk Ome He SO. 190 rs wate TomLHNO, 5 mk water 2oFecy 30 ml water {60 mL. shanol or methanol 1 sodtum servomate ‘9NaGi 4 mtHs SO. 250 ma water Tia Wash, Paros Coan vatcs Gracy wit copper caren ot alay to ba athe. Wr ‘morse or swab 01 min. Fam os esha luminum bronze remo oy No. 82 Use a carted and ested nod, Electcly at 6 V fr $+. Use aluminum cathode \Wen mising, add NaOH plots last, For best ost use before pelts have dssohd, Use a certo’ ana totes hood—Can give of exemaly poisonous hyeogan evan Precauon—Aso pasoneus by ingestion as wel as skin cortact. Uso a ceritos ana testeshood~—Can give of extremely petonous hyeogen cyan Procaulen-Aiso plconcus by ingeston as wal as xn canal Eclat 6 fa) 58 rsa. (©) 206 forfeits ana gonera structure (e) lo 8 min for enriso, tocol a 6-10 V (041A or 5-15 Use cated and testes od. Do not store Electolyte at 15 for 20 60, Use pat ‘Copyiht by ASTM intl sighs reserved; Thu Sep 20 11489 EDT2012_ owloaéedpined by MC MASTER UNIVER:(fly 407 - 07°" TABLE 2 Continued eae Cemooaten Preceaare se 5 ammonium acetate Eloctoyse #03 Aen? for 5:90 8 ‘3 saan Posuele mL NH, OF 1800 mater 8 mt, SO. Use a cette’ and totes hood. Swab gonty 10-18 & nse wih methanol and blow dy. SS mL NOS Yelp to chemically povah, ital ech loo mig, tnaw wie No 8. Donat tore, tom aoe aos ‘SmiH, 70, 86 SomLHNO, Use a cen and tested hood. Saab gery 5-15 s.Pnse wih ebro or methanol and Orn Hy POs Bow ary. Do net store 20 mace tis sr 75 mL acwio aos 25 mL He 0 (90%) Use carted and testes hood. Immerse 6-15 2. Da not ore 38 25.01. HE Saab 3-20 ‘SmL water 0 2g AgNO, Noe AgNO and wate thon ade HF and HNO, Swab 6-2 min 25m HNO, w 25 mL HNO, SE 5 PT a RT HO, DS TARTS, BS EH TS ag SAE EDT 18m acote acs oF OmL FCT TES AT aS SSE TO, ETE Te HOTS 8 TE 0m HNO, 00 mM tng to ul ally. Swab or Inmet few seconds to a ranula. = Ti gc, Tse a oetiied end lesied Rood. Swab few seconds o 8 minute 10 mL HNGy 00 ml co 3m HNO, a Rao 25m Hel (0) Use hot. Worm hl tlm on gel alge uc slivers presen, Ammonia wi so mi water remove tin, 6 a Use a certos ana testes hood—Can give of extremely potonous hyetogen cyanide. 0. ammonium persutste _Prosnuton Also posarcus by ingestion as wel as ein contact Mc 1's 1 mature of So- eo mt water lone and ut bere uae, (A mitre ots cepa ofeach wil cover ne aulace ot + 3 Inia mount) Irmorsa is ~2 mn tog KN 00 mt water 66 some Use cette and testes hood. Swat 9-10 imma to 2 min, 1SmLHNO, aon HCl 7 s0.ml parcione sed Use in wash dounipereno fated fume head. Precaution—Keep oe! when mixing and 10 mL 2butxyotnanel Yom ethane (08%) Om water 68 3 mt peer acis 35 mL 2oueqenaro| emi methan! abe) °° 5 ml pectoris ais 70 S mune 2mLAGNO, (5%) 28 mL water se Elcote at 30-65 V for 10-80 Use in wash douniperenio fated fume head. Precauton—Kgp 06! when mixing and use. Eletoye at 60-150 V fr a0 Use in wash downers rated fue hood. Precaution Keep ooo! when ising and Use: Becvoye at 20-60 V fr 1-5 min Do ha store ‘Swab