DATA REPORT GCMS-QP2010 ULTRA SHIMADZU

Sample Information
Analyzed by : Admin
Analyzed : 9/06/2021 5:09:58 PM
Sample Type : Unknown
Level # :1
Sample Name : Metanol 10
Sample ID :
IS Amount : [1]=1
Sample Amount :1

Chromatogram Metanol 10 C:\GCMSsolution\Data\Project1\Metanol 10.qgd

TIC
52

(Normalized)

112
70

169
53

156
38

179
9394

122 123124
90

138

1501152

170171
25

95

144
5859

127

164163
20 1921

54

71

96
65

180
46

165
61

157 158
88
3132

196
121625
3633 353437

146145
97
42

9998

177
137
131031

155
11141513
14

1012100
72

1111179816

11890
131635

143139
620 63

121928
57

148147
10 3
101907

198
1210
101172819

89

115534

18 7 188
114140421

149
110064

119921

197
7743

111110
698

111616526091

168
5051

11334 3
8586

117723

199
1177465
66667

116667

119943
13

181
4

9291
7765

2
349140

195
78908

1832
118854
84
1
444543

200
23242

448749
1817
16

29876

8832

6
5565
3 1
2

6
5

10.0 20.0 30.0 39.0

min

Peak Report TIC

Peak# R.Time Area Area% A/H Name
1 5.280 4948319 0.51 17.49 1,2,3-PROPANETRIOL
2 5.550 613697 0.06 6.52 1-BUTANAMINE, 2-METHYL-N-(2-METHYLBUTYLIDENE)-
3 5.873 1120832 0.12 14.07 BENZENEACETALDEHYDE
4 7.558 1008386 0.10 8.62 4H-Pyran-4-one, 2,3-dihydro-3,5-dihydroxy-6-methyl-
5 9.046 1007246 0.10 14.62 2,3-DIHYDRO-BENZOFURAN
6 10.133 453057 0.05 6.85 2-METHOXY-4-VINYLPHENOL
7 11.256 369049 0.04 6.07 Trimethylene borate
8 11.392 374173 0.04 3.47 1H-CYCLOPROP[E]AZULENE, 1A,2,3,4,4A,5,6,7B-OCTAHYDRO-1,1,4,7-TETRA
9 11.607 2057343 0.21 2.50 Caryophyllene
10 11.909 333580 0.03 3.98 2H-Pyran-2-one, 3-acetyl-4-hydroxy-6-methyl-
11 11.980 1296612 0.13 4.42 5,7-Dodecadiyn-1,12-diol
12 12.063 945654 0.10 4.73 1,6-METHANONAPHTHALENE, DECAHYDRO-1,4,8A-TRIMETHYL-9-METHYL
13 12.304 5291957 0.54 11.00 Ethanol, 2-(2-butoxyethoxy)-, acetate
14 12.415 4197946 0.43 4.65 1-TETRADECANOL
15 12.554 1156625 0.12 3.93 Naphthalene, decahydro-4a-methyl-1-methylene-7-(1-methylethenyl)-, [4aR-(4a.alpha.,7
16 12.669 1940857 0.20 6.23 Phenol, 2,4-bis(1,1-dimethylethyl)-
17 12.823 3103469 0.32 9.31 D-Allose
18 12.950 1148766 0.12 5.53 Octadecane, 1-chloro-
19 13.117 2054724 0.21 5.31 2(4H)-Benzofuranone, 5,6,7,7a-tetrahydro-4,4,7a-trimethyl-, (R)-
20 13.273 409964 0.04 4.12 Cyclohexanemethanol, 4-ethenyl-.alpha.,.alpha.,4-trimethyl-3-(1-methylethenyl)-, [1R-(1
21 13.386 6997271 0.72 4.39 DODECANOIC ACID
22 13.557 1845242 0.19 5.60 4,4,8,10,14-Pentamethyl-17-(perhydro-2,6,6-trimethyl-2H-pyran-2-yl)-5alpha-gonane-3
23 13.653 588793 0.06 2.74 Caryophyllene
