NM, Ne, Spek

antoin
komponen td A
C
METANOL CH3OH 64.7000 18.5875
H2O H2O 100.0000 18.3036
ASAM KLORIDA HCl -85.0500 16.5040
DIMETIL KLORIDA C2H6O -24.8200 16.8467
METIL KLORIDA CH3Cl -23.7000 16.1052
P (mmHg) 1 atm 760.0000

T °C+273
A
ASAM KLORIDA HCl -85.0500 16.5040
METIL KLORIDA CH3Cl -23.7000 16.1052
ln⁡𝑃𝑖=𝐴 − 𝐵/(𝐶+𝑇)
Pi = inv ln a (shif ln a ) klo dikalkulator
RUMUS DI EXCEL POWER(2,718281828459;KOLOM MANA)
T(C) T(K) ln PA° PA°

-85.05000 187.95000 6.62360 752.64716
-80.00000 193.00000 6.90305 995.30367
-75.00000 198.00000 7.16458 1292.82231
-70.00000 203.00000 7.41225 1656.14377
-65.00000 208.00000 7.64712 2094.59495
-60.00000 213.00000 7.87015 2617.97035
-55.00000 218.00000 8.08224 3236.46287
-50.00000 223.00000 8.28415 3960.59144
-45.00000 228.00000 8.47661 4801.12693
-40.00000 233.00000 8.66026 5769.01797
-35.00000 238.00000 8.83569 6875.31771
-30.00000 243.00000 9.00345 8131.11284
-24.82000 248.18000 9.16968 9601.57691
KESIMPULAN HCL BISA DIPEISAHKAN DENGAN
komponen td
DIMETIL KLORIDA C2H6O -24.8200
METIL KLORIDA CH3Cl -23.7000
NO T(C) T(K) ln PA°
1 -24.82 248.18 6.62755511511165
2 -24.7 248.3 6.63285916955017
3 -24.6 248.4 6.63727501080847
4 -24.5 248.5 6.64168703543647
5 -24.4 248.6 6.64609524838013
6 -24.3 248.7 6.65049965457686
7 -24.2 248.8 6.65490025895554
8 -24.1 248.9 6.65929706643658
9 -24 249 6.66369008193187
10 -23.9 249.1 6.66807931034483
11 -23.8 249.2 6.67246475657044
12 -23.7 249.3 6.67684642549526
KESIMPULAN DIMETIL TIDAK BISA DIPEISAHKA

B C T max Tmin
3626.5000 -34.2900 364.0000 257.0000

3816.4400 -46.1300 441.0000 284.0000
1714.2500 -14.4500 200.0000 137.0000
2361.4400 -17.1000 265.0000 179.0000
2077.9700 -29.5500 266.0000 180.0000
B C T max Tmin
1714.2500 -14.4500 200.0000 137.0000
2077.9700 -29.5500 266.0000 180.0000
NA) XA = (𝑃𝑡𝑜𝑡𝑎𝑙 −𝑃𝐵°)/(𝑃𝐴°−𝑃𝐵°)

YA=𝑃𝐴/𝑃𝑇 ×𝑋𝐴
ln PB° PB° XA YA
2.98670 19.82022 1.01003352556137 1.0002616666624
3.39202 29.72581 0.756307929146212 0.990468495927521
3.76937 43.35289 0.57356114279261 0.975674530982998
4.12498 61.86627 0.437899756195179 0.954243359816749
4.46065 86.54372 0.33537803696156 0.924317294380007
4.77803 118.86952 0.256544464159163 0.883718158749077
5.07856 160.54297 0.194887074210041 0.829927341416818
5.36356 213.48388 0.145850128562138 0.760069434209962
5.63420 279.83489 0.106200861627714 0.670899759325318
5.89154 361.96072 0.073614770048145 0.55879596231224
6.13653 462.44446 0.046399723053027 0.419753733616722
6.37004 584.08092 0.023309703532007 0.249386617973116
6.60069 735.60602 0.002751417083401 0.034760450964706
LAN HCL BISA DIPEISAHKAN DENGAN METIL KLORIDA KARNA LEBIH DARI SATU
A B C T max
16.8467 2361.4400 -17.1000 265.0000
16.1052 2077.9700 -29.5500 266.0000
PA° ln PB° PB° XA
755.632475996146 6.60069467136258 735.606016226523 1.21808767271387
759.651039703499 6.60590857142857 739.451408517299 1.0172755776224
763.012955486729 6.6102491204021 742.668009426242 0.851906440165963
766.386824762021 6.61458570449874 745.895645103547 0.688313466161066
769.772678381739 6.6189183291486 749.134341924278 0.526479355451816
773.170547240926 6.62324699977185 752.384126291723 0.366386966129875
776.580462277269 6.62757172177879 755.645024637353 0.208019313355248
780.002454471072 6.63189250056987 758.917063420768 0.051359568179132
783.436554845231 6.63620934153566 762.200269129657 -0.10360894363196
786.882794465195 6.64052225005693 765.494668279748 -0.256902742769807
790.34120443895 6.64483123150467 768.80028741476 -0.408538197555714
793.811815916983 6.64913629124005 772.117153106356 -0.558531525109412
LAN DIMETIL TIDAK BISA DIPEISAHKAN DENGAN METIL KLORIDA KARNA SAMA ENGAN SATU
𝑃𝑡𝑜𝑡𝑎𝑙 −𝑃𝐵°)/(𝑃𝐴°−𝑃𝐵°)
YA=𝑃𝐴/𝑃𝑇 ×𝑋𝐴 𝛼 𝐴𝐵=𝑃𝐴/𝑃𝐵
ἀ AB=PA°/PB° NO
37.973707658778 1
33.482815793249 2
29.820903347448 3
26.769736060465 4
24.202738023697 5
22.023900230432 6
20.159480442914 7
18.552180173772 8
17.156999063851 9
15.938242983017 10
14.867337257438 11
13.921209393504 12
13.052607913115 13
287.92185834168
∑ ἀab / total T𝐴𝐵 22.1478352570522
Tmin
179.0000
180.0000
YA ἀ AB=PA°/PB°
1.211087636991 1.02722443716863
1.0168084871129 1.02731705011787
0.8552837509332 1.02739440207773
0.6940978575949 1.027471912181
0.5332492415248 1.02754957996512
0.3727363304008 1.02762740496886
0.2125575454316 1.0277053867323
0.052711301632 1.02778352479685
-0.1068039919081 1.02786181870524
-0.2659899317585 1.02794026800149
-0.4248481198888 1.02801887223095
-0.5833801634131 1.02809763094026
12.3319922878863
∑ ἀab / total T𝐴𝐵 1.02766602399052

basis 1 kg/jam bahan baku metanol (kg/jam) 8443.9612
konfersi metanol reaksi utama (CH3CL) 0.9500 0.9500
konfersi metanol reaksi samping ((CH3)2O 0.0300 0.0300
METANOL (BAHAN BAKU) ch3oh

ASAM KLORIDA (STRIPER) HCl
METIL KLORIDA CH3Cl
DIMETIL KLORIDA (CH3)2O
ASAM SULFAT H2O
air H2O
CAIRAN YANG DIUAPKAN MAX 80% 0.8000

PURITY CH3OH (%) 99.9000
IMPURITY H20 (%) 0.1000
MASSA METANOL (KG/JAM)MASUK REAKTOR F-01 F - 01 = 0.8 ×𝐹𝐹 - 01
(KG/JAM) BAHAN BAKU METANOL FF-01 (80%)

FF -01=
(𝐹−01)/(80%)
KOMPOSISI INPUT VAPOURIZER BAHAN BAKU FF-01 CH3OH = KEMURNIAN CH3OH ×𝑀𝐴
MASSA INPUT VAPOURIZER BB (FF - 01) FF-01 (CH3OH) FF-01 CH3OH = 99,9/100×𝐅𝐅−𝟎𝟏(𝟖𝟎%
FF-01 (H2O) FF-01 (H2O) = FF -01 (80%) - FF

FF-01(H2O) = FF-01(80) - FF-01
RECAYCLE (PRODUK BOTOM VAPOURIZER) KG/JAM RC-01 RC - 01 = FF -01 (80%) - F -01

KOMPOSISI RECAYCLE
RC - 01( CH3OH) RC-01 (CH3OH)= KEMURNIAN
RC - 01 (H2O) RC-01 HCl = RC −01- RC-01 (CH
INPUT
KOMPONEN kg/jam
ch3oh 10544.3965
H20 10.5550
TOTAL 10554.9515
total all
KOMPOSISI AWAL HCl PURITY (%) (XFF-02 (HCl)) 33.0000
IMPURITY (%) 67.0000
KOMPOSISI HCl YANG AKAN MASUK REAKTOR PURITY (%) (XF-02 (HCl)) 98.5176
IMPURITY (%) 1.4824
komposisi bottom striper XB (%) PURITY HCL 20.0000
KOMPOSISI B (XB)
komposisi bottom striper PURITY HCL 0.2000
IMPURITY H2O 0.8000
KOMPOSISI FF-02 (HCL) AWAL PURITY HCL 0.3300

IMPURITY H2O 0.6700
INPUT
KOMPONEN kg/jam
HCL 21694.1954
H20 44045.7906
TOTAL 65739.9860
TOTAL ALL
INPUT TOP VAPOUR

KOMPONEN kg/jam
CH3OH 8435.5172
HCL
AIR 8.4440
TOTAL 8443.9612
TOTAL ALL
REAKTOR
REAKSI UTAMA mol (kgmol/jam) CH3OH
mula" 263.2644
bereaksi 250.1012
sisa 13.1632
REAKSI SAMPING mol (kgmol/jam) 2CH3OH
mula" 13.1632
bereaksi 0.3949
sisa 12.7683
INPUT
KOMPONEN kg/jam
ch3oh 8435.5172
HCl 10557.9020
CH3Cl
(CH3)2O
H20 167.3083082
TOTAL 19160.7275
INPUT
KOMPONEN kg/jam
ch3oh 409.1226
HCl 1439.7139
CH3Cl 12626.3570
(CH3)2O 9.0962
H20 4676.4377
TOTAL
TOTAL 19160.7275
INPUT
KOMPONEN kg/jam
ch3oh 0.7364
HCl 1439.7125
CH3Cl 12626.3444
(CH3)2O 9.0953
H20 7.0147
H2O 203.1799
TOTAL 14286.0832
TOTAL
kebutuhan air untuk melarutkan dme

mg
kelarutan dme dlm air 46000.0000
kelarutan metil dlm air 5040.0000
𝜌=𝑚𝑎𝑠𝑠𝑎/𝑣𝑜𝑙𝑢𝑚𝑒
masssa
densitas air 25 c (g/ml) 1.0276 massa
volume (1 L) (ml) 1000.0000
dme 4.4765
metil klorda 0.4905
kg/jam g/jam
dme 9.0953 9095.3354
mtil klorda 12626.3444 12626344.4186

996.5324
10091.8678
INPUT
KOMPONEN kg/jam
ch3oh 0.7364
HCl 1439.7125
CH3Cl 12625.3479
(CH3)2O 0.0000
H20 0.3507
H20 0.0000
TOTAL 14066.1475
TOTAL
NERACA MASSA
BM purity purity
kg/kgnol %
32.0420 0.9990 0.9990
36.4580 0.9852 0.9852
50.4850
46.0690
18.0150
18.0150
VAPOURIZER
FF FRES FEED
F FEED
RC RECAYCLE
f-01=100/(𝑝𝑢𝑟𝑖𝑡𝑦 𝑐ℎ3𝑜ℎ) ×𝑏𝑎𝑠𝑖𝑠

F-01 = BASIS = BAHAN BAKU METANOL
MASUK REAKTOR
0%)
EMURNIAN CH3OH ×𝑀𝐴𝑆𝑆𝐴 𝐶𝐻3𝑂𝐻 (𝐹𝐹−01 (80%))
9,9/100×𝐅𝐅−𝟎𝟏(𝟖𝟎%)
H2O) = FF -01 (80%) - FF-01 (CH3OH)

H2O) = FF-01(80) - FF-01 (CH3OH)
1 = FF -01 (80%) - F -01
(CH3OH)= KEMURNIAN CH3OH × RC −01

HCl = RC −01- RC-01 (CH3OH)
NERACA VAPORIZER
INPUT OUTPUT TOP
kgmol/jam kg/jam kgmol/jam
329.0805 8435.5172 263.2644
0.5859 8.4440 0.4687
329.6664 8443.9612 263.7331

10554.9515 329.6664
KEMURNIAN CH3OH TOP 99.9000
STRIPER 2
FF-02 (HCL) = F -02 (HCL) +B
NERACA BAHAN
FF-02 (HCL) = 1,289020023 +B
NERACA KOMPONEN FF-02 (HCL)× XFF-02 (HCL) = F -02 (HCL) ×XF-02(HCL) + B . XB

(1.289020023+ B ) × 33 %= 1.289020023 × 97% + B . 20%
20 % B = (1.289020023+ B ) ×33 % − (1.250349423×97% )
BB = % KEMURNIAN X B
30 % B - 20%B = (1.289020023×33 %) − (1.289020023×97% )
10971.1102
43884.4408 B = 𝑋/𝑌 = ("(1.289020023 ×97%) -(1.289020023×33 %" ))/"30% −2
X
BB = % KEMURNIAN X FF-02 (HCL)
Y
21694.1954 B (KG/JAM)
44045.7906
NERACA STRIPER
INPUT OUTPUT TOP
kgmol/jam kg/jam (a) kgmol/jam
595.0462 10557.9020 289.5908
2444.9509 158.8643 8.8184
3039.9971 10716.7663 298.4093

65572.3173 3035.3284
KEMURNIAN HCL TOP 98.5176
MIXER
NERACA MIXER satu

INPUT TOP VAPOURZER INPUT TOP STRIPER
kgmol/jam kg/jam (a) kgmol/jam
263.2644
10557.9020 289.5908
0.4687 158.8643 8.8184
263.7331 10716.7663 298.4093

19160.7275 562.1424
HCl CH3Cl
289.5908
250.1012 250.1012
39.4897 250.1012
(CH3)2O H2O
259.3883
0.1974 0.1974
0.1974 259.5858
NERACA REAKTOR
INPUT OUTPUT
kgmol/jam kg/jam kgmol/jam
263.2644 409.122585 12.7683
289.5908 1439.7139071 39.4897
12626.357045 250.1012
9.0962450 0.1974
9.2872 4676.4377302 259.5858
562.1424 19160.7275 562.1424
FLASH DRUM
NERACA FLASH DRUM

INPUT %berat OUTPUT TOP
kgmol/jam kg/jam
12.7683 0.1800% 0.7364
39.4897 99.9999% 1439.7125
250.1012 99.9999% 12626.3444
0.1974 99.9900% 9.0953
259.5858 0.1500% 7.0147
14082.9033
562.1424 19160.7275
KEMURNIAN CH3CL 89.6573
ABSORBSI
NERACA ABSORBER
kgmol/jam kg/jam
0.0230 100.0000% 0.7364
39.4896 100.0000% 1439.7125
250.1009 99.9921% 12625.3479
0.1974 0.0000% 0.0000
0.3894 5.0000% 0.3507
11.2784 0.0000% 0.0000
301.4787 14066.1475
14286.0832
air (L) suhu (c)

1.0000 25.0000
1.0000 25.0000
g
air 1027.5898
ρ X volume (g) dme 46.0000
1027.5898 metil klorida 5.0400
air yang dibutuhkan (x) metil klorida yg karut dlm air yg ditmbhkan ke dme
g/jam KG/JAM KG/JAM (AIR)
203179.8728 9.0953 203.1799
2574345862.1760 0.9965
996.5324
NERACA DESTILASI
kgmol/jam kg/jam
0.0230 20.0000% 0.1473
39.4896 99.9920% 1439.5973
250.0812 0.0010% 0.1263
0.0000 0.0000% 0.0000
0.0195 40.0000% 0.1403
0.0000 0.0000% 0.0000
289.6132 1440.0111
14066.1475
KEMURNIAN HCL 99.9713

NERACA MASSA
impurity air impurity air perbandingan mol

%
0.0010 0.0010 1.0000
0.0148 0.0148 1.1000
APOURIZER
KOMPONEN KG/JAM
F-01 8443.9612
FF-01 10554.9515
KOMPOSISI INPUT VAPOURIZER
MASSA INPUT VAPOURIZER
FF-01 (CH3OH) 10544.3965
FF-01(H2O) 10.5550
UPL (PRODUK BOTOM VAPOURIZER)

KOMPOSISI RCL
RCL -01 2110.9903
RC - 01( CH3OH) 2108.8793

RC - 01 (H2O) 2.1110
NERACA VAPORIZER
OUTPUT BOTTOM komposisi
kg/jam kgmol/jam top %
2108.8793 65.8161 79.9200
2.1110 0.1172 0.0800
2110.9903 65.9333 80.0000

100.0000
KEMURNIAN CH3OH BOTTOM 99.9000
ER 2
HCL) = F -02 (HCL) +B
MOL METANOL 263.2644MOL METANO
CL) = 1,289020023 +B
MOL HCL (KGMOL/JAM) 289.5908MOL HCL = 𝑀
CL)× XFF-02 (HCL) = F -02 (HCL) ×XF-02(HCL) + B . XB MASSA HCL (KG/JAM) 10557.9020 Massa HCl = 𝑀
020023+ B ) × 33 %= 1.289020023 × 97% + B . 20% F-02 (HCl) = 100/(𝑃
(1.289020023+ B ) ×33 % − (1.250349423×97% ) F -02 (HCL) (KG/JAM) 10884.4350
- 20%B = (1.289020023×33 %) − (1.289020023×97% ) MASSA AIR 158.8643
/𝑌 = ("(1.289020023 ×97%) -(1.289020023×33 %" ))/"30% −20 %)"

FF-02 (HCL) = F -02 (HCL) +B
7131.2216
FF-02 (HCL) = 1,289020023 +6,34594473
0.1300
54855.5509 FF-02 (HCL) 65739.9860
NERACA STRIPER
kg/jam (b) kgmol/jam TOP %
10971.1102 300.9246 16.1012
43884.4408 2435.9945 0.2423
54855.5509 2736.9191 16.3434

100.0000
KEMURNIAN HCL BOTTOM 20.0000
ER
NERACA MIXER satu

OUTPUT komposisi
kg/jam (a) kgmol/jam %
8435.5172 263.2644 44.0250
10557.9020 289.5908 55.1018
167.3083 9.2872 5.5509
19160.7275 562.1424
104.6777
H2O
9.2872
250.1012
259.3883
komposisi
%
2.1352 0.126254665739485000
7.5139 0.00250083521322145000
65.8971
0.0475
24.4064
100.0000
LASH DRUM
NERACA FLASH DRUM

OUTPUT TOP %berat OUTPUT BOTTOM
kgmol/jam kg/jam
0.0230 99.8200% 408.3862
39.4896 0.0001% 0.0014
250.1009 0.0001% 0.0126
0.1974 0.0100% 0.0009
0.3894 99.8500% 4669.4231
290.2003 5077.8242
562.1424
KEMURNIAN CH3OH 8.0425
ABSORBSI
NERACA ABSORBER
kgmol/jam kg/jam
0.0230 0.0000% 0.0000
39.4896 0.0000% 0.0000
250.0812 0.0079% 0.9965
0.0000 100.0000% 9.0953
0.0195 95.0000% 6.6639
0.0000 100.0000% 203.1799
289.6132 219.9357
301.4787
kelarutan dalam air
46 gram alrut dalam 1027,58982 air

5,04 gram alrut dalam 1027,58982 air
g/ml 1000.0000
ditmbhkan ke dme
NERACA DESTILASI
kgmol/jam kg/jam
0.0046 80.0000% 0.5891
39.4865 0.0080% 0.1152
0.0025 99.9990% 12625.2216
0.0000 100.0000% 0.0000
0.0078 60.0000% 0.2104
0.0000 100.0000% 0.0000
39.5013 12626.1364
KPSTS TON/TAHUN 99999.00016

Z = KAPASITAS (JG/JAM) / PRODUK KELUARAN ALAT SEBELUM TANG
KAPASITAS
massa PURITY MASSA IMPURITY PRODUK ALAT SEBELUM TNKI
kg/jam KG/JAM Z
8435.5172 8.4440
Produk akhir
bahan baku
% mol hcl 0.9700

bm hcl 36.4580
basis mol larutan 1.0000
massa larutan bm x basis mol larutan
36.4580
% mol air 0.0300
bm air 18.0150
massa air = mol air x bm air
(% mol air x basis mol larutan) x bm air
0.5405
massa larutan utama = massa larutan - massa air
35.9176
% berat HCl (massa larutan utama/massa larutan ) x 100 %

98.5176 %
% berat h2o 1.4824 %
bottom %
19.9800
0.0200
20.0000
100.0000
MOL METANOL =𝑃𝑈𝑅𝐼𝑇𝑌/(𝐵𝑀 𝑀𝐸𝑇𝐴𝑁𝑂𝐿)
MOL HCL = 𝑀𝑂𝐿 𝑀𝐸𝑇𝐴𝑁𝑂𝐿 𝑋 𝑃𝐸𝑇𝐵𝐴𝑁𝐷𝐼𝑁𝐺𝐴𝑁 𝑀𝑂𝐿 𝐻𝐶𝐿 1.1
Massa HCl = 𝑀𝑂𝐿 HCl 𝑋 BM Metanol

F-02 (HCl) = 100/(𝑃𝑈𝑅𝐼𝑇𝑌 𝐻𝐶𝐿 𝑌𝐴𝑁𝐺 𝐷𝐼𝐼𝑁𝐺𝐼𝑁 𝐾𝐴𝑁 (97))×𝑀𝐴𝑆𝑆𝐴 𝐻𝐶𝑙
Massa Air = (𝑖𝑚𝑝𝑢𝑟𝑖𝑡𝑦 ℎ2𝑜 𝑦𝑔 𝑑𝑖𝑖𝑛𝑔𝑖𝑛𝑘𝑎𝑛 (3))/(𝑝𝑢𝑟𝑦𝑡𝑦

𝐻𝐶𝑙 𝑦𝑎𝑛𝑔 𝑑𝑖𝑖𝑛𝑔𝑖𝑛𝑘𝑎𝑛 (97))×𝑚𝑎𝑠𝑠𝑎 𝐻𝐶𝑙
komposisi
BOTTOM %
16.7313
66.9253
83.6566
100.0000
OUTPUT BOTTOM komposisi komposisi
kgmol/jam ATAS BAWAH
12.7453 0.0038 2.1314
0.0000 7.5139 0.0000
0.0003 65.8970 0.0001
0.0000 0.0475 0.0000
259.1964 0.0366 24.3698
271.9420 73.4988 26.5012

100.0000

0.0000 0.0052 0.0000
0.0000 10.0777 0.0000
0.0197 88.3752 0.0070
0.1974 0.0000 0.0637
0.3699 0.0025 0.0466
11.2784 0.0000 1.4222
11.8654 98.4605 1.5395

100.0000
kg/m3
0.0184 0.0010 0.0042
0.0032 10.2345 0.0008
250.0787 0.0009 89.7561
0.0000 0.0000 0.0000
0.0117 0.0010 0.0015
0.0000 0.0000 0.0000
250.1119 10.2374 89.7626

100.0000
KELUARAN ALAT SEBELUM TANGKI
KAPASITAS (TON/TAHUN)
SATU TAHUN BEROPERASI (HARI)
12626.2626 PERHTUNGAN (JAM)
12626.2626 satu hari (24 jam)
1.0000 1 TON (KG)
kapasitas (kg/jam)= (100,000 𝑡𝑜𝑛)/𝑡𝑎ℎ𝑢𝑛×(1 𝑡𝑎ℎ𝑢𝑛)/(330 ℎ𝑎𝑟𝑖)×(1 ℎ𝑎𝑟𝑖)/(24
1.4953 KAPASITAS (KG/JAM)

8443.9612
IN
KOMPONWEN
ch2cl
H20
TOTAL
kg/kgmol
kgmol/jam CAIRAN YANG DIUAPKAN MAX 80%
PURITY CH3OH (%)
kg/jam IMPURITY H20 (%)
kg/kgmol MASSA METANOL (KG/JAM)MASUK REAKTOR
(KG/JAM) BAHAN BAKU METANOL

kg/jam
KOMPOSISI INPUT VAPOURIZER BAHAN BAKU
kg/jam MASSA INPUT VAPOURIZER BB (FF - 01)
RECAYCLE (PRODUK BOTOM VAPOURIZER) K

KOMPOSISI RECAYCLE
KOMPONEN
ch3oh
H20
TOTAL
total all
IN
KOMPONWEN
HCL
H20
TOTAL
KOMPOSISI AWAL HCl
KOMPOSISI HCl YANG AKAN MASUK REAKTOR
komposisi bottom striper
KOMPOSISI B
komposisi bottom striper
KOMPOSISI FF-02 (HCL) AWAL
KOMPONEN
HCL
H20
TOTAL
TOTAL ALL
KOMPONEN
CH3OH
HCL
AIR
CH3Cl
TOTAL
TOTAL ALLL
KOMPONEN
CH3OH
HCL
AIR
CH3Cl
TOTAL
TOTAL ALL
REAKSI UTAMA
REAKSI SAMPING
100000.0000
330.0000
1.0000
24.0000
1000.0000
𝑛)/𝑡𝑎ℎ𝑢𝑛×(1 𝑡𝑎ℎ𝑢𝑛)/(330 ℎ𝑎𝑟𝑖)×(1 ℎ𝑎𝑟𝑖)/(24 𝑗𝑎𝑚)×(1000 𝑘𝑔)/(1 𝑡𝑜𝑛)
12626.2626
INPUT MIXSER 1 SETELH ADA RECYCLE

RC DRI DESTILASI TOP STRIPER 1 (SBLM RC)
0.1473 8435.5172
8435.5172
0.8000
99.9000
0.1000
F-01 F - 01 = 0.8 ×𝐹𝐹 - 01
FF-01 (80%)
FF -01=
(𝐹−01)/(80%)
AHAN BAKU FF-01 CH3OH = KEMURNIAN CH3OH ×𝑀𝐴𝑆𝑆𝐴 𝐶𝐻3𝑂𝐻 (𝐹𝐹−01 (80%))
FF-01 (CH3OH) FF-01 CH3OH = 99,9/100×𝐅𝐅−𝟎𝟏(𝟖𝟎%)
FF-01 (H2O) FF-01 (H2O) = FF -01 (80%) - FF-01 (CH3OH)

FF-01(H2O) = FF-01(80) - FF-01 (CH3OH)
RC-01 RC - 01 = FF -01 (80%) - F -01
RC - 01( CH3OH) RC-01 (CH3OH)= KEMURNIAN CH3OH × RC −01

RC - 01 (H2O) RC-01 HCl = RC −01- RC-01 (CH3OH)
NERACA
INPUT
kg/jam kgmol/jam
10544.2124 329.0747
10.5548 0.5859
10554.7672 329.6606
KEMURNIAN CH3OH TOP
INPUT MIXSER 1 SETELH ADA RECYCLE

RC DRI DESTILASI TOP STRIPER 1 (SBLM RC)
1439.5973 10557.9020
0.1403 158.8643
10716.7663
PURITY (%) (XFF-02 (HCl)) 33.0000

IMPURITY (%) 67.0000
PURITY (%) (XF-02 (HCl)) 98.5176

IMPURITY (%) 1.4824
XB (%) PURITY HCL 20.0000
(XB)
PURITY HCL 0.2000
IMPURITY H2O 0.8000

PURITY HCL 0.3300
IMPURITY H2O 0.6700
NERACA STIPER
INPUT
kg/jam kgmol/jam
18490.4107 507.1702
37541.1369 2083.8821
56031.5476 2591.0523
NERACA al
INPUT TOP DESTILASI
kg/jam kgmol/jam
0.1473 0.0046
1439.5973 39.4865
0.1403 0.0078
0.1263 0.0025
1440.0111 39.5013
10717.0399 298.4164
NERACA MIX
INPUT TOP VAPOURZER
kg/jam kgmol/jam
8435.3699 263.2598
8.4438 0.4687
8443.8137 263.7285
mol (kgmol/jam) CH3OH
mula" 263.2644
bereaksi 250.1012
sisa 13.1632
mol (kgmol/jam) 2CH3OH
mula" 13.1632
bereaksi 0.3949
sisa 12.7683
NERACA RE
INPUT
KOMPONEN kg/jam
ch3oh 8435.5172
HCl 10557.9020
CH3Cl 0.1263
(CH3)2O 0.0000
H20 167.3081608
TOTAL 19160.8536
INPUT
KOMPONEN kg/jam
ch3oh 409.1226
HCl 1439.7139
CH3Cl 12626.4833
(CH3)2O 9.0962
H20 4676.4376
TOTAL
TOTAL 19160.8536
INPUT
KOMPONEN kg/jam
ch3oh 0.7364
HCl 1439.7125
CH3Cl 12626.4707
(CH3)2O 9.0953
H20 7.0147
H2O 203.1799
TOTAL 14286.2094
TOTAL
INPUT
KOMPONEN kg/jam
ch3oh 0.7364
HCl 1439.7125
CH3Cl 12625.4741
(CH3)2O 0.0000
H20 0.3507
H20 0.0000
TOTAL 14066.2737
TOTAL
×(1000 𝑘𝑔)/(1 𝑡𝑜𝑛)
MIXSER 1 SETELH ADA RECYCLE

TOP ST 1 - RC DRI DESTILASI (FEED STRPR 1 ) OUTPUT MIX - 2 (STELH RC)
8435.3699 8435.5172
8435.3699 8435.5172
FF FRES FEED
F FEED
RC RECAYCLE
f-01=100/(𝑝𝑢𝑟𝑖𝑡𝑦 𝑐ℎ3𝑜ℎ) ×𝑏𝑎𝑠𝑖𝑠 KOMPONEN

F-01 = BASIS = BAHAN BAKU METANOL
MASUK REAKTOR F-01
FF-01
KOMPOSISI INPUT VAPOURIZER
IAN CH3OH ×𝑀𝐴𝑆𝑆𝐴 𝐶𝐻3𝑂𝐻 (𝐹𝐹−01 (80%)) MASSA INPUT VAPOURIZER
0×𝐅𝐅−𝟎𝟏(𝟖𝟎%) FF-01 (CH3OH)
FF-01(H2O)
F -01 (80%) - FF-01 (CH3OH)
F-01(80) - FF-01 (CH3OH)
UPL (PRODUK BOTOM VAPOURIZER)
KOMPOSISI RCL
(80%) - F -01 RCL -01
= KEMURNIAN CH3OH × RC −01 RC - 01( CH3OH)

−01- RC-01 (CH3OH) RC - 01 (H2O)
NERACA VAPORIZER
OUTPUT TOP
kg/jam kgmol/jam
8435.3699 263.2598
8.4438 0.4687
8443.8137 263.7285
10554.7672 329.6606
99.9000
MIXSER 1 SETELH ADA RECYCLE

TOP ST 1 - RC DRI DESTILASI (FEED STRPR 1 ) OUTPUT MIX - 2 (STELH RC)
9118.3047 10557.9020
158.7241 158.8643
9277.0287 10716.7663
FF-02 (HCL) = F -02

NERACA BAHAN
FF-02 (HCL) = 9444,66234 +B
NERACA KOMPONEN FF-02 (HCL)× XFF-02 (HCL) = F -02 (HC

(9444,66234 + B
BB = % KEMURNIAN X B 20 % B = (10873,46929 + B ) ×33 %
9350.9038
37403.6151

18490.4107
37541.1369
NERACA STIPER SETELLAH RECAYCLE

OUTPUT TOP
kg/jam (a) kgmol/jam
9118.3047 250.1044
158.7241 8.8107
9277.0287 258.9150
56031.5476 2591.6477
98.2891
NERACA alat T (RECYCLE)
INPUT TOP STRIPER
9118.3047 250.1044
158.7241 8.8107
9277.0287 258.9150
NERACA MIXER Setelah recycle

INPUT ALT T
0.1473 0.0046
10557.9020 289.5908
158.8643 8.8184
0.1263 0.0025
10717.0399 298.4164
19160.8536 562.1449
HCl
289.5908
250.1012
39.4897
(CH3)2O
0.1974
0.1974
NERACA REAKTOR
INPUT OUTPUT
kgmol/jam kg/jam
263.2644 409.122585
289.5908 1439.713907
0.0025 12626.483298
0.0000 9.096245
9.2872 4676.437583
562.1449 19160.8536
N
INPUT %berat
kgmol/jam
12.7683 0.1800%
39.4897 99.9999%
250.1037 99.9999%
0.1974 99.9900%
259.5858 0.1500%
562.1449
KEMURNIAN CH3CL
INPUT %berat
kgmol/jam
0.0230 100.0000%
39.4896 100.0000%
250.1034 99.9921%
0.1974 0.0000%
0.3894 5.0000%
11.2784 0.0000%
301.4812
KEMURNIAN CH3CL
INPUT %berat
kgmol/jam
0.0230 20.0000%
39.4896 99.9920%
250.0837 0.0010%
0.0000 0.0000%
0.0195 40.0000%
0.0000 0.0000%
289.6157
KEMURNIAN HCL
KG/JAM
8443.8137
10554.7672
10544.2124
10.5548
2110.9534
2108.8425
2.1110

kg/jam kgmol/jam top %
2108.8425 65.8149 79.9200
2.1110 0.1172 0.0800
2110.9534 65.9321 80.0000
100.0000
KEMURNIAN CH3OH BOTTOM 99.9000
FF-02 (HCL) = F -02 (HCL) +B

(HCL) = 9444,66234 +B
(HCL)× XFF-02 (HCL) = F -02 (HCL) ×XF-02(HCL) + B . XB

(9444,66234 + B ) × 33 %=9444,66234 × 97% + B . 20%
B = (10873,46929 + B ) ×33 % − (10873,46929 ×97% )
30 % B - 20%B = (9444,66234 ×33 %) − (9444,66234 ×97% )

B = 𝑋/𝑌 = ("(9444,66234 ×97%) −9444,66234(9440,85230×33 %" ))/"33% −20 %)"
X 6078.0875
Y 0.1300
B (KG/JAM) 46754.5189
CLE
kg/jam (b) kgmol/jam TOP %
9350.9038 256.4843 16.2735
37403.6151 2076.2484 0.2833
46754.5189 2332.7327 16.5568

100.0000
20.0000
OUTPUT alat T komposisi
0.1473 0.0046 0.0014
10557.9020 289.5908 98.5151
158.8643 8.8184 1.4824
0.1263 0.0025 0.0012
10717.0399 298.4139 99.9988
OUTPUT MIXCER SETELH RECYCLE komposisi

8435.5172 263.2644 44.0247
10557.9020 289.5908 55.1014
167.3082 9.2872 5.5509
0.1263 0.0025 0.0007
19160.8536 562.1449
104.6778
CH3Cl H2O
0.0025 9.2872
250.1012 250.1012
250.1037 259.3883
H2O
259.3883
0.1974
259.5858
OUTPUT komposisi
kgmol/jam %
12.7683 2.1352
39.4897 7.5138
250.1037 65.8973
0.1974 0.0475
259.5858 24.4062
562.1449 100.0000
NERACA FLASH DRUM

OUTPUT TOP %berat
kg/jam kgmol/jam
0.7364 0.0230 99.8200%
1439.7125 39.4896 0.0001%
12626.4707 250.1034 0.0001%
9.0953 0.1974 0.0100%
7.0147 0.3894 99.8500%
14083.0296 290.2028
19160.8536 562.1449
89.6573 KEMURNIAN CH3OH
NERACA ABSORBER
OUTPUT TOP %berat
kg/jam kgmol/jam
0.7364 0.0230 0.0000%
1439.7125 39.4896 0.0000%
12625.4741 250.0837 0.0079%
0.0000 0.0000 100.0000%
0.3507 0.0195 95.0000%
0.0000 0.0000 100.0000%
14066.2737 289.6157
14286.2094 301.4812
89.7571
NERACA DESTILASI
OUTPUT TOP %berat
kg/jam kgmol/jam
0.1473 0.0046 80.0000%
1439.5973 39.4865 0.0080%
0.1263 0.0025 99.9990%
0.0000 0.0000 100.0000%
0.1403 0.0078 60.0000%
0.0000 0.0000 100.0000%
1440.0111 39.5013
14066.2737
99.9713 KEMURNIAN CH3CL
KPSTS TON/TAHUN
bottom %
19.9800
0.0200
20.0000
MOL METANOL MOL METANOL =𝑃𝑈𝑅𝐼𝑇𝑌/(𝐵𝑀 𝑀𝐸𝑇𝐴𝑁𝑂𝐿)
MOL HCL (KGMOL/JAM) MOL HCL = 𝑀𝑂𝐿 𝑀𝐸𝑇𝐴𝑁𝑂𝐿 𝑋 𝑃𝐸𝑇𝐵𝐴𝑁𝐷𝐼𝑁𝐺𝐴𝑁 𝑀𝑂𝐿 𝐻𝐶𝐿 1.1
MASSA HCL (KG/JAM) 9118.3047 Massa HCl = 𝑀𝑂𝐿 HCl 𝑋 BM Metanol

F-02 (HCl) = 100/(𝑃𝑈𝑅𝐼𝑇𝑌 𝐻𝐶𝐿 𝑌𝐴𝑁𝐺 𝐷𝐼𝐼𝑁𝐺𝐼𝑁 𝐾𝐴𝑁 (97))×𝑀𝐴𝑆𝑆𝐴
F -02 (HCL) (KG/JAM) 9277.0287
MASSA AIR 158.7241 Massa Air = (𝑖𝑚𝑝𝑢𝑟𝑖𝑡𝑦 ℎ2𝑜 𝑦𝑔 𝑑𝑖𝑖𝑛𝑔𝑖𝑛𝑘𝑎𝑛 (3))/(𝑝𝑢𝑟𝑦𝑡𝑦

𝐻𝐶𝑙 𝑦𝑎𝑛𝑔 𝑑𝑖𝑖𝑛𝑔𝑖𝑛𝑘𝑎𝑛 (97))×𝑚𝑎𝑠𝑠𝑎 𝐻𝐶𝑙
FF-02 (HCL) = F -02 (HCL) +B

FF-02 (HCL) =9444,66234 +46496,79921
FF-02 (HCL) 56031.5476
komposisi
BOTTOM %
16.6886
66.7546
83.4432
100.0000
kg/jam kgmol/jam ATAS
408.3862 12.7453 0.0038
0.0014 0.0000 7.5138
0.0126 0.0003 65.8972
0.0009 0.0000 0.0475
4669.4229 259.1964 0.0366
5077.8241 271.9420 73.4990

100.0000
8.0425

0.0000 0.0000 0.0052
0.0000 0.0000 10.0777
0.9965 0.0197 88.3760
9.0953 0.1974 0.0000
6.6639 0.3699 0.0025
203.1799 11.2784 0.0000
219.9357 11.8654 98.4614

100.00

0.5891 0.0184 0.0010
0.1152 0.0032 10.2345
12625.3479 250.0812 0.0009
0.0000 0.0000 0.0000
0.2104 0.0117 0.0010
0.0000 0.0000 0.0000
12626.2626 250.1144 10.2374

100.00
99.9928
100000.00000
KEMURNIAN
ETANOL =𝑃𝑈𝑅𝐼𝑇𝑌/(𝐵𝑀 𝑀𝐸𝑇𝐴𝑁𝑂𝐿)
CL = 𝑀𝑂𝐿 𝑀𝐸𝑇𝐴𝑁𝑂𝐿 𝑋 𝑃𝐸𝑇𝐵𝐴𝑁𝐷𝐼𝑁𝐺𝐴𝑁 𝑀𝑂𝐿 𝐻𝐶𝐿 1.1
HCl = 𝑀𝑂𝐿 HCl 𝑋 BM Metanol 98.2891

0/(𝑃𝑈𝑅𝐼𝑇𝑌 𝐻𝐶𝐿 𝑌𝐴𝑁𝐺 𝐷𝐼𝐼𝑁𝐺𝐼𝑁 𝐾𝐴𝑁 (97))×𝑀𝐴𝑆𝑆𝐴 𝐻𝐶𝑙
Air = (𝑖𝑚𝑝𝑢𝑟𝑖𝑡𝑦 ℎ2𝑜 𝑦𝑔 𝑑𝑖𝑖𝑛𝑔𝑖𝑛𝑘𝑎𝑛 (3))/(𝑝𝑢𝑟𝑦𝑡𝑦 1.7109