or 60 |Add 5-10 cops of nis eoluton one tin! plsing whe! which has besn charged with ‘th posing seluton. The spocmen is plshed on tis whes! url the suraco tus Back sil waters hen slow dodo the whoa and pling contd ul he suaco 's bright Ath ume Pe specimen shoud be ready lor examination va polarized ight Noto—lse ner substance between Goth and wheel to prevent aac of he wheel. Wear appropriate gloves. ‘Copyriht by ASTM intl eights reserved; Thu Sep 2012149 EDT2012. 9 owloaéedpined by MC MASTER UNIVER:(fly 407 - 07°" TABLE 2 Continued eae Cemooaten Preceaare 4s mL ENO, emi water 8 20 mL HC! lectotie teh-use carton ethode and parm wre connacon lo specimen 25 9 Nact (@) 8 ac for + min eS mk water (b) 5-20 Vac 12 min {e) 20 acter 1-2 mn For tch-polshing, use short times. Ate ichng, water ans, alechol ins, and dy. os 1-5 mL HNO, ting at nroased, sonst decroasd wih ineroatod porantage of HNO, 100 mt thant (95%) or mathano! (95 {a} Inmase low soconde to 8 mine. (0) Immerse 5-40 in 5% HNO, sluton To remave san, mmaree 25 8 in 10 % HC Forinoonels and Nimoncs, use § mL HNO, soltton—slectoyc at $-10 V for 5-20 5. (6) Swab or nmore sovra minds. (6) Saab 5-60. 240, may be inereasod to 30 min means! oly depending o alloy {etnandl i netble wit over 5% HNOy) Bont soe, 18 Sgpere aca Immerse 1-2 sa ie and inmesiatoly rinse wih methanol. Repeat as en as neces Sack, sary. (Long immersion times wil result coppe” deposition on surace) Dom HCL 200m ethane! (955) oF methane! (5 8) 6 4 gplcre ada ‘Compostion gen wil sruato with pic ac. Immora few seconds toa minute o mere 100 mt thanal (95 9] oF than! 5 ‘Adding @ wating ager such 35 zophorn chloride wl insoase respons. 7 03 pete see Tarrpbaton giv waar Sion wh pe ac Trees Tow S6cOnSe TP 5 pe Hc minute o more 100 mt ethanol 95%] of ethan (95%) 7 Tog porassum metasiouti Tamarse TTS 5. Bat ress ae somaince cba By Wet SCAN TY Wi Nes TE 100 water S9cu, 0 mL water 25 mL shanol (950) of mothana (95% w Bm Gr Tamers of awa Tow S0cORS 1 TE Tn. Paaclon maybe aSclrod by aang a ew 1 g pete sca chops of 3H Oy. Optional (or por austente gran Boundales temper apecnan st 10 mt ethanl (95 4) or ethan! (95 8) '600-900"F pro te preparaion. e 2 gpiere aca CCompositon given wil strate the gluon wih pire ci 1 9 sodium decyoanzene stone (a) immerse lew soconde fo 8 mine. ‘oo mt water (@) immors 1 15 min wih aoa swabbing Tor Honey gain boundary attack, 2 59 FeCl, Immerse 5-10 Ss rops Ho 100 rs water 2 10900, Use a cerita and tested noc) Elactoyic l6V fr 5-60. Altace eabies 100 me water (o) Bectoipio as V tor 3-55 ee 10 mL He SO, Use a cored and testo hood, Precaution Adel H, S04 sly to water and ool, hen Om HNO, 438 HNO, morse 20, Swab nrunning wale. Repeat oe tines 8a opal gy 86 2gplere ade Use a cortted and tested hood. immerse in bling saison for § min. Pecaution—De not 2g NAOH boi eyanyerou pene ai is unto ard highly expe. Aral: Elect a 100m water 13 for 20 (cor tomportra). Use stainloge