24 13.707 1022257 0.11 3.21 2-Dodecen-1-yl(-)succinic anhydride
25 13.792 5926418 0.61 2.55 Caryophyllene oxide
26 13.908 1073100 0.11 3.60 2,4A,5,5-TETRAMETHYL-4A,5,6,7,8,8A-HEXAHYDRO-1(4H)-NAPHTHALENON
Peak# R.Time Area Area% A/H Name
27 13.940 726104 0.07 2.40 9.beta.-Acetoxy-3,5,8-trimethyltricyclo[6.3.1.0(1,5)]dodec-2-ene
28 13.983 1584881 0.16 5.31 TETRADECANAL
29 14.134 965851 0.10 3.40 Tetrahydroionyl acetate
30 14.237 1460683 0.15 4.98 2-METHYL-7-ENDO-VINYL-BICYCLO[4.2.0]OCT-1(2)-ENE
31 14.308 1244555 0.13 4.27 1,1,4,7-TETRAMETHYLDECAHYDRO-1H-CYCLOPROPA[E]AZULEN-4-OL #
32 14.465 6044208 0.62 5.26 Tetracyclo[6.3.2.0(2,5).0(1,8)]tridecan-9-ol, 4,4-dimethyl-
33 14.575 1356644 0.14 3.13 10,12-HEXADECADIEN-1-OL
34 14.628 2333344 0.24 2.58 1,4,8-Dodecatriene, (E,E,E)-
35 14.683 2315017 0.24 3.36 1,1,4,7-TETRAMETHYLDECAHYDRO-1H-CYCLOPROPA[E]AZULEN-4-OL #
36 14.769 957657 0.10 3.57 Cholestane, 4,5-epoxy-, (4.alpha.,5.alpha.)-
37 14.849 3350244 0.34 3.28 ANDROSTAN-17-ONE, 3-ETHYL-3-HYDROXY-, (5.ALPHA.)-
38 14.961 13042008 1.34 2.76 Patchouli alcohol
39 15.150 1147513 0.12 5.02 2-Heptanone, 6-methyl-6-[3-methyl-3-(1-methylethenyl)-1-cyclopropen-1-yl]-
40 15.222 1426304 0.15 3.23 2(1H)Naphthalenone, 3,5,6,7,8,8a-hexahydro-4,8a-dimethyl-6-(1-methylethenyl)-
41 15.284 577033 0.06 2.24 TETRADECANOIC ACID, METHYL ESTER
42 15.344 4421712 0.45 4.45 2-Cyclohexen-1-one, 2-hydroxy-4,4,6,6-tetramethyl-
43 15.511 1517449 0.16 4.51 1H-Cycloprop[e]azulen-4-ol, decahydro-1,1,4,7-tetramethyl-, [1ar-(1a.alpha.,4.beta.,4a.b
44 15.649 1008368 0.10 5.06 1,3,3-TRIMETHYL-2-(2-METHYLCYCLOPROPYL)-1-CYCLOHEXENE #
45 15.726 928701 0.10 4.08 6-(3-HYDROXY-BUT-1-ENYL)-1,5,5-TRIMETHYL-7-OXA-BICYCLO[4.1.0]HEPT
46 15.811 6511088 0.67 5.12 TETRADECANOIC ACID
47 15.967 524617 0.05 2.76 LACTAROPALLIDIN
48 16.033 405490 0.04 2.45 Cholestan-3-one, cyclic 1,2-ethanediyl acetal, (5.alpha.)-
49 16.146 1749548 0.18 5.76 4,4,7A-TRIMETHYL-1,3-DIMETHYLENEOCTAHYDRO-3AH-INDEN-3A-OL
50 16.240 1503331 0.15 4.93 1-(3,6,6-TRIMETHYL-1,6,7,7A-TETRAHYDRO-CYCLOPENTA[C]PYRAN-1-YL)-
51 16.395 3392578 0.35 6.55 ANDROST-4-EN-3-ONE, 17-HYDROXY-, (17.BETA.)-
52 16.589 33297998 3.42 3.56 Pentacyclo[5.2.1.0(1,5).0(5,9).0(6,8)]decane
53 16.813 22361770 2.30 3.93 1-NAPHTHALENOL, 1,2,3,4-TETRAHYDRO-
54 16.933 5194482 0.53 3.39 2-PENTADECANON, 6,10,14-TRIMETHYL-
55 17.034 1069556 0.11 4.18 14-PENTADECENOIC ACID
56 17.137 860280 0.09 4.31 Ethanone, 1-[1-hydroxy-3,3-dimethyl-2-(3-methyl-1,3-butadienyl)cyclopentyl]-, [1.alpha
57 17.226 5164858 0.53 7.11 2,6,10-TRIMETHYL,14-ETHYLENE-14-PENTADECNE
58 17.443 2218017 0.23 4.31 6.beta.,6.beta.-Dibromo-6,7-methylenetestosterone
59 17.568 9231853 0.95 5.24 2,4-HEXANDION, 3,5,5-TRIMETHYL-1-PHENYL-
60 17.704 2365072 0.24 5.36 1,4,9-Decatriene, 1-phenyl-, (E,E)-
61 17.822 5114108 0.53 4.31 7-PHENYL-5TRANS-HEPTENONE-3
62 17.912 1399664 0.14 3.26 (-)-5-OXATRICYCLO[8.2.0.0(4,6)]DODECANE,,12-TRIMETHYL-9-METHYLENE
63 18.047 5763466 0.59 7.86 Corymbolone
64 18.159 1931795 0.20 4.18 3-Methyl-2-(3,7,11-trimethyldodecyl) furan
65 18.272 4949737 0.51 3.52 HEXADECANOIC ACID, METHYL ESTER
66 18.358 1210971 0.12 2.92 Neoclovene oxide
67 18.406 3286855 0.34 7.05 METHYL ESTER OF 3-(3,5-DI-TERT-BUTYL-4-HYDROXYPHENYL)-PROPIONI
68 18.639 4456099 0.46 7.90 22-Tricosenoic acid
69 18.721 5089576 0.52 9.19 ANDROSTAN-17-ONE, 3-ETHYL-3-HYDROXY-, (5.ALPHA.)-
70 19.097 67153677 6.91 9.78 l-(+)-Ascorbic acid 2,6-dihexadecanoate
71 19.293 9462522 0.97 6.36 1-(2-METHYLPHENYL)-2-PROPEN-1-OL
72 19.421 8236136 0.85 9.94 Hexadecanoic acid, ethyl ester
73 19.617 3712146 0.38 6.21 Corymbolone
74 19.717 5452314 0.56 10.28 1-(2-Hydroxyethyl)-3,6-diazahomoadamantan-9-one
75 19.925 1443956 0.15 3.50 1-O-HEPTYL-D-MANNITOL #
76 19.983 1800702 0.19 4.44 Heptadecanoic acid, methyl ester
77 20.033 1843591 0.19 4.77 2-Hexenal diethyl acetal, trans
78 20.167 2724636 0.28 7.88 D-GLUCONIMIDIC ACID, N-(ACETYLOXY)-4-O-(2,3,4,6-TETRA-O-ACETYL-.B
79 20.283 1787470 0.18 5.45 HEXADECANOIC ACID
80 20.351 1308206 0.13 3.79 Hexadecane-1,2-diol
81 20.444 2193873 0.23 6.68 HEPTYL OCTANOATE
82 20.517 1396238 0.14 4.76 FURAN, 2-ETHYLTETRAHYDRO-5-METHOXY-2-METHYL-
83 20.622 821048 0.08 2.95 1-ETHYL-6-(1-PIPERAZINYLSULFONYL)BENZO[CD]INDOL-2(1H)-ONE
84 20.698 3555793 0.37 10.91 HEPTADECANOIC ACID
85 20.942 1599384 0.16 6.35 2,4-Dimethylpentan-2-ol decanoate
86 21.037 3208110 0.33 6.96 Phytol
87 21.161 4390662 0.45 3.62 9,12-Octadecadienoic acid (Z,Z)-, methyl ester
88 21.268 4267319 0.44 3.83 9,12,15-OCTADECATRIENOIC ACID, METHYL ESTER
89 21.378 1424903 0.15 3.65 2-NONADECANONE
90 21.468 13536040 1.39 4.18 Phytol
91 21.729 2705533 0.28 4.52 Octadecanoic acid, methyl ester
92 21.808 1082091 0.11 3.94 ISOPROPYL 2-METHYLBUTANOATE
93 22.058 33621474 3.46 9.10 9,12-Octadecadienoic acid (Z,Z)-
94 22.157 36534778 3.76 9.47 9,12,15-Octadecatrienoic acid, ethyl ester, (Z,Z,Z)-
95 22.506 13142651 1.35 6.52 Octadecanoic acid
96 22.624 11910073 1.22 8.45 NAPHTHALENE, 1-(PHENYLMETHOXY)-
97 22.789 10656092 1.10 11.17 Hexadecanamide
98 23.016 5951751 0.61 6.41 Tetracosane
99 23.112 4513528 0.46 6.28 1,4-Methanoazulen-7(1H)-one, octahydro-1,5,5,8a-tetramethyl-
100 23.234 5159391 0.53 7.04 2,6,10-TRIMETHYL,14-ETHYLENE-14-PENTADECNE
101 23.400 4238847 0.44 7.39 2,4-DIBUTYL-1,3-CYCLOHEXANEDIONE
102 23.486 3265899 0.34 5.83 8,11,14-Docosatrienoic acid, methyl ester
Peak# R.Time Area Area% A/H Name
103 23.605 5923926 0.61 10.60 Bicyclo[4.1.0]heptane, 7-(phenylmethylene)-
104 23.775 2653257 0.27 5.28 Butanoic acid, 3-methyl-, 3-methylbutyl ester
105 23.842 1597761 0.16 3.43 ETHER, (2-ETHYL-1-CYCLODECEN-1-YL)METHYL METHYL
106 23.974 3223966 0.33 6.87 3,3'-Methylenebis(1,5,8,11-tetraoxacyclotridecane)
107 24.063 4279125 0.44 7.33 HAHNFETT
108 24.200 2446652 0.25 5.45 (1E)-1-(2-TERT-BUTYL-2-METHYLCYCLOPROPYL)ETHANONE SEMICARBAZ
109 24.275 2171864 0.22 4.91 PREGN-5-ENE-3,11-DIONE, 17,20:20,21-BIS[METHYLENEBIS(OXY)]-, CYCLIC
110 24.436 4666555 0.48 9.83 9-Octadecanone
111 24.575 2994376 0.31 7.31 HEXADECANOIC ACID, OCTADECYL ESTER
112 24.750 31653723 3.26 4.11 HEXATRIACONTANE
113 24.877 3174353 0.33 4.24 2-Pentadecanone
114 24.976 1932006 0.20 4.17 Octanamide, N-(2-hydroxyethyl)-
115 25.075 3702980 0.38 5.85 E-11-Hexadecenal
116 25.194 2937710 0.30 4.34 EICOSANOIC ACID, METHYL ESTER
117 25.268 2543332 0.26 5.35 13-Octadecenal, (Z)-
118 25.392 2077381 0.21 4.03 Cyclooctane, tetradecyl-
119 25.425 1029410 0.11 1.99 2,3,3-Trimethyl-2-(4-methylpentanoyl)-cyclopentanone
120 25.461 2210154 0.23 4.21 Cyclohexane, tetradecyl-
121 25.574 3858124 0.40 7.39 4,8,12,16-Tetramethylheptadecan-4-olide
122 25.744 1882556 0.19 4.67 Tridecanedial
123 25.831 5972246 0.61 7.36 9-Octadecenamide, (Z)-
124 26.009 15568625 1.60 4.25 14,16-Hentriacontanedione
125 26.160 9901444 1.02 10.87 .beta.-Sitosterol
126 26.317 1813585 0.19 2.49 Ergost-8-en-3-ol, 14-methyl-, (3.beta.,5.alpha.)-
127 26.407 11252546 1.16 7.19 TETRACONTANE
128 26.567 4672975 0.48 7.83 2-Pentadecanone, 6,10,14-trimethyl-
129 26.733 2655902 0.27 6.83 2,5-METHANO-1H-INDEN-7(4H)-ONE, HEXAHYDRO-
130 26.905 3449537 0.35 5.88 2,6,10-TRIMETHYL,14-ETHYLENE-14-PENTADECNE
131 27.056 4799775 0.49 6.13 Morpholine, 4-[3-[4-(1,1-dimethylethyl)phenyl]-2-methylpropyl]-2,6-dimethyl-, cis-
132 27.272 1817714 0.19 6.00 2-(DIMETHYLAMINO)ETHYL 2-METHYLACRYLATE
133 27.351 2293920 0.24 7.09 1-(1-HEPTADECYNYL)CYCLOPENTANOL
134 27.483 1069811 0.11 3.83 Cholestan-3,22,26-triol, 16-[2-thiohydroxyethyl]-, 3,26-diacetate
135 27.611 4131535 0.42 6.71 9,12-Octadecadienoic acid, ethyl ester
136 27.724 3792353 0.39 7.57 NONANOIC ACID, 9-(3-HEXENYLIDENECYCLOPROPYLIDENE)-, 2-HYDROX