𝑛𝑔 𝑑𝑖𝑖𝑛𝑔𝑖𝑛𝑘𝑎𝑛 (97))×𝑚𝑎𝑠𝑠𝑎 𝐻𝐶𝑙
komposisi
BAWAH
2.1314
0.0000
0.0001
0.0000
24.3696
26.5010
100.0000
komposisi
BAWAH
0.0000
0.0000
0.0070
0.0637
0.0466
1.4222
1.5395
100.00
komposisi
BAWAH
0.0042
0.0008
89.7570
0.0000
0.0015
0.0000
89.7635
100.00
Aliran 1 Aliran 2
Komponen
Kg/Jam Kgmol/Jam Kg/Jam Kgmol/Jam
ASAM KLORIDA 0.0000 0.0000 0.0000 0.0000
DIMETIL ETER 0.0000 0.0000 0.0000 0.0000
METIL KLORIDA 0.0000 0.0000 0.0000 0.0000
METANOL 8435.3699 263.2598 10544.2124 329.0747
AIR 8.4438 0.4687 10.5548 0.5859
TOTAL 8443.8137 263.7285 10554.7672 329.6606
Aliran 11 Aliran 12
Komponen
ASAM KLORIDA 10557.9020 289.5908 10557.9020 289.5908
DIMETIL ETER 0.0000 0.0000 0.0000 0.0000
METIL KLORIDA 0.1263 0.0025 0.1263 0.0025
METANOL 8435.5172 263.2644 8435.5172 263.2644
AIR 167.3082 9.2872 167.3082 9.2872
TOTAL 19160.8536 562.1449 19160.8536 562.1449
Aliran 21 Aliran 22
Komponen
ASAM KLORIDA 0.0000 0.0000 1439.7125 39.4896
DIMETIL ETER 9.0953 0.1974 0.0000 0.0000
METIL KLORIDA 0.9965 0.0197 12625.4741 250.0837
METANOL 0.0000 0.0000 0.7364 0.0230
AIR 209.8438 11.6483 0.3507 0.0195
TOTAL 219.9357 11.8654 14066.2737 289.6157

Aliran 3 Aliran 4 Aliran 5
Kg/Jam Kgmol/Jam Kg/Jam Kgmol/Jam Kg/Jam Kgmol/Jam
0.0000 0.0000 0.0000 0.0000 0.0000 0.0000
0.0000 0.0000 0.0000 0.0000 0.0000 0.0000
0.0000 0.0000 0.0000 0.0000 0.0000 0.0000
10544.2124 329.0747 2108.8425 65.8149 8435.3699 263.2598
10.5548 0.5859 2.1110 0.1172 8.4438 0.4687
10554.7672 329.6606 2110.9534 65.9321 8443.8137 263.7285

10557.9020 289.5908 1439.7139 39.4897 1439.7139 39.4897
0.0000 0.0000 9.0962 0.1974 9.0962 0.1974
0.1263 0.0025 12626.4833 250.1037 12626.4833 250.1037
8435.5172 263.2644 409.1226 12.7683 409.1226 12.7683
167.3082 9.2872 4676.4376 259.5858 4676.4376 259.5858
19160.8536 562.1449 19160.8536 562.1449 19160.8536 562.1449

1439.7125 39.4896 1439.7125 39.4896 0.1152 0.0032
0.0000 0.0000 0.0000 0.0000 0.0000 0.0000
12625.4741 250.0837 12625.4741 250.0837 12625.3479 250.0812
0.7364 0.0230 0.7364 0.0230 0.5891 0.0184
0.3507 0.0195 0.3507 0.0195 0.2104 0.0117
14066.2737 289.6157 14066.2737 289.6157 12626.2626 250.1144

18490.4107 507.1702 18490.4107 507.1702 18490.4107 507.1702
0.0000 0.0000 0.0000 0.0000 0.0000 0.0000
0.0000 0.0000 0.0000 0.0000 0.0000 0.0000
0.0000 0.0000 0.0000 0.0000 0.0000 0.0000
37541.1369 2083.8821 37541.1369 2083.8821 37541.1369 2083.8821
56031.5476 2591.0523 56031.5476 2591.0523 56031.5476 2591.0523

1439.7139 39.4897 0.0014 0.0000 1439.7125 39.4896
9.0962 0.1974 0.0009 0.0000 9.0953 0.1974
12626.4833 250.1037 0.0126 0.0003 12626.4707 250.1034
409.1226 12.7683 408.3862 12.7453 0.7364 0.0230
4676.4376 259.5858 4669.4229 259.1964 7.0147 0.3894
19160.8536 562.1449 5077.8241 271.9420 14083.0296 290.2028

1439.5973 39.4865 1439.5973 39.4865 1439.5973 39.4865
0.0000 0.0000 0.0000 0.0000 0.0000 0.0000
0.1263 0.0025 0.1263 0.0025 0.1263 0.0025
0.1473 0.0046 0.1473 0.0046 0.1473 0.0046
0.1403 0.0078 0.1403 0.0078 0.1403 0.0078
1440.0111 39.5013 1440.0111 39.5013 1440.0111 39.5013

Aliran 9 Aliran 10
9350.9038 256.4843 9118.3047 250.1044
0.0000 0.0000 0.0000 0.0000
0.0000 0.0000 0.0000 0.0000
0.0000 0.0000 0.0000 0.0000
37403.6151 2076.2484 158.7241 8.8107
46754.5189 2332.7327 9277.0287 258.9150
Aliran 19 Aliran 20
0.0000 0.0000 0.0000 0.0000
0.0000 0.0000 0.0000 0.0000
0.0000 0.0000 0.0000 0.0000
0.0000 0.0000 0.0000 0.0000
203.1799 11.2784 203.1799 11.2784
203.1799 11.2784 203.1799 11.2784
Aliran 29
Kg/Jam Kgmol/Jam
0.1152 0.0032
0.0000 0.0000
12625.3479 250.0812
0.5891 0.0184
0.2104 0.0117
12626.2626 250.1144
GAS kJ/kmol
KOMPONEN A B C
HCL 29.244 -0.0012615 1.121E-06
(CH3)2O 34.668 0.070293 0.0001653
CH3CL 27.385 0.026036 0.0001032
CH3OH 40.046 -0.038287 0.00024529
H2O 33.933 -0.0084186 2.9906E-05
H-01
C K
T in 30 303
T ref 25 298
T out 51.65 324.65
MASUK
KOMPONEN mol (kmol/jam) ∫ Cp dT (kJ/kmol) ∫ Cp dT (kJ/jam)
HCL 507.1702 498.1228 252633.0535
H2O 2083.8821 377.5028 786671.3439
TOTAL 1039304.3975
KELUAR
HCL 507.1702 2821.2586 1430858.2502
H2O 2083.8821 2007.0664 4182489.7494
TOTAL 5613347.9996
H-02
C K
T in 248 521
T ref 25 298
T out 350 623
MASUK
HCL 289.5908 6512.8870 1886072.2732
CH3CL 0.0025 14457.7586 36.1561
CH3OH 263.2644 11699.1460 3079968.3972
H2O 9.2872 8264.0696 76749.7247
TOTAL 5042826.5512
KELUAR
HCL 289.5908 9527.5747 2759098.1224
CH3CL 0.0025 24669.0318 61.6926
CH3OH 263.2644 18251.0256 4804844.9098
H2O 9.2872 12618.6920 117191.7930
TOTAL 7681196.5178
H-03
C K
T in -20.68 252.32
T ref 25 298
T out 90 363
MASUK
HCL 39.4865 -4009.5485 -158322.8687
CH3CL 0.0025 -3585.2154 -8.9660
CH3OH 0.0046 -3567.8269 -16.3999
H2O 0.0078 -3483.6102 -27.1289
TOTAL -158375.3635
KELUAR
HCL 39.4865 7722.7565 304944.3026
CH3CL 0.0025 5865.0653 14.6676
CH3OH 0.0046 5407.8119 24.8575
H2O 0.0078 4888.8227 38.0721
TOTAL 305021.8997
BEBAN PANAS : 1152257.8250 KJ/JAM

QP 463397.2632 KJ/JAM
QV 688860.5618 KJ/JAM
C-01
C K BM air (g/mol)
T in 230 503 18.015
T ref 25 298
T out 50 323
MASUK
HCL 39.4897 5983.9156 236302.7737
(CH3)2O 0.1974 16246.5040 3207.8443
CH3CL 250.1037 12935.6059 3235242.3760
CH3OH 12.7683 10623.3870 135642.8298
H2O 259.5858 7542.0843 1957817.7231
TOTAL 5568213.5468
KELUAR
HCL 39.4897 727.1527 28715.0109
(CH3)2O 0.1974 1689.9848 333.6846
CH3CL 250.1037 1224.5875 306273.8266
CH3OH 12.7683 1146.9395 14644.4928
H2O 259.5858 869.3183 225662.6536
TOTAL 575629.6685
D-01
NE Umpan
HCL 39.4896 -1008.7278 -39834.2738
CH3CL 250.0837 -858.0678 -214588.7507
CH3OH 0.0230 -838.5927 -19.2734
H2O 0.0195 -798.7119 -15.5501
TOTAL 289.6157 -254457.8479
C K
T 14.4475 287.4475
T ref 25 298
NE Destilat
HCL 39.4865 1532.5359 60514.4135
CH3CL 0.0025 1254.3980 3.1370
CH3OH 0.0046 1205.8947 5.5430
H2O 0.0078 1128.4440 8.7878
TOTAL 39.5013 60531.8813
C K
T -8.1851 264.8149
T ref 25 298
Menghitung beban kondensor

Energi kondensor = Energi vapour - Energi destilat - Energi refluks
Energi vapor = Q laten + Q sensibel
Q laten dari buku yaws (ΔHvap)
Enthalpy of vaporation (ΔHvap) = A*((1-(T/Tc))^n)
PANAS LATEN
KOMPONEN kJ/jam J/s
HCL 1240331.1789 344536.4386
CH3CL 112.0246 31.1179
CH3OH 190.5405 52.9279
H2O 546.8636 151.9066
TOTAL 1241180.6076 344772.3910
NE Kondensor
HCL 94.4121 -2998.4928 -283093.8598
CH3CL 0.0060 -2635.6375 -15.7598
CH3OH 0.0110 -2607.4548 -28.6571
H2O 0.0186 -2523.2597 -46.9833
TOTAL 94.4476 -283185.2600
C K
T -8.1851 264.8149
T ref 25 298
T umpan = 14.4475 287.4475
Tv = Tdp = -8.1851 264.8149
TR (Trial Tdp) 24.6961 297.6961
TD (Trial Tdp) 24.6961 297.6961
Td
KOMPONEN kmol/jam xi Pi (mmHg)
HCL 94.4121 0.1862 34608.1098
CH3CL 0.0060 0.0000 4254.8136
CH3OH 0.0110 0.0000 123.9152
H2O 0.0186 0.0000 22.9399
TOTAL 94.4476 0.1862 39009.7785
T 24.6961 C 297.6961
P 8.5 atm 6460.0000
Energi vapor = Q laten + Q sensibel

Energi vapor = 266109.8188 J/s
Energi kondensor = 295058.5106 J/s
1062210.6381 kJ/jam
STEAM kg/jam Q/lamda

T (C) lamda (kJ/kg) Q (kJ/jam) kg/jam
70 2334 1840849.8425 788.7103
SUHU MASUK VAPOURIZER
T AIR DARI TANKI 303

MASSA BAHAN 8443.81374808733
cp bahan 1.52235594627699
273
T AIR DARI BOTTOM VAPOURZER 338

MASSA BAHAN 2110.95343702183
cp bahan' 1.76534117888829
QLEPAS=QTERIMA
QPANS QDINGIN
M.C.ΔT M.C.ΔT
2110,9522*1,7528*(65-TC) 8443,8087*1,5211*(TC-30)
3726.55302909041 65-TC 12854.4900686562
65-TC 3.4494316780979
65-TC 3.4494316780979
4.44943167809791 TC 1383.17779846367
TC 310.866173150222
TC 37.8661731502218
SUHU MASUK ACCUMULATOR

T AIR DARI VAPORIZER TOP 338
MASSA BAHAN 8443.81374808734
cp bahan 1.48447341253192
T AIR DARI TOP STRIPER 363.0000

MASSA BAHAN 9277.02874919001
cp bahan' 0.225853064028901
T AIR DARI HETER 3 363

MASSA BAHAN 1440.01112243017
cp bahan' 0.190864008958156
273
QLEPAS=QTERIMA
QPANS QDINGIN
M.C.ΔT M.C.ΔT
(944,6867*0,2325*(90-TC))+((1440,0153*0,1908*(90-TC)) =
2095.24536808877 (90-TC) + 274.846295771355
760574.068616223 2195,8521TC +
-14904.70867327 TC
TC
TC
CAIR kJ/kmol
D E KOMPONEN A
4.9676E-09 -2.4963E-12 HCL 73.993
-1.7675E-07 4.9313E-11 (CH3)2O 48.074
1.0887E-07 3.1642E-11 CH3CL 11.381
-2.1679E-07 5.9909E-11 CH3OH 40.152
1.7825E-08 3.6934E-12 H2O 92.053

200 1938.6 4574043.6021 2359.4571
NERACA PANAS J/s

J/s ALIRAN MASUK KELUAR
70175.8482 IN 288695.6660
218519.8178 OUT 1559263.3332
288695.6660 PANAS 1270567.6672
TOTAL 1559263.3332 1559263.3332
J/s
397460.6250
1161802.7082
1559263.3332

370 452.6 2638369.9666 5829.3636
NERACA PANAS J/s

523908.9648 IN 1400785.1531
10.0434 OUT 2133665.6994
855546.7770 PANAS 732880.5463
21319.3680 TOTAL 2133665.6994 2133665.6994
1400785.1531
J/s
766416.1451
17.1368
1334679.1416
32553.2758
2133665.6994

200 1938.6 463397.2632 239.0371
NERACA PANAS J/s

ALIRAN MASUK KELUAR
J/s IN -43993.1565
-43978.5746 OUT 84728.3055
-2.4906 LATEN 382548.2846
-4.5555 PANAS 511269.7466
-7.5358 TOTAL 467276.5901 467276.5901
-43993.1565
PANAS LATEN
J/s KOMPONEN kJ/jam J/s
84706.7507 HCL 688433.9347 191231.6485
4.0743 CH3CL 53.9242 14.9790
6.9049 CH3OH 99.0534 27.5148
10.5756 H2O 273.6495 191274.1423
84728.3055 TOTAL 688860.5618 382548.2846
-42 -138
-188 -57 -62
AIR PENDINGIN
ALIRAN T (C) T (K)
IN 27 300
OUT 65 338
TOTAL
NERACA PANAS J/s

65639.6594 IN 1546725.9852
891.0679 OUT 159897.1301
898678.4378 PANAS -1386828.8551
37678.5638 TOTAL 159897.1301 159897.1301
543838.2564
1546725.9852 -4992583.8784
J/s
7976.3919 KPUTHN PNAS 1386828.8551
92.6902 AIR PENDINGIN 31463.3546
85076.0629
4067.9147
62684.0704
159897.1301
NE Bottom
J/s KOMPONEN mol (kmol/jam) ∫ Cp dT (kJ/kmol)
-11065.0760 HCL 0.0032 1532.5359
-59607.9863 CH3CL 250.0812 1853.8280
-5.3537 CH3OH 0.0184 1254.3980
-4.3195 H2O 0.0117 1205.8947
-70682.7355 TOTAL 250.1144
C K
T 39.9656 312.9656
T ref 25 298
NE Refuks
J/s KOMPONEN mol (kmol/jam) kg/jam
16809.5593 HCL 54.9256 2002.47729255
0.8714 CH3CL 0.0035 0.17562012249
1.5397 CH3OH 0.0064 0.20487196601
2.4411 H2O 0.0108 0.19514749295
16814.4115 TOTAL 54.9463 2003.0529
C K
T -8.1851 264.8149
T ref 25 298
Rop 1.3910
Destilat 39.5013 kmol/jam
Refluks (Ld) = 54.9463 kmol/jam
Refluks (Ld) = 2003.0529 kg/jam
menghitung REBOILER
ΔH in = ΔH out
ΔH in = ΔH umpan + ΔH reboiler
ΔH out = ΔH bottom + ΔH destilat + ΔH condensor
ΔH umpan + ΔH reboiler = ΔH bottom + ΔH destilat + ΔH condensor
ΔH reboiler = (ΔH bottom + ΔH destilat + ΔH condensor) - ΔH umpan
ΔH reboiler = 511347.1785 J/s
1840849.8425 kJ/jam
J/s Reboiler
-78637.1833 L' = L + F
-4.3777 L' = 16069.3267 kg/jam
-7.9603 V' = L' - B
-13.0509 V' = 3443.0641 kg/jam
-78662.5722
L'
KOMPONEN kmol/jam x
HCL 0.0032 0.0000
CH3CL 250.0812 0.9999
CH3OH 0.0184 0.0001
H2O 0.0117 0.0000
TOTAL 250.1144 1.0000
xi.Pi V'
6442.4580 KOMPONEN kmol/jam x
0.0502 HCL 0.0032 0.0000
0.0027 CH3CL 250.0812 0.9999
0.0008 CH3OH 0.0184 0.0001
6442.5117 H2O 0.0117 0.0000
K TOTAL 250.1144 1.0000
mmHg
NERACA PANAS J/s
ALIRAN MASUK KELUAR
Umpan -70682.7355
Destilat 16814.4115
Bottom 128791.5209
Reboiler 511347.1785
Kondensor 295058.5106
IN 440664.4429
OUT 440664.4429
PANAS 0.0000
TOTAL 440664.4429 440664.4429
AIR PENDINGIN
ALIRAN T (C) T (K)
IN 27 300
OUT 65 338
TOTAL
ALIRAN T (C) T (K)

IN -130 143
OUT -60 213
TOTAL
A B C
59.642 3.28E-01 -1.54E-03
TD TB BM PROPAN
K 231.07 85.49 44.1
C -41.93 -187.51
CP FLUIDA dingin
K KOMPONEN KGMOL/JAM Xi
KG/JAM metanol 263.259781984247 0.99822275489
kj/kg.k H2O 0.468710171972659 0.00177724511
TOTAL 263.72849215622 1
K CP FLUIDA dingin
KG/JAM KOMPONEN KGMOL/JAM Xi
kj/kg.k metanol 65.8149454960618 0.99822275489
H2O 0.117177542993152 0.00177724511
TOTAL 65.9321230390549 1
1,5211*(TC-30)
TC-30
(TC-30)
TC - 1045.17779846
k SUHU MASUK POMPA 1
c
UMULATOR
K CP FLUIDA dingin
KG/JAM KOMPONEN KGMOL/JAM
kj/kg.k metanol 263.259781984
H2O 0.46871017197
TOTAL 263.728492156
K
KG/JAM CP FLUIDA dingin
kj/kg.k KOMPONEN KGMOL/JAM
HCL 250.10435831
H2O 8.81066077781
TOTAL 258.915019088
K
KG/JAM
kj/kg.k CP FLUIDA dingin
KOMPONEN KGMOL/JAM
HCL 1439.5973
DME 0.0000
CH3CL 0.1263
CH3OH 0.1473
H20 0.1403
TOTAL 1440.0111
90-TC)) = 8443,8087*1,20338*(TC-65)
(90-TC) = 12534.6170094 (TC-65)
99769.2053650018 -274,82056TC = 10160,4796TC 4236700.54918
= -5097043.8232
= 341.975407564 K
= 68.9754075638 c
PANAS LATEN
B C D KOMPONEN
-0.12946 -7.898E-05 2.6409E-06 HCL
0.56225 -0.0023915 4.4614E-06 (CH3)2O
0.62328 -0.0024353 3.8333E-06 CH3CL
0.31046 -0.0010291 1.4598E-06 CH3OH
-0.039953 -0.00021103 5.3469E-07 H2O
CM-01
C K
T in 69.14 342.14
T ref 25 298
T out 248 521
MASUK
HCL 289.5908 1284.1415 371875.5731
CH3CL 0.0025 2217.1261 5.5446
CH3OH 263.2644 2050.4124 539800.5557
H2O 9.2872 1541.9608 14320.4342
TOTAL 7093.6408 926002.1076
KELUAR
HCL 289.5908 6512.8870 1886072.2732
CH3CL 0.0025 14457.7586 36.1561
CH3OH 263.2644 11699.1460 3079968.3972
H2O 9.2872 8264.0696 76749.7247
TOTAL 40933.8613 5042826.5512
CM-02
C K
T in 25.26 298.26
T ref 25 298
T out 220.3 493.3
MASUK
HCL 39.4896 7.5607 298.5675
CH3CL 250.0837 12.3382 3085.5760
CH3OH 0.0230 11.7421 0.2699
H2O 0.0195 8.9915 0.1751
TOTAL 40.6325 3384.5884
KELUAR
HCL 39.4896 5699.1802 225058.4465
CH3CL 250.0837 12146.2830 3037587.0424
CH3OH 0.0230 10053.6759 231.0634
H2O 0.0195 7158.0422 139.3594
TOTAL 3263015.9118
E-01
C K
T in 350 623
T ref 25 298
T out 230 503
MASUK
HCL 39.4897 9527.5747 376240.6531
(CH3)2O 0.1974 28246.9249 5577.3068
CH3CL 250.1037 24669.0318 6169815.1656
CH3OH 12.7683 18251.0256 233034.9781
H2O 259.5858 12618.6920 3275632.8358
TOTAL 10060300.9395
KELUAR
HCL 39.4897 5983.9156 236302.7737
(CH3)2O 0.1974 16246.5040 3207.8443
CH3CL 250.1037 12935.6059 3235242.3760
CH3OH 12.7683 10623.3870 135642.8298
H2O 259.5858 7542.0843 1957817.7231
TOTAL 5568213.5468
∫ Cp dT (J/mol) Cp/BM (J/g) Q/lamda (g/s) kg/jam

151.0672
3009.6752
2858.6080 158.6793 -8739.8207 -31463.3546
∫ Cp dT (kJ/jam) J/s
4.8415 1.3449
463607.4833 128779.8565
23.0638 6.4066
14.0865 3.9129
463649.4752 128791.5209
xi ∫ Cp dT (kJ/kmol) ∫ Cp dT (kJ/jam) J/s

0.999623177224561 -2998.4928 -164693.9984 -45748.3329
6.33101689988E-05 -2635.6375 -9.1685 -2.5468
0.00011636556343 -2607.4548 -16.6717 -4.6310
0.00019714704301 -2523.2597 -27.3332 -7.5926
1.0000 -164747.1718 -45763.1033
Vapor
KOMPONEN kgmol/jam kg/jam
HCL 94.4121 3442.0746
CH3CL 0.0060 0.3019
CH3OH 0.0110 0.3522
H2O 0.0186 0.3354
TOTAL 94.4476 3443.0641
Vapor = Ld +D = 94.4476 kgmol/jam
stilat + ΔH condensor
ondensor) - ΔH umpan
lb = vb + b
vd = vb = 94.4476 kgmol/jam
lb = 344.5620 kgmol/jam
kg/jam kmol/jam
0.2030 0.0056
16067.1919 318.2567
1.1813 0.0369
0.7505 0.0417
16069.3267 318.3408
kg/jam kmol/jam
0.0435 0.0012
3442.6067 68.1907
0.2531 0.0079
0.1608 0.0089
3443.0641 68.2087
kJ/jam
-254457.8479
60531.8813
463649.4752
1840849.8425
1062210.6381
BM air Tref:
18.015 25
298

151.0672
3009.6752
2858.6080 158.6793 1859.4641 6694.0708

-15221.6420
-8912.0785
6309.5635 143.0740 2062.2790 7424.2044
D T MIN T MAX
3.65E-06 86 333 K
CP FLUIDA dingin
cP(j/kmol.k) (Xi . Cp)/BM
48.5790246 1.513410141885
90.67891963 0.008945804392
1.522355946277 kj/kg.k
0.363599786543 btu/lbm.°F

56.384850075 1.7565894880518
88.71129249125 0.0087516908365
1.7653411788883 kj/kg.k
0.4216344261598 btu/lbm.°F
37.2436
Xi cP(j/kmol.k) (Xi . Cp)/BM

0.998222754894094 47.53858716335 1.48099679926261
0.001777245105906 35.240602344919 0.003476613269314
1 1.48447341253192 kj/kg.k
0.354551914908864 btu/lbm.°F

0.965970839355551 29.128056092391 0.878124111864516
0.034029160644449 35.734468694653 0.06750008191809
1 0.945624193782606 kj/kg.k
0.225853064028901 btu/lbm.°F

0.999712618886793 29.143002698157 0.799128519106901
0 42.20768467593 0
8.7676226462E-05 30.64560226162 5.3221566088E-05
0.000102279856274 18.25388257949 5.82674142271E-05
9.74250304717E-05 30.970554352974 0.000167488604028
0.999712618886793 0.799128519106901 kj/kg.k

0.190864008958156 btu/lbm.°F
69.1427
kJ/mol K YAWS pd 1 atm
A Tc n Td (C) Td (K)
30.54 324.65 0.647 -84.85 188.15
27.769 400.1 0.261 -24.69 248.31
32.534 416.25 0.452 -24.07 248.93
52.723 512.58 0.377 64.85 337.85
52.053 647.13 0.321 100.15 373.15
NERACA PANAS J/s

103298.7703 IN 257222.8077
1.5402 OUT 1400785.1531
149944.5988 PANAS 1143562.3454
3977.8984 TOTAL 1400785.1531 1400785.1531
257222.8077
J/s 4116824.4436
523908.9648
10.0434
855546.7770
21319.3680
1400785.1531
NERACA PANAS J/s

82.9354 IN 940.1634
857.1044 OUT 906393.3088
0.0750 PANAS 905453.1454
0.0486 TOTAL 906393.3088 906393.3088
940.1634
3259631.3234
J/s
62516.2351
843774.1784
64.1843
38.7110
906393.3088
NERACA PANAS J/s

104511.2925 IN 2794528.0387
1549.2519 OUT 1546725.9852
1713837.5460 PANAS -1247802.0535
64731.9384 TOTAL 1546725.9852 1546725.9852
909898.0100
2794528.0387
-4492087.3926
J/s
65639.6594
891.0679
898678.4378
37678.5638
543838.2564
1546725.9852
CD-01
C K BM air
T in 220.3 493.3 18.015
T ref 25 298
T out 14.4475 287.44746397441
MASUK
KOMPONEN mol (kmol/jam) ∫ Cp dT (kJ/kmol) ∫ Cp dT (kJ/jam) J/s
HCL 39.4896 5699.1802 225058.4465 62516.2351
CH3CL 250.0837 12146.2830 3037587.0424 843774.1784
CH3OH 0.0230 10053.6759 231.0634 64.1843
H2O 0.0195 7158.0422 139.3594 38.7110
TOTAL 3263015.9118 906393.3088
KELUAR
HCL 39.4896 -306.8371 -12116.8795 -3365.7999
CH3CL 250.0837 -494.0100 -123543.8461 -34317.7350
CH3OH 0.0230 -473.3835 -10.8798 -3.0222
H2O 0.0195 -364.1247 -7.0891 -1.9692
TOTAL -135678.6945 -37688.5262
FD-01
C K
T in 50 323
T ref 25 298
T out atas 50 323
T out bawah 50 323
MASUK
HCL 39.4897 727.1527 28715.0109 7976.3919
(CH3)2O 0.1974 1689.9848 333.6846 92.6902
CH3CL 250.1037 1224.5875 306273.8266 85076.0629
CH3OH 12.7683 1146.9395 14644.4928 4067.9147
H2O 259.5858 869.3183 225662.6536 62684.0704
TOTAL 575629.6685 159897.1301
KELUAR ATAS
HCL 39.4896 727.1527 28714.9822 7976.3839
(CH3)2O 0.1974 1689.9848 333.6512 92.6809
CH3CL 250.1034 1224.5875 306273.5203 85075.9779
CH3OH 0.0230 1146.9395 26.3601 7.3222
H2O 0.3894 869.3183 338.4940 94.0261
TOTAL 335687.0078 93246.3911
KELUAR BAWAH
HCL 0.0000 727.1527 0.0287 0.0080
(CH3)2O 0.0000 1689.9848 0.0334 0.0093
CH3CL 0.0003 1224.5875 0.3063 0.0851
CH3OH 12.7453 1146.9395 14618.1327 4060.5924
H2O 259.1964 869.3183 225324.1596 62590.0443
TOTAL 239942.6606 66650.7391
TOTAL KELUAR 575629.6685 159897.1301
SUHU OPERASI ABSORBER
T AIR AIR PROSES 298
MASSA BAHAN 203.1798727571
cp bahan 5.047495741396
T AIR DARI FD 323

MASSA BAHAN 14083.02955181
cp bahan' 0.000569633453
273
QLEPAS=QTERIMA
QPANS QDINGIN
M.C.ΔT M.C.ΔT
2110,9522*1,7528*(60-TC) 8443,8087*1,5211*(TC-25)
8.0221647530171 60-TC 1025.549542479
60-TC 127.8395014379
60-TC 127.8395014379
128.83950143793 TC 38419.1714285
TC 298.1940398691
TC 25.19403986915
pd 1 atm pd 8,5 atm
kJ/mol kJ/kmol Td (C) Td (K) kJ/mol
17.4347 17434.6844 -36.49 236.51 13.1374
21.5625 21562.4802 38.52 311.52 18.7348
21.5493 21549.2904 39.84 312.84 17.3369
35.1393 35139.2517 131 404 29.3696
39.5026 39502.5596 173.7 446.7 35.7312
ACC-01
C K
T in atas 65 338
T in tengah 90 363
T in bawah 90 363
T ref 25 298
T out 68.97540756384 341.975407563838
MASUK ATAS
CH3OH 263.2598 1853.0657 487837.6633
H2O 0.4687 1395.9051 654.2749
TOTAL 488491.9383
MASUK TENGAH
HCL 250.1044 1891.5405 473082.5212
H2O 8.8107 2282.9597 20114.3839
TOTAL 493196.9051
MASUK BAWAH
HCL 39.4865 1891.5405 74690.2345
CH3CL 0.0025 3357.3741 8.3962
CH3OH 0.0046 3061.3892 14.0720
H2O 0.0078 2282.9597 17.7787
TOTAL 74730.4814
TOTAL MASUK 1056419.3248
KELUAR
HCL 289.5908 1279.3505 370488.1420
CH3CL 0.0025 2208.3771 5.5227
CH3OH 263.2644 2042.5460 537729.6128
H2O 9.2872 1536.1480 14266.4496
TOTAL 922489.7272
V-01
C K
T in 37.87 310.87
T ref 25 298
T out atas 65 338
T out bawah 65 338
MASUK
CH3OH 329.0747 1035.8036 340856.7788
H2O 0.5859 970.6778 568.7082
TOTAL 341425.4870
KELUAR ATAS
CH3OH 263.2598 1853.0657 487837.6633
H2O 0.4687 1395.9051 654.2749
TOTAL 488491.9383
KELUAR BAWAH
CH3OH 65.8149 3272.1386 215355.6211
H2O 0.1172 3009.6752 352.6663
TOTAL 215708.2875
TOTAL KELUAR 704200.2258
ALIRAN T (C) T (K) ∫ Cp dT (J/mol) Cp/BM (J/g)

IN -100 173 -12595.0062
OUT -60 213 -8912.0785
TOTAL 3682.9277 83.5131
AIR PENDINGIN
ALIRAN T (C) T (K) ∫ Cp dT (kJ/kmol) Cp/BM (J/g)
IN 27 300 151.0672
OUT 65 338 3009.6752
TOTAL 2858.6080 158.6793
NERACA PANAS J/s

ALIRAN MASUK KELUAR
IN 906393.3088
OUT -37688.5262
LATEN 1348844.3768
PANAS 404762.5417
TOTAL 1311155.8506 1311155.8506
PANAS LATEN
KOMPONEN kJ/jam J/s
HCL 518791.8562 144108.8489
CH3CL 4335677.2519 1204354.7922
CH3OH 675.0004 187.5001
H2O 695.6482 193.2356
TOTAL 4855839.7566 1348844.3768
NERACA PANAS J/s

ALIRAN MASUK KELUAR
IN 159897.1301
OUT 159897.1301
PANAS 0.0000
TOTAL 159897.1301 159897.1301
ABSORBER
CP FLUIDA dingin
k KOMPONEN KGMOL/JAM Xi
KG/JAM H2O 11.2783720653373 1
kj/kg.k
TOTAL 11.2783720653373 1
k
KG/JAM CP FLUIDA DINGIN
KJ/KG.K KOMPONEN KGmol/JAM Xi
HCL 39.48962 0.1360759264615
(CH3)2O 0.19743 0.0006803122747
CH3CL 250.10341 0.8618228183763
CH3OH 0.02298 7.91962684E-05
H2O 0.38938 0.0013417466192
TOTAL 290.202817825757 1
8087*1,5211*(TC-25)
TC-30
(TC-30)
TC - 38096.1714285017
k SUHU MASUK POMPA 1
c
mmHg (Pi)
kJ/kmol komponen A B
13137.4243 HCL 16.504 1714.25
18734.7913 CH3CL 16.1052 2077.97
17336.9066 CH3OH 18.5875 3626.55
29369.5747 H2O 18.3036 3816.44
35731.1931
R-01
NERACA PANAS J/s
ALIRAN MASUK KELUAR T in
IN 293449.8124 T ref
OUT 256247.1464 T out
PANAS -37202.6660
TOTAL 256247.1464 256247.1464 MASUK
-133929.5976 KOMPONEN
HCL
J/s CH3CL
135510.4620 CH3OH
181.7430 H2O
135692.2051 TOTAL
KELUAR
J/s KOMPONEN
131411.8114 HCL
5587.3289 (CH3)2O
136999.1403 CH3CL
CH3OH
J/s H2O
20747.2874 TOTAL
2.3323 REAKSI UTAMA
3.9089 KOMPONEN
4.9385 CH3OH
20758.4671 HCL
293449.8124 CH3CL
H2O
J/s Hf
102913.3728 REAKSI SAMPING
1.5341 KOMPONEN
149369.3369 CH3OH
3962.9027 (CH3)2O
256247.1464 H2O
Hf
200 1938.6 9632041.7215 4968.5555
NERACA PANAS J/s

94682.4386 IN 94840.4131
157.9745 OUT 195611.1738
94840.4131 LATEN 2574796.3841
PANAS 2675567.1449
J/s TOTAL 2770407.5579 2770407.5579
135510.4620
181.7430 PANAS LATEN 1 atm
135692.2051 KOMPONEN kJ/jam J/s
CH3OH 9250751.7313 2569653.2587
J/s H2O 18515.2515 5143.1254
59821.0059 TOTAL 9269266.9828 2574796.3841
97.9629 BEBAN PANAS 9632041.7215
59918.9687 9632041.7215 QV 9269266.9828
195611.1738 QP 362774.7387
ST-01
Q/lamda (g/s) kg/jam NE Umpan
KOMPONEN mol (kmol/jam)
HCL 507.1702
4846.6952 17448.1028 H2O 2083.8821
TOTAL 2591.0523
C
Q/lamda (g/s) kg/jam T 70.0000
T ref 25
2550.8209 9182.9553 NE Atas

HCL 250.1044
H2O 8.8107
TOTAL 258.9150
C
1457145.1503 T 90.0000
4720161.0621 4720161.0621 T ref 25
NE Bawah
HCL 256.4843
H2O 2076.2484
TOTAL 2332.7327
C
T 95.0000
T ref 25
CP FLUIDA dingin
90.9306357813 5.047495741396
5.047495741396 kj/kg.k
1.205544852133 btu/lbm.°F
CP FLUIDA DINGIN
cP(Kj/kmol.k) (Xi . Cp )/bm
29.1843328481 0.108927673774
38.5741144563 0.000569633453
28.9586065125 0.494348576426
38.7181506813 9.56973052E-05
33.5890862088 0.002501695413
0.606443276371 KJ/KG.K
0.144843028582 BTU/LBM.°F
BM TABEL STEAM (LAMDA
C HCl 36.4580
-14.45 CH3Cl 50.4850 (CH3)2O
-29.55 ch3oh 32.0420
-34.29 H2O 18.0150
-46.13
AIR PENDINGIN
C K BM air ALIRAN T (C)
350 623 18.015 IN 27
25 298 OUT 65
350 623 TOTAL
NERACA PANAS
mol (kmol/jam) ∫ Cp dT (kJ/kmol) ∫ Cp dT (kJ/jam) J/s ALIRAN
289.5908 -9527.5747 -2759098.1224 -766416.1451 IN
0.0025 -24669.0318 -61.6926 -17.1368 OUT
263.2644 -18251.0256 -4804844.9098 -1334679.1416 Hf
9.2872 -12618.6920 -117191.7930 -32553.2758 HR
-7681196.5178 -2133665.6994 TOTAL
mol (kmol/jam) ∫ Cp dT (kJ/kmol) ∫ Cp dT (kJ/jam) J/s HR

39.4897 9527.5747 376240.6531 104511.2925 -1725583.7297
0.1974 28246.9249 5577.3068 1549.2519
250.1037 24669.0318 6169815.1656 1713837.5460
12.7683 18251.0256 233034.9781 64731.9384
259.5858 12618.6920 3275632.8358 909898.0100
10060300.9395 2794528.0387
Hf (kJ/mol) kmol/jam koef kJ/jam J/s reaktan

-201.17 250.1012 1 -50312850.2870 -13975791.7464 -73397187.3229
-92.3 250.1012 1 -23084337.0358 -6412315.8433 -20388107.5897
-86.32 250.1012 1 -21588732.1011 -5996870.0281
-241.8 250.1012 1 -60474460.4037 -16798461.2232
Hf -8666005.1819 -2407223.6616
Hf (kJ/mol) kmol/jam koef kJ/jam J/s reaktan

-201.17 0.3949 2 -158882.6851 -44134.0792 -158882.6851
-184.05 0.1974 1 -36340.3567 -10094.5435 -44134.0792
-241.8 0.1974 1 -47742.9951 -13261.9431
Hf 74799.3334 20777.5926
ST-01
C K STEAM
T in 51.65 324.65 T (C)
T ref 25 298 200
T out atas 90 363
T out bawah 95 368
MASUK
HCL 507.1702 2821.2586 1430858.2502 397460.6250
H2O 2083.8821 2007.0664 4182489.7494 1161802.7082
TOTAL 5613347.9996 1559263.3332
KELUAR ATAS
HCL 250.1044 1891.5405 473082.5212 131411.8114
H2O 8.8107 2282.9597 20114.3839 5587.3289
TOTAL 493196.9051 136999.1403
KELUAR BAWAH
HCL 256.4843 8448.1472 2166816.9214 601893.5893
KJ/JAM H2O 2076.2484 5265.6570 10932811.8884 3036892.1912
KJ/JAM TOTAL 13099628.8099 3638785.7805
KJ/JAM TOTAL KELUAR 13592825.7149 3775784.9208
L'
∫ Cp dT (kJ/kmol) ∫ Cp dT (kJ/jam) J/s KOMPONEN kmol/jam
5028.6005 2550356.2800 708432.3000 HCL 256.4843
3385.1309 7054213.9012 1959503.8614 H2O 2076.2484
9604570.1812 2667936.1614 TOTAL 2332.7327
K
343.0000 V'
298 KOMPONEN kmol/jam
HCL 256.4843
H2O 2076.2484
∫ Cp dT (kJ/kmol) ∫ Cp dT (kJ/jam) J/s TOTAL 2332.7327
1891.5405 473082.5212 131411.8114
2282.9597 20114.3839 5587.3289 NERACA PANAS J/s
493196.9051 136999.1403 ALIRAN MASUK
K Umpan 2667936.1614
363.0000 Destilat
298 Bottom
Reboiler 2415774.9263
Laten
∫ Cp dT (kJ/kmol) ∫ Cp dT (kJ/jam) J/s IN 5083711.0877
8448.1472 2166816.9214 601893.5893 OUT
5265.6570 10932811.8884 3036892.1912 PANAS 0.0000
13099628.8099 3638785.7805 TOTAL 5083711.0877
K
368.0000
298
TABEL STEAM (LAMDA) DI BUKU SMITH
TOTAL STEAM 50688.3347
46.0690 TOTAL AIR PENDIN 77404.6269
T (K) ∫ Cp dT (kJ/kmol) Cp/BM (J/g) Q/lamda (g/s) kg/jam

300 151.0672
338 3009.6752
2858.6080 158.6793 -10874.6601 -39148.7764
J/s
MASUK KELUAR
-2133665.6994
2794528.0387
-2386446.0690
1725583.7297
4520111.7684 4520111.7684 -16272402.3663 16272402.3663
-6212101.4268
-8591205.8485
Tekanan in 4.9 atm

tekanan out 4.9 atm
produk MASSA AIR DINGIN 39148.7764 KG/JAM
beban panas 1725583.7297 j/s
-82063192.5048
-22795331.2513
produk
-84083.3517
-23356.4866
kg/jam Q/lamda
lamda (kJ/kg) Q (kJ/jam) kg/jam
1938.6 12688011.9163 6544.9355
NERACA PANAS J/s

ALIRAN MASUK KELUAR
IN 1559263.3332
OUT 3775784.9208
LATEN 1307926.1669
PANAS 3524447.7545
TOTAL 5083711.0877 5083711.0877
PANAS LATEN
KOMPONEN kJ/jam J/s
HCL 4360490.5486 1211247.3746
H2O 348043.6523 96678.7923
TOTAL 4708534.2009 1307926.1669
12688011.9163
REBOILER
x kg/jam kmol/jam ΔH in = ΔH out
0.1100 7180.6869 196.9578 ΔH in = ΔH umpan + ΔH reboiler
0.8900 58127.8895 3226.6383 ΔH out = ΔH bottom + ΔH destilat + ΔH laten
1.0000 65308.5764 3423.5961 ΔH umpan + ΔH reboiler = ΔH bottom + ΔH destila
ΔH reboiler = (ΔH bottom + ΔH destilat + ΔH laten
ΔH reboiler =
x kg/jam kmol/jam
0.1100 2040.0212 55.9554
0.8900 16514.0363 916.6826 Reboiler
1.0000 18554.0575 972.6379 L' = D + F
L' =
V' = L' - B
KELUAR kJ/jam V' =
9604570.1812
136999.1403 493196.9051 lb = vb + b
3638785.7805 13099628.8099 PANAS LATEN
8696789.7347 KOMPONEN kJ/jam
1307926.1669 4708534.2009 HCL 4360490.5486
H2O 348043.6523
3775784.9208 TOTAL 4708534.2009
5083711.0877
EV-01
C K
T in -8.1851 264.8148880606
T ref 25 298
T out -20.68 252.32
MASUK
HCL 39.4865 -2998.4928 -118399.8614
CH3CL 0.0025 -2635.6375 -6.5913
CH3OH 0.0046 -2607.4548 -11.9854
H2O 0.0078 -2523.2597 -19.6501
TOTAL -10764.8448 -118438.0882
KELUAR
HCL 39.4865 -4009.5485 -158322.8687
CH3CL 0.0025 -3585.2154 -8.9660
CH3OH 0.0046 -3567.8269 -16.3999
H2O 0.0078 -3483.6102 -27.1289
TOTAL -14646.2010 -158375.3635
EV-02
C K
T in 39.9656 312.9655643871
T ref 25 298
T out 32.6 305.6
MASUK
HCL 0.0032 1532.5359 4.8415
CH3CL 250.0812 1254.3980 313701.3128
CH3OH 0.0184 1205.8947 22.1720
H2O 0.0117 1128.4440 13.1818
TOTAL 5121.2726 313741.5081
KELUAR
HCL 0.0032 762.5448 2.4090
CH3CL 250.0812 631.1812 157846.5319
CH3OH 0.0184 609.8605 11.2131
H2O 0.0117 573.5967 6.7004
TOTAL 2577.1832 157866.8544
AB-01
T in atas
T in bawah
T ref
T out atas
T out bawah
MASUK ATAS
KOMPONEN
H2O pelarut
TOTAL
MASUK BAWAH
KOMPONEN
HCL
(CH3)2O
CH3CL
CH3OH
H2O
TOTAL
H umpan + ΔH reboiler TOTAL MASUK
ΔH bottom + ΔH destilat + ΔH laten KELUAR ATAS
+ ΔH reboiler = ΔH bottom + ΔH destilat + ΔH laten KOMPONEN
er = (ΔH bottom + ΔH destilat + ΔH laten) - ΔH umpan HCL
8696789.7347 kJ/jam CH3CL
2415774.9263 J/s CH3OH
H2O
TOTAL
KELUAR BAWAH
65308.5764 kg/jam KOMPONEN
(CH3)2O
18554.0575 kg/jam CH3CL
H2O
2591.6477 kgmol/jam H2O pelarut
TOTAL
J/s TOTAL KELUAR
1211247.3746
96678.7923
1307926.1669
NERACA PANAS J/s
-32888.8504 IN -32899.4689
-1.8309 OUT -43993.1565
-3.3293 PANAS -11093.6876
-5.4584 TOTAL -43993.1565 -43993.1565
-32899.4689
J/s -39937.2753
-43978.5746
-2.4906
-4.5555
-7.5358
-43993.1565
NERACA PANAS J/s

1.3449 IN 87150.4189
87139.2536 OUT 43851.9040
6.1589 PANAS -43298.5149
3.6616 TOTAL 43851.9040 43851.9040
87150.4189
J/s -155874.6537
0.6692
43846.2588
3.1148
1.8612
43851.9040
C K
25 298
50 323
25 298
25.194039869147 298.19403986915
25.194039869147 298.19403986915
mol (kmol/jam) ∫ Cp dT (kJ/kmol) ∫ Cp dT (kJ/jam) J/s

11.2784 0.0000 0.0000 0.0000
0.0000 0.0000

39.4896 727.1527 28714.9822 7976.3839
0.1974 1689.9848 333.6512 92.6809
250.1034 1224.5875 306273.5203 85075.9779
0.0230 1146.9395 26.3601 7.3222
0.3894 869.3183 338.4940 94.0261
335687.0078 93246.3911
TOTAL MASUK 335687.0078 93246.3911

39.4896 5.6426 222.8230 61.8953
250.0837 9.2073 2302.5955 639.6099
0.0230 8.7629 0.2014 0.0559
0.0195 6.7103 0.1306 0.0363
2525.7505 701.5974

0.1974 12.8102 2.5291 0.7025
0.0197 9.2073 0.1817 0.0505
0.3699 6.7103 2.4822 0.6895
11.2784 17.6432 198.9870 55.2742
5.1931 1.4425
TOTAL KELUAR 2530.9436 703.0399
NERACA PANAS J/s
ALIRAN MASUK KELUAR
IN 93246.3911
OUT 703.0399
PANAS -92543.3512
TOTAL 703.0399 703.0399
-333156.0642
TANGKI METANOL
kode : T-01
fungsi : Menyimpan bahan baku glukosa
kondisi operasi : T= 30
P= 1
tujuan : 1. menentukan tipe tangki
2. menentukan bahan konstruksi
3. menentukan dimensi tangki
(1) menentukan tipe tangki

dalam perancangan ini dipilih tipe tangki silinder tegak dengan dasar datar (flat bottom) dan bagian atas b
* tangki mampu menampung dalam kapsitas yang besar dengan konstruksi yang mudah, sehingga lebih e
* kondisi operasi pada tekanan lebih dari 1 atm, sehingga bisa digunakan torispherical roof
(2) menentukan bahan konstruksi

dalam perancangan dipilih bahan konstruksi Carbon Steel SA 283 grade C, karena :
* suhu operasi -20 sampai 650 °F
* harga murah dan mudah difabrikasi
densitas A * B^-(1-T/Tc)^n
Komponen Td
CH3OH 64.7000
H2O 100.0000
H2SO4 290.0000
ch3cl -23.7000
hcl 85.0500
data de
komponen massa (kg/jam)
ch3oh 8435.3699
h2o 8.4438
total 8443.8137
782.9905
(3) menentukan dimensi tangki

Laju alir, F :
Density, p :
lama penyimpanan :
Menghitung kebutuhan bahan baku selama

kapasitas bahan baku metanol yang dapat disimpan selama 14 hari
Volume tanngki metanol =

over design =
volume perancangan =
tangki kecil <= 71534 ft3

tangki besar > 71534 ft3
(a) menentukan diameter dan tinggi tangki

karena tangki masuk ke dalam kategori tangki besa
berdasarkan (Lioyd E. Brownell, Process Equipment Vessel Design, 1959, app. E, item 1, pg. 346), ukuran t
D=
H=
V=
(b) menentukan tebal dinding shell

bahan konstruksi yang dipilih :
tebal plate dirumuskan sebagai berikut :

𝑃= 𝑃𝑖𝑛 + 𝑃ℎ
sehingga :
dengan :
ts =
Pin =
D=
f=
E=
C=
H=
ρ=
ts =
tebal shell standar =
cara sitek
ph =
pd=
r=
ts=
ts =
(c) design Head
rc = 1080.0000
icr = 64.8000
w 1.7706
th = 1.7919
sf = 3.0000
b= 182.8846
tinggi head = 187.6765
tinggi total tangki = 45.8259
th= 0.5068
1.2874
kode alat fungsi alat bentuk

T-01 menyimpan bahan baku ethylene dichloride silinder
TANGKI METANOL
°C 303 K
atm 14.7 psia
ar (flat bottom) dan bagian atas berbentuk TORISPERIKAL, dengan alasan :

ksi yang mudah, sehingga lebih ekonomis
torispherical roof
g/ml
a b n Tc
0.2720 0.2719 0.2331 512.5800
0.3471 0.2740 0.2857 647.1300
0.4217 0.1936 0.2867 925.0000
0.3582 0.2611 0.2869 416.2500
0.4413 0.2696 0.3187 324.6500
data densitas (yaws)

xi ρ (kg/m3) xi/ρ V (m3)
0.9990 782.8067 0.0013 10.7758
0.0010 1023.0130 0.0000 0.0083
1.0000 1805.8197 0.0013 10.7841
kg/m3 782.9905 kg/m3
8443.8137 kg/jam
782.9905 kg/m3
48.8805 lb/ft3
14.0000 hari
14.0000 hari
2837121.4194
6254774.6235
3623.4428 m3 127960.7954 ft3
20%
4348.1314 m3
153552.9545 ft3
2025.6173 m3
2025.6173 m3
uk ke dalam kategori tangki besar maka
D 80.4981 ft
H 30.1868 ft
app. E, item 1, pg. 346), ukuran tangki standar yang mendekati hasil perhitungan :
90.0000 ft 27.4320 m 1080.0000

30.0000 ft 9.1440 m
33990.0000 bbl 191736.1315 ft3
5429.3626 m3 1434284.0493 gal
jumlah tangki yang dibutuhkan = 0.8009 tangki ≈ 1.0000 tangki standar

V campuran / jumlah tangki
ketinggian cairan tangki =
A
= 20.124368 ft 6.1340
yang dipilih : Carbon Steel SA 283 grade C

allowable stress (f) = 12650.0000 lb/in2 (Lioyd E. Brownell, Process Equipm
corrossion allowance (c) = 0.1250 in (Peter & Timmerhaus, 1991)
effisiensi pengelasan = 0.8000 (double welded butt joint) (Lioyd E. Brownell, Process Equipm
skan sebagai berikut :
(Lioyd E. Brownell, Process Equipment Vessel Design, 1959, eq. 3.16, pg

𝑃= 𝑃𝑖𝑛 + 𝑃ℎ
(Lioyd E. Brownell, Process Equipment Vessel Design, 1959, eq. 3.17, pg
tebal shell minimum, in

tekanan dalam tangki, psi
Pin untuk perancangan dengan over design = 20%
Pin = 17.6400 psi
diameter tangki, in
allowable stress, psi
efisiensi pengelasan
faktor korosi, in
tinggi tangki, ft
densitas campuran, lb/ft3
1.5915 in
1.6250 in satu 5/8
6.4917 psi
8.0851 psi
540.0000
0.1250 in
2.5000 in
6.3500 cm
1.0817
1.1250 satu 1/8
in
in
in dipakai plat standar 2,5 in
in untuk th = 2,5, dari tabel
in
in 15.6391 ft
ft
in
cm
bentuk tutup volume (m3) diameter (m) tinggi (m) tebal (cm)
torispherical 0.0000 tebal shell minimumtekanan dalam tan 0.0000
k
303.0000
ρ(g/ml) kg/m3
0.7828 782.8067
1.0230 1023.0130
1.8259 1825.9087
0.9028 902.8000
0.7673 767.3262
kg
lb
24.5361 m
9.2010 m
in
E. Brownell, Process Equipment Vessel Design, 1959, tab. 13.1, pg. 251)
& Timmerhaus, 1991)
E. Brownell, Process Equipment Vessel Design, 1959, tab. 13.2, pg. 254)
sel Design, 1959, eq. 3.16, pg. 45)

sel Design, 1959, eq. 3.17, pg. 46)
jumlah P tangki (at T tangki (Obahan konstruksi

0.0000 0.0000 0.0000 carbon steel SA-283 grade C
TANGKI PENYIMPANAN BAHAN BAKU asam klorida
density A B^-(1-T/TC)^n
A B
HCl 0.44134 0.26957
H2O 0.3471 0.274
komponenmassa fraksi (xi)

HCl 18490.41070875 0.33
H2O 37541.1368935227 0.67
Total 56031.5476022728 1
volume tangki
Torispherical 14
a volume tangki
menghitung volume cairan total laju alir massa * waktu penyimpanan / ρ komponen
491311.657562136
menghitung volume tangki 589573.98907456
b dimensi tangki
D/H=2
Vtangki=1/4*π*D^2*H
1/4*π*D^2*D/2
1/8*π*D^3 34.9071597862815
D= (8*Vtangki/π)^1/3 114.52480244843
H= D/2 57.2624012242151
17.4535798931408
c menghitung tebal tangki
Acairan=1/4*π*D^2 11304
Hcairan=Vcairan/Acairan 43.4635224311868
Phidrostatis=ρ*(H-1)/144 24.9116567127493
Pdesign=(Phidrostatis+Poperasi)-Patmosferik 135.131656712749
r=D/2 60
tebal silinder tangki 1.69789905665958

ts=(Pdesign*r/s*E-0,6*Pdesign)+C 0.668464195535267
tebal tutup tangki 1.53364540278557

th=(0,885*Pdesign*r/s*E-0,1*Pdesign)+C 0.603797402671484
n Tc T g/ml
0.3187 324.65 30 1.573178357585
0.28571 647.13 30 1.244888143879
densitas (ρ) g/ml ρ * xi lbm/jam lbm/ft^3

1.573178357585 0.519148858003051
1.2448881438792 0.834075056399067
1.35322391440212 123528.4 84.47906253
hari 336 1 atm 14.696 psi

8.5 124.916
penyimpanan / ρ komponen
ft^3
ft^3 16695.475 m^3
m
ft standarisasi diameter, tinggi dan volume diperoleh dari Appendix E Brownell dan Young
ft didapat, volume 120900 120 60
m 19221.891 barrel D H
m^3
ft^2 Allowable Working Stre 18750 psi
ft join efisiensi (E) 0.8
psi faktor korosi (C) 0.125 in
psi
ft jumlah tangki 0.869 jadi 1
cm
in
cm
in
wnell dan Young
TANGKI PENYIMPANAN PRODUK metil klorida
density A B^-(1-T/TC)^n
A B n
HCL 0.44134 0.26957 0.3187
CH3CL 0.35821 0.26109 0.2869
CH3OH 0.27197 0.27192 0.2331
H2O 0.3471 0.274 0.28571
komponenmassa fraksi (xi) densitas (ρ) g/ml

HCL 0.115176997394209 9.122018194E-06 1.573178357585
CH3CL 12625.3478730515 0.9999275515457 1.33341352694569
CH3OH 0.589136522537937 4.665961259E-05 0.98216553572415
H2O 0.210439691223534 1.666682354E-05 1.2448881438792
Total 12626.2626262626 1
volume tangki
Torispherical 14 hari
a volume tangki
menghitung volume cairan total laju alir massa * waktu penyimpanan / ρ komp
112359.34094993 ft^3
menghitung volume tangki 134831.20913992 ft^3
b dimensi tangki
D/H=2
1/4*π*D^2*D/2
1/8*π*D^3 21.346755969511 m
D= (8*Vtangki/π)^1/3 70.035288613883 ft
H= D/2 35.017644306941 ft
10.673377984756 m
Acairan=1/4*π*D^2 5024 ft^2
Hcairan=Vcairan/Acairan 22.364518501181 ft
Phidrostatis=ρ*(H-1)/144 12.35008052861 psi
Pdesign=(Phidrostatis+Poperasi)-Patmosferik 35.017644306941 psi
r=D/2 40 ft
tebal silinder tangki 0.669791948822 cm

ts=(Pdesign*r/s*E-0,6*Pdesign)+C 0.2636976176465 in
tebal tutup tangki 0.628738773752 cm
th=(0,885*Pdesign*r/s*E-0,1*Pdesign)+C 0.2475349502961 in
Tc T g/ml
324.65 30 1.5731783576
416.25 30 1.3334135269
512.58 30 0.9821655357
647.13 30 1.2448881439
ρ * xi lbm/jam lbm/ft^3
1.43505615997017E-05
1.33331692319669
4.58274633912322E-05
2.07483310271776E-05
1.33339784955271 27836.14 83.241360952
336 1 atm 14.696 psi
u penyimpanan / ρ komponen
3818.132 m^3
standarisasi diameter, tinggi dan volume diperoleh dari Appendix E Brownell dan Young
didapat, volume 32230 80 36
5124.2477 barrel D H
m^3
Allowable Working Stress (s) 12650 psi
join efisiensi (E) 0.8
faktor korosi (c) 0.125 in
jumlah tangki = volume standarisasi 0.745111 jadi 1

MENARA DESTILASI (D-01)
mmHg (Pi)
komponen A
HCL 16.504
CH3CL 16.1052
CH3OH 18.5875
H2O 18.3036
Bubble Point FEED

KOMPONEN kmol/jam
HCL 39.4896
CH3CL 250.0837
CH3OH 0.0230
H2O 0.0195
TOTAL 289.6157
T 14.4475
P 8.5
Dew Point DESTILAT

KOMPONEN kmol/jam
HCL 39.4865
CH3CL 0.0025
CH3OH 0.0046
H2O 0.0078
TOTAL 39.5013
T -8.1851
P 8.5
Bubble Point BOTTOM

KOMPONEN kmol/jam
HCL 0.0032
CH3CL 250.0812
CH3OH 0.0010
H2O 0.0010
TOTAL 250.0864
T 39.9656
P 8.5
relativ volatilitas rata-rata

Destilat
KOMPONEN
Ki
HCL 2.4196
CH3CL 0.2230
CH3OH 0.0027
H2O 0.0004
TOTAL 2.6457
Menentukan jumlah plate minimum

Nm = log[(xLK/xHK)D * (xHK/xLK)B] / log αavg,LK
Menentukan refluks minimum

Karena feed masuk adalah liquid pada boiling point, maka q=1 sehingga
Nilai Ø harus berada di antara nilai volatilitas realtif komponen LK dan HK, antara 1 - 8,8861
Ø
Hasil trial Ø
KOMPONEN
kgmol/jam
HCL 39.4896
CH3CL 250.0837
CH3OH 0.0230
H2O 0.0195
TOTAL 289.6157
Hasil perhitungan Rm
KOMPONEN αavg
HCL 8.9012
CH3CL 1.0000
CH3OH 0.0222
H2O 0.0037
TOTAL 9.9271
Σαi * XiD / (αi - Ø)

1.9273
Rm=
R operasi berkisar antara 1.2 - 1.5 Rm (geankoplis, 1993)
R operasi =
Jumlah stage ideal

Rop / (Rop + 1) [sumbu y]
Rm / (Rm + 1)
Nm / N
Nm =
N=
Penentuan effisiensi plat
Menghitung µavg produk atas D-01 pada T = 287.4475
Viskositas cairan (log µ = A + (B/T) + CT + D(T^2))
Komponen (Umpan masuk) A
HCL -1.515
CH3CL -7.3473
CH3OH -9.0562
H2O -10.2158
KOMPONEN BM(kg/kgmol)
HCL 36.4580
CH3CL 50.4850
CH3OH 32.0420
H2O 18.0150
TOTAL
Viskositas rata-rata komponen adalah = 0.1746
Untuk mengetahui efisiensi kolom, dihitung dengan cara
αLK x µavg = 1.5538
Effisiensi kolom diperoleh dengan cara memplotkan nilai αLK.µavg dengan grafik pada fig. 8.16, Chopey,2003
Dari grafik didapat efisiensi kolom sebesar 0.6700
N aktual = N ideal / E 22.3881
Menentukan letak umpan masuk

log Nr/Ns = 0.206 x log [((B.XHk,F)/(D.XLk,F)) x ((XLk,B/XHk,D)^2)] 0.0131
Nr/Ns = 1.0307
Nr + Ns = 23.0000
Ns = Nr + Ns / (Nr/Ns +1) 11.3259
Ns artinya, umpan masuk dari plate ke 47 dari bawah
Nr = 79 - NS = 11.0000
Nr artinya, umpan masuk dari plate ke 11 dari atas
Menentukan sifat-sifat fisika DESTILAT

A. Densitas liquid
d = AB^-(1-T/Tc)^n
keterangan
d = densitas, g/ml
A,B dan n = koefisien regresi
T = suhu komponen, K
Tc = suhu kritil, K
Komponen A
HCL 0.44134
CH3CL 0.35821
CH3OH 0.27197
H2O 0.3471
Total
T top = 264.8149
P= 6460.0000
Komponen Top kg/jam
HCL 1439.5973
CH3CL 0.1263
CH3OH 0.1473
H2O 0.1403
Total 1440.0111
Jadi densitas cairan di top adalah = 948.17804
B. Densitas uap
d = (BM x P)/(R x T)
R= 8314.3000
T top = 264.8149
P= 6460.0000
Komponen Top BM
HCL 36.4580
CH3CL 50.4850
CH3OH 32.0420
H2O 18.0150
Total
C. Tegangan permukaan
σ = [Pch(dl-dv)/BM]^4 x 10^-12
keterangan :
σ = tegangan permukaan, dyne/cm
Pch =Sudgen's parchor (dari tabel 8.7, buku coulson & richardson hal.335)
dl = densitas cairan (kg/m3)
dv = densitas uap (kg/m3)
BM
Tabel tegangan permukaan di TOP
atom group or bond kontribusi
C 4.8
H 17.1
OH 11.3
O 20
Cl 54.3
Komponen BM
HCL 36.45800
CH3CL 50.48500
CH3OH 32.04200
H2O 18.01500
Total
Jadi, tegangan permukaan di top adalah 1.61780
Menentukan diameter menara

Tinggi tray spacing, di buku coulson hal.568, fig.11.27 =
A. Laju alir massa bagian atas
Umpan (F) 14066.27375
Top (D) 1440.01112
V = (1+R) x D = 3443.06405
L=RxD 2003.05293
B. Liquid-vapor flow factor dan konstanta flooding

FLv = L/V √dv/dl 0.02825
FLv = liquid-vapor flow factor
L = Laju alir massa cairan, kg/jam
V = Laju alir massa uap, kg/jam
dl = densitas cairan, kg/m3
dv = densitas uap, kg/m3
Untuk tray spacing 0.45 m dan FLv 0.03, didapat K = (Coulson hal.568) 0.03000
Tray spacing = (buku treyball hal.162 (ketik 176)) 0.15000
Koreksi nilai K
K' = K [σ /0.02]^0.2 0.01814
C. Menentukan kecepatan flooding dan kecepatan uap

uf = K'√ dl - dv/dv 0.37323
kecepatan uap pada umumnya 80-85% dari kecepatan floding (coulson hal.568)
uv = 80% x uf = 0.29859
D. Menentukan laju alir volumetrik maksimum

Qv = V/dv = 0.42789
Qv = laju alir volumetrik mask. (m3/s)
V = laju alir massa uap (kg/jam)
E. Menentukan luas area bersih untuk kontak uap-cair

An = Qv/uv = 1.43307
An = luas area bersih, m2
Qv = laju alir volumetrik maks.(m3/s)
uv = kecepatan uap (m/s)
F. Menentukan luas penampang lintang menara

Ac = An / 1-Ad = 1.79134
Ac = luas penampang, m2
An = luas bersih, m2
Ad = luas penampang downcomer, 20% (buku treyball hal.162 (ketik 176))
G. Menentukan diameter menara
D = √ (4 x Ac)/(3.14) (Treyball hal.162) 1.51062
H. Menentukan tinggi tutup atas dan bawah

ha = hb = 0.169 x D 0.25529
ha = tinggi tutup atas, m
hb = tinggi tutup bawah, m
D = diameter menara, m
I. Menentukan tinggi menara

htot = hshell + ha + hb
htot = tinggi menara, m
hshell = tinggi shell, m
N aktual = jumlah stage aktual
t' = tray pacing, m
htot = hshell + ha + hb = (N aktual x t') +ha +hb = 3.96059
J. Pemilihan bahan konstruksi, perhitungan shell dan standarisasi

Bahan konstruksi yang dipilih adalah carbon steel SA-285 Grade A
f 11250.0000
E 0.8500
C 0.1250
P 8.5000
D 3.4946
ts =( P x D/ (2(F x E - 0.6 x P) )+ C 1.0307
ts = 0.0262
2.6181
Diamater luar (OD)
OD = D + (2xts) 139.6459
3.5470
Diameter dalam (ID)
ID = OD - (2 x ts) 137.5844
3.4946
Heavy Komponen =
Light Komponen =
a=
B C
1714.25 -14.45
2077.97 -29.55 16.0569
3626.55 -34.29
3816.44 -46.13
xi Pi (mmHg) Ki=Pi/P yi = Ki . xi
0.1364 27574.2498 4.2685 0.5820
0.8635 3127.0661 0.4841 0.4180
0.0001 70.9678 0.0110 0.0000
0.0001 12.0442 0.0019 0.0000
1.0000 30784.3279 4.7654 1.0000
C 287.4475 K
atm 6460.0000 mmHg
yi Pi (mmHg) Ki=Pi/P Xi = yi / Ki
0.9996 15630.7212 2.4196 0.4131
0.0001 1440.4780 0.2230 0.0003
0.0001 17.3882 0.0027 0.0432
0.0002 2.3439 0.0004 0.5434
1.0000 17090.9313 2.6457 1.0000
C 264.8149 K
atm 6460.0000 mmHg
xi Pi (mmHg) Ki=Pi/P yi = Ki . xi
0.000013 47165.5182 7.3012 0.0001
0.999979 6459.5578 0.9999 0.9999
0.0000 263.4807 0.0408 0.0000
0.0000 54.6533 0.0085 0.0000
1.0000 53943.2100 8.3503 1.0000
C 312.9656 K
atm 6460.0000 mmHg
Destilat Bottom
αavg = √α top x α bottom
α Ki α
10.8511 7.3012 7.3017 8.9012
1.0000 0.9999 1.0000 1.0000
0.0121 0.0408 0.0408 0.0222
0.0016 0.0085 0.0085 0.0037
11.8648 8.3503 8.3509 9.9271
9.5812
4.2846
FEED
fraksi mol (xi) αavg αavg * xi αavg * xi / (αi - Ø)
0.1364 8.9012 1.2137 0.2629
0.8635 1.0000 0.8635 -0.2629
0.0001 0.0222 0.0000 0.0000
0.0001 0.0037 0.0000 0.0000
1.0000 9.9271 2.0772 0.0000
XiD αavg x XiD αi * XiD / (αi - Ø)

0.9996 8.8978 1.9274
0.0001 0.0001 0.0000
0.0001 0.0000 0.0000
0.0002 0.0000 0.0000
1.0000 8.8979 1.9273
= Rm + 1
= Rm +1
0.9273
1.3910
0.5818
0.4811
0.6200 didapat dari grafik penentuan stage ideal (File lampiran _1_2 menghitung…..
9.5812
15.4536 plate = 16 plate (dg reboiler)
15 plate (tanpa reboiler)
K (Contoh pdf) 288.8902 K
B C D
1.95E+02 3.07E-03 -1.38E-05
8.54E+02 1.95E-02 -2.35E-05
1.25E+03 2.24E-02 -2.35E-05
1.79E+03 1.77E-02 -1.26E-05
(kmol/jam) Xi,f µ Xi,f*µ
39.4896 0.1364 0.0788 0.0107
250.0837 0.8635 0.1896 0.1637
0.0230 0.0001 0.6124 0.0000
0.0195 0.0001 1.1399 0.0001
289.6157 1.0000 2.0206 0.1746
cP
pada fig. 8.16, Chopey,2003

,
plate = 23 plate
plate = 12 plate
n sifat-sifat fisika DESTILAT
B n Tc 0.8157
0.26957 0.3187 324.65 0.1843
0.26109 0.2869 416.25 0.5833
0.27192 0.2331 512.58 2.1484
0.274 0.28571 647.13 0.9482
K
mmHg = 861260.1200 Pa
Xi densitas (g/mL) densitas (Kg/m3) Xi.d
0.9997 0.9482 948.1782 947.9057
0.0001 0.9783 978.3445 0.0858
0.0001 0.8164 816.4353 0.0835
0.0001 1.0573 1057.3245 0.1030
1.0000 3.8003 3800.2825 948.1780
kg/m3
m3.Pa/kmol.K
K
mmHg = 101325.0000 Pa
kmol/jam Xi,D Densitas (kg/m3) Xi,D.d
39.4896 0.1364 1.6778 0.2288
250.0837 0.8635 2.3233 2.0062
0.0230 0.0001 1.4746 0.0001
0.0195 0.0001 0.8291 0.0001
289.6157 1.0000 6.3048 2.2351
KOMPONEN Pch
HCL 71.4
CH3CL 110.4
CH3OH 67.4
H2O 54.2
xi Pch Densitas cair Densitas uap σ (dyne/cm)

0.1364 71.4000 947.9057 0.2288 11.8649
0.8635 110.4000 0.0858 2.0062 0.0000
0.0001 67.4000 0.0835 0.0001 0.0000
0.0001 54.2000 0.1030 0.0001 0.0000
1.0000
dyne/cm = 0.00162 N/m
kg/jam
kg/jam
kg/jam
kg/jam
0.04000
m
m/s
m/s
m3/s
m2
m2
m 151.06154 cm
psi
in
atm = 124.9160 psia
m 137.5844 in
in = 0.0859 ft =
m
cm
in
m
in
m
CH3CL
HCL
(y*/(1-y*))/(x/(1-x))
Bubble Point FEED campuran

KOMPONEN kmol/jam xi Pi (mmHg) xi.Pi
HCL 39.4896 0.1364 27574.1353 3759.7820
CH3CL 250.0837 0.8635 3127.0485 2700.2116
CH3OH 0.0230 0.0001 70.9671 0.0056
H2O 0.0195 0.0001 12.0440 0.0008
TOTAL 289.6157 1.0000 30784.1949 6460.0000
T 14.4473 C 287.4473 K
P 8.5 atm 6460.0000 mmHg
Bubble Point DESTILAT

KOMPONEN kmol/jam yi Pi (mmHg) Ki=Pi/P
HCL 39.4865 0.9996 6462.4730 1.0004
CH3CL 0.0025 0.0001 424.1732 0.0657
CH3OH 0.0046 0.0001 1.8722 0.0003
H2O 0.0078 0.0002 0.1696 0.0000
TOTAL 39.5013 1.0000 6888.6879 1.0664
T -36.7908 C 236.2092 K
P 8.5 atm 6460.0000 mmHg
Dew Point BOTTOM

KOMPONEN kmol/jam xi Pi (mmHg) Ki=Pi/P
HCL 0.0032 0.0000 47188.0530 7.3047
CH3CL 250.0812 1.0000 6463.7085 1.0006
CH3OH 0.0010 0.0000 263.7864 0.0408
H2O 0.0010 0.0000 54.7260 0.0085
TOTAL 250.0864 1.0000 53970.2740 8.3545
T 39.9904 C 312.9904 K
P 8.5 atm 6460.0000 mmHg
0.63
xi.σ
1.6178
0.0000
0.0000
0.0000
1.6178
yi = Ki . yi
1.0000
0.0000
0.0000
0.0000
1.0000
Xi = xi / Ki
0.0000
0.9994
0.0001
0.0005
1.0000
Menentukan sifat-sifat
A. Densitas liquid
d = AB^-(1-T/Tc)^n
keterangan
d = densitas, g/ml
Tc = suhu kritil, K
Komponen A B
HCL 0.44134 0.26957
CH3CL 0.35821 0.26109
CH3OH 0.27197 0.27192
H2O 0.3471 0.274
Total
T bottom= 312.9656 K
P= 6460.0000 mmHg =
Komponen Top kg/jam Xi
HCL 1439.5973 0.9997
CH3CL 0.1263 0.0001
CH3OH 0.1473 0.0001
H2O 0.1403 0.0001
Total 1440.0111 1.0000
Jadi densitas cairan di bottom adalah = 695.26556 kg/m3
B. Densitas uap
R= 8314.3000 m3.Pa/kmol.K
T bottom = 312.9656 K
P= 6460.0000 mmHg =
Komponen Top BM kmol/jam
HCL 36.45800 39.4896
CH3CL 50.48500 250.0837
CH3OH 32.04200 0.0230
H2O 18.01500 0.0195
Total 289.6157
C. Tegangan permukaan
σ = [Pch(dl-dv)/BM]^4 x 10^-12
keterangan :
σ = tegangan permukaan, dyne/cm
Pch =Sudgen's parchor (dari tabel 8.7, buku coulson & richardson hal.335)
dl = densitas cairan (kg/m3)
BM
Tabel tegangan permukaan di BOTTOM
atom group or bond kontribusi KOMPONEN
C 4.8 HCL
H 17.1 CH3CL
OH 11.3 CH3OH
O 20 H2O
Cl 54.3
Komponen BM xi
HCL 36.45800 0.1364
CH3CL 50.48500 0.8635
CH3OH 32.04200 0.0001
H2O 18.01500 0.0001
Total 1.0000
Jadi, tegangan permukaan di BOTTOM adalah 0.4675 dyne/cm =
Menentukan diameter menara

Tinggi tray spacing, di buku coulson hal.568, fig.11.27 =
A. Laju alir massa bagian bawah
Umpan (F) 14066.2737 kg/jam
Bottom (B) 12626.2626 kg/jam
V = (1+R) x D = 30189.3717 kg/jam
L=RxD 17563.1090 kg/jam
B. Liquid-vapor flow factor dan konstanta flooding

FLv = L/V √dv/dl 0.0303
FLv = liquid-vapor flow factor
L = Laju alir massa cairan, kg/jam
V = Laju alir massa uap, kg/jam
dl = densitas cairan, kg/m3
dv = densitas uap, kg/m3
Untuk tray spacing 0.45 m dan FLv 0.03, didapat K = (Coulson ha 0.0800
Tray spacing = 0.4500 m
Koreksi nilai K
K' = K [σ /0.02]^0.2 0.0377
C. Menentukan kecepatan flooding dan kecepatan uap

uf = K'√ dl - dv/dv 0.7227 m/s
kecepatan uap pada umumnya 80-85% dari kecepatan floding (coulson hal.568)
uv = 80% x uf = 0.5781 m/s
D. Menentukan laju alir volumetrik maksimum

Qv = V/dv = 4.4340 m3/s
Qv = laju alir volumetrik mask. (m3/s)
V = laju alir massa uap (kg/jam)
E. Menentukan luas area bersih untuk kontak uap-cair

An = Qv/uv = 7.6695 m2
An = luas area bersih, m2
Qv = laju alir volumetrik maks.(m3/s)
uv = kecepatan uap (m/s)
F. Menentukan luas penampang lintang menara

Ac = An / 1-Ad = 9.5868 m2
Ac = luas penampang, m2
An = luas bersih, m2
Ad = luas penampang downcomer, 20%
G. Menentukan diameter menara
D = √ (4 x Ac)/(3.14) 3.4946 m
H. Menentukan tinggi tutup atas dan bawah

ha = hb = 0.169 x D 0.5906 m
D = diameter menara, m
I. Menentukan tinggi menara

htot = hshell + ha + hb
htot = tinggi menara, m
hshell = tinggi shell, m
N aktual = jumlah stage aktual
t' = tray pacing, m
htot = hshell + ha + hb = (N aktual x t') +ha +hb = 11.5312 m

Menentukan sifat-sifat fisika BOTTOM
n Tc 0.9640
0.3187 324.65 0.0360
0.2869 416.25 0.3466
0.2331 512.58 1.5752
0.28571 647.13 0.6952
861260.1200 Pa 861.26012
densitas (g/mL) densitas (Kg/m3) Xi.d
0.6952 695.2102 695.0104
0.8813 881.2952 0.0773
0.7735 773.5173 0.0791
1.0138 1013.8095 0.0988
3.3638 3363.8322 695.2656
101325.0000 Pa
Xi,D Densitas (kg/m3) Xi,D.d
0.1364 1.4197 0.1936
0.8635 1.9659 1.6975
0.0001 1.2477 0.0001
0.0001 0.7015 0.0000
1.0000 5.3348 1.8913
Pch
71.4
110.4
67.4
54.2
Pch Densitas cair Densitas uap σ (dyne/cm) xi.σ

71.4000 695.0104 0.1936 3.4285 0.4675
110.4000 0.0773 1.6975 0.0000 0.0000
67.4000 0.0791 0.0001 0.0000 0.0000
54.2000 0.0988 0.0000 0.0000 0.0000
0.4675
0.0005 N/m
KOMPRESOR 1 (CM-01) aliran 11-12 centrifugal
DASAR PERANCANGAN
T in 69.15 C 342.15 K 101.32500
T out 248 C 521 K 496.49250
P in 1.0000 atm 101325 Pa 1.01325
P out 4.9 atm 496492.5 Pa 4.964925
laju alir 19160.8536 kg/jam 5.3225 kg/dtk
umpan masuk 562.1449 kmol/jam 0.1562 kmol/dtk
densitas 1.2141 kg/m3
bahan carbon steel type SA-183 grade C 72.0101490000159 57.31414900002
densitas gas (ρg)

R= 8314.3000 m3.Pa/kmol.K
T= 342.1500 K
P= 101325.0000 Pa
KOMPONEN BM kmol/jam Xi Densitas (kg/m3) Xi,D.d
HCL 36.4580 289.5908 0.5152 1.2986 0.6690
CH3CL 50.4850 0.0025 0.0000 1.7982 0.0000
CH3OH 32.0420 263.2644 0.4683 1.1413 0.5345
H2O 18.0150 9.2872 0.0165 0.6417 0.0106
TOTAL 562.1449 1.0000 4.8797 1.2141
menghitung rate volumetrik (Q)

(Q) = kapasitas/densitas 4.3840 m3/dtk 154.8198 ft3/dtk
15782.4297 m3/jam
menghitung T dan P rata2
T rata2 = (T in + T out)/2 431.575 K
P rata2 = (P in + P out)/2 2.95 atm
dari fig.3.6 coulson hal.83 didapat Efisiensi 0.72
cp campuran 7093.640784631 J/mol K 7093640.7846 J/kmol K
γ = Cp/ (Cp-R) 1.0012

Cv = Cp - R 7085326.4846 J/kmol K
k = Cp/Cv 1.0012
menghitung nilai m dan n

m= (γ - 1) / (γ x E) 0.0016
n=1/(1-m) 1.0016
menghitung BM campuran
komponen kmol/jam xi BM BM campuran
HCl 289.5908 0.5152 36.4580 18.7815
CH3Cl 0.0025 0.0000 50.4850 0.0002
CH3OH 263.2644 0.4683 32.0420 15.0059
H20 9.2872 0.0165 18.0150 0.2976
TOTAL 562.1449 1.0000 34.0853
berdasarkan Yaws (1999), diperoleh nilai Tc dan Pc untuk gas...

menghitung Z campuran
komponen kmol/jam xi Pc (atm) Tc (K) w (OMEGA)
HCl 289.5908 0.5152 82.0035 324.6500 0.1320
CH3Cl 0.0025 0.0000 65.9166 416.2500 0.1530
CH3OH 263.2644 0.4683 79.9013 512.5800 0.5660
H20 9.2872 0.0165 217.6659 647.1300 0.3450
TOTAL 562.1449 1.0000
Tr = T rata2/(xi*Tc) 1.0325
Pr = P rata2/(xi*Pc) 0.0354
B° = 0,083 - (0,422/(Tr^1,6)) -0.3179
B' = 0,139 - (0,172/(Tr^4,2)) -0.0114
BPc/RTc = B°+(W*B') -0.3218
menghitung faktor kompresibilitas

Z = 1+((BPc/RTc)*(Pr/Tr)) 0.9890
menghitung power kompresor
 w
z x R xT1 n
M
x
n 1

x  P2 / P1  1 
n1/ n
131341.8576 kJ/kmol
kerja nyata kompresor

W = (-w)/eff 182419.2466 kJ/kmol
power kompresor 28485.0113

Power = W*umpan masuk/3600 28485.0113 W
38.19902942576 Hp
head kompresor
Head = (53.3)*Z*(T in/densitas)*(k*eff/(k-1))*(Pout/Pin)^((k-1)/(k*eff)) - 1 9149128.509048
2788654.369558
PERHITUNGAN KAK JONI

CM-01 CM-02
mv = m/densitas 15782.4297 m3/jam mv = m/densitas
4.3840 m3/s
de = 0,363 mv^0,45 densitas^0,13 0.7239 m de = 0,363 mv^0,45 densitas^0
28.5014 in
daya kompresor daya kompresor

P = 2,87*10^-4*mv*p1*ln(p2/p1) 729.3912 kW P = 2,87*10^-4*mv*p1*ln(p2/
jika eff motor pompa adalah 0.8000 jika eff motor pompa adalah
P = daya/eff 911.7391 kW P = daya/eff
911739.0616 W
1222.6622 Hp
maka dipilih kompresor dengan daya 1223 Hp maka dipilih kompresor denga
KOMPRESOR 2 (CM-02)
DASAR PERANCANGAN
kPa T in 25.26
kPa T out 220.3
bar P in 1.0000
bar 72.010149 psi P out 8.5
laju alir 14066.2737
umpan masuk 289.6157
densitas 1.9845
bahan carbon steel type SA-183 grade C
densitas gas (ρg)

R= 8314.3000
T= 298.2600
P= 101325.0000
KOMPONEN BM
HCL 36.4580
CH3CL 50.4850
CH3OH 32.0420
H2O 18.0150
TOTAL

(Q) = kapasitas/densitas

T rata2 = (T in + T out)/2
P rata2 = (P in + P out)/2
dari fig.3.6 coulson hal.83 didapat Efisiensi
cp campuran
γ = Cp/ (Cp-R)
Cv = Cp - R
k = Cp/Cv
menghitung nilai m dan n

m= (γ - 1) / (γ x E)
n=1/(1-m)
menghitung BM campura
Pc (bar) Pc (atm) Zc komponen kmol/jam
83.09 82.003454231 0.249 HCl 39.4896
66.79 65.916604984 0.268 CH3Cl 250.0837
80.96 79.901307673 0.224 CH3OH 0.0230
220.55 217.66592647 0.229 H20 0.0195
TOTAL 289.6157
berdasarkan Yaws (1999), diperoleh nilai Tc dan Pc untuk

m
xi*Pc xi*Tc xi*w komponen kmol/jam
42.2444 167.2445 0.0680 HCl 39.4896172974
0.0003 0.0019 0.0000 CH3Cl 250.083670948
37.4195 240.0521 0.2651 CH3OH 0.02298298025
3.5960 10.6912 0.0057 H20 0.01946893248
83.2602 417.9897 0.3388 TOTAL 289.615740158
Tr = T rata2/(xi*Tc)
Pr = P rata2/(xi*Pc)
B° = 0,083 - (0,422/(Tr^1,6))
B' = 0,139 - (0,172/(Tr^4,2))
BPc/RTc = B°+(W*B')
menghitung faktor kompresibilitas

Z = 1+((BPc/RTc)*(Pr/Tr))
menghitung power kompresor
 w
z x R xT1 n
M
x
n 1

x  P2 / P1  1 
n1/ n
kerja nyata kompresor

W = (-w)/eff
power kompresor
Power = W*umpan masuk/3600
head kompresor
ft Head = (53.3)*Z*(T in/densitas)*(k*eff/(k-1))*(Pout/Pin)^
m
7088.0415 m3/jam
1.9689 m3/s
363 mv^0,45 densitas^0,13 0.5383 m
21.1918 in
7*10^-4*mv*p1*ln(p2/p1) 441.1151 kW
motor pompa adalah 0.8000

551.3939 kW
551393.9237 W
739.4314 Hp
dipilih kompresor dengan daya 739 Hp

aliran 22-23 centrifugal
C 298.26 K 101.33 kPa

C 493.3 K 861.26 kPa
atm 101325 Pa 1.01325 bar
atm 861262.5 Pa 8.612625 bar
kg/jam 3.9073 kg/dtk
kmol/jam
kg/m3
on steel type SA-183 grade C
m3.Pa/kmol.K
K
Pa
kmol/jam Xi Densitas (kg/m3) Xi,D.d
39.4896172973878 0.1364 1.4897 0.2031
250.083670947663 0.8635 2.0628 1.7812
0.02298298025006 0.0001 1.3092 0.0001
0.01946893248437 0.0001 0.7361 0.0000
289.6157 1.0000 5.5978 1.9845
rate volumetrik (Q)

1.9689 m3/dtk 69.5311 ft3/dtk
7088.0415 m3/jam
395.78 K
4.75 atm
3 didapat Efisiensi 0.69
40.6324616064886 J/mol K 40632.46160649 J/kmol K
1.25726401461928
32318.1616 J/mol K
1.25726401461928
ung nilai m dan n

0.29655378159524
1.42157278529089
xi BM BM campuran Pc (bar) Pc (atm) Zc
0.13635176484494 36.4580 4.971112642717 83.09 82.00345 0.249
0.86350165502543 50.4850 43.59388105396 66.79 65.9166 0.268
7.93568064966E-05 32.0420 0.002542750794 80.96 79.90131 0.224
6.72233231307E-05 18.0150 0.001211028166 220.55 217.6659 0.229
1.0000 48.5687
), diperoleh nilai Tc dan Pc untuk gas...

xi Pc (atm) Tc (K) w (OMEGA) xi*Pc xi*Tc xi*w
0.13635176484494 82.0034542314 324.65 0.132 11.18132 44.2666 0.017998
0.86350165502543 65.916604984 416.25 0.153 56.9191 359.4326 0.132116
7.93568064966E-05 79.9013076733 512.58 0.566 0.006341 0.040677 4.492E-05
6.72233231307E-05 217.665926474 647.13 0.345 0.014632 0.043502 2.319E-05
1 68.12139 403.7833 0.150182
0.98017911477783
0.06972846955745
-0.35273629839406
-0.04808784818353
-0.35995824175632
0.97439311149988
P2 / P1 
n1/ n

1 148696.478551647 kJ/kmol
215502.142828474 kJ/kmol
17336.8924 W
23.2491556587513 Hp
nsitas)*(k*eff/(k-1))*(Pout/Pin)^((k-1)/(k*eff)) - 1 49649.41084 ft
15133.14042 m
EXPANDER (E-01) ALIRAN 14-15 RECIPROCATING
DASAR PERANCANGAN
T in 350 C 623 K
T out 230 C 503 K
P in 4.9 atm 496492.5 Pa
P out 1 atm 101325 Pa
laju alir 19160.8536 kg/jam 5.3225 kg/dtk
umpan masuk 562.1449 kmol/jam
densitas 3.2671 kg/m3
bahan carbon steel type SA-183 grade C
densitas gas (ρg)

R= 8314.3000 m3.Pa/kmol.K
T= 623.0000 K
P= 496492.5000 Pa
KOMPONEN BM kmol/jam Xi Densitas (kg/m3)
HCL 36.4580 39.4896568 0.0702 3.4946
(CH3)2O 46.0690 0.19744828 0.0004 4.4158
CH3CL 50.4850 250.10366 0.4449 4.8391
CH3OH 32.0420 12.7683224 0.0227 3.0713
H2O 18.0150 259.585766 0.4618 1.7268
TOTAL 562.1449 1.0000 17.5474

(Q) = kapasitas/densitas 1.6291 m3/dtk 5864.7470
5864.74704 m3/jam
T rata2 = (T in + T out)/2 563 K
P rata2 = (P in + P out)/2 2.95 atm
komponen kmol/jam xi BM BM campuran
HCl 39.4897 0.0702 36.4580 2.5611
(CH3)2O 0.1974 0.0004 46.0690 0.0162
CH3Cl 250.1037 0.4449 50.4850 22.4613
CH3OH 12.7683 0.0227 32.0420 0.7278
H20 259.5858 0.4618 18.0150 8.3189
TOTAL 562.1449 1.0000 34.0853
berdasarkan Yaws (1999), diperoleh nilai Tc dan Pc untuk gas...

komponen kmol/jam xi Pc (atm) Tc (K)
HCl 39.4897 0.0702 82.0035 324.6500
(CH3)2O 0.1974 0.0004 52.9978 400.1000
CH3Cl 250.1037 0.4449 65.9166 416.2500
CH3OH 12.7683 0.0227 79.9013 512.5800
H20 259.5858 0.4618 217.6659 647.1300
TOTAL 562.1449 1.0000
Tr = T rata2/(xi*Tc) 1.0856
Pr = P rata2/(xi*Pc) 0.0215
B° = 0,083 - (0,422/(Tr^1,6)) -0.2870
B' = 0,139 - (0,172/(Tr^4,2)) 0.0172
BPc/RTc = B°+(W*B') -0.2828
menghitung kerja yg dibangkitkan oleh ekspander Ulrich,1984 hal.93

Ws = eff*(m*∆P/densitas) 65.3593 Hp 48738.3844
Ws = kerja yg dibangkitkan oleh ekspander (Hp)
eff = efisiensi ekspander 0.7 Ulrich,1984
m = laju alir (kg/jam)
∆P = peubahan tekanan (psia) P in - P out 57.3142 psia
densitas (kg/m3)
496.49 kPa
101.33 kPa
4.96 bar 72.0101 psia
1.01 bar 14.6959 psia
PERHITUNGAN KAK JONI
mv = m/densitas 5864.7470 m3/jam

1.6291 m3/s
jika eff motor pompa adalah 0.6000
Xi,D.d daya kompresor
0.2455 P = Eff*m*(p2-p1)/densitas -386.2596
0.0016 -386259.5710
2.1529 -517.9826
0.0698
0.7974 maka dipilih kompresor dengan daya -518
3.2671
m3/jam
Pc (bar) Pc (atm) Zc
83.09 82.003454231 0.249
53.7 52.997779423 0.274
66.79 65.916604984 0.268
80.96 79.901307673 0.224
220.55 217.66592647 0.229
mpuran
w (OMEGA) xi*Pc xi*Tc xi*w
0.1320 5.7606 22.8061 0.0093
0.2040 0.0186 0.1405 0.0001
0.1530 29.3269 185.1936 0.0681
0.5660 1.8148 11.6425 0.0129
0.3450 100.5132 298.8300 0.1593
137.4342 518.6127 0.2496
W 48.7384 kW
AN KAK JONI
kW
W
Hp
Hp
Hp
EXPANSION VALVE (EV-01) aliran 26-27
"Valve Sizing Calculation (Standardized Method)" oleh Emerson
Bahan Konstruksi : Carbon Steel

tipe ; expantion valve
kondisi proses
w 1440.0111 kg/jam
P in 8.5 atm 861262.5 Pa
P out 1 atm 101325 Pa
T in -8.18 C 264.82 K
densitas 948.1583 kg/m3 59.1915 lb/ft3
densitas liquid (ρl)

d = AB^-(1-T/Tc)^n
keterangan
d = densitas, g/ml
Tc = suhu kritil, K
T= 264.8200 K
KOMPONEN A B n Tc
HCL 0.44134 0.26957 0.3187 324.65
CH3CL 0.35821 0.26109 0.2869 416.25
CH3OH 0.27197 0.27192 0.2331 512.58
H2O 0.3471 0.274 0.28571 647.13
TOTAL
menentukan laju alir volumetrik (Q), pressure drop (∆P), dan specific gravity
Q = w/densitas 1.5187 m3/jam 6.6870 Gallon Per Minutes (GPM)

∆P = P in - P out 110.2196 psia 7.5 atm
0.9471
menentukan konstanta persamaan (N)

konstanta persamaan untuk perhitungan valve dapat ditentukan berdasarkan tabel berikut :
Tabel 1. Pemilihan Konstanta Perhitungan Valve
dipiilih nilai N yang sesuai dengan satuan yang digunakan. Untuk perhitungan valve
ini, satuan yang digunakan adalah GPM untuk laju alir volumetrik (Q) dan psia untuk
tekanan (P). Sehingga nilai N dipilih adalah 1
menghitung nilai koefisien ukuran valve (N)

0.6199
memilih spesifikasi valve yg sesuai
setelah memperoleh nilai Cv, spesifikasi (ukuran) valve dapat ditentukan dengan
melihat pada tabel yang disajikan.
Tabel 2. Pemilihan spesifikasi valve berdasarkan nilai Cv
Dari tabel 2 diatas, dipilih valve dengan nilai Cv yang paling mendekati perhitungan
yaitu valve dengan ukuran 1/2 in, 'Post guided' plug style, karakteristik aliran 'equal percentage'
ukuran diameter port sebesar 0,38 in (9,7 mm) dengan nilai Cv yaitu 2,41.
0.5 0.0127
9.7 0.0097
8,5 atm 30
1 atm -24.15
124.9156 psia
14.6959 psi
17.276 F
A,B dan n = koefisien
kg/jam Xi densitas (g/mL) densitas (Kg/m3) Xi.d

1439.597290431 0.9997 0.9482 948.1585 947.8860
0.126254741278 0.0001 0.9783 978.3350 0.0858
0.147284130634 0.0001 0.8164 816.4310 0.0835
0.140293127482 0.0001 1.0573 1057.3200 0.1030
1440.0111 1.0000 3.8002 3800.2444 948.1583
rop (∆P), dan specific gravity
er Minutes (GPM)
EXPANSION VALVE (EV-02) aliran 25-29
"Valve Sizing Calculation (Standardized Method)" oleh Emerson
Bahan Konstruksi : Carbon Steel

tipe ; expantion valve
kondisi proses
w 12626.26 kg/jam
P in 8.5 atm 861262.5 Pa 124.916 psia
P out 7 atm 709275 Pa 102.872 psi
T in 39.97 C 312.97 K 103.946 F
densitas 881.2809 kg/m3 55.0164 lb/ft3

d = AB^-(1-T/Tc)^n
keterangan
d = densitas, g/ml
Tc = suhu kritil, K
T = 312.9700
KOMPONEN A B n Tc kg/jam Xi
HCL 0.44134 0.26957 0.3187 324.65 0.115176997 0.0000
CH3CL 0.35821 0.26109 0.2869 416.25 12625.34787 0.9999
CH3OH 0.27197 0.27192 0.2331 512.58 0.589136523 0.0000
H2O 0.3471 0.274 0.28571 647.13 0.210439691 0.0000
TOTAL 12626.2626 1.0000
menentukan laju alir volumetrik (Q), pressure drop (∆P), dan specific gravity
Q = w/densitas 14.3272 m3/jam 63.0825 Gallon Per Minutes (GPM)

∆P = P in - P out 22.044 psia 1.5 atm
0.8803
60 15.55555556
menentukan konstanta persamaan (N)

konstanta persamaan untuk perhitungan valve dapat ditentukan berdasarkan tabel berikut :
Tabel 1. Pemilihan Konstanta Perhitungan Valve
dipiilih nilai N yang sesuai dengan satuan yang digunakan. Untuk perhitungan valve
ini, satuan yang digunakan adalah GPM untuk laju alir volumetrik (Q) dan psia untuk
tekanan (P). Sehingga nilai N dipilih adalah 1
menghitung nilai koefisien ukuran valve (N)

12.60582
memilih spesifikasi valve yg sesuai
setelah memperoleh nilai Cv, spesifikasi (ukuran) valve dapat ditentukan dengan
melihat pada tabel yang disajikan.
Tabel 2. Pemilihan spesifikasi valve berdasarkan nilai Cv
Dari tabel 2 diatas, dipilih valve dengan nilai Cv yang paling mendekati perhitungan
yaitu valve dengan ukuran 1-1/2 in, 'Micro-From TM' plug style, karakteristik aliran 'equal percentage'
ukuran diameter port sebesar 3/4 in (19,1 mm) dengan nilai Cv yaitu 10,2.
19.1 0.0191
8,5 atm 30
7 atm 30.02
densitas (g/mL) densitas (Kg/m3) Xi.d

0.6952 695.1720 0.0063
0.8813 881.2854 881.2216
0.7735 773.5131 0.0361
1.0138 1013.8054 0.0169
3.3638 3363.7759 881.2809
gravity
percentage'
AKUMULATOR
TYPE
BAHAN KONSTRUKSI stainless steel SA-167 grade 11 typ
SISTEM OPERASI kontinyu
WAKTU PENGISIAN DAN PENGURASAN 5 DTK (MAX UTK GAS)
DASAR PERANCANGAN
T in atas 65 C 338 K
T in 90 C 363 K
T in bwh 90 C 363 K
T out 69.14 C 342.14 K 156.452
P 1 atm
m 19160.85362 kg/jam
R 0.08206 atm.L/gmol.K
waktu tinggal 5s
menghitung densitas umpan utk gas

komponen BM kmol/jam xi densitas densitas*xi
HCl 36.4580 289.5908 0.5152 1.2985 0.6690
CH3Cl 50.4850 0.0025 0.0000 1.7982 0.0000
CH3OH 32.0420 263.2644 0.4683 1.1413 0.5345
H2O 18.0150 9.2872 0.0165 0.6417 0.0106
TOTAL 562.1449 1.0000 4.8796 1.2140
menghitung volume gas

laju volumetrik (Q) = kapasitas/densitas gas 15782.78365
volume gas = Q * waktu tinggal 21.92053 m3
faktor keamanan desain 20%

V = 1,2 * volume gas 928.939574 ft3 26.3046
menghitung diameter dan tangki silinder

volume 2 tutup siliinder (0,000049D^3)*2
dipilih rasio D/H=1 jadi D=1H
volume akumulator = volume silinder + volume 2 tutup silinder

volume akumulator = 1/4*π*D^2*H + (0,000049D^3)*2
26.3046 1/4*3,14*1 H^2*H + (0,000098 H^3
26.3046394214024 0.7850 H^3 + 9.8E-05 H^3
26.3046394214024 0.7851 H^3
H^3 = 33.5049 m3 8851.0614 gal
H= 3.2238 m 10.5768 ft
D=1H 3.2238 m 10.5768 ft

standarisasi dr brownell and young appendix E hal. 346 didapat ukuran tangki yg mendekati
Ds 15 ft 4.5720 m
Hs 12 ft 3.6576 m
menghitung tebal dinding sislinder

direncanakan akan menggunakan
allowable stress (S) 13750 psia
joint Eff. (E) 0.8
Faktor korosi (C) 0.125 in
tekanan gas (P op) 1 atm 14.696 psia
faktor kelonggaran 20% 0.2
P design 17.6352 psia
Diameter (D) 15 ft 180 in
ts=((Pdesign*D)/((2S*E)-(1,2*P op)))+C 0.269404 in

distandarisasi menjadi 0.625 in
0.015875 m
15.8750 cm
menghitung tebal tutup

ID 15 ft 180 in
4.572 m
OD=ID+(2*tebal dinding) 4.60375 m
181.25 in
15.1041667 ft
dipilih OD standar 126 in 3.2004 m

jenis tutup torispherical flanged head
ts 5/8
icr 7.625 in 7 5/8
rc 120 in
P design 17.6352 psia
r1=0,06*ID 10.8 in
W=1/4*(3+((rc/r1)^(1/2))) 1.58333333
th=((P design*rc*W)/(2*S*E)-(1,2*Pdesign))+C 0.277450645

distandarisasi menjadi 1.125 in 1 1/8
0.028575 m
28.575 cm
menghitung tinggi tutup ts 5/8 in

a = ID/2 90 in sf 2 1/2 in
AB = a - icr 82.375 in
BC = rc - icr 112.375 in
AC=(BC^2 - AB^2)^0,5 76.43624795 in
tinggi head (b) = rc - AC 43.56375205 in
tinggi head OA = b + sf + th 47.1888 in 1.1985943 m
tinggi total = Hs + 2 * tinggi head OA 6.054788604 m
inless steel SA-167 grade 11 type 316
DTK (MAX UTK GAS)
densitas = P * BM * / (R*T)
m3/jam
774.1163 ft3
m3
brownell 1959 hal.88

timmerhaus hal. 542
4.572 m
5/8 in
tabel 5.7 brownell 1959
in
in
tabel brownell, 1959

ABSORBER (AB-01) PACKED COLUMN
Data Operasi
T op 25.26 C 298.26
P op 1 atm 101325
R 8314.3000 m3.Pa/kmol.K
viskositas gas (µg) 0.0115 cP 0.0000114507
viskositas cair (µL) 0.9090 cP 0.0009090034
densitas gas (ρg) 1.9829 kg/m3
densitas cair (ρL) 1027.3525 kg/m3
BM campuran gas 48.5282
sifat fisik
gas 1 c = 10000 µ
viskositas A+BT+(C*(T^2)) (micropoise)
KOMPONEN A B C
HCL -9.118 5.55E-01 -1.11E-04
(CH3)2O -4.276 3.03E-01 6.35E-05
CH3CL -1.374 3.86E-01 -4.87E-05
CH3OH -14.236 3.89E-01 -6.28E-05
H2O -36.826 4.29E-01 -1.62E-05
TOTAL
T 298.26 K
densitas gas (ρg)

R= 8314.3000 m3.Pa/kmol.K
T= 298.2600 K
P = 101325.0000 Pa
KOMPONEN BM kmol/jam Xi
HCL 36.4580 39.4896172973878 0.1361
(CH3)2O 46.0690 0.19742853910683 0.0007
CH3CL 50.4850 250.103410359325 0.8618
CH3OH 32.0420 0.02298298025006 0.0001
H2O 18.0150 0.38937864968736 0.0013
TOTAL 290.2028 1.0000
komponen kg/jam xi BM
HCl 39.4896 0.13607592646154 36.4580
(CH3)2O 0.1974 0.00068031227466 46.0690
CH3Cl 250.1034 0.86182281837626 50.4850
CH3OH 0.0230 7.91962683969E-05 32.0420
H20 0.3894 0.00134174661916 18.0150
TOTAL 290.2028 1.0000
menghitung diameter tower

nilai basis (L/G)*((ρg/(ρL-ρg))^0,5) 0.0006
dari gambar 6.34 Treybal, 1981 hal.195
berdasarkan nilai absis dgn pressure drop gas 50
diperoleh ordinat 0.013
jenis packing yg digunakan berupa ceramic rasching ring 50 mm dgn spesifikasi sbg brkt
t wall (tebal dinding 6 mm
Cf 65
ε (effisiensi pengelasan) 0.74
CD 135.6
ap 92 m2/m3
G'=((ordinat*ρg*(ρL-ρg)*gc)/(Cf*(µL^0,1)*1))^0,5 0.9050
G=G'/BM campuran 0.0186
Fg 14083.0296 kg/jam 3.9120
luas penampang tower
A=Fg/G' 4.3224 m2
diameter tower
Dt=(4*A/π)^0,5 2.3465 m
7.6986 ft
92.3830 in
Perhitungan liquid/gas hold up

dari tabel 6.5 Treybal,1981 hal.206, untuk ceramic raschig ring 50 mm diperoleh
ds 0.0725 m
dari tabel yaws, 1999 untuk solvent H2O diperoleh
A 132.674
Tc 647.13 K
n 0.955
maka surface tension (σ) solvent H2O

σ=A*((1-(T-Tc))^n) 73.5415 dyne/cm 0.0735
dari tabel 8.5 coulson & richardson, 2005 hal 332 diperoleh
diffusion volume gas (Via) untuk key komponen (CH3)2O 50.36
diffusion volume cair (Vib) untuk pelarut H2O 9.44
dari coulson hal. 333

association factor (Φ) untuk H2O 2.6
dari tebel 8.6 coulson hal. 334 diperoleh

molar volume (Vm) (CH3)2O 0.0691 m3/kmol
difusi gas (Eq. 8.21 Coulson)

Dg=(1,013E-7*(T^1,75)*(((1/BMa)+(1/BMb))^0,5))/(P*(((Via^(1/3))+Vib^(1/3))^2))
difusi liquid
Dl=(1,173E-13*(Φ*BM)^0,5*T)/(µ*(Vm^0,6))
β=1,508*(ds^0,376)
L'=L/A
menghitung gas hold up (Treybal,1981)

Scg=µg/ρg*Dg 0.3274
menghitung liquid hold up

Scl=µL/ρL*Dl 0.6759
dari tabel 6.5 Treybal, 1981 hal 206

ΦLsW=0,000247/(ds^1,21) 0.0059
ΦLtW=(2,09E-6*((737,5*L')^β))/(ds^2) 0.0014
ΦLoW=ΦLtW-ΦLsW -0.0045
dari tabel 6.5 Treybal, 1981 hal 206, diperoleh persamaan

H=((975,7*(L'^0,57)*(µL^0,13))/(ρL^0,84*((2,024*(L'^0,43))-1)))*(σ/0,073)^(0,1737-0,262*(LogL'))
ΦLo=ΦLoW*H 0.0006
ΦLs=(0,0486*(µL^0,02)*(σ^0,99))/((ds^1,21)*(ρL^0,37)) 0.0059
ΦLt=ΦLo+ΦLs 0.0065
menghitung luas kontak antar muka (interface area)

dari tabel 6.4 Treybal, 1981 hal.205 untuk ceramic raschig ring 50 mm
m 34.03
n 0
p 0.362
ε 0.74
aAw=m*(((808*G')/(ρg^0,5))^n)*(L'^P) 7.0762 m2/m3
dari pers. 6.73 Treybal,1981

aA=aAw*ΦLo/ΦLoW -1.0086 m2/m3

εLo=ε-ΦLt 0.7335

Fg=((1,195*G)/(Scg^2/3))*(((ds*G')/(µg*(1-εLo)))^-0,36) 0.0013

kL=25,1*(((ds*L')/µL)^0,45)*(Scl^0,5)*(Dl/ds) 0.0004
C=ρL/BM liquid 57.0276

Fl=kL*C 0.0216
Fg*aA -0.0013
Fl*aA -0.0218
menghitung height of gas phase transfer unit (Htg)

Htg=G/(Fg*aA) -14.2988 m
Eq. 8.24 Treybal,1981
menghitung height of liquid phase transfer unit (Htl)

L=L'/BM liquid 0.0007 kmol/m2.s
Htl=L/Fl*aA -0.0332 m
faktor absorbsi (A) berkisar antara 1,25-2 (Treybal, 1981 hal.292) maka dipilih A
fraksi mol (CH3)2O masuk (y1) 0.0007

fraksi mol (CH3)2O keluar (y2) 0.0166
x2 0
rasio distribusi kesetimbangan

m=L/(G*A) 0.0311
Treybal,1981
NtoG=(ln((y1-(m*x2))/(y2-(m*x2)))*(1-(1/A))+(1/A))/(1-(1/A)) -1.0649
menghitung height of transfer unit (HtoG

HtoG=Htg+(m*G/L)*Htl=Htg+(Htl/A) -14.3254 m
menghitung tinggi absorber

tinggi packing (z) = HtoG*NtoG 15.2546 m
tinggi head packing (h) = 1/4*Dt 0.5866 m
tinggi absorber (Hab) = z+2h 16.4279 m
menghitung tebal dinding

bahan konstruksi carbon steel SA-285 grade C
Allowable stress (S) 13750 psi
(Brownell,1959)
tipe pengelasan double welded butt joint
efisiensi pengelasan (Ef) 0.8 %
Corrosion allowance (Cc) 0.125 in (Peters&Timmerhaus,1991)
Faktor keamanan tekanan 20 %
P design (Pd) = (1+0,2)*Pop 17.6351 psia
2.9391 psig
t=((Pd*r)/((S*Ef)-(0,6*Pd)))+Cc 0.1373 in
0.0035 m
0.3489 cm
K G 14083.0296 kg/jam 250.6902
Pa 1.0133 bar L 203.1799 kg/jam
14.6959 psi
kg/m*s
kg/m*s
cair
viskositas
µ cP kmol/jam xi cP*xi KOMPONEN
146.5418 0.0147 39.48962 0.136075926 0.00199408 H2O
91.6348 0.0092 0.197429 0.000680312 6.23403E-06 TOTAL
109.5070 0.0110 250.1034 0.861822818 0.00943757 T
96.3083 0.0096 0.022983 7.91963E-05 7.62726E-07
89.6864 0.0090 0.389379 0.001341747 1.20336E-05
533.6784 0.0534 290.2028 1.0000 0.0115

d = AB^-(1-T/Tc)^n
keterangan
d = densitas, g/ml
Densitas (kg/m3) Xi,D.d T = suhu komponen, K
1.4897 0.2027 Tc = suhu kritil, K
1.8824 0.0013 T=
2.0628 1.7778 KOMPONEN
1.3092 0.0001 H2O
0.7361 0.0010 TOTAL
7.4802 1.9829
BM campuran
4.9610561269346
0.0313413061812
43.509124985725
0.002537606832
0.0241715653441
48.5282
N/m2.m
0.0055
(tabel 6.3 Treybal, 1981 hal 196)
kg/m2.s
kmol/m2.s
kg/s
N/m
C 16.5
H 1.98
O 5.48
C 0.0148
H 0.0037
O 0.0074
1.7639614715E-05 m2/s in methyl ethe 0.0099
1.3090146603E-06 m2/s
0.5622
47.0066 kg/m2.jam
0.0131 kg/m2.s
-0,262*(LogL')) -0.1425
kmol/m2.s
kmol/m2.s(kmol/m3)
kmol/m3
kmol/m2.s
kmol/m3.s
kmol/m3.s
1.25
mmerhaus,1991)
cP
A B C D kmol/jam xi µ (cP)
-10.2158 1.79E+03 1.77E-02 -1.26E-05 203.1799 1.0000 0.9090
203.1799
298.26 K
efisien regresi
298.2600 K
A B n Tc kg/jam Xi densitas (g/mL)
0.3471 0.274 0.28571 647.13 203.1799 1.0000 1.0274
203.1799
xi*µ (cP)
0.9090
densitas (Kg/m3) Xi.d

1027.3525 1027.3525
ST-01 PACKED COLUMN
Data Operasi
T op 51.65 C 324.65
P op 1 atm 101325
R 8314.3000 m3.Pa/kmol.K
viskositas gas (µg) 0.5374 cP 0.000537400163211
viskositas cair (µL) 0.0112 cP 1.12216064781144E-05
densitas gas (ρg) 0.6763 kg/m3
densitas cair (ρL) 817.5682 kg/m3
BM campuran gas 18.0150 24.1012
sifat fisik
cair 1 c = 10000 µ
viskositas A+BT+(C*(T^2)) (micropoise)
KOMPONEN A B C
HCL -9.118 5.55E-01 -1.11E-04
H2O -36.826 4.29E-01 -1.62E-05
TOTAL
T 324.65 K

d = AB^-(1-T/Tc)^n
keterangan
d = densitas, g/ml
Tc = suhu kritil, K 324.6500
T= 324.6500 K 51.6500
KOMPONEN A B n
HCL 0.44134 0.26957 0.3187
H2O 0.3471 0.274 0.28571
TOTAL
menghitung diameter tower

nilai basis (L/G)*((ρg/(ρL-ρg))^0,5) 0.0431
dari gambar 6.34 Treybal, 1981 hal.195
berdasarkan nilai absis dgn pressure drop gas 400
diperoleh ordinat 0.08
jenis packing yg digunakan berupa ceramic rasching ring 50 mm dgn spesifikasi sbg brkt
t wall (tebal dinding 6 mm
Cf 65
ε (effisiensi pengelasan) 0.74
CD 135.6
ap 92 m2/m3
G'=((ordinat*ρg*(ρL-ρg)*gc)/(Cf*(µL^0,1)*1))^0,5 1.0321
G=G'/BM campuran 0.0573
Fg 37403.6151 kg/jam 10.3899
luas penampang tower
A=Fg/G' 10.0667 m2
diameter tower
Dt=(4*A/π)^0,5 3.5810 m
11.7488 ft
140.9859 in
Perhitungan liquid/gas hold up

dari tabel 6.5 Treybal,1981 hal.206, untuk ceramic raschig ring 50 mm diperoleh
ds 0.0725 m
dari tabel yaws, 1999 untuk solvent H2O diperoleh
A 132.674
Tc 647.13 K
n 0.955
maka surface tension (σ) solvent H2O

σ=A*((1-(T-Tc))^n) 68.2196 dyne/cm 0.0682
dari tabel 8.5 coulson & richardson, 2005 hal 332 diperoleh
diffusion volume gas (Via) untuk key komponen H2O 9.44
diffusion volume cair (Vib) untuk HCl 21.48
dari coulson hal. 333

association factor (Φ) untuk H2O 2.6
dari tebel 8.6 coulson hal. 334 diperoleh

molar volume (Vm) HCl 0.0253 m3/kmol
difusi gas (Eq. 8.21 Coulson)

Dg=(1,013E-7*(T^1,75)*(((1/BMa)+(1/BMb))^0,5))/(P*(((Via^(1/3))+Vib^(1/3))^2))
difusi liquid
Dl=(1,173E-13*(Φ*BM)^0,5*T)/(µ*(Vm^0,6))
β=1,508*(ds^0,376)
L'=L/A
menghitung gas hold up (Treybal,1981)

Scg=µg/ρg*Dg 26.6154
menghitung liquid hold up
Scl=µL/ρL*Dl 0.000065079043
dari tabel 6.5 Treybal, 1981 hal 206

ΦLsW=0,000247/(ds^1,21) 0.0059
ΦLtW=(2,09E-6*((737,5*L')^β))/(ds^2) 0.0208
ΦLoW=ΦLtW-ΦLsW 0.0149
dari tabel 6.5 Treybal, 1981 hal 206, diperoleh persamaan

H=((975,7*(L'^0,57)*(µL^0,13))/(ρL^0,84*((2,024*(L'^0,43))-1)))*(σ/0,073)^(0,1737-0,262*(LogL'))
ΦLo=ΦLoW*H 0.0105
ΦLs=(0,0486*(µL^0,02)*(σ^0,99))/((ds^1,21)*(ρL^0,37)) 0.0054
ΦLt=ΦLo+ΦLs 0.0159
menghitung luas kontak antar muka (interface area)

dari tabel 6.4 Treybal, 1981 hal.205 untuk ceramic raschig ring 50 mm
m 34.03
n 0
p 0.362
ε 0.74
aAw=m*(((808*G')/(ρg^0,5))^n)*(L'^P) 39.8444 m2/m3

aA=aAw*ΦLo/ΦLoW 28.1409 m2/m3

εLo=ε-ΦLt 0.7241

Fg=((1,195*G)/(Scg^2/3))*(((ds*G')/(µg*(1-εLo)))^-0,36) 0.0008

kL=25,1*(((ds*L')/µL)^0,45)*(Scl^0,5)*(Dl/ds) 0.0371
C=ρL/BM liquid 33.9223

Fl=kL*C 1.2601
Fg*aA 0.0230
Fl*aA 35.4614
menghitung height of gas phase transfer unit (Htg)
Htg=G/(Fg*aA) 2.4914 m
menghitung height of liquid phase transfer unit (Htl)

L=L'/BM liquid 0.0642 kmol/m2.s
Htl=L/Fl*aA 0.0018 m
faktor absorbsi (A) berkisar antara 1,25-2 (Treybal, 1981 hal.292) maka dipilih A
fraksi mol gas masuk (y1) 0.8043

fraksi mol gas keluar (y2) 0.0171 h2o
x2 0
rasio distribusi kesetimbangan

m=L/(G*A) 0.5599
Treybal,1981
NtoG=(ln((y1-(m*x2))/(y2-(m*x2)))*(1-(1/A))+(1/A))/(1-(1/A)) 6.3564
menghitung height of transfer unit (HtoG

HtoG=Htg+(m*G/L)*Htl=Htg+(Htl/A) 2.4923 m
menghitung tinggi absorber

tinggi packing (z) = HtoG*NtoG 15.8420 m
tinggi head packing (h) = 1/4*Dt 0.8953 m
tinggi absorber (Hab) = z+2h 17.6325 m
menghitung tebal dinding

bahan konstruksi carbon steel SA-285 grade C
Allowable stress (S) 13750 psi
(Brownell,1959)
tipe pengelasan double welded butt joint
efisiensi pengelasan (Ef) 0.8 %
Corrosion allowance (Cc) 0.125 in (Peters&Timmerhaus,1991)
Faktor keamanan tekanan 20 %
P design (Pd) = (1+0,2)*Pop 17.6351 psia
2.9391 psig
t=((Pd*r)/((S*Ef)-(0,6*Pd)))+Cc 0.1438 in
0.0037 m
0.3653 cm
K G 37403.6151 kg/jam
Pa 1.01325 bar L 56031.5476 kg/jam
14.69594878 psi
kg/m*s
kg/m*s
µ cP kmol/jam xi cP*xi
159.3636 0.0159 507.1701879 0.195739075149 0.003119368639767
100.7414 0.0101 2083.882148 0.804260924851 0.008102237838347
260.1050 0.0260 2591.0523 1.0000 0.0112
25C 0.796
Tc kg/jam Xi densitas (g/mL) densitas (Kg/m3) Xi.d
324.65 18490.41071 0.33 0.4413 441.3400 145.6422
647.13 37541.13689 0.67 1.0029 1002.8747 671.9260
56031.5476 1.0000 1.4442 1444.2147 817.5682
N/m2.m
(tabel 6.3 Treybal, 1981 hal 196)

kg/m2.s
kmol/m2.s
kg/s
N/m
C 16.5
H 1.98
O 5.48
Cl 19.5
C 0.0148
H 0.0037
O 0.0074
2.98576503E-05 m2/s in RCl 0.0216
0.00021090646 m2/s
0.5622
5566.0141 kg/m2.jam
1.5461 kg/m2.s
0.7063
kmol/m2.s
kmol/m2.s(kmol/m3)
kmol/m3
kmol/m2.s
kmol/m3.s
kmol/m3.s
2
rhaus,1991)
BM
HCl 36.4580
CH3Cl 50.4850
ch3oh 32.0420
H2O 18.0150
gas
viskositas cP
KOMPONEN A B C D kmol/jam
H2O -10.2158 1.79E+03 1.77E-02 -1.26E-05 2076.2484
TOTAL 2076.2484
T 324.65 K
densitas gas (ρg)

R= 8314.3000 m3.Pa/kmol.K
T= 324.6500 K
P= 101325.0000 Pa
KOMPONEN BM kmol/jam Xi Densitas (kg/m3)
H2O 18.0150 2076.2484 1.0000 0.6763
TOTAL 2076.2484 1.0000 0.6763
komponen kg/jam xi BM BM campuran
HCl 18490.4107 0.33 36.4580 12.03114
H20 37541.1369 0.67 18.0150 12.07005
TOTAL 56031.5476 1.0000 24.1012
xi µ (cP) xi*µ (cP)
1.0000 0.5374 0.5374
Xi,D.d
0.6763
0.6763
kode : T-01
fungsi : Menyimpan bahan bakuMETANOL
P= 1

dalam perancangan ini dipilih tipe tangki silinder tegak dengan dasar datar (flat bottom) dan bagian a
* tangki mampu menampung dalam kapsitas yang besar dengan konstruksi yang mudah, sehingga le

dalam perancangan dipilih bahan konstruksi Stainless steel SA 167 grade 11 tipe 316
DENSITAS
Komponen Td
CH3OH 64.7000
H2O 100.0000
ch3cl -23.7000
hcl 85.0500

METANOL 8435.3699
h2o 8.4438
total 8443.8137
782.9905

Laju alir, F :
Density, p :
lama penyimpanan :
a volume tangki
Volume tangki metanol =
over design =

b dimensi tangki
3 8 𝑥 𝑉𝑡𝑎𝑛𝑔𝑘𝑖
D= ට
𝜋
Vtangki = 1/4 X π x D2 x H
1 2𝐷
=4Xπx D x 2
1
= x π x D3
8
H= D/2,5
berdasarkan (Lioyd E. Brownell, Process Equipment Vessel Design, 1959, app. E, item 1, pg. 346), uku
D=
H=
V=
jumlah tangki yang dibutuhkan =
bahan konstruksi yang dipilih : Stainless steel SA 167 grade 11 tipe 316
Allowable Working Stress (s) 18750
faktor korosi (C) 0.125

- 1
Acairan = 4 X π x D2
5024 ft^3
- Hcairan = Vcairan
Acairan
25.4697 ft
𝜌 𝑥 (𝐻−1)
Phidrostatis =
144
𝜌 𝑥 (𝐻−1)
P-hidrostatis = 144
8.3062 psi
P-design = (Phidrostatis + Poperasi) - Patmosferik

8.3062 psi
𝐷
- r= 2
r 40
Tebal silinder tangki

Pdesign x r
ts = 𝑠 𝑥 𝐸−0,6 𝑥 Pdesign + C
0.3909 in
ts standar (in) 0.4375
Tebal tutup tangki

0,885 𝑥 Pdesign 𝑥 𝑟
th = 𝑠 𝑥 𝐸−0,1 𝑥 Pdesign + C
0.3602 in

T-01 menyimpan bahan bakumetanol silinder
°C 303 K
atm 14.696 psia
r datar (flat bottom) dan bagian atas berbentuk TORISPERIKAL, dengan alasan :
nstruksi yang mudah, sehingga lebih ekonomis
akan torispherical roof
rade 11 tipe 316
DENSITAS (data densitas (yaws)

C
g/ml 30.0000
a b n Tc ρ(g/ml)
0.2720 0.2719 0.2331 512.5800 0.7828
0.3471 0.2740 0.2857 647.1300 1.0230
0.3582 0.2611 0.2869 416.2500 0.9028
0.4413 0.2696 0.3187 324.6500 0.7673
densitas
0.9990 782.8067 0.0013 10.7758
0.0010 1023.0130 0.0000 0.0083
1.0000 1805.8197 0.0013 10.7841
kg/m3 782.9905 kg/m3
8443.8137 kg/jam 18615.4007 lbm/jam

782.9905 kg/m3
48.8807 lb/ft3
14 hari
14 hari
127959.9816191 ft3 3623.442799509 m3

20%
153551.977943 ft3
4348.131359411 m3
2025.617304112 m3
2025.617304112 m3
D= 78.7847 ft 24.0136 m
H= 31.5139 ft 9.6054 m
959, app. E, item 1, pg. 346), ukuran tangki standar yang mendekati hasil perhitungan :
80 ft 24.3840 m 960 in
36 ft 10.9728 m
32230 bbl 180958.5580 ft3
5124.2477 m3 1353660.0000 gal
0.8485 tangki ≈ 1 tangki standar
de 11 tipe 316
psi
in
ft 480 in
+C
0.9929 cm
1.1113 cm
0.9150 cm
bentuk tutup volume (m3) diameter (m) tinggi (m) tebal (cm) jumlah
torispherical 5124.2477 24.3840 10.9728 1.1113 1.0000
k
303.0000
kg/m3
782.8067
1023.0130
902.8000
767.3262
P tangki (atm) T tangki (Oc) bahan konstruksi
1.0000 30.0000 Stainless steel SA 167 grade 11 tipe 316
kode : T-02
fungsi : Menyimpan bahan baku ASAM KLORIDA
P= 1

dalam perancangan ini dipilih tipe tangki silinder tegak dengan dasar datar (flat bottom) dan bagian a
* tangki mampu menampung dalam kapsitas yang besar dengan konstruksi yang mudah, sehingga le

dalam perancangan dipilih bahan konstruksiStainless steel SA 167 grade 11 tipe 316
DENSITAS (
Komponen Td
CH3OH 64.7000
H2O 100.0000
ch3cl -23.7000
hcl 85.0500

HCL 18490.4107
h2o 37541.1369
total 56031.5476
921.6650

Laju alir, F :
Density, p :
lama penyimpanan :
a volume tangki
Volume tangki hcl =
over design =

b dimensi tangki
D= ට
𝜋
Vtangki = 1/4 X π x D2 x H
1 𝐷
= 4 X π x D2 x 2
1
= x π x D3
8
H= D/2,5
berdasarkan (Lioyd E. Brownell, Process Equipment Vessel Design, 1959, app. E, item 1, pg. 346), uku
D=
H=
V=
jumlah tangki yang dibutuhkan =
bahan konstruksi yang dipilih : Stainless steel SA 167 grade 11 tipe 316
Allowable Working Stress (s) 18750
faktor korosi (C) 0.125

- 1
20096 ft^3
- Hcairan = Vcairan
Acairan
35.8957 ft
𝜌 𝑥 (𝐻−1)
Phidrostatis =
144
𝜌 𝑥 (𝐻−1)
- Phidrostatis =
144
13.9432 psi
- Pdesign = (Phidrostatis + Poperasi) - Patmosferik

13.9432 psi
𝐷
- r=2
r 80
Tebal silinder tangki

Pdesign x r
ts = +C
𝑠 𝑥 𝐸−0,6 𝑥 Pdesign
1.0179 in
ts standar (in) 1.2500
Tebal tutup tangki

0.9148 in

T-02 menyimpan bahan baku hcl silinder
°C 303 K
atm 14.696 psia
an dasar datar (flat bottom) dan bagian atas berbentuk TORISPERIKAL, dengan alasan :
ngan konstruksi yang mudah, sehingga lebih ekonomis
sa digunakan torispherical roof
A 167 grade 11 tipe 316
g/ml
a b n Tc
0.2720 0.2719 0.2331 512.5800
0.3471 0.2740 0.2857 647.1300
0.3582 0.2611 0.2869 416.2500
0.4413 0.2696 0.3187 324.6500
densitas
0.3300 767.3262 0.0004 24.0972
0.6700 1023.0130 0.0007 36.6966
1.0000 1790.3392 0.0011 60.7938
kg/m3 921.6650 kg/m3
56031.5476 kg/jam 123528.27047492 lbm/jam

921.6650 kg/m3
57.5379 lb/ft3
14 hari
14 hari
721359.1862104 ft3 20426.728075921 m3

20%
865631.0234525 ft3
24512.0736911 m3
2025.617304112 m3
2025.617304112 m3
𝑡𝑎𝑛𝑔𝑘𝑖
𝜋
D= 140.2171 ft 42.7382 m
H= 56.0868 ft 17.0953 m
esign, 1959, app. E, item 1, pg. 346), ukuran tangki standar yang mendekati hasil perhitungan :
160 ft 48.7680 m 1920
60 ft 18.2880 m
214900 bbl 1206577.5400 ft3
34166.9510 m3 9025800.0000 gal
0.7174 tangki ≈ 1 tangki standar
de 11 tipe 316
psi
in
ft 960 in
r
+C
esign
2.5854 cm
3.1750 cm
2.3236 cm
bentuk tutup volume (m3) diameter (m) tinggi (m) tebal (cm)
torispherical 34166.9510 48.7680 18.2880 3.1750
k
30.0000 303.0000
ρ(g/ml) kg/m3
0.7828 782.8067
1.0230 1023.0130
0.9028 902.8000
0.7673 767.3262
in
jumlah P tangki (atm) T tangki (Oc) bahan konstruksi
1.0000 1.0000 30.0000 Stainless steel SA 167 grade 11 tipe 316
kode : T-03
fungsi : MenyimpanPRODUK METIL KLORIDA
kondisi opeT = 32.6 °C 305.6
P= 7 atm 102.872

dalam perancangan ini dipilih tipe tangki silinder tegak dengan dasar datar (flat bottom) dan bagian atas berbentuk
* tangki mampu menampung dalam kapsitas yang besar dengan konstruksi yang mudah, sehingga lebih ekonomis

dalam perancangan dipilih bahan konstruksiStainless steel SA 167 grade 11 tipe 316
densitas A * B^-(1-T/Tc)^n g/ml

Komponen Td a b
CH3OH 64.7000 0.2720 0.2719
H2O 100.0000 0.3471 0.2740
ch3cl -23.7000 0.3582 0.2611
hcl 85.0500 0.4413 0.2696
densitas
komponen massa (kg/jam) xi ρ (kg/m3)
HCL 0.1152 0.0000 750.5556
CH3CL 12625.3479 0.9999 897.2746
CH3OH 0.5891 0.0000 780.4057
H20 0.2104 0.0000 1020.6224
total 12626.2626 1.0000 3448.8583
897.3167 kg/m3

Laju alir, F : 12626.2626 kg/jam
Density, p : 897.3167 kg/m3
56.0179 lb/ft3
lama penyimpanan : 14 hari
a volume tangki
Volume tangki metil klorida = 166963.3395 ft3
over design = 20%
volume perancangan = 200356.0074 ft3
5673.4811 m3
tangki kecil <= 71534 ft3 2025.61730411213
tangki besar > 71534 ft3 2025.61730411213
b dimensi tangki
D= ට
𝜋
Vtangki = 1/4 X π x D2 x H D= 86.0910

1 2 𝐷
= 4X π x D x 2
1
= x π x D3
8
H= D/2,5 H= 34.4364
berdasarkan (Lioyd E. Brownell, Process Equipment Vessel Design, 1959, app. E, item 1, pg. 346), ukuran tangki stan
D= 90 ft
H= 36 ft
V= 40790 bbl
6485.2021 m3
jumlah tangki yang dibutuhkan 0.8748 tangki ≈
bahan konstruksi yang dipilih Stainless steel SA 167 grade 11 tipe 316 18 CR-10NI-2 M0
Allowable Working 18750 psi
faktor korosi (C) 0.125 in

- 1
6358.5 ft^3
- Hcairan = Vcairan
Acairan
26.2583 ft 8.00362423631213 m
𝜌 𝑥 (𝐻−1)
Phidrostatis =
144
𝜌 𝑥 (𝐻−1)
- Phidrostatis =
144
9.8258 psi
Pdesign = (Phidrostatis + Poperasi) - Patmosferik
-
9.8258 psi
𝐷
- r=2 45 ft 540
Tebal silinder tangki Pdesign x r

ts = 𝑠 𝑥 𝐸−0,6 𝑥 Pdesign + C
0.4789 in 1.2163 cm
ts standar (in) 0.5000 1.2700 cm
Tebal tutup tangki

0.4381 in 1.1127 cm
kode alat fungsi alat bentuk bentuk tutup volume (m3)

T-02 menyimpan bahansilinder torispherical 6485.2021
K
psia
t bottom) dan bagian atas berbentuk TORISPERIKAL, dengan alasan :

ng mudah, sehingga lebih ekonomis
pherical roof
C K
32.6000 305.6000
n Tc ρ(g/ml) kg/m3
0.2331 512.5800 0.7804 780.4057
0.2857 647.1300 1.0206 1020.6224
0.2869 416.2500 0.8973 897.2746
0.3187 324.6500 0.7506 750.5556
densitas
xi/ρ V (m3)
0.0000 0.0002
0.0011 14.0708
0.0000 0.0008
0.0000 0.0002
0.0011 14.0719
897.2685 kg/m3
27836.1111 lbm/jam
14 hari
4727.9009 m3
m3
m3
ft 26.2405 m
ft 10.4962 m
E, item 1, pg. 346), ukuran tangki standar yang mendekati hasil perhitungan :
27.4320 m 1080 in
10.9728 m
229019.5340 ft3
1713180.0000 gal
1 tangki standar
HAL.342
in
diameter (m) tinggi (m) tebal (cm) jumlah P tangki (atm)

27.4320 10.9728 1.2700 1.0000 7.0000
T tangki (Oc) bahan konstruksi
32.6000 Stainless steel SA 167 grade 11 tipe 316

Komponen Td a b n
CH3OH 64.7000 0.2720 0.2719 0.2331
H2O 100.0000 0.3471 0.2740 0.2857
ch3cl -23.7000 0.3582 0.2611 0.2869
hcl 85.0500 0.4413 0.2696 0.3187
densitas
komponen massa (kg/jam) xi ρ (kg/m3) xi/ρ
METANOL 10544.2124 0.9990 775.4940 0.0013
h2o 10.5548 0.0010 1015.7575 0.0000
total 10554.7672 1.0000 1791.2516 0.0013
suhu 37.866 C
Tekanan 1 atm POMPA METANOL
1. Menghitung Densitas Fluida
komponen massa (kg/jam) xi densitas densitas campuran (xi*ρ)

CH3OH 10544.2124 0.9990 775.4940 774.7186
H2O 10.5548 0.0010 1015.7575 1.0158
Total 10554.7672 1.0000 775.7343
2. Menghitung Laju Alir Volumetrik (Q)

F = 10554.7672 kg/jam 6.4637
ρ = 775.6775 kg/m3
Q = F/ρ
= 13.6072 m3/jam 0.0038
H = 58.5000 m Fig. 1.1.6 (Grundfos, 2014)

191.9268 ft
3. Menghitung Energi Mekanis Teoritis (Ws)
Ws = H x g/gc ft*lbf/lbm
= 191.9268 ft*lbf/lbm
4. Menghitung Energi Pompa (Wp)

eff pompa = 75%
= 0.7500
Wp = Ws/η x F/550
= 255.9024 x 0.0118
= 3.0074 hp 2242.6231
c k
37.866 310.8662
Tc ρ(g/ml) kg/m3
512.5800 0.7755 775.4940
647.1300 1.0158 1015.7575
416.2500 0.8859 885.9009
324.6500 0.7125 712.5035
V (m3)
13.5968 Densitas = 1 / (Xi/ρ)
0.0104
775.6775
13.6072
POMPA METANOL
lb/detik 58,5
m3/detik
kpsts head daya
watt 13.4801 58.5000 2242.6218

KomponenTd a b n Tc
CH3OH 64.7000 0.2720 0.2719 0.2331 512.5800
H2O 100.0000 0.3471 0.2740 0.2857 647.1300
ch3cl -23.7000 0.3582 0.2611 0.2869 416.2500
hcl 85.0500 0.4413 0.2696 0.3187 324.6500
densitas
komponenmassa (kg/jam) xi ρ (kg/m3) xi/ρ V (m3)
HCL 18490.4107 0.3300 782.8067 0.0004 23.6207
h2o 37541.1369 0.6700 1023.0130 0.0007 36.6966
total 56031.5476 1.0000 1805.8197 0.0011 60.3173
suhu 30 C
Tekanan 1 atm POMPA ASAM KLORIDA
komponenmassa (kg/jam) xi densitas densitas campuran

HCL 18490.4107 0.3300 767.3262 253.2177
H2O 37541.1369 0.6700 1023.0130 685.4187
Total 56031.5476 1.0000 938.6364

F = 56031.5476 kg/jam 34.3134 lb/detik
ρ = 928.9466 kg/m3
Q = F/ρ
= 60.3173 m3/jam 0.0168 m3/detik
H = 45.0000 m Fig. 1.1.6 (Grundfos, 2014)

147.6360 ft
Ws = -H*g/gc ft*lbf/lbm
= 147.6360 ft*lbf/lbm

eff pompa = 0.7500
= 0.7500
Wp = Ws/η x F/550
= 196.8480 x 0.0624
= 12.2810 hp 9157.9212 watt
c k
30.0000 303.0000
ρ(g/ml) kg/m3
0.7828 782.8067
1.0230 1023.0130
0.9028 902.8000
0.7673 767.3262
Densitas = 1 / (Xi/ρ)
928.9466
A ASAM KLORIDA
45
kpsts head daya
60.2205 44.2000 8980.6749

KomponenTd a b n Tc
CH3OH 64.7000 0.2720 0.2719 0.2331 512.5800
H2O 100.0000 0.3471 0.2740 0.2857 647.1300
ch3cl -23.7000 0.3582 0.2611 0.2869 416.2500
hcl 85.0500 0.4413 0.2696 0.3187 324.6500
densitas
komponenmassa (kg/jam) xi ρ (kg/m3) xi/ρ V (m3)
h2o 203.1799 1.0000 1027.5898 0.0010 0.1977
total 203.1799 1.0000 1027.5898 0.0010 0.1977
suhu 30 C
Tekanan 1 atm POMPA AIR PROSES
komponenmassa (kg/jam) xi densitas densitas campuran
H2O 203.1799 1.0000 1027.5898 1027.5898

Total 203.1799 1.0000 1027.5898

F = 203.1799 kg/jam 0.1244 lb/detik
ρ = 1027.5898 kg/m3
Q = F/ρ
= 0.1977 m3/jam 0.0001 m3/detik
H = 60.0500 m Fig. 1.1.6 (Grundfos, 2014)

197.0120 ft
Ws = -H*g/gc ft*lbf/lbm
= 197.0120 ft*lbf/lbm

eff pompa = 0.7500
= 0.7500
Wp = Ws/η x F
= 262.6827 x 0.0002
= 0.0594 hp 44.3145 watt
k
25.0000 298.0000
ρ(g/ml) kg/m3
0.7874 787.3807
1.0276 1027.5898
0.9133 913.2686
0.7969 796.9392
Densitas = 1 / (Xi/ρ)
1027.5898
IR PROSES
60,05
kpsts head daya
0.1986 60.05 44.3144
DENSITAS (data densitas (yaws) hal 185

Komponen Td A B
CH3OH 64.7000 0.2720 0.2719
H2O 100.0000 0.3471 0.2740
ch3cl -23.7000 0.3582 0.2611
hcl 85.0500 0.4413 0.2696
(ch3)2O -24.82 0.2639 0.2633
Fungsi : Memisahkan campuran gas dan liquid yang keluar reaktor

Tipe : Silinder vertikal dengan head dan bottom
Bahan : Carbon Steel, SA-283 Grade C
Jumlah : 1 unit
Langkah Perancangan
1. Menetukan Tipe Tangki
Dipilih tangki berbentuk silinder vertikal dengan head berbentuk
hemispherical dengan pertimbangan :
a. Memiliki struktur yang kuat
2. Menentukan Bahan Konstruksi Flash Tank

Bahan konstuksi yang dipilih adalah Carbon Steel, SA-283 grade C
dengan pertimbangan :
a. Suhu operasi -20 sampai 650 °F
b. Korosi dan temperatur masih bisa dipertimbangkan sebagai faktor yang
diijinkan.
c. Penggunaannya paling murah dan mudah.
3. Perhitungan Faktor Separasi, FLV

kondisi operasi T 50 C Dari neraca massa, diperoleh:
323 K
122 F
P 14.696 PSIA
1 ATM
R 0.08206 L.atm/gmol.K
0,5
Wl  ρv 
FLV  x
 ρ 
 (Pers 5-1 Evans 1974, hal. 154)
Wv  l 
DENSITAS VAPOUR
komponen LAJU ALIR (KG/JAM) LAJU ALIR MOL BM
HCL 1439.7125 39.4896 36.4580
CH3)2O 9.0953 0.1974 46.0690
CH3CL 12626.4707 250.1034 50.4850
CH3OH 0.7364 0.0230 32.0420
H2O 7.0147 0.3894 18.0150
∑ 14083.0296 290.2028
DENSITAS LIQUID
LAJU ALIR LAJU ALIR MOL
komponen
(KG/JAM) (KGMOL/JAM) Xi
HCL 0.0014 0.0000 0.0000
CH3)2O 0.0009 0.0000 0.0000
CH3CL 0.0126 0.0003 0.0000
CH3OH 408.3862 12.7453 0.0804
H2O 4669.4229 259.1964 0.9196
∑ 5077.8241 271.9420 1.0000
sehingga :
0,5
Wl  ρv 
FLV  x
 ρ 
 = 3.1096
x
Wv  l  8.6244
= 0.0156
4. Menghitung Kecepatan Gas Maksimum (Vvmax)
Dari nilai FLV maka dari Fig. 5-1, Evans hal.154, didapat harga Kv adalah sebesar :
Kv = 0.32 ft/s
Kecapatan gas maksimum, (Vvmax)
0,5
 ρl  ρ v 
Vv max  Kv 
 
 (Pers Evans, hal. 154)
 ρv 
= 61.1557 -
0.3200
0.1143
= 7.3951 ft/s
5. Menentukan Dimensi Flash Tank

a. Menghitung Diameter (D)
● Luas penampang flash drum (A)
Qv (ft3/s) (Persamaan 5-2 Evans, hal 154)

A=
Vvmax (ft/s)
Wv (L]lbm/s)
Qv=
ρv (lbm/ft3)
8.6244
= =
0.1143
SEHINGGA
75.4551
A= =
7.3951
● Diameter (D)
D= (A x 4 : π )^0,5 (Persamaan 5-3 Evans, hal.154)

0.5
40.8137
3.14
= 3.6053 ft =
- Menghitung tinggi gas dalam tangki

Hv/D adalah sebesar 1,5 (Evans, hal 156)
Hv= 1.5 x
= 1.5 X
= 64.8949 in
- Menghitung Tinggi larutan dalam vessel

Holding times diperoleh dari 5-4, Evans, 1974) :
QL= WL (kg/jam) =
𝝆L (kg/m3)
Total time T (t)= 7.8 menit

Sehingga=
Vliq= QL (ft3/s) x
= 0.0508 x
= 23.7968 ft3
Sehingga, tinggi cairan adalah

π . D² . HL
V=
4
4 x
HL=
3.14 x
- SHELL FLASH DRUM (Hs)
Menurut Evans, F.L 1974 hal 156 bahwa jarak feed nozzle dengan cairan (nf)
adalah sebesar 6 in
Sehingga Tinggi shell flash drum adalah :
Hs = Hv
= 5.4079
= 8.2401
b. Menghitung Tebal Dinding
Tebal shell dihitung dengan menggunakan persamaan
Pd . D
ts= + nC
2(f .E - 0,6.Pd)
dimana: ts= Tebal shell

f= Tekanan yang diijinkan
12650 psi
E= Effisiensi pengelasan
80%
D= Diameter shell (ID)
n= umur tangki
C= Faktor korosi, 0.125
Pd= Tekanan design, psi
Tekanan design flash drum:
Pd= (P opr + P hidrostais x 1,1 )
digunakan faktor keamanan = 10%
Tekanan hidrostatis dihitung dengan menggunakan persamaan :
ρL (lbm/ft3) x H liq (ft)

Ph =
144 lbf/ft2
= 61.1557 x 2.3322
144
= 0.9905 psi
Sehingga,
(P (psia) +
Pd= ( 14.6960 +
17.2551
ts=
2 ( psi 12650
= 1.2869 in =
tebal standar 1.375 in 1+(3/8)
c. Menghitung Ukuran Head

Digunakan head jenis standard hemispherical head dimana dengan
ketebalan yang diberikan, head jenis ini adalah yang terkuat,
A
t
Keterangan Gambar :
ID = Diameter (in)
r
t= Tebal head
r= 1/2
O sf = 1/2
= 21.6316
ID
Ht= tinggi head total
sf= Straight flange
Tebal head dihitung dengan persamaan:

P.di psi x in +
th =  cn 4 x psi x 0,8 - 0,4 x psi
4.f.E 0,4P
17.2551
th =
4 x 12650
= 1.2684 in =
Tebal head distandarisasi dari Tabel 5.6 Brownell&Young menjadi:

sf 1½ -4½ in
diambil sf = 4 in
Hh= th + r + sf
= 26.9001 in
Jadi, tinggi head (Hh) = 26.9001 in =
Total Tinggi Flash Drum (Ht) = Hs

= 2.5116
= 3.8781
e. Menghitung Volume Tangki
Tutup atas dan bawah dipilih tipe hemisperical.
Sehingga, volume untuk kedua tutup:
π . D³ π . D² . 2sf
Vh = +
6 4
3.14 x 43.2633 ^
=
6
= 54131.9496 in3 31.3262
π . D² . Hs 3,14 x ft 2 x ft
Vs=
Vs=
4
^
= 3.14 x 3.6053
4
84.0777 ft3
Sehingga, Volume total tangki adalah

Vt = Vh + Vs
= 115.4038 ft3
= 3.2679 m3
Kode : FD-01
Fungsi : Memisahkan campuran gas dan liquid yan
Jenis : Silinder vertikal dengan
Bahan : Carbon Steel, SA-283 Grade C
Jumlah : 1
Harga :
Spesifikasi
Suhu Operasi : 50.00
Tekanan Operasi : 1
Diameter : 43.2633
Volume Tangki : 115.404
Tebal Shell : 1.375
Tebal Tutup Atas : 1.375
Tebal Tutup Bawah : 1.375
Tinggi Tangki : 12.7235
ta densitas (yaws) hal 185
c k
50.0000 323.0000
n Tc ρ(g/ml) kg/m3
0.2331 512.5800 0.7639 763.9151
0.2857 647.1300 1.0044 1004.4285
0.2869 416.2500 0.8587 858.6644
0.3187 324.6500 0.5630 563.0214
0.2806 400.1000 0.6118 611.7951
gas dan liquid yang keluar reaktor

head dan bottom berbentuk hemispherical
flash drum (CARA KA NANA)
ari neraca massa, diperoleh:

F laju alir campuran massa liquid dan gas (ALIRAN 16) =
Wv lau alir massa gas (ALIRAN 18) =
WL lau lair massa liquid (ALIRAN 17) =
ers 5-1 Evans 1974, hal. 154)
UR BM * Pt
V 
RT
BM * Pt
yi BM X yi V 
RT
0.1361 4.9611
0.0007 0.0313 = 48.5282
x
0.8618 43.5091 0.08206
0.0001 0.0025
0.0013 0.0242 densitas vapour= 1.8309 g/L
ρv= 0.1143 lb/ft3
1.0000 48.5282
ID
ρ (kg/m3) Xi/ρ
563.0214 0.0000 Densitas = 1 ; (Xi/ρ)
611.7951 0.0000
858.6644 0.0000 Densitas liquid= 979.6224 kg/m3
763.9151 0.0001 ρL= 61.1557 lb/ft3
1004.4285 0.0009
0.0010
0,5
0.1143
61.1557
0.5
0.1143
ersamaan 5-2 Evans, hal 154)

75.4551 ft3/s
10.2034 ft2
D= 2 1/ xA x4
43.2633 in = 1.0989 m
vans, hal 156)

D (in)
43.2633
5.4079 ft
1 m3
1h
5077.8241 = 5.1835 m3/jam 1369.3121
979.6224 0.0508 ft3/s 22.8219
sama hasilnya
468 s 3.1096
0.0508
61.1557 ft3/s
t (s) 5.18364 m3/jam
468
673.833904002686 L
HL= 4 x ft3
3,14 x (ft)^2
23.7968
= 2.3322 ft 27.9868
3.6053^2
^2
zzle dengan cairan (nf)

= 0.5 ft
+ HL + nf
+ 2.3322 + 0.5000
ft = 2.5116 m
(Pers 13.1 Brownell & Young hal 254)
(Tabel 13.1 Brownell & Young hal 251)

Carbon Steel, SA-283 grade C
(Tabel 13.2 Brownell & Young hal 254)
untuk double welded butt joint
10 TTAHUN
(Peter & Timmerhaus,
0.125 in/tahun
1991)
psi 144 lb/ft2
32,2 FT/S2
x g/gc 32,2 lbm. Ft/lbf.s2
f/ft2
x 1
4
(psia)Ph) X 1.1
0.9905 ) x 1.1 = 17.2551
psi X in 43.2633
X 80% - 0.6 X
0.1072 ft
3.4925 cm
(in)
D
43.2633 in
in
nggi head total
raight flange (in)
in/tahun
tahun
x 43.2633
x 80% - 0.4 x
0.1057 ft
1 3/8 in 1.3750 in
untuk th = 1.3750 in (Tabel 5.6 Brownell&Young)
0.6833 m
+ 2Hh
+ 1.36652405486
m
3,13 x in3 + 3,14 x in2 x IN

6 4
^3 3.14 x 43.2633 ^
+
4
ft3
^
2 x 8.2401
4
RESUME FD-01
emisahkan campuran gas dan liquid yang keluar reaktor

inder vertikal dengan head dan bottom berbentuk hemispherical
rbon Steel, SA-283 Grade C
unit
50.00 °C
1 atm
43.2633 in 1.0989 meter
115.404 ft 3
1.375 in 3.4925 cm
1.375 in
1.375 in
12.7235 ft 3.8781 meter
Spesifikasi tangki dapat diterima karena L/D = 4

NANA)
kg/jam KG/KGMOL lbm/s

19160.8536 562.1449 11.7340
14083.0296 290.2028 8.6244
5077.8241 271.9420 3.1096
1
323
7,8
3,6053
nj
ft
264.17 galon
60 menit
gal/h
gal/s
1 ft3 7.48052 gallon

1369.3243 gal/jam
in
psi
tahun in/tahun
+ 10 X 0.125
17.2551 psi
+ 10 x 0.125
17.2551
^2 x 2 x 4.0000
4
3.26787197108 m3
L/D 3.5291
karena L/D = 4
1369,3243
3,6053
FUNGSI : TEMPAT BERLANGSUNGNYA REAKSI HIDROKLORINASI METANOL DAN ASAM KLORIDA DENGAN MENG
Jenis : fixed bed multitube reactor
1. Dasar Perancangan
Suhu bahan masuk : 350

Suhu bahan keluar : 350
Tekanan masuk : 4.9
Tekanan keluar : 4.9
Laju alir bahan : 19,160.854
Bahan konstruksi : low-allow stell Sa=A-318
2. Menghitung BM campuran
Komponen kmol/jam BM(kg/kgmol)
ASAM KLORIDA 289.590816438327 36.458

DIMETIL ETER 0 46.069
METIL KLORIDA 0.002500811703358 50.485
METANOL 263.264378580297 32.042
AIR 9.2871585230226 18.015
Total 562.14485435335
3. Menghitung Z umpan 1.01325
komponen Yi Pc (ATM)
ASAM KLORIDA 0.5151534 82.0034542314335

DIMETIL ETER 0.0000000 52.9977794226499
METIL KLORIDA 0.0000044 65.9166049839625
METANOL 0.4683212 79.8420922773255
AIR 0.0165209 217.665926474217
Total 1.0000000
T
Tr =
∑ Yi * Tc
P
Pr =
∑ Yi * Pc
B° = 0,083 -
B¹ = 0,139 -
BPc
=
RTc
4. Menghitung faktor kompresiblitas
Z =
5. Megnhitung densitas campuran
ρ=
6. Laju volumetrik umpan

Q=
n=
Laju volumetrik umpan (V) = ZnRT

P
7. Menghitung viskositas campuran umpan
KOMPONEN A
HCL -9.118
(CH3)2O -4.276
CH3CL -1.374
CH3OH -14.236
H2O -36.826
Total
(Yaws, 1999)
Viskositas umpan =
8. Menghitung konduktifitas panas (Kg)
KOMPONEN A
HCL 0.00119
(CH3)2O -0.0315
CH3CL -0.00185
CH3OH 0.00234
H2O 0.00053
Total
(Yaws, 1999)
Konduktifitas =
A. Menghitung jumlah tube

Laju alir massa gas 19160.8536184495 kg/jam
> Katalis yang digunakan mememiliki kriteria berikut
Diameter (D) 0.43 cm
Tinggi (H) 0.43 cm
Densitas 1.14 g/cm3
> V katalis 0.062412995
> V katalis = V bola, sehingga
V katalis
Dp 0.492227124297933
> Pemilihan Pipa tube
Dalam pemilihan pipa harus diperhatikan faktor perpindahan panas. Pengaruh bahan isian didalam pipa
katalis dengan diameter pipa dengan koefisie
Dp/Dt 0.05 0.1

hw/h 5.5 7.0
Dimana
Dimana : = rasio diameter katalis per diameter pipa
Dp/Dt = rasio koefisien transfer panas pipa berisi katalis terh
hw/h transfer panas pada pipa kosong
Dari data diatas dipilih (hw/h) terbesar 7.8 pada (Dp/Dt) = 0.15
Dp/Dt = 0.15
Dt= Dp/0,15 3.28151416198622 cm
Dipilih Pipa dengan ukuruan standar diperoleh dari table 11 kern 1959
NPs = 1.5 in
OD= 1.9 in
ID= 1.61 in
Sch= 40
at"= 2.04 in2
> Menghitung mas velocity (G)
Untuk pipa berkatalis 1000 < NRe/(1-e)< 5000. Agar reaksi dapat berlangsung, maka aliran gas
didalam tube harus turbulen dengan NRe> 2100 (dipilih NRe = 4500)
Nre 4500
Dari Hill chales pg.452 diperoleh Porositas (ε) = 0,51
ε 0.51
Luas area bola = π x Dp2
0.760782881549083 cm2
Luas area katalis = πxDxH+

0.580586 0.290293
0.870879 cm2
Faktor sphericity(ϕ ) =
0.873580464736299
Dari Figure. 219 (Brown, 1959) diperoleh FRe = 32
NRe =
G= 0.067344680686804 g/cm2.s
> Menghitung jumlah pipa (tube)

Jumlah maksimum
Ao = 13.1277060026 cm2
Ntmaks =
6020.32881789421 tube
Jumlah tube minimum

Dari Figure. 70 (Brown, 1959) diperoleh fD = 1,2
ρB = ρs x (1 – ε) = 0.5586 g/cm3
g 9,8 m/s2 980
V maks
167.210935475907 cm/s
Q= 630828.677561986 cm3/s
A= 3772.65204435677 cm2
Ntmin = 287.380905971658 tube

Sehingga diperoleh jumlah pipa (tube) pada 258 – 5667 tube
Jika kecepatan linier gas dirancang = 60% x vmaks, maka kecepatan maksimumsebesar
v = 60% x vmaks 100.326561285544 cm/s
A= 6287.75340726128 cm2
Nt = 478.968176619431 tube
B Menghitung diametershell
> Pola tube adalah triangular pitch
Pt = 1,25 x OD 2.375 in
C’ = Pt – OD = 0.475 in
> Luas segitiga = = 0,5 x Pt2 x sin 60o

2.442390625 in2
> Luas seluruh segitiga (a) = luas segitiga x
389.968369791667 in2
> Luas lubang segitiga (b) = 0,5 x x OD2 x
226.235691666667 in2
> Luas tanpa lubang = a – b

163.732678125 in2
> Luas shell = luas tanpa lubang + ( x OD2 x Nt)
1521.146828125 in2
> Faktor keamanan: 20%, sehingga
Luas shell = (Luas shell x 20%)+ Luas shell

1825.37619375
> Diameter shell =
48.2215718536654 in
1.2248 m
4.01846432113878 ft
C. Menghitung massa katalis dan waktu tinggal
> Menghitung nilai k
Reaksi yang terjadi
M=
Xa =
∫ dx/(1-xa).(m.xa)
maka = ∫ I . dx = ΔX / 3 (I0 + 4. I1 + 2. I2+ ...+ 2. In-2 + 4 .
ΔX = 0,95/4
untuk N = 8, Maka
Ea
No Xi
0 0
1 0.2375
2 0.475
3 0.7125
4 0.95
TOTAL
0,95
Jadi = ∫ I . dx 0.2375
0 3
14.4340225578752
t 3600
> k= 1
t . Cao
1
3600
K 0.003997343895469
> Menghitung laju reaksi (-rA)
Data Laju alir
komponen
HCL
CH3)2O
CH3CL
CH3OH
H2O
Total
Cao = mol/ volume
CA= Cao (1-Xa/(1+(εa . Xa))
CA=
(-rA) = k CA CB
k x Cao (1-Xa) x Cbo ((M-Xa))
0.0040
densitas
6.92340958297668E-06
Menghitung panjang tube

z=
Menghitung berat katalis Menghitung berat katalis

w = ρB x z x x IDt2 x Nt x (1 – ε)
w=
Meghitung volume katalis

V =
Menghitung volume bed

Volume bed =
Menghitung Residence Time
Vgas masuk =
τ =
volume gas masuk (v)
Menghitung tebal Shell

r= 48.2215718536654
2
Ts =
ts =
P =
ri =
f =
C =
E =
Direncanakan menggunakan bahan konstruksi Staniless Steel SA 167 Grade 10, 2
20 Ni dengan karakteristik sebagai berikut :
c =
f =
E =
ri =
P =
Faktor keamanan 20% sehingga:
Tekanan perancangan
Ts =
Menghitung tebal head

Direncanakan bentuk head adalah elliptical dished head dengan bahan yang sama
dengan bahan shell. Persamaan yang dihitung berdasarkan persamaan Brownell.
Th
Th
Standarisasi Brownell and Young app E hal 346 didapatkan Th : 0,3125 in
Menghitung tinggi head

IDs =
ODs =
=
=
Standarisasi Brownell and Young app E hal 346 didapatkan tinggi head 4 ft
Untuk perancangan digunakan ODS standar 54 in. dari tabel 5.7 Brownell hal 90.
ODs =
ts =
icr =
r =
Direncanakan head dipasang dengan flane and dish, maka persamaan yang
berlaku dari Brownell and Young tahun 1959 hal 87 adalah :
a =
AB =
BC =
AC =
b =
Dari tabel 5.6 Brownell and Young dengan th 5/16 inch didapatkan sf 1,5 - 3 inch,
untuk perancangan dipilih sf 2,5 inch, maka tinggi head adalah :
Hh =
=
=
=
Menghitung tinggi reaktor
Tinggi Reaktor (HR) = panjang tube + 2 tinggi head
Panjang tube (z) = 747.4265
Tinggi Reaktor (HR) = 24.5218680010081
= 26.1132262810384
Menghitung volume reaktor

Vr =
=
=
=
26 Menghitung koefisien perpindahan panas overall
Pada bagian tube (koefisien perpindahan pada bed (tube) dihitung menurut
Froment and Bischoff, 749)
TUBE
hi =
mass velocity (Gt) =

Konduktivitas (k) =
IDt =
ODt =
Diameter (Dp) =
Viskositas (μ) =
hi =
=
=
=
hio =
SHELL
Pada bagian shell (menggunakAN AIR PENDINGIN sebagai pendingin) d
data yang terdapat di Kern, 1965
as
Gs
Cross flow area (as)

Kecepatan massa pendingin (W)
Diameter dalam shell (IDs)
Pitch pipa (Pt)
C'
Baffle spacing (B)
Untuk design triangular pitch

De
Res
ho =
27 Menghitung Koefisien perpindahan panas overall (Uc)
Uc =
28 Menghitung Koefisien perpindahan design overall (Rd)
Dipilih Rd = 0.002
Area perpindahan panas (a")

a"
29 Menghitung pressure drop shell

Res
jH
c
k
visko
f
s
ώ
B
N+1
∆Ps
Tube
Diameter partikel (Dp)
IDt
ODt
Nt
a’t
Rea
L DAN ASAM KLORIDA DENGAN MENGGUNAKAN KATALIS KROMIA ALUMNA
°C T 350
°C P 4.9
ATM R 82.06
ATM
KG/JAM
Yi BM * Yi
0.5151534 18.7814615822706
0.0000000 0
0.0000044 0.000224592429987
0.4683212 15.0059493618837
0.0165209 0.297624641578746
1.0000000 34.085260178163
bar
Tc (K) w Yi * Pc Yi * Tc
324.65 0.132 42.2443558412735 167.244541738

400.1 0.204 0 0
416.25 0.153 0.000293242953152 0.0018517698125
512.58 0.566 37.3917481324635 240.05210423552
647.13 0.345 3.59604459343849 10.691192578676
1.4 83.2324418101286 417.98969032201
623
= = 1.4904673833464
417.9897
4.9
= = 0.0588712753517
83.2324
0.422 0.422
= 0.083
Tr^0,16 1.0659371445185
0.172 0.172
= 0.139
Tr^4,2 5.3450823626471
B° + (ώ * B¹) = -0.312895763807546 0.3387704732795
= -0.276708000770326
BPc Pr
1 + x
RTc Tr
0.0588712753517
1 + -0.276708000770326 x
1.4904673833464
0.989070439858403
P BM 4.9 34.085260178163
=
ZRT 0.989070439858403 82.06
= 0.003303055809515 g/cm3
562.14485435335 KMOL/JAM
156.151348431486 MOL/S
0.989070439858403 156.151348431486 82.06