sel ease 86 Sg one ac Use a cette and estes nod, Salton shoul be ‘rsh repered, Immerse 15-25 min 4mbHe0, (0%) when specimens or pars cannot be given usal metallographic posh Mupe tong 00m water ray be murs ” s0mL HNO, Use a cere and lst hood—Can give fl trogen done gas, Precauton Mx HCL 25-59 mL Hel and gycerl oroughlybetore aang HNO, Do not store Properly lscard before solution 0 mL ghyeoral tars a dak orange color. Immerse or swab few secon o few minutes. Higher poor {ge of HCl maize peng, Ao! watering just prior fo etching may be used Yo ache “he reactan, Sometimes few pases onthe nl posshing whee ase necessary 1 remove a passive surce 8 10 mLHNO, Use a certtios and tested hood-Can give of nirogen side gas, Precaution Properly 2onL Net ‘deca Dolor sluion asi dark range clr lnmore few secaras loa mst som waler Mach stonger reaction than No.7. ‘Copyriht by ASTM intl eights reserved; Thu Sep 20121459 EDT 2012. owloaéedpined by MC MASTER UNIVER:(fly 407 - 07°" TABLE 2 Continued eae Cemooaten Preceaare Ime 2-8 oops Goel 20 s0mLHNO, Use a cetied and tested naocinaree 2-10 8 De not lore. Property acd ater 2omL HF se. Seluton decomposes on slandng, 20-40 mk gyearol 1 5 mL HNO, G pete aca 200 mi ethane! {8 ) or methane! (5 we tame Ho! 100 mt ethanol (85%) oF mathanat (85 23 concentatod HNO, o 29cuoy 40-80 mL ant (95 4) or mathal (9 96 29CuG, aomcHel 40-80 mt tant (95%) oF metal (9 ‘fom water 96 85.9 NaOH 50 mt water or 4sqKoH eo mL water 28 10.6 KyFOICNy 10g KOH or Naoe 100 rs water 9 25 mH! few grains potassium metabisufte 100 109 Foc, 11 2900, 20m Hel 0 mt water 10 20mLHNO, “dm HC! 20 mi metanel (29%) 14 SmLHNo, “SmLHCL 0'ml water ‘Sm HNO, 0 mH! sami metrane (99%) ‘Copyriht by ASTM ital eights reserved) Th Sep 20102145 owloaéedpined by MC MASTER UNIVER: “This etchant is equivalent to@ 1 1 more of No. 6D an No, 74 (5% HNO,), Swab for "o's ertonger, Immerse 5-20 min or lecyie at 6 Vf 3-5 Use a cent and tested nood. Beco at 0.2 Alem? for few second ‘Submerged smabing for tw seconds to several minutes Alas ferfte more rex than 5) Immerse or swab fow seconds to fow minutes 5) loco at 6 V for 5-10 Comscston of saaions approximately 10 N. Eecboje at 25 V fr few seconds. Stans sigma and cn yolow wo red brown eto gray t lve gay, carides bal touched, aus tent not toed, Use a certios ana totes hood~Can give of exvemely posonous hyetogen cyanide Pracauton—Aso pasonous by ingostion as wal as skin eoract. Use as. (a) Inmmarse or svab 15-60 5. Stans caridos and sma. To erent, No.3 electo- Wyte at 4 V wil tack sigma, but rt carbides. ping occurs, roduc vage ) (by Immerse in Fresh, ho san 2-20 min. Sains crises dark foe yoson gra ue, Austen une brown on averting (9 Swab 50 5 mmarson we produce asian ach) Flow wth water tree, sano! se, dy. ox fosh (For stock solution, mix ist tree toms, Ads potas mabisve jst lore 0) Immerse few seconds © afew mento, Imnmers ow seconds Use a cenit’ and tested noos-immere 5-60 (CxO, may be nereased up 020g Yor ‘fel alloy, Staring ana pting neease as CxO, nereased) Use 8 canted and tested nod. lett at 6 V for 30-60, Aacks caries ony, Use a certiog ana testes hood. Immerse 10-60 Use a cena and tated hood, mmr 10 mn er ngs Use canta and tasted nood.Praautlon—aca H $0, slow ta HC wih string, coo ‘en ads HNO, Proper Gacard wnen dark erange cle Swab 10-30 EDTION2 1g(fly 407 - 07°" TABLE 2 Continued eae Cemooaten Preceaare 07 som HPO, se «cared and tested rood. Precavion—Mix Ha PO, and HNO. throug, then a som. He SO, H, $0, siowy wih sting, Use een, bt alow o ooo. ecboye a V fr few seconds “om HNO, Sow alscloraten wil form at eos of specimen. To sow easton, ade water 0 100 ‘iL vry cart ah sting, ack Beatle mounts. 108 SHOMLH, 80, xectrotytie at 6 V for 5-10. Tands opt wit longer tines 109 50 mLHCI Make tosh but alow to stand 30 min o ave plating out copper Immerse fw seconds to 25 mL HNO, Yon minutos, 1acuce. 10 tom Hor Immors to soverl minutes unl deeply ches, Follow with ght repli Sm HNO, 185 mL hana! (25%) of mebanal (95%) 1 SmLH. 0, Use a corte’ and estes hood, Elect at 10 V (0.2 Alon fr 6-50 5. Rove T 8 gc:0, fra Chih ars aftr rato than gram boundries sO ml He 0.30 19 15 aot acs Use a cored and tested hood, Dont store, Use fresh soliton at 80°C (176°), eomL gyro! 4 15m cote ack Use a corttod and tested hood. Use rsh soliton at 40-42°C (104-108°F). nmorse 20 HNO, 420 min dopeneing on doph of worked mt ayo. Clash with eatonn ning wate. 1s. 100 mt acto acd Use a corttied and teste hood. Immerse 10-30 min depending on depth of worked metal 10 mL He 0 (90%) Tayor. Clan In HNO, necessary 16 5-10 @ AgNO, 90 mt water Sma. uw? tometer (a) immerse for 45min Fatow wih lacy toh at low curent dety in same so 80 mL water Ihton T specmon has conerablo sutace fw, immerse n conconatod HCI fra Yow (2) marae for 2 mi TF TRL ARO, Swab SS aor and 76-2 min or Te an O WRT, 75: ethylene gyal 25 ml water oo Trt RO; ae 9 STH TOT TE SWOE TT HTS F BITS TOG TE BE PAT DD 60 mL diethylene goo! 20.m wale 7a “Ont HE Traore wih go agaon 33T 7H D7 att PO, Capoatin aa “4g pene acd 100 ml thanal (95%) oF rthanol (05 (a) Immerse with gor agtaion 10-30. (0) Te nceasestahing immerse and wh wh & meniscus lye, Listy sep ‘lenant over surtace url dark iin Sevaons 12 2g cxale aca Sab, 123 60 mi My PO. Eectolic: Use slaniess sol cathode, Space elecraos 2 cm apart, Sta at 8 de. At 400 ethanol (85%) ter30' mainian at, sa SmLacete oa Use a cortied and tested hood, immerse win gentle agtaton 10-60 Som water 6 pore aes 100 mL tana (95%) er methane (95%) rs tomL acete acs Use a cortied and tested hood, Immerse wih gentle aghaton 15-0 5 6g pete ace 100 mt thanal 95%) or ethanol (85% 126 a0 mL svete ane Use a certiid and teste hood. Immerse wih gone agitation 1-30. ‘Sri water 6g pete ace 100 mk ethana (96%) er methane (95%) ‘Copyriht by ASTM intl eights reserved; Thu Sep 2012149 EDT2012 owloaéedpined by MC MASTER UNIVER: