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  • India Test House: SAMPLE: Steels For Piston Pins Measuran TEST METHIS 228 (Part 6) : 1987 (RA 2018)

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    Gaurav Kumar
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    This document summarizes the results of a test measuring the chromium content of a steel sample using standard volumetric analysis methods. It reports the individual test results, calculates the mean chromium content as 0.4586% with a standard deviation of 0.0135%. It then lists sources of uncertainty and calculates a combined standard uncertainty of 0.0079% and an expanded uncertainty of 0.0157% at a 95% confidence level. The final reported chromium content is 0.46±0.016%.

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    This document summarizes the results of a test measuring the chromium content of a steel sample using standard volumetric analysis methods. It reports the individual test results, calculates the mean chromium content as 0.4586% with a standard deviation of 0.0135%. It then lists sources of uncertainty and calculates a combined standard uncertainty of 0.0079% and an expanded uncertainty of 0.0157% at a 95% confidence level. The final reported chromium content is 0.46±0.016%.

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    © All Rights Reserved
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    9 views2 pages

    India Test House: SAMPLE: Steels For Piston Pins Measuran TEST METHIS 228 (Part 6) : 1987 (RA 2018)

    Uploaded by

    Gaurav Kumar
    This document summarizes the results of a test measuring the chromium content of a steel sample using standard volumetric analysis methods. It reports the individual test results, calculates the mean chromium content as 0.4586% with a standard deviation of 0.0135%. It then lists sources of uncertainty and calculates a combined standard uncertainty of 0.0079% and an expanded uncertainty of 0.0157% at a 95% confidence level. The final reported chromium content is 0.46±0.016%.

    Copyright:

    © All Rights Reserved
    Download as XLSX, PDF, TXT or read online from Scribd
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    of 2

    India Test House

    45/7 , Village Prahalad Pur Bangar , Near Kali Mata Mandir , Rohini Sec - 30 , New Delhi - 110042

    SAMPLE: Steels for Piston Pins


    MEASURAN Chromium
    TEST METHIS 228 (Part 6): 1987 (RA 2018)

    Sources of Uncertainty:
    TYPE: A By Human error(Repeatability)
    TYPE: B Subsidiary factors as sources of uncertainty

    Standard Uncertainty= Std.Deviation/√No.of Observation

    TYPE :A
    Abbreviation:W = Weight of Sample
    V1= Vol. in ml of Std. FAS Sol. added
    N1 = Normality of Std. FAS
    V2 = Vol. in of Std. KMnO4 Sol.
    N2 = Normality of Std. KMnO4
    Calculation , (V1*N1-V2*N2)*1.734/W

    Normal Volume Results


    Volum
    Normalit ity of
    weight of e of of Chromiu Actual- sq (Mean-
    Sr.No. y of Std. Std.
    sample FAS KMnO4 m As Cr Mean Actual)
    FAS (N1) (V1) KMnO4 (V2)
    in %
    (N2)
    1 1.0243 0.03 25 0.03 16.2 0.4469 0.0117 0.0001364
    2 1.0008 0.03 25 0.03 16 0.4678 -0.0092 0.0000849
    3 1.0037 0.03 25 0.03 15.9 0.4716 -0.0130 0.0001701
    4 1.0245 0.03 25 0.03 15.8 0.4671 -0.0085 0.0000730
    5 1.0345 0.03 25 0.03 16.3 0.4375 0.0211 0.0004457
    6 1.0052 0.03 25 0.03 16.1 0.4606 -0.0020 0.0000040
    1.0155 25 16.1 0.4586 0.0009141
    Standard Dev. = Square Root ((Sum)/(n- 0.0135
    TYPE:B

    std.Unc
    No.of ertaint
    Human errorStd dev Values(x) Ob./CF y or Ux R(Ux)=Ux/x
    0.4469 0.0135 1.016 2.449 0.0055 0.0054
    0.4678 Balance(U1B) 1.0155 2 0.0003 0.0001
    0.4716 Oven(U2B) 105 2 1.1 0.0052
    0.4671 Pippet(U3B) 25 2 0.12 0.0024
    0.4375 Burette(U4B) 9.0 2 0.0600 0.0034
    0.4606
    Env. Condition(U3B) 27 2 0.8000 0.0148
    0.4586 R(Uc) 0.0171
    Uc(y) combined 0.0079

    Expanded Uncertainty(U) =
    Combined Uncertainty*Coverage Factor0.01571
    Coverage Factor =2 at 95% confidence level
    Total Uncertainty for result= 0.46 ± 0.016
    3.4263

    Chemist Checked By

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