=
4.9
viskositas gas (micropoise) T=K

A + B T + CT2
B C kmol/jam Yi
5.55E-01 -1.11E-04 289.590816438327 0.515153370516
3.03E-01 6.35E-05 0 0
3.86E-01 -4.87E-05 0.002500811703358 4.4486962462E-06
3.89E-01 -6.28E-05 263.264378580297 0.4683212459236
4.29E-01 -1.62E-05 9.2871585230226 0.0165209348642
562.14485435335 1
250.458193195945 µP
0.0250 cP
0.060610882753419 lbm/ft.jam
0.000250458193196 g/cm.s
KONDUKTIVITAS gas (W/m.k)

A + B T + CT2
B C kgmol/jam Yi
4.48E-05 2.10E-10 289.590816438327 0.515153370516
1.50E-04 1.39E-09 0 0
2.03E-05 7.32E-08 0.002500811703358 4.4486962462E-06
5.43E-06 1.32E-07 263.264378580297 0.4683212459236
4.71E-05 4.96E-08 9.2871585230226 0.0165209348642
562.14485435335 1
0.042427718916156 W/(M.K) 0.000101406842311

0.02451434881013 BTU/FT.JAM.F 0.000424278659098
0.00010140224821 cal/cm.s. K 0.0245
0.000424277189162 j/cm.s k
5322.4593384582 g/s 42242.4011043061 lbm/jam

1140 kg/m3
cm3
cm
Pengaruh bahan isian didalam pipa terhadap koefisien transfer panas konveksi diteliti oleh Colburn (Smith, p.571) dan dipero
ngan diameter pipa dengan koefisien transfer panas pipa berisi katalis dibanding koefisien transfer panas konveksi pada pipa
0.15 0.2 0.25

7.8 7.5 7.0
atalis per diameter pipa

ansfer panas pipa berisi katalis terhadap koefisien
da pipa kosong
3.81 cm
4.826 cm
4.0894 cm
langsung, maka aliran gas

34
1,5
496.823490048187 lbm/ft2.Jam
6021 tube
R 0.08206
T 623
1.5000 DENSITAS V
komponen LAJU ALIR (KG/
HCL 10557.9020
cm/s2 CH3)2O 0.0000
CH3CL 0.1263
CH3OH 8435.5172
H2O 167.3082
∑ 19160.8536
288 tube
aksimumsebesar
479 tube
in2
122.48279250831 cm
CH3OH + HCl
mula" 263.2644 289.5908
bereaksi 250.1012 250.1012
sisa 13.1632 39.4897
sisa= 562.1448543533500000
Mula= 562.1448543533500000
DENSITAS VAPOUR
komponen LAJU ALIR (KG/
HCL 10557.9020
CH3OH 8435.5172
∑ 18993.4192
CA= Cao (1-Xa) >

CB= Cbo - Cao.Xa
Xa= konversi
Cao= laju mol / volume total
Xa= konversi 0.950
1.1 CA=
1.1 0.002282060901816 KMOL/M3
CB=
0.95 0.006846182705447 KMOL/M3
X / 3 (I0 + 4. I1 + 2. I2+ ...+ 2. In-2 + 4 . In-1+ I)
0.2375
18.86 kal/mol
POLA A=dx/(1-xa).(m-xa) A*POLA

1 0.909090909090909 0.909090909090909
4 1.52055119980993 6.08220479923973
2 3.04761904761905 6.0952380952381
4 8.97615708274895 35.9046283309958
1 133.333333333333 133.333333333333
154.482027020905 182.324495467898
182.324495467898
0,95
Jadi = ∫ dx/(1-xa)-(m-xa)
0
1 14.4340225578752
10.9033736715456
M3/KMOL.S
LAJU ALIR (KG/JAM) Densitas (kg/m3) Laju alir volumetrik (m3/jam)

10557.9020 796 13.26369596195
0.0000 0 0
0.1263 913 0.000138284205
8435.5172 787 10.71857333986
167.3082 1027.6 0.162814481114
19160.8536 24.1452
263.264378580297 Cbo = mol/ volume 289.5908

24.1452 24.1452
10.9033736715456 kgmol/m3 11.9937110387
(1+(εa . Xa)) CB= Cbo (1-Xa/(1+(

0.54516868357728 kgmol/m3
0.54516868357728 CB
Cbo ((M-Xa)) m3/kmol.s kgmol/m3
0.54516868357728 3.62178331006855
1140 KG/M3
0.277890177390314 7.47426537 m
0.03717959742614 747.426536670727 cm
x x IDt2 x Nt x (1 – ε)
0.5586 747.42653667 0.785 16.72319236
1286441.02040374 gram
1286.44102040374 KG
1.286 ton
W
ρB
1286441.02040374
0.5586
2302973.54171812 cm3
volume katalis
(1 - ε)
2302973.54171812
0.49
4699946.00350637 cm3
5322.4593384582
0.008437250124754
630828.677561986 cm3/s
volume bed
volume gas masuk (v)
4699946.00350637 7.45043174268903 s
630828.677561986
24.1107859268327 in
P.r (Brownell and Young, 1959)

+ C
fE - 0.6 P
tebal shell, cm
tekanan operasi, atm
IDs/2, cm
tegangan maksimum yang diijinkan, atm
faktor koreksi (0.125)
efisiensi pengelasan maksimum, %
ksi Staniless Steel SA 167 Grade 10, 25 Cr HAL.342
0.125
18750 psi
0.8
61.2413962541551 cm = 24.1107
4.9 atm
= 1.2 x (4,9 atm)

= 5.88 atm =
86.4125 x 24.1107
18750 0.8 - 0.6
0.2644 in = 0.3125
0.0079375
an yang sama
n Brownell.
P.d
= + C
2fE - 0.2 P
= 86.4125 x
2 18750 0.8
= 0.263978250147523 in 0.3125
0.0079375
hal 346 didapatkan Th : 0,3125 in
48.222 in
IDs + (2 x ts)
48.222 + 2 x
48.8465718536654 in 4.07054765447212 ft
wnell hal 90.

54
0.3125
3.25
54
IDs/2 = 48.222 2
a - icr = 24.1108 -
r - icr = 54 -
(BC2 – AB2)0.5 = 2575.5625 -
r - AC = 54 -
f 1,5 - 3 inch,
th + b + sf
0.3125 7.7356 1.5
9.5481 in = 0.7957
24.2523001876619 cm
tinggi head
cm 24.5218680010081 ft
+ 1.59135828003031
ft 7.9593 m
Vvess + 2 Vh
[(3.14/4) x IDs2 x z + (2 x 0.000049 x IDs3)]
0.785 15002.0344606338 747.4265 2
8802321.2222 cm3 = 8.8023
2325.32768213455 GAL
anas overall
n pada bed (tube) dihitung menurut
-4,6
3.5 x k Dp
x (DpxGt/μ)è
IDt IDt
496.823490048187 lbm/ft2.Jam
0.0245 btu/ft.jam.F
1.610 in = 0.134166666667
1.90 in = 0.158333333333
0.492227124297933 cm = 0.016149183868
0.060610882753419 lbm/ft.jam
3.5 0.0245
x 0.016149183868
0.134166666666667
-0.5536863040472
0.639504751568609 132.373816817545 e
84.6536848380923 0.574826913185703
48.661216345276 btu/ft2.Jam.°F
IDt
hi x
ODt
48.661216345276 0.134166666666667
0.158333333333333
41.2339780609971 btu/ft 2.
Jam.°F
PENDINGIN sebagai pendingin) dengan
= ID x C' x B
144 x Pt
= W
as
= ft
a pendingin (W) = 39148.7764062024 kg/jam =
= 48.2216 in
= 2.375 in
= 0.4750 in
= 12 in
as = 48.2216 0.4750
144 x
= 0.803692864227757 ft2
Gs = 86308.1754406419 =
0.803692864227757
angular pitch
= 4 x
0.5 x 3.14
= 4 0.5
= 8.28495 =
2.983
= Gs x De
μs
= 107389.500743636 0.231449044586
0.060610882753419
= 410,078
jH = 400
Cp = 1.19664568392512 btu/lb.°F
k = 0.365027268782537 btu/jam.ft2. (°F/ft)
visko = 1.4377 lbm/ft.jam
f = 0.004821641823558
s = 1.0082
ώ = 1
k Cps
jH x x
De μs
400 0.365027268782537 1.19664568392512 0.3333
0.231449044585987 1.4377
593.421973417506 btu/ft2.Jam.°F
anas overall (Uc)
hi0 x ho 41.2339780609971 593.42197341751

=
hio + ho 41.2339780609971 593.42197341751
= 38.5549817594988 btu/ft2.Jam.°F
esign overall (Rd)

table 12
Uc 38.554981759498
Ud = =
(Uc x Rd) + 1 38.554981759499
= 35.794842741531
Rd Uc-Ud 2.76013901796772
=
Uc.Ud 1380.06950898386
= Q
Ud x ∆T
=
Beban panas (Q) = 1725583.72967985 j/s 6212101.4268

∆T 350 °C =
a" = 5888016.0954
23696.1858948935
= 248.4794861724 ft2
= 410,078
= 400 (Kern, 1983. fig 28)
= 1.19664568392512 btu/lb.°F
= 0.365027268782537 btu/jam.ft2. (°F/ft) (Kern, 1983. fig 1)
= 1.43768728568412 lbm/ft.jam
= 0.004821641823558 (Kern, 1983. Eq. 3.47b)
= 1.0082
= 1
= 12 in =
= 12 x L/B
= 12 x 24.5219
1.0000
= 294.262416012097 ft
= f.Gs2. IDs. (N+1) (Kern, 1983. Eq. 7.44)

5.22 x 1010 x De . s. ώ
= 0.004821641823558 11532504869.9675 4.0185

5.22 10000000000 0.231449044586
= 5.39819571121511 psi
= 0.492227124297933 cm
= 1.610 in
= 1.90 in
= 479.0000 tube
= 2.04 in2
at = Nt x a’t
144 x n
= 977.16
288
= 3.39291666666667 ft2
Gt = wt
at
= 42242.4011043061 lb/jam
3.39291666666667 ft2
= 12450.1734803309 lb/jam.ft2
Ret = Dp x Gt
μ
= 0.193789818836096 496.8235
0.060610882753419
= 1588.48262483893
Laju alir massa (Gt) = 496.8235 lb/jam.ft2

Viskositas = 6.06E-02 lbm/ft.jam
Konduktivitas (kg) = 0.0245 btu/ft.jam.F
Ƶ (panjang pipa) = 747.4265 cm
ε = 0.51
Pt = 2.375 in
f = 3.74E-02
s = 5.9338
фt = 1
V2 =
0.032
2g’
∆Pt = f x Gt2 x L x n
5.22 x 1010 x D x s x фt
= 3.77325807877293E-06
∆Pr = 4xn x
s
= 0.021571201530711
∆PT = ∆Pt +
= 3.77325807877293E-06 +
= 0.0216
Reaktor FIXED BED MULTITUBE
°C 623 K
ATM
ATM.CM3/G.MOL. K
Yi * w
0.068000244908106
0
6.8065052566206E-07
0.265069825192753
0.005699722528153
0.338770473279537
= -0.312895763807546
= 0.106820888747761
0.106820888747761
623
623
= 1611374.32892483 Cm3/s
µ Yi * µ
293.564681 151.23083488159
208.913319112 0
220.38973415 0.000980446983005
203.969297702 95.5231556299607
224.1533102 3.70322223741129
1150.990342164 250.458193195945 MIKROPOISE

0.0250 cP
konduk Yi * konduk
0.02917 0.015025128283372
0.06269 0
0.03922 1.74471848515724E-07
0.05678 0.026591219770872
0.04910 0.000811196390064
0.23695400161023 0.042427718916156 W/(M.K)
01406842311 cal/cm.s.K
24278659098 J/cm.s.K
btu/ft.jam.F
eh Colburn (Smith, p.571) dan diperoleh hubungan pengaruh rasio (D P/Dt) atau perbandingan diameter
en transfer panas konveksi pada pipa kosong.
L.atm/gmol.K
K
DENSITAS VAPOUR
LAJU ALIR MOL (KGMOBM yi BM X yi
289.5908 36.4580 1.3304 48.5051
0.0000 46.0690 0.0000 0.0000
0.0025 50.4850 0.0000 0.0006
263.2644 32.0420 1.2095 38.7544
9.2872 18.0150 0.0427 0.7686
562.1449 2.5826 88.0287

CH3Cl + H2O
0.0025 9.2872
250.1012 250.1012
250.1037 259.3883
ε= (sisa-mula)/mula 0.000000000
(KGMOL/JAM) BM yi BM X yi
289.5908 36.4580 0.5238 19.0970
263.2644 32.0420 0.4762 15.2581
552.8552 1.0000 34.3551
Menentukan laju volumetrik

LAJU ALIR MOL m3/jam
komponen (KG/JAM)(xi) densssita campuranxi/density (m3/jam)
HCL 10557.9020 3.2928 3206.338326901
CH3OH 8435.5172 3.2928 2561.789473081
∑ 18993.4192 6.5856 5768.12779998
komponen kmol/jam laju volumetrik Cao (kmol/m3)

HCL (cbo) 289.5908 5768.1278 0.05020533984
CH3OH (Cao) 263.2644 5768.1278 0.045641218036
∑ 552.8552 11536.2556 0.09584655788
No Xi
0 0
1 0.2375
2 0.475
3 0.7125
4 0.95
5 1.1875
6 1.425
7 1.6625
8 1.9
9 2.1375
10 2.375
11 2.6125
12 2.85
13 3.0875
14 3.325
15 3.5625
16 3.8
17 4.0375
18 4.275
19 4.5125
20 4.75
21 4.9875
22 5.225
23 5.4625
24 5.7
25 5.9375
26 6.175
27 6.4125
28 6.65
29 6.8875
30 7.125
ir volumetrik (m3/jam)
kgmol/m3
bo (1-Xa/(1+(εa . Xa))
0.599685551935008 kgmol/m3
3.62178331006855
kgmol/m3
479 0.49
nell and Young, 1959)
BROWNELL AND YOUNG
in
86.4125 psi
24.1107
+ 0.125
86.4125
in 0.79375 cm
m
48.2215718536654
+
- 0.2 86.4125
in 0.79375 cm
m
0.3125
= 24.1107859268327 in
3.25 = 20.8608 in
3.25 = 50.75 in
435.1724 = 46.264350319818 in
46.2644 = 7.7356 in
ft
4.9E-05 1837491.07404432
m3
ft
ft
ft
-4.6
496.823490048187 0.060610882753419 e
86308.1754406419 lbm/jam
VOLUME = MASSA PENDINGIN =

DENSITAS AIR PENDINGIN =
12.0553929634164
12
2.375
107389.500743636 lbm,/ft2.Jam
(0.5 x Pt x (0.86 Pt)) - (0.5 x 3.14 x (ODt^2)/4)

0.5 x 3.14 x ODt
2.375 0.86 2.375 -
0.5 x 3.14 x
2.77738853503185 in 0.231449044586 ft
(Kern, 1983. fig 28)
(Kern, 1983. fig 1)
(Kern, 1983. Eq. 3.47b)
0.3333
38.5549817594988
0.002 1
btu/ft2.Jam.°F
0.002
kj/jam 5888016.0954 btu/jam

662 °F
1983. fig 28)
1983. fig 1)
1983. Eq. 3.47b)
1.0000 ft
1983. Eq. 7.44)
294.262416012097
1.0082 1
= 0.193789818836096 ft
= 0.134166666666667 ft
= 0.158333333333333 ft
3.4584 lb/detik . ft2
24.5219 FT
(Kern, 1983. Eq. 7.45)

V2 (Kern, 1983. Eq. 7.46)
2g’
∆Pr (Kern, 1983. Eq. 7.47)

0.0216
34
BM * Pt
V 
RT
= 88.0287 4.9
x
0.08206 623
densitas vapour= 8.4373 g/L

ρv= 0.5267 lb/ft3
0.008437250124754 g/cm3
BM * Pt
V 
RT
= 34.3551 4.9
x
82.06 623
densitas vapour= 0.0033 g/cm3

ρv= 0.2056 lb/ft3
3.2928221882043 kg/m3
sity (m3/jam)
POLA A=dx/(1-xa).(m-xa) A*POLA

1 0.909090909090909 0.909090909090909
4 1.52055119980993 6.08220479923973
2 3.04761904761905 6.0952380952381
4 8.97615708274895 35.9046283309958
2 133.333333333333 266.666666666667
4 60.952380952381 243.809523809524
2 7.23981900452489 14.4796380090498
4 2.68343815513627 10.7337526205451
2 1.38888888888889 2.77777777777778
4 0.847345425658678 3.38938170263471
2 0.570409982174688 1.14081996434938
4 0.410019860336985 1.64007944134794
2 0.308880308880309 0.617760617760618
4 0.241027379203857 0.964109516815426
2 0.193306753654706 0.386613507309412
4 0.158474681193513 0.63389872477405
2 0.132275132275132 0.264550264550265
4 0.112074249190089 0.448296996760354
2 0.096171184708782 0.192342369417563
4 0.083427841434959 0.333711365739836
2 0.073059360730594 0.146118721461187
4 0.064510276285418 0.258041105141671
2 0.057378518916981 0.114757037833961
4 0.051367251771769 0.205469007087076
2 0.046253469010176 0.092506938020352
4 0.041867006836097 0.167468027344389
2 0.038076199995241 0.076152399990481
4 0.03477788343975 0.139111533759
2 0.031890297377023 0.063780594754046
4 0.029347970633687 0.117391882534748
1 0.027097976119909 0.027097976119909
598.877980713634
0.125
0.016149183868042
0.134166666666667
39148.7764062024 KG/JAM
1008.18210411791 KG/M3
38.8310566576214 M3/JAM
0.5 3.14 3.61 4

1.90
LOG 10 VISKOSITAS LIQUID = A +

KOMPONEN A
H2O -10.2158
KOMPONEN A
H2O -0.2758
CAIR kJ/kmol
KOMPONEN A
H2O 92.053
densitas A * B^-(1-T/Tc)^
Komponen Td
H2O 100.0000
Densitas = 1 ; (∑Xi/ρ) 1008.18210411791
1 kg/m3
S
suhu in
suhu out
viskositas LIQUID (cP)

OG 10 VISKOSITAS LIQUID = A + B/T + CT + DT2 suhu
B C D BM(kg/kgmol)
1.79E+03 1.77E-02 -1.26E-05 18.01500
KONDUKTIVITAS LIQUID (W/m.k)

LOG10=A+B [ 1-T/C]2/7 (yg organik)
K= A + BT + CT2 (INORGANIK)
B C KG/JAM XI
4.61E-03 -5.54E-06 39148.77641 1
cp cair ( j/mol.K)
(A + B T + C T2 + D T3 )
B C D KGmol/JAM
-0.039953 -0.00021103 5.3469E-07 2173.12109
DENSITAS (data densitas (yaws) g/ml

A * B^-(1-T/Tc)^n
a b n Tc
0.3471 0.2740 0.2857 647.1300
Kg/m3 62.9408 lb/ft3
0.06243 lbm/ft3
1.00818210411791
GAS kJ/kmol
KOMPONEN A
HCL 29.244
(CH3)2O 34.668
CH3CL 27.385
CH3OH 40.046
H2O 33.933
Total
Densitas (fluida dingin)

Komponen mOL (Kg/jam)
HCl 289.59082
(CH3)2O 0.00000
CH3CL 0.00250
CH3OH 263.26438
air 9.28716
TOTAL 562.14485
BMZAT
densitaszat R *T
spgr  
denstasrefrensi BMref *
R *T
R 0.08206
tzat 289.5908
bm zat 34.08526
p zat 4.9
S= 5.9338
300 k
338 k
319
(kg/jam) (kmol/jam) Xi,f µ Xi,f*µ
39148.77641 2173.12109 1.00000 0.59409 0.59409
1.4377
K XI . K
0.63176 0.631764 W/(M.K)
0.365027268782537 BTU/FT.JAM.F
T + C T2 + D T3 )
Xi cP(Kj/kmol.k) (Xi . Cp )/bm
1 90.25939818968 5.01023581402609 KJ/KG.K
1.19664568392512 BTU/LBM.°F
g/ml
319.0000 k
massa (Kg/jam) Fraksi (xi) p, Kg/m 3
Xi / pi
39148.77641 1.000 1008.1821 0.00099
cp gas ( j/mol.K)
(A + B T + C T2 + D T3 + E T4 )
B C D E BM
-0.0012615 1.121E-06 4.9676E-09 -2.4963E-12 36.458
0.070293 0.0001653 -1.7675E-07 4.9313E-11 46.069
0.026036 0.0001032 1.0887E-07 3.1642E-11 50.485
-0.038287 0.00024529 -2.1679E-07 5.9909E-11 32.042
-0.0084186 2.9906E-05 1.7825E-08 3.6934E-12 18.015
suhu tc 623.0000 k
Fraksi (Yi) BM YI*BM
0.515 36.4580 18.78146
0.000 46.0690 0.00000
0.000 50.4850 0.00022
0.468 32.0420 15.00595
0.017 18.0150 0.29762
1.000 34.08526
BMZAT * Pzat
szat R * Tzat BMzat* Pzat * Rref * Tref
 
frensi BMref * Pr ef BMref * Pr ef * Rzat * Tzat
R * Tre
L.atm/gmol.K R 0.08206 L.atm/gmol.K

k tref 298 k
g/gmol bm ref 28.964 g/gmol
atm p ref 1 atm
cp
lb/ft.jam
+ E T4 )
KGmol/JAM Xi cP(Kj/kmol.k) (Xi . Cp )/bm
289.5908164 0.51515337052 29.71831256415 0.419921
0 0 107.3080543539 0
0.002500812 4.4486962E-06 114.7522635006 1E-05
263.2643786 0.46832124592 68.00153131155 0.993901
9.287158523 0.01652093486 45.16214991095 0.041417
562.1448544 1 1.455249 KJ/KG.K

0.347572 BTU/LBM.°F
tm/gmol.K
Heater-01 ( suh
Kode : H-01
Fungsi : Menaikkan temperatur umpan STRIPPER dari 30
Tipe : DOUBLE PIPE
Dasar Perancangan
Suhu bahan masuk :
Tekanan masuk :
Laju alir :
Bahan Konstruksi :
1. Data Perhitungan
Beban Panas (Q) =
=
=
Fluida Panas = Steam

Massa Fluida Panas =
=
Th in(T1) =
Th Out(T2) =
Fluida Dingin = ASAM KLORIDA

Massa Fluida dingin =
=
Tc in(t1) =
Tc Out(t2) =
2. Menghitung LMTD
Fluida Panas (˚F)
392 Suhu tinggi
392 Suhu rendah
0 Selisih
∆t LMTD =
Aliran dari fluida memiliki viskositas < 1 cP

Tc = T1 + T2
2
= 392
2
= 392
tc = t1 + t2
2
= 86
2
= 105.485
Menentukan viskositas masing-masing Fluida

Berdasarkan Yaws 1999, tabel 21-1 halaman 474 diperoleh :
Annulus = Steam
Pada, T = 392
µ = 0.0163
0.0395
Pipa = Fluida Dingin
Pada, T = 105.485
µ = 0.53194
1.287294
Menghitung Luas Total Perpindahan Panas

Fluida Dingin = AQUOOUS SOLUTION
Berdasarkan Kern 1965, tabel 8 halaman 840 diperoleh :
UD = 200-700 Btu/jam Ft^2 ˚F
Dipilih = 200
A =
Karena nilai A < 200ft^2, maka alat perpindahan panas yang digunakan adalah tipe Double Pipe Exchanger
Berdasarkan Kern 1965, tabel 6.2 halaman 110 Digunakan hairpin dengan IPS pipa 4 x 3
Annulus
IPS (in) 4
Sch. No 40
OD (in) 4.5
ID (in) 4.026
Annulus : Hot Fluid
4. Menghitung Flow Area (a)
D2 = ID Annulus
= 4.026
= 0.3355
D1 = OD Pipe
= 3.5
= 0.2917
aa = π (D2^2 - D1^2)
4
= 3.14
4
= 0.021580282361111
Equivalent Diameter (De)

Berdasarkan Kern 1965, persamaan 6.3 halaman 105 diperoleh:
De = (D2^2 - D1^2)
D1
= 0.1126
0.2917
= 0.09425419047619
5. Menghitung mass velocity

Ga = W
aa
=
6. Reynold Number (Rea)

Pada Tc = 392
µ Steam = 0.0395
De = 0.09425419047619
Rea = De x Ga
µ
= 0.09425419047619
0.039491093143781
= 575,295
7. Menentukan Heat Transfer

Berdasarkan Kern 1950, fig. 24 halaman 834 diperoleh:
jH = 1000
8. Menghitung Thermal Konduktivity

Tc = 392
Berdasarkan yaws 1999, halaman 552 diperoleh:
K = 0.019676459902843
Cp = 0.449878669779053
µ Steam = 0.039491093143781
Cp X µ ⅓ 0.449878669779053
K = 0.019676459902843
= 0.966531170033359
9. Menghitung ho
Berdasarkan kern 1950, persamaan 6.15b halaman 114 diperoleh:
ho= jH k Cp X µ
De K
1000 0.019676459902843
0.09425419047619
201.772586618454 Btu/jam ft ˚F
11. Menghitung Clean Overall Coefficient (Uc)

Uc =
12. Menghitung Design Overall Coefficient (Ud)

Berdasarkan kern 1950, tabel 12 halaman 845 diperoleh:
Rd = 0.001 jam ft^2 ˚F /Btu
1
Ud
1
Ud
1
Ud
Ud
13. Menghitung Luas Perpindahan Panas yang Dibutuhkan

Berdasarkan kern 1950, persamaan 6.11 halaman 107 diperoleh:
A =
=
Berdasakan kern 1950, tabel 11 dengan nilai IPS : 3 in, didapatkan nila
Panjang pipa =
Hairpin terdiri dari 2 pipa (n=2) maka jumlah hairpin yang diperlukan :
Hairpin =
Koreksi panjang P :
14. Menghitung Luas Perpindahan Panas yang Tersedia Sebenarnya

A =
=
=
15. Menghitung Actual Design Overall Coefficient (UD aktual)

UD aktual =
16. Menghitung Dirt factor (Rd)

Rd
17. MenghitungNre dan Friksi
De' : Untuk Pressure Drop
De : Untuk perpindahan panas
De' = (D2 - D1)

= 0.3355
= 0.0438
re,a' = De'
µ
= 0.0438
0.0394910931
= 267543.284609223
Berdasarkan Kern 1950, persamaan 3.47b Hal 53 diperoleh:

f = 0.0035
= 0.0035
= 0.0048870701443
S = 0.3904
ρ = 24.373370371776
18. Menentukan ΔP karena panjang pipa

∆Fa = 4 x F x Ga^2 x L
2 x g x ρ^2 x de'
= 4
2
= 136291017499.23
21769174040.8926
= 6.26073443315821
Va = Ga
3600
= 241039.77427
3600
= 2.74707567453976
ΔFt = 1x
= 1
= 0.117180508721244
Pressure drop pada Anulus:
∆Pa = ∆Fa
144
= 6.26073443315821
144
= 1.07952279915355
∆Pa untuk Steam < 10 psi (memenuhi)

Heater-01 ( suhu 200)
tur umpan STRIPPER dari 30˚C menjadi 90˚C
30 C
1 atm
56031.5476 KG/JAM
Carbon Steel SA 285 Grade C
1270567.6672 J/S
4574043.6021 kj/jam cp 1.06247675561829
4335415.7474 btu/jam 221067.68512162 btu/hr
2359.4571 kg/jam
5201.70638916637 lb/jam
200 ˚C = 392
200 ˚C = 392
ASAM KLORIDA DAN AIR

56031.5476 kg/jam
123528.270474923 lb/jam
30 ˚C = 86
51.65 ˚C = 124.97
Fluida Dingin (˚F) Selisih (˚F) ∆t R

124.97 267.03 ∆t2 S
86 306 ∆t1 FT
38.97 -38.97 ∆t2 - ∆t1 delta T
∆t2 - ∆t1
ln (∆t2 /∆t1)
-38.97 ˚F
ln 1,0986 ˚F
286.072749029455 ˚F
+ 392
2
˚F
+ 124.97
2
˚F
˚F = 474.7400 K
cP
lb/ft.jam
˚F = 314.2916 K
cP
lb/ft.jam
(µ cP < 0,2 cP )
dipilih 100-200 karena viskositas dibawah 0,5 cP

Btu/jam Ft^2 ˚F
Qs
UD x ∆t LMTD
4335415.7474
200 x 286.07274902946
75.7747069945804 ft^2
Double Pipe Exchanger
Inner Pipe shell and tube

IPS (in) 3
Sch. No 40
OD (in) 3.5
ID (in) 3.068
: Hot Fluid Inner Pipe : Cold Fluid
in
ft
in
ft
0.1126 0.0851
4
ft^2
- 0.0851
0.2917
ft
5201.70638916637 lb/jam
0.021580282361111 ft^2
241039.774277474 lb/jam ft^2
˚F
lb/ft.jam
ft
241039.774277474
0.039491093143781
˚F
btu/jam ft ˚F
btu/lb ˚F
lb/ft.jam
0.039491093143781 ⅓
0.019676459902843
⅓ µ 0.14
µw
0.966531170033359 1
Uc)
hio x ho
hio + ho
1430.80910443021 x 201.77258661846
1430.80910443021 + 201.77258661846
176.835288268287 Btu/jam ft^2 ˚F
(Ud)
845 diperoleh:
1
= + Rd
Uc
= 1
+ 0.001
176.835288268287
= 0.006654979895658
= 150.26341411677 Btu/jam ft^2 ˚F

200
ang Dibutuhkan
laman 107 diperoleh:
Q
Ud x ∆t LMTD
4335415.7474
200 x 286.07274902946
75.7747069945804 ft^2
ai IPS : 3 in, didapatkan nilai a" = 0.917 ft^2/ft

L = A
a"
= 75.77470699458 ft^2
0.917 ft^2/ft
= 82.633268260175 lin ft
Panjang hairpin : 12, 15, dan 20 ft
Diambil Lh = 20 ft
h hairpin yang diperlukan :
L
2 x Lh
82.6332682601749
2 x 20
2.06583170650437 ≈ 3 buah
L koreksi = (2 x Lh) x jumlah hairpin

= (2 x 20 ft) x 3
= 120 ft linier
ang Tersedia Sebenarnya

L x a"
120 x 0.917
110.04 Ft^2 10.2230 m2
fficient (UD aktual)

Q
A x ∆t LMTD
4335415.7474
110.04 x 286.07274902946
137.722113766958 Btu/jam ft^2 ˚F
= Uc - Ud
Uc x Ud
= 176.835288268287 - 137.722113766958
176.835288268287 x 137.722113766958
= 0.001606018157945 Btu/jam ft^2 ˚F
Pressre Drop
- 0.2917
ft
x Ga
µ
x 241039.774277474
0.039491093143781
+ 0.264
(Re,p)^0,42
+ 0.264
190.329235392231
lb/ft3
0.0048870701443 58100172783.7356 120

418000000 594.061183279766 0.0438
ft
Ga
x S
241039.774277474
x 24.373370371776
fps
Va^2
2 x g'
7.54642476164809
2 x 32.2
ft
+ Ft
S
144
+ 0.117180508721244
24.373370371776
144
psi
si (memenuhi)
GAS
KOMPONEN
HCL
(CH3)2O
CH3CL
CH3OH
H2O
densitas
Komponen
CH3OH
H2O
ch3cl
hcl
dme
˚F 474.74 K
˚F 474.74 K viskositas ga
A+
KOMPONEN
HCL
(CH3)2O
CH3CL
˚F 303.38 K CH3OH
˚F 325.2032 K H2O
0 R=(T1-T2)/(t2-t1) LOG 10 V
0.127352941176471 S=(t2-t1)/(T1-t1) KOMPONEN
0.96 FT=fig.13 hal;328 HCL
297.992446905682 delta T=lmtd/ft (CH3)2O
CH3CL
CH3OH
H2O
Komponen
H2O
Total
Komponen
HCl
H2O
Total
Komponen
HCl
H2O
Total
Komponen
H2O
Total
KOMPONEN
H2O
TOTAL
KOMPONEN
HCL
H2O
TOTAL
Inner Pipe : Cold Fluid
D = ID Pipe
= 3.068 in
= 0.2557 ft
ap = π (D^2)
4
= 3.14 0.0654
4
= 0.051311873888889 ft^2

Gp = W 123528.270474923
ap 0.051311873888889
= 2407401.27211903
6. Reynold Number (Rep)

Pada tc = 105.485 ˚F
µ light organik = 1.287294 lb/ft.jam
D = 0.2557 ft
Rep = D x Gp
µ
= 0.2557 2407401.27211903
1.28729370852736
= 478,129

jH = 900

Tc = 105.485 ˚F
K = 0.269985495839836 btu/jam ft ˚F
Cp = 1.06247675561829 btu/lb ˚F
µ campuran = 1.28729370852736 lb/ft.jam
Cp X µ ⅓ 1.06247675561829 1.28729370852736
K = 0.269985495839836
= 1.71745572573294
9. Menghitung hi
Berdasarkan kern 1950, persamaan 6.15a halaman 114 diperoleh:
hi = jH k Cp X µ
D K
= 900 0.269985495839836
0.2557
= 1632.2789652887 Btu/jam ft ˚F
10. Menghitung hio

hio = hi ID
OD
= 1632.2789652887 3.068
3.5
= 1430.80910443021 Btu/jam ft ˚F
Pressre Drop
Untuk re,p = 478,129

f = 0.0035 +
= 0.0035 +
= 0.004586913664388
ρ = 0.873706954660106
= 54.5437777655211 lb/ft^3
18. Menentukan ΔP pipa

∆Fp = 4 x F x G0^2 x L
2 x g x ρ^2 x D
= 4 0.004586913664388
2 418000000
= 12760237994146.4
635873630731.316
= 20.067254525826 ft
∆Pp = ∆Fp x
144
= 20.067254525826 x
144
= 7.60099910570001 psi
∆Pp untuk fluida < 10 psi (memenuhi)
cp gas ( j/mol.K)
kJ/kmol (A + B T + C T2 + D T3 + E T4 )
A B C D
29.244 -0.0012615 1.121E-06 4.9676E-09
34.668 0.070293 0.0001653 -1.7675E-07
27.385 0.026036 0.0001032 1.0887E-07
40.046 -0.038287 0.00024529 -2.1679E-07
33.933 -0.0084186 2.9906E-05 1.7825E-08

A * B^-(1-T/Tc)^n
Td a b n
64.7000 0.2720 0.2719 0.2331
100.0000 0.3471 0.2740 0.2857
-23.7000 0.3582 0.2611 0.2869
85.0500 0.4413 0.2696 0.3187
-24.5000 0.2639 0.2633 0.2806

A + B T + CT2
A B C
-9.118 5.55E-01 -1.11E-04
-4.276 3.03E-01 6.35E-05
-1.374 3.86E-01 -4.87E-05
-14.236 3.89E-01 -6.28E-05
-36.826 4.29E-01 -1.62E-05
viskositas LIQUID (micropoise)

LOG 10 VISKOSITAS LIQUID = A + B/T + CT + DT2
A B C D
-1.515 1.95E+02 3.07E-03 -1.38E-05
-7.4844 5.84E+02 2.78E-02 -4.04E-05
-7.3473 8.54E+02 1.95E-02 -2.35E-05
-9.0562 1.25E+03 2.24E-02 -2.35E-05
-10.2158 1.79E+03 1.77E-02 -1.26E-05
VISKOS fase gas (steam)

BM(kg/kgmol) (kg/jam) (kmol/jam) Xi,f
18.01500 2359.45714 130.97181 1.00000
2359.45714 130.97181 1.00000

viskositas fluida masuk (dingin)
BM(kg/kgmol) (kg/jam) (kmol/jam) Xi,f
36.45800 18490.41071 507.17019 0.19574
18.01500 37541.13689 2083.88215 0.80426
56031.54760 2591.05234 1.00000
konduktivitas FLUIDA DINGIN

KG/JAM XI K XI . K
18490.41071 0.33 0.14386 0.047473
37541.13689 0.67 0.62656 0.419799
56031.5476022728 1 0.467272
0.269985495839836
konduktivitas FLUIDA panas

KG/JAM XI K XI . K
2359.45714 1 0.03405 0.034055
2359.45713509193 1 0.034055
0.019676459902843
CP FLUIDA panas (steam)

KGMOL/JAM Xi cP(j/kmol.k) (Xi . Cp)/BM
130.97181 1 33.933 1.88359700249792
130.971808775572 1 1.88359700249792
0.449878669779053
CP FLUIDA DINGIN (fluida masuk)

KGmol/JAM Xi cP(Kj/kmol.k) (Xi . Cp )/bm
507.17019 0.195739075148962 71.1576019223916 0.382037500414366
2083.88215 0.804260924851038 91.0861514356088 4.06644642768384
2591.05233570342 1 4.44848392809821
1.06247675561829
lb/jam
ft^2
lb/jam ft^2
w/mK
⅓
⅓ µ
µw
1.71745572573294 1
0.264
(Re,p)^0,42
0.264
242.889576835657
5795580885000.34 120
2975.0237 0.2557
54.5437777655211
cp cair ( j/mol.K)
CAIR kJ/kmol (A + B T + C T2 + D T3 )
E KOMPONEN A B
-2.4963E-12 HCL 73.993 -0.12946
4.9313E-11 (CH3)2O 48.074 0.56225
3.1642E-11 CH3CL 11.381 0.62328
5.9909E-11 CH3OH 40.152 0.31046
3.6934E-12 H2O 92.053 -0.039953
ensitas (yaws) g/ml

303.0000 k
Tc ρ(g/ml) kg/m3 ρ(g/ml) 25 C
512.5800 0.7828 782.8067 0.787
647.1300 1.0230 1023.0130 1.027
416.2500 0.9028 902.8000 0.913
324.6500 0.7673 767.3262 0.796
400.1000 0.6472 647.1724 0.655

A + B T + CT2
KOMPONEN A B C
HCL 0.00119 4.48E-05 2.10E-10
(CH3)2O -0.0315 1.50E-04 1.39E-09
CH3CL -0.00185 2.03E-05 7.32E-08
CH3OH 0.00234 5.43E-06 1.32E-07
H2O 0.00053 4.71E-05 4.96E-08

LOG10=A+B [ 1-T/C]2/7 (yg organik)
KOMPONEN A B C
HCL 0.8045 -2.10E-03 -2.32E-16
(CH3)2O -1.5099 0.9936 4.00E+02
CH3CL -1.7528 1.3686 4.16E+02
CH3OH -1.1793 0.6191 5.13E+02
H2O -0.2758 4.61E-03 -5.54E-06
µ Xi,f*µ
163.1863 163.18634
163.18634 163.18634 micropoise