137 27.937 2288521 0.24 6.50 1-Tetracosanol
138 28.034 9991248 1.03 3.91 HEXATRIACONTANE
139 28.253 6098044 0.63 8.48 HEXADECANOIC ACID, 2-HYDROXY-1-(HYDROXYMETHYL)ETHYL ESTER
140 28.384 1592305 0.16 4.43 4-HEPTANONE, 2,6-DIMETHYL-
141 28.493 2022859 0.21 4.25 DOCOSANOIC ACID, METHYL ESTER
142 28.533 1803870 0.19 4.15 1,2-BENZENEDICARBOXYLIC ACID
143 28.694 1655408 0.17 6.06 2-METHOXY-2-OXO-1-PHENYLETHYL OCTANOATE
144 29.096 26400365 2.71 15.70 OLEAN-12-EN-3-OL, (3.BETA.)-
145 29.309 3956960 0.41 4.84 Nonadecane-2,4-dione
146 29.443 3495831 0.36 6.23 3,6-Nonadecadione
147 29.603 3172754 0.33 5.87 Dotriacontane
148 29.808 1648187 0.17 7.01 5-DECANONE
149 30.054 7618802 0.78 16.93 Lupan-3-ol, acetate
150 30.469 7213173 0.74 10.28 PREGN-4-ENE-3,20-DIONE, 11,17,21-TRIHYDROXY-, (11.BETA.)-
151 30.525 3265610 0.34 4.62 STIGMAST-7-EN-3-OL, (3.BETA.,5.ALPHA.,24S)-
152 30.641 8673329 0.89 3.70 1-Triacontanol
153 30.768 2701760 0.28 5.55 1-Triacontanol
154 30.869 4317217 0.44 8.49 17-HYDROXY-10,13,17-TRIMETHYL-1,2,6,7,8,9,10,11,12,13,14,15,16,17-TETRA
155 31.019 3955569 0.41 5.49 9,12-Octadecadienoic acid (Z,Z)-, 2,3-dihydroxypropyl ester
156 31.133 19324921 1.99 4.02 HEXATRIACONTANE
157 31.351 2424428 0.25 5.12 2-Pentacosanone
158 31.582 17462753 1.80 17.67 4,4,6a,6b,8a,11,11,14b-Octamethyl-1,4,4a,5,6,6a,6b,7,8,8a,9,10,11,12,12a,14,14a,14b-
159 31.976 2652339 0.27 7.86 Lanosterol
160 32.058 1124508 0.12 3.40 Acetic acid, 3-cyclohex-1-enyl-1-methylprop-2-ynyl ester
161 32.113 1555202 0.16 4.31 1-Eicosene
162 32.200 970238 0.10 3.86 Octadecane, 3-methyl-
163 32.397 7858673 0.81 5.51 Tricosane-2,4-dione
164 32.528 7552183 0.78 6.30 3,6-Nonadecadione
165 32.779 4848283 0.50 4.73 2,6,10,14,18,22-Tetracosahexaene, 2,6,10,15,19,23-hexamethyl-, (all-E)-
166 32.908 1815059 0.19 7.39 OXECAN-2-ONE
167 33.039 1693117 0.17 5.72 Pentacosanoic acid, methyl ester
168 33.209 3542761 0.36 11.25 1-Pyrrolidinebutanoic acid, 2-[(1,1-dimethylethoxy)carbonyl]-.alpha.-nitro-, 2,6-bis(1,1-
169 33.580 30042290 3.09 5.23 17-Pentatriacontene
170 33.927 3131239 0.32 6.75 6-Tetradecanone
171 34.083 13791726 1.42 6.43 Hexatriacontane
172 34.381 2062893 0.21 7.71 2-Heptacosanone
173 34.584 2833616 0.29 9.59 TETRATRIACONTANE
174 34.787 1236919 0.13 5.35 5-Undecen-4-one
175 34.883 1535080 0.16 5.44 CELIDONIOL, DEOXY-
176 34.966 2073358 0.21 7.62 DOTRIACONTANE
177 35.175 3904267 0.40 5.14 2,5-METHANO-1H-INDEN-8-OL, 2,3,3A,4,5,7A-HEXAHYDRO-, ACETATE, (2.AL
178 35.293 1327065 0.14 5.73 13-Docosen-1-ol, (Z)-

Peak# R.Time Area Area% A/H Name

179 35.651 24206167 2.49 6.12 Tricosane-2,4-dione
180 35.821 8858997 0.91 8.06 3,6-Nonadecadione
181 36.042 1308582 0.13 5.86 3.beta.-Acetoxystigmasta-4,6,22-triene
182 36.167 968636 0.10 7.23 3'H-Cycloprop(1,2)-5.alpha.-cholest-1-en-3-one, 1',1'-dicarboethoxy-1.beta.,2.beta.-dihyd
183 36.351 852138 0.09 6.61 TETRAPENTACONTANE
184 36.456 1095467 0.11 6.32 2H-1-BENZOPYRAN-6-OL, 3,4-DIHYDRO-2,5,8-TRIMETHYL-2-(4,8,12-TRIMET
185 36.600 1064980 0.11 11.57 2-BENZYL-2-PROPENYL ISOPROPYL ETHER
186 36.782 866967 0.09 7.52 2H-1-BENZOPYRAN-6-OL, 3,4-DIHYDRO-2,5,8-TRIMETHYL-2-(4,8,12-TRIMET
187 36.965 696447 0.07 6.37 HAHNFETT
188 37.108 2241694 0.23 5.24 1-Triacontanol
189 37.282 2744164 0.28 5.45 1-Triacontanol
190 37.427 4242891 0.44 7.12 17-Pentatriacontene
191 37.673 3313512 0.34 8.29 5,8-Tridecadione
192 37.830 1971156 0.20 6.03 HEXATRIACONTANE
193 38.001 2582884 0.27 9.97 1-EICOSANOL
194 38.179 1785403 0.18 9.00 Lup-20(29)-en-3-one
195 38.320 970960 0.10 5.78 CHOLEST-5-EN-3-OL (3.BETA.)-
196 38.486 5326167 0.55 6.29 .alpha.-Tocopherol-.beta.-D-mannoside
197 38.791 3165575 0.33 9.05 14,15-DIDEHYDRO-1,4,5,8,9,10,11,12,13,16,17,18,19,20-TETRADECAHYDROCY
198 39.063 3019506 0.31 6.70 3,7,11,15-Tetramethyl-2-hexadecen-1-ol
199 39.435 2896893 0.30 12.30 6.beta.,6.beta.-Dibromo-6,7-methylenetestosterone
200 39.688 620373 0.06 7.60 Cyclodecacyclotetradecene, 14,15-didehydro-1,4,5,8,9,10,11,12,13,16,17,18,19,20-tetra
972432724 100.00