CERTIFICATE OF ANALYSIS © LX Complies with ISO 17034, ISO Guide 31, EDP ES) ISO Guide 35, and ISO 9001 TRACEABLE® CERTIFIED REFERENCE MATERIAL This certificate indicates traceability to standards provided by (NIST) National Institute of Standards and Technology and/or @ National Standards Laboratory. Certificate No.: 4281-10846856 Description : Buffer 7.000 pH Catalog Number: 4281, Lot : €C647817 Certificate Date ; 04 Nov 2019 Expiration Date : 04 Nov 2021 Certified Value: 7.001 pH U: £0,011 pH (k=2) at 25°C Certification measurements are performed under ISO 17034, A2LA accreditation no. 1750.02. They are traceable to recognized national and international standards via an unbroken chain of comparisons. pH is defined as the negative logarithm of the hydrogen ion activity MEASUREMENT: Minimum twelve (12) 100 ri samples were measured from this lot. The pH of each sample was determined using a pH meter and electrode. UNCERTAINTY: The certified value is given as the average of the measured samples. The reported expended uncertainty (U) is determined from the measurement variation from sample to sample, change due to shelf life, and uncertainty of the ‘Measurement process. The value of uncertainty is multiplied by k=2, which for a normal distribution cocresponds to a coverage probability of approximately 95%. Uncertainty is calculated in accordance with the ISO "Gude to the Expression of Uncertainty in Measurement”, METHOD: The certified reference material is produced and analyzed by Control Company. The certified reference material is Comprised of deionized water, 0.029 mol/kg H20 disodium hydrogen phosphate, 0.021 mol/kg H20 potassium dihydrogen phosphate, and germiclde. {issue Date '04 Nov 2018 = Mak oti ‘Traceability: Standards and Equipment Used eserintion Seria Number Due Date ‘Traceable Rateronce ilton Meter sn0e7.6023 PA Reference Material 7.0000 ELzo0018 15mg 2001 owo-18 tal Trerometer rozo0sse3 21 Fep 2020 ‘000-10197008 pH econ 1s20.-F16 ‘avoratory Environment Conditions: 92.00%4RH 25,20°C 1029mBar CONTROL COMPANY 12554 Galveston RD Suite 8230 Webster TX USA 77598 Phone 281 482-1714 Fax 281 482-9448 sales@control3.com | www.traceable.com Coneol Company ean 160 170342016 Certed Reference Matera (CRM) Praducer Acad by American Asscaton for Laboratory Accedtation iS Cri i, 175002) Ths ea nth gure 150 Ge #205 renee Haas” Contre of Cotes ek Labels) 180 170342016 “qusly Sys Guolmes forthe Feguction of Kternce atcsus” and 150 Sule 38-2019 Sencar toe Msierals~ Gonera and Stattal incl Contra Conny ison 150/lec: 17025 2005 CatralontoratryAcseated ty Amnesn Renee for Laboratory Accreditation (A2.A Cait No. 17301), Cool Company e150 B00 045 cred by BMG: [caren Ne CENT OL ISOS “ASHOU-ANAB). Troceatisd rn apitered Vaderar of Cal 3 neey; CERTIFICATE OF ANALYSIS ng Complies with ISO 17034, ISO Guide 31, fast ica ISO Guide 35, and ISO 9001 scare 102 TRACEABLE® CERTIFIED REFERENCE MATERIAL Frit Pi Note: PACKAGING: This reference material is available in a 500 mL bottle, 120 mL One-Shot™, 1 L bottle, and 3.8 L bottle, INTENDED USE: The certified reference material is intended for the calibration of pH meters and electrodes used for pH measurement, for the validation of analytical methods, and for the preparation of working reference standards, INSTRUCTIONS FOR USE: Open for a minimum period of time, quickly extract the sample. Remove a sample size of 100 mi Return the cap to the sample, Rinse the electrode in a small amount of the certified reference material and discard, Sample should be stirred while being measured. Discard the reference material sample after use. Reference materials which have been opened {are not protected from growth. Discard the reference material bottle of One-Shot™ under the following circumstances: if the expiration date is past due, or if any color, turbidity, or visible microbiological growth become evident. DH buffers are sensitive to temperature. For measurements at a temperature other than 25°C, refer to the temperature correction table provided (reference page 3 of this certificate) HOMOGENEITY: Minimum twelve (12) 100 rl samples were selected for analytical control. Results from different samples showed ‘no statistically differences, nor was there any correlation between values obtained and the bottling sequence, Gottle-to-bottle (One-Shot™ to One-Shot) variations of the samples measured are included as a part of the calculated measurement uncertainty stated on page 1 of this certificate. A minimum sample size of 100 ml should be used to maintain the certified value and the associated statement of uncertainty. STABILITY STUDY: The expiration date stated on page 1 indicates the period of time over which the certified reference material stored under environmentally controlled and monitored conditions in an unused and unopened package remains within the Specified uncertainty range. Stability tests take place at six month