0.0163 cP
µ Xi,f*µ
0.05116 0.01001
0.64895 0.52193
0.70011 0.53194 CP
W/(M.K)
BTU/FT.JAM.F
W/(M.K)
BTU/FT.JAM.F
kj/kg.k
btu/lbm.°F
KJ/KG.K
BTU/LBM.°F
Densitas shell (fluida dingin) suhu
Komponen massa (Kg/jam)Fraksi (xi)
HCl 18490.41071 0.330
air 37541.136894 0.670
TOTAL 56031.5476 1.000
Densitas = 1 ; (∑Xi/ρ) 873.70695466 Kg/m3
1 kg/m3 0.06243
ir ( j/mol.K)
(A + B T + C T2 + D T3 )
C D
-7.898E-05 2.6409E-06
-0.0023915 4.4614E-06
-0.0024353 3.8333E-06
-0.0010291 1.4598E-06
-0.00021103 5.3469E-07
tc 314.2916 k
p, Kg/m 3
Xi / pi V (m3)
683.4136 0.00048 27.0559599206847
1012.5765 0.00066 37.0748648408859
0.00114 64.1308247615706
54.5455 lb/ft3 densitaszat

spgr  
denstasrefrensi
lbm/ft3
Densitas tube (fluida panas) suhu Tc 474.7400 k
Komponen mol (Kgmol/jam) Fraksi (Yi) BM Yi * BM
air 130.971808775572 1.000 18.0150 18.01500
TOTAL 130.9718 1.000 18.01500
BMZAT * Pzat
densitaszat R * Tzat BMzat* Pzat * Rref * Tref
gr   
denstasrefrensi BMref * Pr ef BMref * Pr ef * Rzat * Tzat
R * Tre
R 0.08206 L.atm/gmol.K R
tzat 474.7400 k tref
bm zat 18.01500 g/gmol bm ref
p zat 1 atm p ref
S= 0.390424
BM * Pt
V 
RT
0.462431 gr/l
0.0005 gr/cm3
0.462431 KG/M3
ref * Tref 0.02887 lbm/ft3
Rzat * Tzat
0.08206 L.atm/gmol.K
298 k
28.964 g/gmol
1 atm
Heater-02 SUHU 20
Kode : H-02
Fungsi : Menaikkan temperatur umpan REAKTOR dari 248˚C
Tipe : shel and tube
Dasar Perancangan
Suhu bahan masuk :
Tekanan masuk :
Laju alir :
Bahan Konstruksi :
1. Data Perhitungan
Beban Panas (Q) =
=
=

=
Th in(T1) =
Th Out(T2) =
Fluida Dingin = ALIRAN 12

=
Tc in(t1) =
Tc Out(t2) =
2. Menghitung LMTD
Fluida Panas (˚F)
698 Suhu tinggi
698 Suhu rendah
0 Selisih
∆t LMTD =
=
3. Menghitung Suhu Caloric (Tc dan tc)
Tc = T1 + T2
2
= 698
2
= 698
tc = t1 + t2
2
= 478.4
2
= 570.2

Annulus = Steam
Pada, T = 698
µ = 0.0234
0.0565
Pada, T = 570.2
µ = 0.02325
0.0563

Fluida Dingin = gases
UD = 5-50 Btu/jam Ft^2 ˚F
Dipilih = 50
A =
=
Karena nilai A > 200ft^2, maka alat perpindahan panas yang digunakan adalah tipe shell and tube
Dari uku Kern tabel 10 hal.843, spesifikasi tube direncanakan
Laju alir fluida dingin

Laju alir fluida panas (wt)
Dari uku Kern tabel 10 hal.843, spesifikasi tube direncanakan sebagai berikut
OD 0.750 in
BWG 18
ID 0.652 in
Flow area per tube (A't) 0.334 in^2
Surface per in ft (Ao) 0.1963 ft^2
Panjang tube 16 ft
Pitch 1.000 in, square
Nt = A / (L.Ao) 156.837881426636 =
Dari uku Kern tabel 9 hal.842, spesifikasi HE direncanakan sebagai berikut
Shell
ID 17.25 in
B 5 in
Pass 1
Shell ID dari fig.28 Hal.838 (de) 0.95 0.079166666666667
A koreksi = Nt x L x Ao 521.3728 ft^2
Ud Kor. = Q / (A kor. x ∆t) 47.2403
C' = pitch - OD 0.2500
Bagian tube (steam)
A't 0.334 in^2
At = (Nt*A't)/(144*n) 0.192513888888889 ft2
Gt = Wt/At 219425.213152734 lb/ft2.jam
Shell side/fluida dingin

aa = ID
= 0.149739583333333

Ga = W
aa
=

Pada Tc = 698
µ air pendingin = 0.056528
De = 0.079166666666667
Rea = De x Ga
µ
= 0.079166666666667
0.056528365598716
= 120,197

Dari buku kern fig.28 hal 838 diperoleh jh =
jH = 230

Tc = 698
K = 0.029838
Cp = 0.449878669779053
Cp X µ ⅓ 0.449878669779053
K = 0.029838
ho = = 0.948121029440716
= 9. Menghitung ho
= jH k Cp X µ
De K
230 0.029838
0.948121029440716
0.079166666666667
82.1901454940264 Btu/jam ft ˚F
10. tube well temperature

tw= tc+((ho/Øs)/((hio/Øt)+(ho/Øs))*(Tc- tc)
570.2
619.353291490089
11. At tw 619.353291490089
Øs =(µ/µw)^0,14
12. corrected coeficient,hio = (ho/Øs) x Øs

= 83.1182470187358
Uc = hio x ho
hio + ho
= 131.506644196131
131.506644196131
= 50.5789077860395

a" 0.1963
Total surface A 492.5964
Ud Q 2500726.2054
A.delta t 50014.5241089037
50
15. Menghitung dirt factor (Rd)

Rd Uc-Ud 0.578907786039544
Uc.Ud 2528.94538930198
SUMMARY
Uc 50.5789077860395 Btu/jam ft^2 ˚F

Ud 50 Btu/JAM ft^2 oF
Rd Calculated 0.000228913 hr ft^2 oF/Btu
Rd Required 0.01 hr ft^2 oF/Btu

1 Res 120,197
sg = densitas f 0.0013
zat/ ensitas s 0.2869
standar (aor
1000 kg/m3) Ds' 1.4375
2 No. Of crosses N+1

3 ΔPs f x (Gs^2) x Ds' x (N+1)
(5.22x10^10 x DE x s x Os)
0.44089708381773
∆P < 2 psi
Heater-02 SUHU 200
mperatur umpan REAKTOR dari 248˚C menjadi 350˚C
248 C
4.9 atm
19160.8536 KG/JAM
732880.5463 J/S
2638369.9666 kj/jam
2500726.2054 btu/jam
5829.36360274604 kg/jam
12851.531585886 lb/jam
370 ˚C = 698
370 ˚C = 698
ALIRAN 12
19160.8536 kg/jam
42242.4011043061 lb/jam
248 ˚C = 478.4
350 ˚C = 662

662 36 ∆t2 S
478.4 219.6 ∆t1 FT
183.6 -183.6 ∆t2 - ∆t1 delta T
∆t2 - ∆t1
ln (∆t2 /∆t1)
-183.6 ˚F
ln 1,0986 ˚F 0.1639
101.5325 ˚F -1.8082887711793
+ 698
2
˚F
+ 662
2
˚F
˚F = 646.1000 K
cP
lb/ft.jam
˚F = 574.5320 K
cP
lb/ft.jam
(µ < 0,5 cP)

Btu/jam Ft^2 ˚F
Qs
UD x ∆t LMTD
2500726.2054
50 x 101.53245594744
492.5964 ft^2
h tipe shell and tube
kg/jam lbm/jam
19160.85362 42242.4011043061
5829.36360 12851.531585886
166 Nt = Jumlah tube, dibulatkan ke atas (hal.842)
Tube
Jumlah tube 166
OD 0.7500 in =
ID 0.652 in =
ft BWG 18
Pass 2
A't 0.334 in^2
eam)
de/fluida dingin
ft^2
12851.531585886 lb/jam
0.149739583333333 ft^2
85825.8805040037 lb/jam ft^2
˚F
lb/ft.jam
ft
85825.8805040037
0.056528365598716
˚F 646.1 K
btu/jam ft ˚F
btu/lb ˚F
lb/ft.jam
0.056528 ⅓
0.029838
⅓ µ 0.14
µw
1
hio/Øt)+(ho/Øs))*(Tc- tc) eq (5,1)

82.1901454940264 127.8
213.696789690157
F 602.0578 K
F µw=0,56 x 2,42
0.052172 lb/ft.jam
1
eq 6.36
btu/jam.ft2.°F
x 82.1901454940264
+ 82.1901454940264
Btu/jam ft^2 ˚F
ft^2/linft
ft2 45.7637 m2
BTU/JAM
FT.°f
Btu/JAM ft^2 oF
0.000229 Btu/hr ft^2 oF
Rd Uc-Ud 0.0002289127272
Uc.Ud
Pressre Drop
1
ft2/in2 fig 29
ft
2
12L/B
38.4
x DE x s x Os) 3
psi
GAS 4
cp gas ( j/mol.K)
GAS kJ/kmol (A + B T + C T2 + D
KOMPONEN A B
HCL 29.244 -0.0012615
(CH3)2O 34.668 0.070293
CH3CL 27.385 0.026036
CH3OH 40.046 -0.038287
H2O 33.933 -0.0084186
densitas
Komponen
HCL
(CH3)2O
ch3cl
CH3OH
H2O
˚F 646.1 K
˚F 646.1 K viskositas gas (micro
A + B T + CT2
KOMPONEN
HCL
(CH3)2O
CH3CL
˚F 523.124 K CH3OH
˚F 625.94 K H2O
visk
0 R=(T1-T2)/(t2-t1) LOG 10 VISKOSIT
0.836065573770492 S=(t2-t1)/(T1-t1) KOMPONEN
CH3CL
CH3OH
H2O
VISKOS (steam)
233.5883 micropoise
0.0234 cP
viskositas fluida masuk

Komponen BM(kg/kgmol) (kg/jam)
HCl 36.45800 10557.90199
(CH3)2O 46.06900 0.00000
CH3CL 50.48500 0.12625
CH3OH 32.04200 8435.51722
H2O 18.01500 167.30816
Total 19160.85362

Komponen KG/JAM XI
HCl 10557.90199 0.551014176922817
(CH3)2O 0 0
CH3CL 0.126253478844047 6.58913644236E-06
CH3OH 8435.51721846989 0.440247464254282
H2O 167.30816 0.008731769686459
Total 19160.8536184495 1

Komponen KG/JAM XI
H2O 5829.36360274604 1
Total 5829.36360274604 1
Tube
0.0625 ft L/D 294.478527607362

0.0543 ft
Tube Side/fluida panas

ap = 0.192513888888889 ft^2

Gp = W 42242.4011043061
ap 0.192513888888889
= 219425.213152734

Pada Tc = 570.2 ˚F
µ organik = 0.056255 lb/ft.jam
D = 0.0543 ft
Rep = D x Gp
µ
= 0.0543 219425.213152734
0.056255301706445
= 211,929

jH = 450

Tc = 570.2 ˚F
K = 0.021246814427813 btu/jam ft ˚F
Cp = 0.239935489065647 btu/lb ˚F
Cp X µ ⅓ 0.239935489065647 0.0563
K = 0.021246814427813
= 0.859649419726537
9. Menghitung hi
hi = jH k Cp X µ
D K
= 450 0.021246814427813 0.859649419726537
0.0543
= 151.27298028696 Btu/jam ft ˚F
10. Menghitung hio

hio = hi ID
OD
= 151.27298028696 0.0543
0.0625
= 131.506644196131 Btu/jam ft ˚F
11. At tw 602.0578 K
Øt =(µ/µw)^0,14 1
12. corrected coeficient,hio = (ho/ØT) x ØT

= 150.360039347842 btu/jam.ft2.°F
Densitas (fluida dingin) suhu tc
Komponen mOL (Kg/jam) Fraksi (Yi) BM
HCl 289.59082 0.515 36.4580
(CH3)2O 0.00000 0.000 46.0690
CH3CL 0.00250 0.000 50.4850
CH3OH 263.26438 0.468 32.0420
air 9.28716 0.017 18.0150
TOTAL 562.1449 1.000
BMZAT * Pzat
densitaszat R * Tzat BMzat* Pzat * Rref * Tre
spgr   
denstasrefrensi BMref * Pr ef BMref * Pr ef * Rzat * Tz
R * Tre
R
tzat
bm zat
p zat
S=
densitas
For Ret 211,929
f 0.00012 fig 26
s 2.9909
ΔPt f x (Gt^2) x panjang tube x passes

(5.22x10^10 x ID x s x Ot)
= 0.021927552835009
Gt 219,425 V^2/2g' 0.0061
ΔPn (4 x passes /s) *(v^2/2g)

0.016315997351158
∆P = ∆Pt + ∆Pn eq. 7.47

0.038243550186167 psi
∆P < 2 psi GAS

s ( j/mol.K)
(A + B T + C T2 + D T3 + E T4 ) CAIR
C D E KOMPONEN
1.121E-06 4.9676E-09 -2.4963E-12 HCL
0.0001653 -1.7675E-07 4.9313E-11 (CH3)2O
0.0001032 1.0887E-07 3.1642E-11 CH3CL
0.00024529 -2.1679E-07 5.9909E-11 CH3OH
2.9906E-05 1.7825E-08 3.6934E-12 H2O

A * B^-(1-T/Tc)^n
Td a b n Tc
85.0500 0.4413 0.2696 0.3187 324.6500
-24.5000 0.2639 0.2633 0.2806 400.1000
-23.7000 0.3582 0.2611 0.2869 416.2500
64.7000 0.2720 0.2719 0.2331 512.5800
100.0000 0.3471 0.2740 0.2857 647.1300
A B C
-9.118 5.55E-01 -1.11E-04
-4.276 3.03E-01 6.35E-05
-1.374 3.86E-01 -4.87E-05
-14.236 3.89E-01 -6.28E-05
-36.826 4.29E-01 -1.62E-05
viskositas LIQUID (CP)

A B C D
-1.515 1.95E+02 3.07E-03 -1.38E-05
-7.4844 5.84E+02 2.78E-02 -4.04E-05
-7.3473 8.54E+02 1.95E-02 -2.35E-05
-9.0562 1.25E+03 2.24E-02 -2.35E-05
-10.2158 1.79E+03 1.77E-02 -1.26E-05
289.59082 0.51515 273.10760 140.69230
0.00000 0.00000 190.55864 0.00000
0.00250 0.00000 204.49174 0.00091
263.26438 0.46832 188.74111 88.39147
9.28716 0.01652 204.30082 3.37524
562.14485 1.00000 1061.19992 232.45992 MIKROPOISE

0.0232 cP
INGIN
K XI . K
0.02698 0.014869
0.05532 0.000000
0.03398 0.000000
0.04888 0.021520
0.04394 0.000384
0.036772 W/(M.K)
0.0212 BTU/FT.JAM.F
panas
K XI . K
0.05164 0.051642
0.051642 W/(M.K)
0.0298 BTU/FT.JAM.F
lb/jam
ft^2
lb/jam ft^2
w/Mk 574.532 k
0.14
⅓ µ Øt
µw sama
1
µw=1,5 x 2,42
0.058741 lb/ft.jam
eq 6.37
574.5320 k Densitas (fluida panas)
YI*BM Komponen mol (Kg/jam)
18.78146 air 323.5838802523
0.00000 TOTAL 323.5839
0.00022
15.00595 R 0.08206
0.29762 tzat 646.1000
34.08526 bm zat 18.01500
p zat 1
zat* Pzat * Rref * Tref S= 0.2869

ref * Pr ef * Rzat * Tzat
0.08206 L.atm/gmol.K R 0.08206

574.5320 k tref 298
34.08526 g/gmol bm ref 28.964
4.9 atm p ref 1
2.9909
3.54255790673322 kG/L DENSITAS ZAT 3.54255790673322 g/L
0.2212 lb/ft3
3.54255790673322 kg/M3
Va = Ga
3600
fig 27 = 219425.21315273
3600
= 13.479666285005
Va^2
2 x g'
13.4796662850045
2 x 32.2
0.209311588276467
cp cair ( j/mol.K)
kJ/kmol (A + B T + C T2 + D T3 )
A B C D
73.993 -0.12946 -7.898E-05 2.6409E-06
48.074 0.56225 -0.0023915 4.4614E-06
11.381 0.62328 -0.0024353 3.8333E-06
40.152 0.31046 -0.0010291 1.4598E-06
92.053 -0.039953 -0.00021103 5.3469E-07
s) g/ml
303.0000 k
ρ(g/ml) kg/m3 ρ(g/ml) 25 C
0.7673 767.3262 0.796
0.6472 647.1724 0.655
0.9028 902.8000 0.913
0.7828 782.8067 0.787
1.0230 1023.0130 1.027

A + B T + CT2
KOMPONEN A B C
HCL 0.00119 4.48E-05 2.10E-10
(CH3)2O -0.0315 1.50E-04 1.39E-09
CH3CL -0.00185 2.03E-05 7.32E-08
CH3OH 0.00234 5.43E-06 1.32E-07
H2O 0.00053 4.71E-05 4.96E-08

LOG10=A+B [ 1-T/C]2/7 (yg organik
KOMPONEN A B C
HCL 0.8045 -2.10E-03 -2.32E-16
(CH3)2O -1.5099 0.9936 4.00E+02
CH3CL -1.7528 1.3686 4.16E+02
CH3OH -1.1793 0.6191 5.13E+02
H2O -0.2758 4.61E-03 -5.54E-06
CP FLUIDA DINGIN
KOMPONEN KGmol/JAM Xi cP(Kj/kmol.k) (Xi . Cp )/bm
HCL 289.59082 0.515153370515951 29.1312680855557 0.4116262807
(CH3)2O 0.00000 0 43.4560572535764 0
CH3CL 0.00250 4.448696246157E-06 31.2747226979851 2.75590257E-06
CH3OH 263.26438 0.468321245923592 38.4735460141564 0.56232379391
H2O 9.28716 0.01652093486421 33.403359823787 0.03063306866
TOTAL 562.1448543534 1 1.00458589917

0.23993548907
CP FLUIDA panas
KOMPONEN KGMOL/JAM Xi cP(j/kmol.k) (Xi . Cp)/BM
H2O 323.5838802523 1 33.933 1.8835970025
TOTAL 323.5838802523 1 1.8835970025

0.4499
VISKOS AIR Air fase gas (steam)
215.58474 micropoise
0.0216 cP
0.052172 lb/ft.jam

Komponen BM(kg/kgmol) (kg/jam) (kmol/jam) Xi,f
HCl 36.45800 10557.90199 289.59082 0.51515
(CH3)2O 46.06900 0.00000 0.00000 0.00000
CH3CL 50.48500 0.12625 0.00250 0.00000
CH3OH 32.04200 8435.51722 263.26438 0.46832
H2O 18.01500 167.30816 9.28716 0.01652
Total 19160.85362 562.14485 1.00000

suhu Tc 646.1000 k
Fraksi (Yi) BM Yi * BM
1.000 18.0150 18.01500
1.000 18.01500
L.atm/gmol.K
BM * Pt
k V 
RT
g/gmol
atm DENSITAS ZAT 0.339784068968829 g/L
0.0212 lb/ft3
0.339784068968829 kg/M3
L.atm/gmol.K
k
g/gmol
atm
x ρ
x ρ
x 0.2212
fps
625
X
144
KJ/KG.K
BTU/LBM.°F
kj/kg.k
btu/lbm.°F
µ Xi,f*µ
284.78953 146.71029
200.94597 0.00000
213.54854 0.00095
197.42565 92.45863
215.58474 3.56166
1112.29443 242.73152 MIKROPOISE

0.0243 cP
0.058741 lb/ft.jam
Coller-01
Kode : C-01
Fungsi : Menurunkan temperatur umpan flash drum dari 23
Tipe : SHELL TUBE
Dasar Perancangan
Suhu bahan masuk :
Tekanan masuk :
Laju alir :
Bahan Konstruksi :
1. Data Perhitungan
Beban pendingin (Q) =
=
=
Fluida Panas =
=
Th in(T1) =
Th Out(T2) =
Fluida Dingin = AIR PENDINGIN

=
Tc in(t1) =
Tc Out(t2) =
2. Menghitung LMTD
Fluida Panas (˚F)
446 Suhu tinggi
122 Suhu rendah
324 Selisih
∆t LMTD =
=
Tc = T1 + T2
2
= 446
2
= 284
tc = t1 + t2
2
= 80.6
2
= 114.8

Annulus = FLUIDA PANAS
Pada, T = 284
µ = 0.0148
0.0358
Pipa = AIR PROSES
Pada, T = 114.8
µ = 0.58861
1.424427

Fluida Panas = FLUIDA PANAS
Fluida Dingin = water
Dipilih = 50
A =
=

kg/jam
OD 1.500 in
BWG 18
ID 1.4 in
Panjang tube 16 ft
Pitch 1.875 in, SQUERE
Nt = A / (L.Ao) 116.179905639122 =
Shell
ID 29 in
B 5 in
Pass 2
Ud Kor. = Q / (A kor. x ∆t) 48.4082940163009
C' = pitch - OD 0.3750
Bagian tube (steam)
A't 1.54 in^2
At = (Nt*A't)/(144*n) 0.320833333333333 ft2
Gt = Wt/At 131664.626818617 lb/ft2.jam

aa = ID
= 0.7080078125

Ga = W
aa
=

Pada Tc = 114.8
De = 0.123333333333333
Rea = De x Ga
µ
= 0.123333333333333
1.424427
= 8,483

jH = 45

Tc = 114.8
K = 0.365343
Cp = 1.19642916922255
Cp X µ ⅓ 1.19642916922255
K = 0.365343
ho = = 1.67086811887614
= 9. Menghitung ho
= jH k Cp X µ
De K
45 0.365343
1.67086811887614
0.123333333333333
222.728018892336 Btu/jam ft ˚F

114.8
240.859563277368
11. At tw 240.859563277368
Øs =(µ/µw)^0,14

= 253.082850862096
Uc = hio x ho
hio + ho
= 76.2225709464051
76.2225709464051
= 56.788321544811

a" 0.3925
Ud Q 4732120.7774
A.delta t 94642.4155484705
50

Rd Uc-Ud 6.78832154481096
Uc.Ud 2839.41607724055
SUMMARY
Uc 56.788321544811 Btu/jam ft^2 ˚F


1 Res 8,483
sg = densitas zat/ ensitas f 0.002
standar (aor 1000 kg/m3) s 1.00770644500938
Ds' 2.41666666666667

(5.22x10^10 x DE x s x Os)
0.27459612158979
∆P < 10
Coller-01
temperatur umpan flash drum dari 230˚C menjadi 60˚C
230 ˚C
1 atm
19160.8536 KG/JAM
1386828.8551 J/S
4992583.8784 kj/jam
4732120.7774 btu/jam
ALIRAN 15
19160.8536 kg/jam
42242.4011043061 lb/jam
230 ˚C = 446
50 ˚C = 122
AIR PENDINGIN
31463.3546 kg/jam
69364.7407965887 lb/jam
27 ˚C = 80.6
65 ˚C = 149

149 297 ∆t2 S
80.6 41.4 ∆t1 FT
68.4 255.6 ∆t2 - ∆t1 delta T
∆t2 - ∆t1
ln (∆t2 /∆t1)
255.6 ˚F
ln 1,0986 ˚F
129.7165 ˚F
+ 122
2
˚F
+ 149
2
˚F
˚F = 414.2600 K
cP
lb/ft.jam
˚F = 319.5080 K
cP
lb/ft.jam
(µ cP<0.5 cP)

Btu/jam Ft^2 ˚F
Qs
UD x ∆t LMTD
4732120.7774
50 x 129.71647939322
729.609807413688 ft^2
kg/jam lbm/jam
31463.3546 69364.7407965887
19160.8536 42242.4011043061
lb/jam
Tube
Jumlah tube 120
OD 1.5000 in =
ID 1.4 in =
ft BWG 18
Pass 4
A't 1.54 in^2
eam)
de/fluida dingin
ft^2
69364.7407965887 lb/jam
0.7080078125 ft^2
97971.7166561474 lb/jam ft^2
˚F
lb/ft.jam
ft
97971.7166561474
1.424427
˚F 319.508 K
btu/jam ft ˚F
btu/lb ˚F
lb/ft.jam
1.424427 ⅓
0.365343
⅓ µ 0.14
µw
1

222.728018892336 169.2
298.950589838741
F 390.1014 K
F µw=0,56 x 2,42
0.571871 lb/ft.jam
1
eq 6.36
btu/jam.ft2.°F
x 222.728018892336 82.4169017224728
+ 222.728018892336 82.4169017224728
Btu/jam ft^2 ˚F
ft^2/linft
ft2 67.7829 m2
BTU/JAM
FT.°f
Btu/JAM ft^2 oF
0.002391 Btu/hr ft^2 oF Uc-Ud

Uc.Ud
Pressre Drop
1
ft2/in2 fig 29
ft
2
12L/B
38.4
x DE x s x Os) 3
psi
liquid 4
cp gas ( j/mol.K)
KOMPONEN A B
HCL 29.244 -0.0012615
(CH3)2O 34.668 0.070293
CH3CL 27.385 0.026036
CH3OH 40.046 -0.038287
H2O 33.933 -0.0084186
densitas
Komponen
HCL
(CH3)2O
ch3cl
CH3OH
H2O
˚F 504.98 K
A + B T + CT2
KOMPONEN
HCL
(CH3)2O
CH3CL
˚F 300.356 K CH3OH
˚F 338.66 K H2O
visk
4.73684210526316 R=(T1-T2)/(t2-t1) LOG 10 VISKOSIT
0.187192118226601 S=(t2-t1)/(T1-t1) KOMPONEN
CH3CL
CH3OH
H2O
VISKOS AIR PENDINGIN (steam)
0.58861
Komponen
HCl
(CH3)2O
CH3CL
CH3OH
H2O
Total
kondu
Komponen
HCl
(CH3)2O
CH3CL
CH3OH
H2O
Total
kondu
Komponen
H2O
Total
Tube
0.125 ft L/D 137.142857142857

0.1167 ft

ap = 0.320833333333333 ft^2

Gp = W 42242.4011043061
ap 0.320833333333333
= 131664.626818617

Pada Tc = 284 ˚F
D = 0.1167 ft
Rep = D x Gp
µ
= 0.1167 131664.626818617
0.035805826797165
= 429,005

jH = 800

Tc = 284 ˚F
K = 0.0125 btu/jam ft ˚F
Cp = 0.301511346283805 btu/lb ˚F
Cp X µ ⅓ 0.301511346283805 0.0358
K = 0.012509119622589
= 0.952087522519909
9. Menghitung hi
hi = jH k Cp X µ
D K
= 800 0.012509119622589 0.952087522519909
0.1167
= 81.6670402997197 Btu/jam ft ˚F
10. Menghitung hio

hio = hi ID
OD
= 81.6670402997197 0.1167
0.125
= 76.2225709464051 Btu/jam ft ˚F
11. At tw 390.1014 K
Øt =(µ/µw)^0,14 1

= 82.4169017224728 btu/jam.ft2.°F
X 253.082850862096
+ 253.082850862096
62.1708489692161
0.002390745618165
For Ret 429,005

f 0.0001 fig 26
s 0.8465

(5.22x10^10 x ID x s x Ot)
= 0.021520361810355
Gt 131,665 V^2/2g' 0.0022

0.041580654940937
∆P = ∆Pt + ∆Pn eq. 7.47

0.0631 psi
∆P 1,5 - 2 psi GAS

s ( j/mol.K)
(A + B T + C T2 + D T3 + E T4 ) CAIR
C D E KOMPONEN
1.121E-06 4.9676E-09 -2.4963E-12 HCL
0.0001653 -1.7675E-07 4.9313E-11 (CH3)2O
0.0001032 1.0887E-07 3.1642E-11 CH3CL
0.00024529 -2.1679E-07 5.9909E-11 CH3OH
2.9906E-05 1.7825E-08 3.6934E-12 H2O

A * B^-(1-T/Tc)^n
Td a b n Tc
85.0500 0.4413 0.2696 0.3187 324.6500
-24.5000 0.2639 0.2633 0.2806 400.1000
-23.7000 0.3582 0.2611 0.2869 416.2500
64.7000 0.2720 0.2719 0.2331 512.5800
100.0000 0.3471 0.2740 0.2857 647.1300
A B C
-9.118 5.55E-01 -1.11E-04
-4.276 3.03E-01 6.35E-05
-1.374 3.86E-01 -4.87E-05
-14.236 3.89E-01 -6.28E-05
-36.826 4.29E-01 -1.62E-05

A B C D
-1.515 1.95E+02 3.07E-03 -1.38E-05
-7.4844 5.84E+02 2.78E-02 -4.04E-05
-7.3473 8.54E+02 1.95E-02 -2.35E-05
-9.0562 1.25E+03 2.24E-02 -2.35E-05
-10.2158 1.79E+03 1.77E-02 -1.26E-05
OS AIR PENDINGIN (steam)
cP

BM(kg/kgmol) (kg/jam) (kmol/jam) Xi,f µ
36.45800 1439.71391 39.48966 0.07025 201.74744
46.06900 9.09624 0.19745 0.00035 131.98949
50.48500 12626.48330 250.10366 0.44491 150.29332
32.04200 409.12259 12.76832 0.02271 136.28546
18.01500 4676.43758 259.58577 0.46178 138.11144
19160.85362 562.14485 1.00000 758.42714

KG/JAM XI K XI . K
1439.71391 0.075138296853 0.01977 0.001486
9.09624499261179 0.000474730676 0.03101 0.000015
12626.4832984738 0.658972901203 0.01913 0.012603
409.12258509579 0.021352002016 0.02716 0.000580
4676.43758 0.244062069252 0.02854 0.006966
19160.8536184495 1 0.021650 W/(M.K)

0.0125 BTU/FT.JAM.F
konduktivitas FLUIDA dingin

KG/JAM XI K XI . K
31463.3546 1 0.63231 0.632310
31463.3545901737 1 0.632310 W/(M.K)

0.3653 BTU/FT.JAM.F
VISKOS AIR Air fase air proses
0.23631 CP
0.0000 cP
0.571871 lb/ft.jam
Komponen BM(kg/kgmol)
HCl 36.45800
(CH3)2O 46.06900
CH3CL 50.48500
CH3OH 32.04200
H2O 18.01500
Total
Densitas (fluida PANAS)

Komponen massa (Kg/jam)
HCl 1439.71391
(CH3)2O 9.09624
CH3CL 12626.48330
CH3OH 409.12259
air 4676.43758
TOTAL 19160.8536
Densitas = 1 ; (∑Xi/ρ)
1121.2533
lb/jam 1 kg/m3
ft^2
lb/jam ft^2
w/Mk 414.26 k
0.14
⅓ µ Øt
µw sama
1
µw=1,5 x 2,42
0.033543 lb/ft.jam
eq 6.37
fig 27
cp cair ( j/mol.K)
A B C D
73.993 -0.12946 -7.898E-05 2.6409E-06
48.074 0.56225 -0.0023915 4.4614E-06
11.381 0.62328 -0.0024353 3.8333E-06
40.152 0.31046 -0.0010291 1.4598E-06
92.053 -0.039953 -0.00021103 5.3469E-07
ws) g/ml
303.0000 k
0.7673 767.3262 0.796
0.6472 647.1724 0.655
0.9028 902.8000 0.913
0.7828 782.8067 0.787
1.0230 1023.0130 1.027

A + B T + CT2
KOMPONEN A B C
HCL 0.00119 4.48E-05 2.10E-10
(CH3)2O -0.0315 1.50E-04 1.39E-09
CH3CL -0.00185 2.03E-05 7.32E-08
CH3OH 0.00234 5.43E-06 1.32E-07
H2O 0.00053 4.71E-05 4.96E-08

KOMPONEN A B C
HCL 0.8045 -2.10E-03 -2.32E-16
(CH3)2O -1.5099 0.9936 4.00E+02
CH3CL -1.7528 1.3686 4.16E+02
CH3OH -1.1793 0.6191 5.13E+02
H2O -0.2758 4.61E-03 -5.54E-06
Xi,f*µ
14.17239
0.04636
66.86694
3.09553
63.77673
147.95796 MIKROPOISE
0.0148 cP
CP FLUIDA panas
KOMPONEN KGmol/JAM Xi
HCL 39.48966 0.07024818689
(CH3)2O 0.19745 0.00035124093
CH3CL 250.10366 0.44490963232
CH3OH 12.76832 0.02271358043
H2O 259.58577 0.46177735943
TOTAL 562.14485435335 1
CP FLUIDA dingin
KOMPONEN KGMOL/JAM Xi
H2O 1746.50871996523 1
TOTAL 1746.50871996523 1
1439.71391 39.48966 0.07025 190.49638 13.38203
9.09624 0.19745 0.00035 123.44410 0.04336
12626.48330 250.10366 0.44491 141.90694 63.13576
409.12259 12.76832 0.02271 128.09890 2.90958
4676.43758 259.58577 0.46178 128.06218 59.13622
19160.85362 562.14485 1.00000 712.00850 138.60695

0.0139
0.033543
suhu t2-t1 181.44 k

Fraksi (xi) p, Kg/m 3
Xi / pi V (m3)
0.075 1211.6810 0.00006 1.18819547514051
0.000 814.1050 0.00000 0.01117330751089
0.659 1119.4563 0.00059 11.2791210349125
0.021 881.6912 0.00002 0.46402025728504 Densitas = 1 ; (∑X
0.244 1127.8656 0.00022 4.14627199009858
1.000 0.00089 17.088782064948
Kg/m3 69.9998 lb/ft3
0.06243 lbm/ft3
CP FLUIDA panas
29.0789838323638 0.05603011385114
51.8614157571989 0.00039540367996
36.1909473607045 0.31894030075658
39.9442901829737 0.02831526894957
33.5005219919971 0.85871676851842
1.26239785575566 KJ/KG.K
0.3015 BTU/LBM.°F
CP FLUIDA dingin
90.2430671344515 5.0093292886179
5.0093292886179 kj/kg.k
1.1964 btu/lbm.°F
MIKROPOISE
cP
lb/ft.jam
Densitas (fluida DINGIN) suhu tc 319.5080

Komponen massa (Kg/jam) Fraksi (xi) p, Kg/m 3
Xi / pi
air 19160.85361845 1.000 1007.7064 0.00099
TOTAL 19160.8536 1.000 0.00099
Densitas = 1 ; (∑Xi/ρ) 1007.706445009 Kg/m3 62.9111
1 kg/m3 0.06243 lbm/ft3
Densitas PANAS suhu TC 414.2600

Komponen mOL (Kg/jam) Fraksi (Yi) BM YI*BM
HCl 39.48966 0.07025 36.4580 2.56111
(CH3)2O 0.19745 0.00035 46.0690 0.01618
CH3CL 250.10366 0.44491 50.4850 22.46126
CH3OH 12.76832 0.02271 32.0420 0.72779
air 259.58577 0.46178 18.0150 8.31892
TOTAL 562.1449 1.000 34.08526
BMZAT * Pzat
spgr   
R * Tre
BMZAT * Pzat
spgr   
R * Tre
R 0.08206
tzat 414.2600
bm zat 34.08526
p zat 1
S= 0.8465
k
V (m3)
19.0143208008074
19.0143208008074
lb/ft3
* Rref * Tref densitas zat campuran 1.002679 g/l

0.0010 gr/cm3
* Rzat * Tzat
1.0027 KG/M3
* Rref * Tref
* Rzat * Tzat

k tref 298 k
atm p ref 1 atm
SUHU MASUK heter : -20.68 C
SUHU KELUAR heter : 90 C
TEKANAN : 1 ATM
LAJU ALIR MASSA : 1440.01112243017 KG/JAM
Bahan Konstruksi : Carbon Steel SA 285 Grade C
1. Data Perhitungan
Beban Panas =
=
SHELL
Fluida Panas = Stem
=
Th in =
Th Out =
Fluida Dingin = komponen msu

=
Tc in =
Tc Out =
Menghitung LMTD preheating

Fluida Panas (˚F)
392 Suhu tinggi
338 Suhu rendah
54 Selisih
1. ∆t LMTD =
=
3. Menghitung Suhu Caloric (Tc dan tc) Preheating
Tc = T1 + T2
2
= 392
2
= 365
tc = t1 + t2
2
= -5.224
2
= 94.388

Berdasarkan Kern 1965, fig. 15 halaman 825 diperoleh :
Annulus = stem
Pada, T = 365
µ = 0.01569
0.037976750525734
Pipa = fluida dingin
Pada, T = 94.388
µ = 0.05715
0.138292870287547

Fluida Panas = stem
Fluida Dingin = fluida dingin
UD = 200-700 Btu/jam Ft^2 ˚F
Dipilih = 200
A =
=
kg/jam
Laju alir fluida dingin 1440.01112243017
Laju alir fluida panas 607.779468081226
Karena nilai A < 200ft^2, maka alat perpindahan panas yang digunakan adalah tipe Double Pipe Exchanger
Berdasarkan Kern 1965, tabel 6.2 halaman 110 Digunakan hairpin dengan IPS pipa 4 x 3
Annulus
IPS (in) 4
Sch. No 40
OD (in) 4.5
ID (in) 4.026
Annulus : Hot Fluid

D2 = ID Annulus
= 4.026
= 0.3355
D1 = OD Pipe
= 3.5
= 0.2917
aa = π (D2^2 - D1^2)
4
= 3.14
4
= 0.021580282361111
Equivalent Diameter (De)

Berdasarkan Kern 1965, persamaan 6.3 halaman 105 diperoleh:
De = (D2^2 - D1^2)
D1
= 0.1126
0.2917
= 0.09425419047619

Ga = W
aa
=

Pada Tc = 365
µ Steam = 0.0380
De = 0.09425419047619
Rea = De x Ga
µ
= 0.09425419047619
0.037976750525734
= 154,101

jH = 350

Tc = 365
K = 0.018860573506881
Cp = 0.446872654987264
µ Steam = 0.0380
Cp X µ ⅓ 0.446872654987264
K = 0.018860573506881
= 0.965418379129429
9. Menghitung ho
ho= jH k Cp X µ
De K
350 0.018860573506881
0.09425419047619
67.6141874898655 Btu/jam ft ˚F

UP =
=

1
Ud
1
Ud
1
Ud
Ud

AP =
Berdasakan kern 1950, tabel 11 dengan nilai IPS : 3 in, didapatkan nilai a
Panjang pipa =
Hairpin =
Koreksi panjang P :
A =
=
=

UD aktual =

Rd

De' : Untuk Pressure Drop
De : Untuk perpindahan panas
De' = (D2 - D1)

= 0.3355
= 0.0438
re,a' = De'
µ
= 0.0438
0.037976750525734
= 71665.3689948309

f = 0.0035
= 0.0035
= 0.005911981672645
S = 0.4033
ρ = 25.1752
18. Menentukan ΔP karena panjang pipa

∆Fa = 4 x F x Ga^2 x L
2 x g x ρ^2 x de'
= 4
2
= 13029278552.1383
23225002295.3524
= 0.561002250352654
Va = Ga
3600
= 62090.1408285487
3600
= 0.685090032751808
ΔFt = 1x
= 1
= 0.007288017903352
Pressure drop pada Anulus:

∆Pa = ∆Fa
144
= 0.561002250352654
144
= 0.099352825356019
∆Pa untuk Steam < 10 psi (memenuhi)

HETER 3 DASAR PERANCANGAN D
TD STEAM JENUH 200 YAWS
Panas laten
Komponen A Tc n
Steam 52.053 647.13 0.321
n=Q/λ 33.73741149493 Kgmol/jam
m = n x BM 607.7794680812 kg/jam
1152257.8250 Kj/jam
1092144.53426556 btu/jam
Stem
607.779468081226 kg/jam
1339.92277092123 lb/jam
200 ˚C = 392 ˚F
170 ˚C = 338 ˚F
komponen msuk
1440.01112243017 kg/jam
3174.67732073199 lb/jam
-20.68 ˚C = -5.224 ˚F
90 ˚C = 194 ˚F
Fluida Dingin (˚F) Selisih (˚F) ∆t

194 198 ∆t2
-5.224 343.224 ∆t1
199.224 -145.224 ∆t2 - ∆t1
∆t2 - ∆t1 Qp
ln (∆t2 /∆t1) 463,397.2632 Kj/jam
-145.224 ˚F 439,221.8280 btu/jam
ln 7 ˚F qp
263.98783195462 ˚F ∆t LMTD 1663.79573161 btu/jam.°F
q qp qv
+ 338
3.
t  t  t
2
˚F
Δt LMTD = Q
∑q/Δt
+ 194
2
˚F
˚F = 459.6200 K
cP
lb/ft.jam
˚F = 308.0773 K
cP
lb/ft.jam
(µ cP<0.5 cP)
tu/jam Ft^2 ˚F
Btu/jam Ft^2 ˚F
Qs
UD x ∆t LMTD
1092144.53426556
200 x 198.05782
27.571355689657 ft^2
shell and tube
lbm/jam
3174.67732073199
1339.92277092123
Double Pipe Exchanger
Inner Pipe shell and tube