intervals over the certification period of the certified reference ‘material. Each test, two (2) 100 ml samples are taken from each of three (3) bottles and then measured to study stability over time. The mast significant contributor to instability is carbon dioxide absorption. The long-term stability of the certified reference ‘material over the certification period is included in the uncertainty calculation EXPIRATION DATE: The date after which a certified reference material should be discarded. STORAGE: Store below 40°C and above 4°C, SHIPPING: Ship below 50°C and above 4°C. MAINTENANCE OF CERTIFICATION: Control Compeny monitors representative samples from this lot over the period of its certification. If a change occurs that affects the certification before the expiration date, Control Company posts amended certificate(s) at wivw.treceable.com\crmupdate,him. MSDS INFORMATION: Please refer to the Material Safety Data sheet for information regarding this certified reference material at hntins://traceable,com/safety-data-sheets, Use only the first four digits of the certificate number to locate the MSOS. QUALITY STANDARD DOCUMENTATION: 180 170342016 General Requirements for the Competence of Reference Material Producers, accredited A2LA Certificate Number 1750.02 TSO Guide 31:2015 Reference Materials - Contents of Certificates, Labels and accompanying documentation. 180 Guide 35:2006 Certification of Reference Materials - General and Statistical Principals. ISO/IEC 17025:2005 General Requirements for the Competence of Testing and Calibr Certificate Number 1750.01, ANSI/NCSL 7540-1: 1994 Calibration Laboratories and Measuring and Test Equipment-General Requirements. 450 9001:2015 Quality Management System Requirements - DNV GL Certificate Number CERT-01805-2006-AQ-HOU-RVA, Laboratories, accredited A2LA CONTROL COMPANY 12554 Galveston RD Suite B230 Webster TX USA 77598 Phone 281 482-1714 Fax 281 482-9448 sales@control3.com | www.traceable.com “(hata carte Na, 7a fa) tac erent fs hs roqrement 50 Gage aT-a015 Retararce Maeno Contents of Caress oh sta) 150 70543086" Quay Sym Gudees fr the Pesan ference ters’ and 186 de 982017 Canton o cence Hatt" Geer an ttt cane Cal crsay an BOE es me aetan ahr Aten sretesn Aston ‘Sano Ararat (AA Corsten N90) Ctl Campo SOL SE eed ty BY (Cas No. CER R05 3006 NOD Ann Macobce evrageel uxbenark ono ne 202 tor: cose7ai7 {© 2017 conto CompanyComplies with ISO 17034, ISO Guide 31, aeeneWeren ISO Guide 35, and ISO 9001 AaACatae ne 75082 TRACEABLE® CERTIFIED REFERENCE MATERIAL ‘etwrce ors Pac CERTIFICATE OF ANALYSIS © ‘Temperature Correction Information: Use the chart below only for making absolute measurements. That is, measurements without any automatic temperature correction (temperature coefficient set to 0}, ‘Temperature Correction Chart in micromhos/em ce] oo | oa fuea] os | on | os | oe [e7 | oa [vas 1870s 7025 70m 76M 7023-702 7003 702 70 700 19 Fon 7021 70:0 700 79m 7019 7019 7019 7.018 7.018 27017 70177017 70187016 7018 | 7015. 7015 -7o1s7ot4 zi 70i4 701 7013 7970 7012 70 Foz 70 7011 7010 7010 7010 7008 700 7.009 7.008 7.008 7.000 7.008 237007 7.007 7007 7.006 7.006 7.006 7.005 7005 | 7.005 7.008 247008 3004 7.003.003 7003 7.002 70027002 7.002 7.001 25 7001 7001 7.000 7.000 7.000 7.000 6.990 6.99 6.999 ane 2 | 6988 Gas 6998 6957 Goer 687 6.986 6096 6006 686 | 6988 cons e995 605s com 954 | 00s 6003 6503 Gon 3 6583 es82 ces2 6562 Gam G8 e901 e961 6ssi 6.80 ‘The above data are derived values based upon IUPAC data (Pure and Applied Chemistry 74, 2169-2200) and data/algorithm obtained using a temperature controlled calibration bath ‘Shown on the chart is temperature (in the far left column) in whole degrees. Shown across the top row is temperature in tenths of a degree. Using a thermometer, measure the temperature of this certified reference material. Locate the measured temperature in whole numbers on the far left column. Follow acrass the row to the temperature in tenths of a degree. At the intersection is the certified reference material value at that specific temperature. Standardize the meter using that value. Example: Measured temperature is 24.5°C. Find 24°C in the far left column, find the row 0.5°C. Where 24°C end 0.5°C intersect, read the value in pH CONTROL COMPANY 12554 Galveston RD Suite 8230 Webster TX USA 77598 Phone 281 482-1714 Fax 281 482-9448 sales@control3.com www.traceable.com ene Company is 150 170342916 Carifed Refrnce Matra (CRM) Produce Acredted by American Associaton or Lbortery hes eatin (AGta Grice No, 179902), a creat Ashe rasreents of 50 Gade 20S (eacioes Mates Cone Seen bei 50 70342016 Quay Sater Gude rte freson st Reeeae aetna Se ee es eee eee fst Geveral and Staite napot" ContlCorpaw fan ISO/IEC I7G05 205 cftatin Labsatry scheaeaat eg Neen {or aerator Acretaton A2UA Crete Ne. 178061; Comet Crmpany 0 900 01S ced oy OC Ae ees Ae CERT nee “AGMMANAS) oceabee es agatred teoenal af Corea ine