IPS (in) 3
Sch. No 40
OD (in) 3.5
ID (in) 3.068

D
in
ft
ap
in
ft
0.1126 0.0851
ft^2
- 0.0851
ft

1339.92277092123 lbm/jam Gp
0.021580282361111 ft^2
62090.1408285487 lb/jam ft^2

˚F Pada tc
lb/ft.jam µ light organik
ft D
Rep
62090.1408285487

Berdasarkan Kern 1950, fig. 24 halaman
jH

˚F Tc
Berdasarkan yaws 1999, halaman 552 d
btu/jam ft ˚F K
Berdasarkan yaws 1999, halaman 78 dip
btu/lb ˚F Cp
lb/ft.jam µ campuran
0.037976750525734 ⅓ Cp X µ
K
9. Menghitung hi
Berdasarkan kern 1950, persamaan 6.15
⅓ µ 0.14 hi =
µw
0.965418379129429 1 =
10. Menghitung hio

hio
hio x ho
hio + ho
79.6181010654903 x 67.61418748987
79.6181010654903 + 67.61418748987
36.5634010436856 Btu/jam ft^2 ˚F
an 845 diperoleh:
= 1 + Rd
Uc
= 1 + 0.002
36.5634010436856
= 0.029349753345024
= 200 Btu/jam ft^2 ˚F
as yang Dibutuhkan
1 halaman 107 diperoleh:
Q AP
UP x ∆t LMTD
439221.8280
36.5634010436856 x 263.98783
45.5044028759867 ft^2
nilai IPS : 3 in, didapatkan nilai a" = 0.917 ft^2/ft

L = A
a"
= 131.05432 ft^2
0.917 ft^2/ft
= 142.916380517 lin ft
Diambil Lh = 20 ft
mlah hairpin yang diperlukan :
L
2 x Lh
142.916380517035
2 x 20
3.57290951292588 ≈ 4 buah
L koreksi = (2 x Lh) x jumlah hairpin

= (2 x 20 ft) x 13
= 160 ft linier
as yang Tersedia Sebenarnya
L x a"
160 x 0.917
146.72 Ft^2
Coefficient (UD aktual)

Q
A x ∆t LMTD
439221.8280
146.72 x 263.9878319546
11.339938192531 Btu/jam ft^2 ˚F
= Uc - Ud
Uc x Ud
= 36.5634010436856 - 11.3399381925
36.5634010436856 x 11.3399381925
= 0.06083414880875 Btu/jam ft^2 ˚F
Pressre Drop
Untuk re,p
pindahan panas
Berdasarkan Kern 1950, persamaan 3.47

- 0.2917 f
ft
x Ga
x 62090.1408285487
+ 0.264
(Re,p)^0,42
+ 0.264
109.453567991043
lb/ft3

∆Fp
0.005911981672645 3855185588.10901 142.916380517

418000000 633.789427165912 0.0438
ft
∆Pp
x ρ
x 25.1751748189742
fps ∆Pp
Va^2
2 x g' ∆Pp
0.469348352975874
2 x 32.2
ft
+ Ft ρ
+ 0.007288017903352 25.17517481897
psi
am < 10 psi (memenuhi)

RANCANGAN DOUBLE PIPE
anas laten
Td Lambda (Kj/mol) Lambda (KJ/kgmol)
473 34.1537116790546 34153.7116790546
474.74 K
444.5 K
R 0.27105168052 R=(T1-T2)/(t2-t1)
S 0.50154069241 S=(t2-t1)/(T1-t1)
Ft 0.98 FT=fig.13 hal;328
252.29456 K delta T 258.708075316 delta T=lmtd/ft
363.86 K
Menghitung LMTD vaporizing

Fluida Panas (˚F) Fluida Dingin (˚F) Selisih (˚F)
392 Suhu tinggi 194 198
338 Suhu rendah 194 144
54 Selisih 0 54
2. ∆t LMTD = ∆t2 - ∆t1

ln (∆t2 /∆t1)
= 54 ˚F
ln 7 ˚F
= 169.569374522 ˚F
qp qv
 5514.27113793139 btu/jam.°F
t t
1092144.534 btu/jam
5514.271 btu/jam.°F
198.05782 °F
pe : Cold Fluid
enghitung Flow Area (a)
= ID Pipe
= 3.068 in
= 0.2557 ft
= π (D^2)
4
= 3.14 0.0654
4
= 0.05131187388889 ft^2
enghitung mass velocity

= W 3174.67732073199 lbm/jam
ap 0.051311873888889 ft^2
= 61870.2276905042 lb/jam ft^2
ynold Number (Rep)

= 94.388 ˚F
= 0.138293 lb/ft.jam
= 0.2557 ft
= D x Gp
µ
= 0.2557 61870.2276905042
0.13829287028755
= 114,382
enentukan Heat Transfer

asarkan Kern 1950, fig. 24 halaman 834 diperoleh:
= 300
enghitung Thermal Konduktivity

= 94.388 ˚F w/mK
asarkan yaws 1999, halaman 552 diperoleh:
= 0.0906816126836 btu/jam ft ˚F
= 0.40784375416297 btu/lb ˚F
= 0.13829287028755 lb/ft.jam
⅓ 0.40784375416297 0.138292870287547 ⅓
= 0.0906816126836
= 0.85360730644578
enghitung hi
asarkan kern 1950, persamaan 6.15a halaman 114 diperoleh:
jH k Cp X µ ⅓ µ
D K µw
300 0.0906816126836 0.85360730645 1
0.2557
90.828994045 Btu/jam ft ˚F
Menghitung hio
asarkan kern 1950, persamaan 6.5 halaman 111 diperoleh:
= hi ID
OD
= 90.8289940447249 3.068
3.5
= 79.6181010654903 Btu/jam ft ˚F
= Q
Ud x ∆t LMTD
= 1092144.5343
36.5634010436856 x 198.05782
= 150.813955500009 ft^2
= 114,382
asarkan Kern 1950, persamaan 3.47b Hal 53 diperoleh:

= 0.0035 + 0.264
(Re,p)^0,42
= 0.0035 + 0.264
133.201628305
= 0.00548195775352
=
= 45.7913 lb/ft^3
Menentukan ΔP pipa
= 4 x F x G0^2 x L
2 x g x ρ^2 x D
= 4 0.005481957753516 3827925074.47 142.916380517035
2 418000000 2096.84092442 0.2557
= 11996128605.9291
448173187609.35
= 0.0267667253142 ft
= ∆Fp x ρ
144
= 0.0267667253142 x 45.7912756365
144
= 0.0085116840052 psi
untuk fluida < 10 psi (memenuhi)
0.008511684 + 0.42048337317114
0.4289950572
GAS
KOMPONEN
HCL
(CH3)2O
CH3CL
CH3OH
H2O
densitas
Komponen
CH3OH
H2O
ch3cl
hcl
dme
viskositas g
A
KOMPONEN
HCL
(CH3)2O
CH3CL
CH3OH
H2O
∆t LOG 10 V
∆t2 KOMPONEN
∆t1 HCL
∆t2 - ∆t1 (CH3)2O
CH3CL
Qv CH3OH
688,860.5618 Kj/jam H2O
652,922.7063 btu/jam
qv
∆t LMTD 3850.47540632325 btu/jam.°F
Komponen
HCl
(CH3)2O
CH3CL
CH3OH
H2O
Total
Komponen
HCl
(CH3)2O
CH3CL
CH3OH
H2O
Total
Komponen
H2O
Total
kg/jam lbm/jam
Laju alir fluida dingin 8443.80870230992 18615.3895412865
tc = t1 + t2
2
= 194
2
= 194
= 363.86
kg/jam lbm/jam
Laju alir fluida dingin 1440.01529197953 3174.67732073199

D = ID Pipe
= 3.068
= 0.2557
ap = π (D^2)
4
= 3.14
4
= 0.05131187388889

Gp = W 3174.67732073199
ap 0.05131187388889
= 61870.2276905042

Pada tc = 363.86 ˚F
µ light organik = 0.017811 lb/ft.jam
D = 0.2557 ft
Rep = D x Gp
µ
= 0.2557 61870.2276905042
0.01781067881708
k = 888,128

jH = 1000

Tc = 363.86 ˚F
K = 0.01011741673755 btu/jam ft ˚F
Cp = 0.19090791298419 btu/lb ˚F
µ campuran = 0.017811 lb/ft.jam
Cp X µ ⅓ 0.19090791298419 0.01781067881708
K = 0.01011741673755
= 0.69525628096338
9. Menghitung hi
hi = jH k Cp X µ
D K
= 1000 0.01011741673755
0.2557
= 27.5131585420125 Btu/jam ft ˚F
10. Menghitung hio

hio = hi ID
OD
= 27.5131585420125 3.068
3.5
= 24.1172486876841 Btu/jam ft ˚F
UV = hio x ho
hio + ho
= 24.1172486876841 x
24.1172486876841 +
= 17.7765468683229 Btu/jam ft^2 ˚F

1 = 1
Ud Uc
1 = 1
Ud 17.7765468683229
1 = 0.05825389494413
Ud
Ud = 17.1662341369468

AV = Q
UV x
= 652922.7063
17.7765468683229 x
= 216.604238992256 ft^2
14. TOTAL CLEAN SURFACE = Ac =

Ac = Ap + Av
= 131.05432 ft2
15 Weighted clean overall coefisien Uc :

Uc= ∑U A 1663.79573160814
Ac 131.05432
42.07623
16 Berdasakan kern 1950, tabel 11 dengan nilai IPS : 3 in, didapatkan nilai a" =
Panjang pipa = L =
=
=
Diambil Lh = 20
Hairpin = L
2 x Lh
= 142.916380517035
2 x
= 3.57290951292588 ≈
Koreksi panjang P : L koreksi =

=
=

A = L x a"
= 160 x
= 146.72 Ft^2
Densitas shell (fluida dingin)

HCl 1439.59729
(CH3)2O 0.00000
CH3CL 0.12625
CH3OH 0.14728
H2O 0.14029
TOTAL 1440.0111
Densitas = 1 ; (∑Xi/ρ) 733.481909923165
1 kg/m3
Untuk re,p = 888,128

f = 0.0035 +
= 0.0035 +
= 0.00433800050286
ρ = 0.0008
= 0.7335 lb/ft^3

∆Fp = 4 x F x G0^2 x L
2 x g x ρ^2 x D
= 4 0.00433800050286
2 418000000
= 9492815206.67588
114997136.818062
= 82.5482744122103 ft
∆Pp = ∆Fp x
144
= 82.5482744122103 x
144
= 0.42048337317114 psi
∆Pp untuk fluida < 10 psi (memenuhi)
cp gas ( j/mol.K)
A B C D E
29.244 -0.0012615 1.121E-06 4.9676E-09 -2.4963E-12
34.668 0.070293 0.0001653 -1.7675E-07 4.9313E-11
27.385 0.026036 0.0001032 1.0887E-07 3.1642E-11
40.046 -0.038287 0.00024529 -2.1679E-07 5.9909E-11
33.933 -0.0084186 2.9906E-05 1.7825E-08 3.6934E-12

A * B^-(1-T/Tc)^n
Td a b n Tc
64.7000 0.2720 0.2719 0.2331 512.5800
100.0000 0.3471 0.2740 0.2857 647.1300
-23.7000 0.3582 0.2611 0.2869 416.2500
85.0500 0.4413 0.2696 0.3187 324.6500
-24.5000 0.2639 0.2633 0.2806 400.1000

A + B T + CT2
A B C
-9.118 5.55E-01 -1.11E-04
-4.276 3.03E-01 6.35E-05
-1.374 3.86E-01 -4.87E-05
-14.236 3.89E-01 -6.28E-05
-36.826 4.29E-01 -1.62E-05

A B C D
-1.515 1.95E+02 3.07E-03 -1.38E-05
-7.4844 5.84E+02 2.78E-02 -4.04E-05
-7.3473 8.54E+02 1.95E-02 -2.35E-05
-9.0562 1.25E+03 2.24E-02 -2.35E-05
-10.2158 1.79E+03 1.77E-02 -1.26E-05
viskositas fluida masuk (CAIR)
36.458 1439.59729 39.48646 0.99962 0.05696
46.069 0.00000 0.00000 0.00000 0.13886
50.485 0.12625 0.00250 0.00006 0.15796
32.042 0.14728 0.00460 0.00012 0.47481
18.015 0.14029 0.00779 0.00020 0.73439
1440.01112 39.50134 1.00000 1.56298

KG/JAM XI K XI . K
1439.59729 0.99971261888679 0.15692 0.156876
0.00000 0 0.03145 0.000000
0.12625 8.7676226462E-05 0.01821 0.000002
0.14728 0.00010227985627 0.06836 0.000007
0.14029 9.7425030472E-05 0.61933 0.000060
1440.01112243017 1 0.156945 W/(M.K)

0.0906816126836 BTU/FT.JAM.F

KG/JAM XI K XI . K
607.77947 1 0.03264 0.032643
607.779468081226 1 0.032643 W/(M.K)

0.0188605735069 BTU/FT.JAM.F
+ 194
˚F
K
in
ft
0.0654
ft^2
lbm/jam
ft^2
lb/jam ft^2
w/mK
⅓ µ
µw
0.695256280963381 1
67.6141874898655
67.6141874898655
+ Rd
+ 0.002
Btu/jam ft^2 ˚F
∆t LMTD
922.7063
169.56937
3850.47540632325
131.05432
Btu/jam ft^2 ˚F
0.917 ft^2/ft 18
A
a"
131.05432 ft^2
0.917 ft^2/ft
142.916380517035 lin ft
ft
19
20
4 buah
(2 x Lh) x jumlah hairpin

(2 x 20 ft) x 13
160 ft linier
0.917
13.6307 m2
suhu tc 308.0773 k
Xi / pi
0.999712618886793 733.4462 0.001363034726
0 638.5473 0
8.767622646196E-05 891.9554 9.82966471E-08
0.000102279856274 778.1034 1.31447635E-07
9.742503047171E-05 1018.3377 9.56706485E-08
1.0000 4060.3900 0.0014
Kg/m3 45.7913 lb/ft3
0.06243 lbm/ft3
0.264
(Re,p)^0,42
0.264
315.035610477546
3827925074.47484 142.916380517035
0.5380 0.2557
0.733505408414545
cp cair ( j/mol.K)
KOMPONEN A B C D
HCL 73.993 -0.12946 -7.898E-05 2.6409E-06
(CH3)2O 48.074 0.56225 -0.0023915 4.4614E-06
CH3CL 11.381 0.62328 -0.0024353 3.8333E-06
CH3OH 40.152 0.31046 -0.0010291 1.4598E-06
H2O 92.053 -0.039953 -0.00021103 5.3469E-07
aws) g/ml
303.0000 k
0.7828 782.8067 0.787
1.0230 1023.0130 1.027
0.9028 902.8000 0.913
0.7673 767.3262 0.796
0.6472 647.1724 0.655

A + B T + CT2
KOMPONEN A B C
HCL 0.00119 4.48E-05 2.10E-10
(CH3)2O -0.0315 1.50E-04 1.39E-09
CH3CL -0.00185 2.03E-05 7.32E-08
CH3OH 0.00234 5.43E-06 1.32E-07
H2O 0.00053 4.71E-05 4.96E-08

LOG10=A+B [ 1-T/C]^2/7 (yg organik)
KOMPONEN A B C
HCL 0.8045 -2.10E-03 -2.32E-16
(CH3)2O -1.5099 0.9936 4.00E+02
CH3CL -1.7528 1.3686 4.16E+02
CH3OH -1.1793 0.6191 5.13E+02
H2O -0.2758 4.61E-03 -5.54E-06
Xi,f*µ Komponen BM(kg/kgmol) (kg/jam) (kmol/jam)
0.05694 H2O 18.01500 607.77947 33.73741
0.00000
0.00001 Total 607.77947 33.73741
0.00006
0.00014
0.05715 CP
CP FLUIDA DINGIN
KOMPONEN KGmol/JAM Xi cP(Kj/kmol.k)
HCL 39.48646 0.999623177225 62.2339402426061
(CH3)2O 0.00000 0 87.2303026818772
CH3CL 0.00250 6.3310169E-05 55.9287660366174
CH3OH 0.00460 0.000116365563 64.0066896033043
H2O 0.00779 0.000197147043 85.7114586243483
TOTAL 39.5013431338 1
U/FT.JAM.F
CP FLUIDA panas
KOMPONEN KGMOL/JAM Xi cP(j/kmol.k)
H2O 33.73741 1 33.7062653117787
TOTAL 33.7374114949 1
U/FT.JAM.F
viskositas fluida KELUAR GAS

Komponen BM(kg/kgmol) (kg/jam) (kmol/jam)
HCl 36.45800 1439.59729 39.48646
(CH3)2O 46.06900 0.00000 0.00000
CH3CL 50.48500 0.12625 0.00250
CH3OH 32.04200 0.14728 0.00460
H2O 18.01500 0.14029 0.00779
Total 1440.01112 39.50134

Komponen KG/JAM XI K
HCl 1439.59729 0.999712618887 0.01751
(CH3)2O 0.00000 0 0.02338
CH3CL 0.12625 8.767622646E-05 0.01523
CH3OH 0.14728 0.000102279856 0.02173
H2O 0.14029 9.742503047E-05 0.02423
Total 1440.01112243 1
CP FLUIDA DINGIN
HCL 39.48646 0.999623177225 29.1289525388494
(CH3)2O 0.00000 0 74.4793605585968
CH3CL 0.00250 6.3310169E-05 56.3207427500099
CH3OH 0.00460 0.000116365563 49.1965309675632
H2O 0.00779 0.000197147043 35.7526070386454
TOTAL 39.5013431338 1
UD aktual = Q
A x ∆t LMTD
= 1092144.5343
146.72 x 198.05782
= 37.58363643628 Btu/jam ft^2 ˚F

Rd = Uc - Ud
Uc x Ud
= 42.07623 - 37.5836364362827
42.07623 x 37.5836364362827
= 0.00284093377 Btu/jam ft^2 ˚F
Densitas tube (fluida panas) suhu Tc 459.6200

Komponen mol (Kg/jam) Fraksi (Yi) BM Yi * BM
air 33.73741 1.000 18.0150 18.01500
TOTAL 33.7374 1.000 18.01500
BM * Pt
tzat 459.6200 k V 
RT
bm zat 18.01500 g/gmol
p zat 1 atm DENSITAS ZAT
S= 0.4033
Densitas shell (fluida dingin) suhu tc 363.8600
HCl 39.48646 0.99962317722 36.4580 0.02741848640146
(CH3)2O 0.00000 0 46.0690 0
CH3CL 0.00250 6.3310169E-05 50.4850 1.2540391997E-06
CH3OH 0.00460 0.00011636556 32.0420 3.631657307E-06
H2O 0.00779 0.00019714704 18.0150 1.0943493922E-05
TOTAL 39.5013 1.0000 183.0690 0.0274
p zat 1 atm p ref
S= 0.0008
BMZAT * Pzat
densitaszat R * Tzat BMzat* Pzat * Rref *
spgr   
denstasrefrensi BMref * Pr ef BMref * Pr ef * Rzat *
R * Tre
as (steam)
Xi,f µ Xi,f*µ
1.00000 156.9287 156.92872
1.00000 156.92872 156.92872 micropoise

0.0157 cP
(Xi . Cp )/bm
1.7063604443
0
7.013687E-05
0.0002324504
0.0009379828
1.7076010143 KJ/KG.K
0.4078437542 BTU/LBM.°F
(Xi . Cp)/BM
1.8710111192
1.8710111192 kj/kg.k
0.446872655 btu/lbm.°F
KELUAR GAS
Xi,f µ Xi,f*µ
0.99962 178.12855 178.06143
0.00000 114.24605 0.00000
0.00006 132.73323 0.00840
0.00012 119.12357 0.01386
0.00020 117.12516 0.02309
1.00000 661.35656 178.10679 MCROPOISE

0.0178 cP
XI . K
0.017505
0.000000
0.000001
0.000002
0.000002
0.017511 W/(M.K)
0.0101174167 BTU/FT.JAM.F
(Xi . Cp )/bm
0.7986717891
0
7.062842E-05
0.0001786649
0.0003912584
0.7993123409 KJ/KG.K
0.190907913 BTU/LBM.°F
k
BM * Pt

RT
0.0009188155 kG/L
0.0001 lb/ft3
k
298 k
28.964 g/gmol
1 atm
at* Pzat * Rref * Tref

ef * Pr ef * Rzat * Tzat
CD
Kode : C-01
Tipe : SHELL TUBE
Dasar Perancangan
Suhu bahan masuk :
Tekanan masuk :
Laju alir :
Bahan Konstruksi :
1. Data Perhitungan
=
=
Fluida Panas =
=
Th in(T1) =
Th Out(T2) =

=
Tc in(t1) =
Tc Out(t2) =
2. Menghitung LMTD
Fluida Panas (˚F)
428.54 Suhu tinggi
58.0054351539398 Suhu rendah
370.53456484606 Selisih
∆t LMTD =
=
Tc = T1 + T2
2
= 428.54
2
= 243.27271757697
tc = t1 + t2
2
= -247
2
= -161.5

Pada, T = 243.27271757697
µ = 0.0149
0.0361
Pipa = AIR PROSES
Pada, T = -161.5
µ = 0.48995
1.185690

Dipilih = 15
A =
=

kg/jam
OD 1.500 in
BWG 10
ID 1.23 in
Panjang tube 16 ft
Nt = A / (L.Ao) 36.9833526196635 =
Shell
ID 17.25 in
B 5 in
Pass 1
Ud Kor. = Q / (A kor. x ∆t) 14.2243663921783
C' = pitch - OD 0.3750
Bagian tube (steam)
A't 1.19 in^2
At = (Nt*A't)/(144*n) 0.161145833333333 ft2
Gt = Wt/At 192439.281800707 lb/ft2.jam

aa = ID
= 0.421142578125

Ga = W
aa
=

Pada Tc = -161.5
De = 0.123333333333333
Rea = De x Ga
µ
= 0.123333333333333
1.185690
= 4,156

jH = 40

Tc = -161.5
K = 0.037853
Cp = 1.0631
Cp X µ ⅓ 1.06313175959134
K = 0.037853
ho = = 3.21725485137186
= 9. Menghitung ho
= jH k Cp X µ
De K
40 0.037853
3.21725485137186
0.123333333333333
39.497253737348 Btu/jam ft ˚F

-161.5
-15.4736445051541
11. At tw -15.4736445051541
Øs =(µ/µw)^0,14

= 45.6516655115127
Uc = hio x ho
hio + ho
= 69.9857959348584
69.9857959348584
= 25.2481708202827

a" 0.3925
Ud Q 1381125.8878
A.delta t 92075.0591862149
15

Rd Uc-Ud 10.2481708202827
Uc.Ud 378.72256230424
SUMMARY
Uc 25.2481708202827 Btu/jam ft^2 ˚F


1 Res 4,156
standar (aor 1000 kg/m3) s 1.14136120679346
Ds' 1.4375

(5.22x10^10 x DE x s x Os)
0.029976546106756
∆P < 10
CD
220.3 ˚C
1 atm
14066.2737 KG/JAM
404762.5417 J/S
1457145.1503 kj/jam
1381125.8878 btu/jam
ALIRAN 15
14066.2737 kg/jam
31010.7884318431 lb/jam
220.3 ˚C = 428.54
14.447463974411 ˚C = 58.0054351539398
AIR PENDINGIN
7631.9181 kg/jam
16825.479281622 lb/jam
-155 ˚C = -247
-60 ˚C = -76

-76 504.54 ∆t2 S
-247 305.00543515394 ∆t1 FT
171 199.53456484606 ∆t2 - ∆t1 delta T
∆t2 - ∆t1
ln (∆t2 /∆t1)
199.53456484606 ˚F
ln 1,0986 ˚F
396.4387 ˚F
+ 58.0054351539398
2
˚F
+ -76
2
˚F
˚F = 391.4527 K
cP
lb/ft.jam
˚F = 164.7800 K
cP
lb/ft.jam
(µ cP<0.5 cP)

Btu/jam Ft^2 ˚F
Qs
UD x ∆t LMTD
1381125.8878
15 x 396.43873769797
232.255454451487 ft^2
kg/jam lbm/jam
7631.9181 16825.479281622
14066.2737 31010.7884318431
lb/jam
Tube
Jumlah tube 39
OD 1.5000 in =
ID 1.23 in =
ft BWG 10
Pass 2
A't 1.19 in^2
eam)
de/fluida dingin
ft^2
16825.479281622 lb/jam
0.421142578125 ft^2
39951.9786304485 lb/jam ft^2
˚F
lb/ft.jam
ft
39951.9786304485
1.185690
˚F 164.78 K
btu/jam ft ˚F
btu/lb ˚F
lb/ft.jam
1.185690 ⅓
0.037853
⅓ µ 0.14
µw
1

39.497253737348 404.77271757697
109.483049672206
F 246.5548 K
F µw=0,56 x 2,42
0.421462 lb/ft.jam
1
eq 6.36
btu/jam.ft2.°F
x 39.497253737348 90.9009907733456
+ 39.497253737348 90.9009907733456
Btu/jam ft^2 ˚F
ft^2/linft
ft2 21.5772 m2
BTU/JAM
FT.°f
Btu/JAM ft^2 oF

Uc.Ud
Pressre Drop
1
ft2/in2 fig 29
ft
2
12L/B
38.4
x DE x s x Os) 3
psi
liquid 4
cp gas ( j/mol.K)
KOMPONEN A B
HCL 29.244 -0.0012615
(CH3)2O 34.668 0.070293
CH3CL 27.385 0.026036
CH3OH 40.046 -0.038287
H2O 33.933 -0.0084186
densitas
Komponen
HCL
(CH3)2O
ch3cl
CH3OH
H2O
Propane
˚F 495.2024 K
A + B T + CT2
KOMPONEN
HCL
(CH3)2O
CH3CL
˚F 116.9 K CH3OH
˚F 212.66 K H2O
visk
0.253130828670397 S=(t2-t1)/(T1-t1) KOMPONEN
CH3CL
CH3OH
propane
0.48995
Komponen
HCl
(CH3)2O
CH3CL
CH3OH
H2O
Total
kondu
Komponen
HCl
(CH3)2O
CH3CL
CH3OH
H2O
Total
kondu
Komponen
PROPANE
Total
Tube
0.125 ft L/D 156.09756097561

0.1025 ft

ap = 0.161145833333333 ft^2

Gp = W 31010.7884318431
ap 0.161145833333333
= 192439.281800707

Pada Tc = 243.27271757697 ˚F
D = 0.1025 ft
Rep = D x Gp
µ
= 0.1025 192439.281800707
0.036063540461493
= 546,952

jH = 1000

Tc = 243.27271757697 ˚F
Cp = 0.1823 btu/lb ˚F
Cp X µ ⅓ 0.182327957185158 0.0361
K = 0.01009064820456
= 0.866963579991265
9. Menghitung hi
hi = jH k Cp X µ
D K
= 1000 0.01009064820456 0.866963579991265
0.1025
= 85.3485316278761 Btu/jam ft ˚F
10. Menghitung hio

hio = hi ID
OD
= 85.3485316278761 0.1025
0.125
= 69.9857959348584 Btu/jam ft ˚F
11. At tw 246.5548 K
Øt =(µ/µw)^0,14 1

= 90.9009907733456 btu/jam.ft2.°F
X 45.6516655115127
+ 45.6516655115127
30.3896074844062
0.027059837042531
For Ret 546,952

f 0.0001 fig 26
s 1.2765

(5.22x10^10 x ID x s x Ot)
= 0.017350330538705
Gt 192,439 V^2/2g' 0.0042

0.026321095779569
∆P = ∆Pt + ∆Pn eq. 7.47

0.0437 psi
∆P 1,5 - 2 psi GAS

s ( j/mol.K)
(A + B T + C T2 + D T3 + E T4 ) CAIR
C D E KOMPONEN
1.121E-06 4.9676E-09 -2.4963E-12 HCL
0.0001653 -1.7675E-07 4.9313E-11 (CH3)2O
0.0001032 1.0887E-07 3.1642E-11 CH3CL
0.00024529 -2.1679E-07 5.9909E-11 CH3OH
2.9906E-05 1.7825E-08 3.6934E-12 H2O
PROPANE
A * B^-(1-T/Tc)^n
Td a b n Tc
85.0500 0.4413 0.2696 0.3187 324.6500
-24.5000 0.2639 0.2633 0.2806 400.1000
-23.7000 0.3582 0.2611 0.2869 416.2500
64.7000 0.2720 0.2719 0.2331 512.5800
100.0000 0.3471 0.2740 0.2857 647.1300
-188.0000 0.2215 0.2774 0.2870 369.8200
A B C
-9.118 5.55E-01 -1.11E-04
-4.276 3.03E-01 6.35E-05
-1.374 3.86E-01 -4.87E-05
-14.236 3.89E-01 -6.28E-05
-36.826 4.29E-01 -1.62E-05

A B C D
-1.515 1.95E+02 3.07E-03 -1.38E-05
-7.4844 5.84E+02 2.78E-02 -4.04E-05
-7.3473 8.54E+02 1.95E-02 -2.35E-05
-9.0562 1.25E+03 2.24E-02 -2.35E-05
-3.1759 2.97E+02 9.55E-03 -1.88E-05
cP

36.45800 1439.71247 39.48962 0.13635 191.12915
46.06900 0.00000 0.00000 0.00000 123.92015
50.48500 12625.47413 250.08367 0.86350 142.37755
32.04200 0.73642 0.02298 0.00008 128.55877
18.01500 0.35073 0.01947 0.00007 128.62481
14066.27375 289.61574 1.00000 714.61042

KG/JAM XI K XI . K
1439.71247 0.102352086498 0.01875 0.001919
0 0 0.02756 0.000000
12625.47413 0.897570625551 0.01732 0.015543
0.73642 5.235364151E-05 0.02462 0.000001
0.35073 2.493430918E-05 0.02656 0.000001
14066.27375 1 0.017464 W/(M.K)

0.0101 BTU/FT.JAM.F

KG/JAM XI K XI . K
7631.9181 1 0.06551 0.065514
7631.9181 1 0.065514 W/(M.K)

0.0379 BTU/FT.JAM.F
0.17416 CP
0.0000 cP
0.421462 lb/ft.jam
HCl 36.45800
(CH3)2O 46.06900
CH3CL 50.48500
CH3OH 32.04200
H2O 18.01500
Total

HCl 1439.71247
(CH3)2O 0.00000
CH3CL 12625.47413
CH3OH 0.73642
air 0.35073
TOTAL 14066.2737
1083.7693
lb/jam 1 kg/m3
ft^2
lb/jam ft^2
w/Mk 391.4527218431 k
0.14
⅓ µ Øt
µw sama
1
µw=1,5 x 2,42
0.022991 lb/ft.jam
eq 6.37
fig 27
cp cair ( j/mol.K)
A B C D
73.993 -0.12946 -7.898E-05 2.6409E-06
48.074 0.56225 -0.0023915 4.4614E-06
11.381 0.62328 -0.0024353 3.8333E-06
40.152 0.31046 -0.0010291 1.4598E-06
92.053 -0.039953 -0.00021103 5.3469E-07
59.642 0.32831 -0.0015377 3.6539E-06
ws) g/ml
303.0000 k
0.7673 767.3262 0.796
0.6472 647.1724 0.655
0.9028 902.8000 0.913
0.7828 782.8067 0.787
1.0230 1023.0130 1.027
0.7984 798.4069 0.493

A + B T + CT2
KOMPONEN A B C
HCL 0.00119 4.48E-05 2.10E-10
(CH3)2O -0.0315 1.50E-04 1.39E-09
CH3CL -0.00185 2.03E-05 7.32E-08
CH3OH 0.00234 5.43E-06 1.32E-07
H2O 0.00053 4.71E-05 4.96E-08

LOG10=A+B [ 1-T/C]2/7 (yg organik BMZA
densitaszat R*
KOMPONEN A B C spgr  
HCL 0.8045 -2.10E-03 -2.32E-16denstasrefrensi BMre
(CH3)2O -1.5099 0.9936 4.00E+02 R*
CH3CL -1.7528 1.3686 4.16E+02
CH3OH -1.1793 0.6191 5.13E+02
H2O -0.2758 4.61E-03 -5.54E-06
Propane -1.2127 0.6611 3.70E+02
Xi,f*µ
26.06080
0.00000
122.94325
0.01020
0.00865
149.02289 MIKROPOISE
0.0149 cP
CP FLUIDA panas
HCL 39.48962 0.13635176484
(CH3)2O 0.00000 0
CH3CL 250.08367 0.86350165503
CH3OH 0.02298 7.93568065E-05
H2O 0.01947 6.72233231E-05
TOTAL 289.615740157785 1
CP FLUIDA dingin
PROPANE 423.642414654455 1
TOTAL 423.642414654455 1
1439.71247 39.48962 0.13635 120.97228 16.49478
0.00000 0.00000 0.00000 74.19822 0.00000
12625.47413 250.08367 0.86350 90.90531 78.49689
0.73642 0.02298 0.00008 77.94484 0.00619
0.35073 0.01947 0.00007 67.96121 0.00457
14066.27375 289.61574 1.00000 431.98186 95.00242

0.0095
0.022991
suhu t2-t1 207.499356313794 k

Xi / pi V (m3)
0.102 1138.1295 0.00009 1.26498118859746
0.000 782.6472 0.00000 0
0.898 1077.9139 0.00083 11.7128777293833
0.000 862.2831 0.00000 0.00085403584281 Densitas = 1 ; (∑X
0.000 1106.3836 0.00000 0.00031700833917
1.000 0.00092 12.979029962163
Kg/m3 67.6597 lb/ft3
0.06243 lbm/ft3
-49.4342769592
BMZAT * Pzat
ensitaszat R * Tzat BMzat* Pzat * Rref * Tref
 
stasrefrensi BMref * Pr ef BMref * Pr ef * Rzat * Tzat
R * Tre
CP FLUIDA panas
29.0702586129618 0.10872184613463
54.8832233489722 0
38.2621434118204 0.65444041122962
40.8369134493845 0.00010113872538
33.6398751644471 0.00012552784892
0.76338892393854 KJ/KG.K
0.1823 BTU/LBM.°F
CP FLUIDA dingin
80.1888429516568 4.45122636423296
4.45122636423296 kj/kg.k
1.0631 btu/lbm.°F
MIKROPOISE
cP
lb/ft.jam

Xi / pi
air 7631.9181 1.000 1141.3612 0.00088
TOTAL 7631.9181 1.000 0.00088
Densitas = 1 ; (∑Xi/ρ) 1141.361206793 Kg/m3 71.2552
1 kg/m3 0.06243 lbm/ft3

HCl 39.48962 0.13635 36.4580 4.97111
(CH3)2O 0.00000 0.00000 46.0690 0.00000
CH3CL 250.08367 0.86350 50.4850 43.59388
CH3OH 0.02298 0.00008 32.0420 0.00254
air 0.01947 0.00007 18.0150 0.00121
TOTAL 289.6157 1.000 48.56875
R 0.08206
tzat 391.4527
bm zat 48.56875
p zat 1
S= 1.2765
k
V (m3)
6.68668082862316
6.68668082862316
lb/ft3
densitas zat campuran 1.51198 g/l

0.0015 gr/cm3
1.5120 KG/M3
k tref 298 k
atm p ref 1 atm
SUHU MASUK VAPOURIZER : 37.87 C
SUHU KELUAR VAPOURIZER : 65 C
TEKANAN : 1 ATM
LAJU ALIR MASSA : 10554.7671851092 KG/JAM
Bahan Konstruksi : Carbon Steel SA 285 Grade C
1. Data Perhitungan
Beban Panas =
=
SHELL
Fluida Panas = Stem
=
Th in =
Th Out =
Fluida Dingin = komponen msu

=
Tc in =
Tc Out =
Menghitung LMTD preheating

Fluida Panas (˚F)
392 Suhu tinggi
338 Suhu rendah
54 Selisih
1. ∆t LMTD =
=
3. Menghitung Suhu Caloric (Tc dan tc) Preheating
Tc = T1 + T2
2
= 392
2
= 365
tc = t1 + t2
2
= 100.166
2
= 124.583

Annulus = stem
Pada, T = 365
µ = 0.01569
0.037976750525734
Pipa = fluida dingin
Pada, T = 124.583
µ = 0.39039
0.944747905192447

Fluida Panas = stem
Fluida Dingin = fluida dingin
UD = 200-700 Btu/jam Ft^2 ˚F
Dipilih = 200
A =
=
kg/jam
Laju alir fluida dingin 10554.7671851092
Laju alir fluida panas 4968.55551507546
OD 0.750 in
BWG 10
ID 0.482 in
Panjang tube (L) 16 ft
Pitch 0.938 in,SQ
Nt = A / (L.Ao) 67.3691665849054 =
Shell (Dingin)
ID 12 in
B 5 in
Pass 1
Shell ID dari fig.28 Hal.838 0.55 0.045833333333333
Ud Kor. = Q / (A kor. x ∆t) 4.64678595536493
C' = pitch - OD 0.1875
Bagian tube (steam)
A't 0.182 in^2
At = (Nt*A't)/(144*n) 0.061930555555556 ft2
Gt = Wt/At 176871.929556961 lb/ft2.jam

aa = ID
= 0.083333333333333
id x c x B / 144 x Ptc

Ga = W
aa
=

Pada Tc = 365
De = 0.045833333333333
Rea = De x Ga
µ
= 0.045833333333333
0.03798
= 158,639

jH = 250

Tc = 365
K = 0.01886
Cp = 0.35857
Cp X µ ⅓ 0.358568
K = 0.018861
= 0.897108451532505
9. Menghitung ho
ho = jH k Cp X µ
De K
250 0.018860573506881
0.045833333333333
92.2907994205807 Btu/jam ft ˚F

Up =
=
11. menghitung luar area yang di buruhkan preheting :

Ap =
12. TOTAL CLEAN SURFACE = Ac =

Ac = Ap + Av
= 298.98624
13. Weighted clean overall coefisien Uc :

Uc= ∑U A
Ac
1
=
Ud
1
200
0.005
rd
Preaheter SHELL
1 Res
f
2 lenght pf preheat zone
Lp = L . Ap/Ac
=
3. No. Of crosses
ID
s
Ds'
PRESSURE DROP Os
4. ΔPs
total ΔPs =
total ΔPt =
DASAR PERANCANGAN steam d
TD STEAM JENUH 200 YAWS
Panas laten
Komponen A Tc n
Steam 52.053 647.13 0.321
n=Q/λ 78.3389861111 Kgmol/jam
m = n x BM 1411.276834792 kg/jam
2675567.1449 Kj/jam
2535982.80692037 btu/jam
Stem
4968.55551507546 kg/jam
10953.7768596457 lb/jam
200 ˚C = 392 ˚F
170 ˚C = 338 ˚F
komponen msuk
10554.7671851092 kg/jam
23269.2508316354 lb/jam
37.87 ˚C = 100.166 ˚F
65 ˚C = 149 ˚F
Fluida Dingin (˚F) Selisih (˚F) ∆t

149 243 ∆t2
100.166 237.834 ∆t1
48.834 5.166 ∆t2 - ∆t1
∆t2 - ∆t1 Qp
ln (∆t2 /∆t1) 362,774.7387 Kj/jam
5.166 ˚F 343,848.7806 btu/jam
ln 7 ˚F qp
240.407749275381 ˚F ∆t LMTD 1430.2732822 btu/jam.°F
q qp qv
+ 338
3.
t  t  t
2
˚F
Δt LMTD = Q
∑q/Δt
+ 149
2
˚F
˚F = 459.6200 K
cP
lb/ft.jam
˚F = 324.9865 K
cP
lb/ft.jam
(µ cP<0.5 cP)
tu/jam Ft^2 ˚F
Btu/jam Ft^2 ˚F
Qs
UD x ∆t LMTD
2535982.80692037
200 x 59.92594
211.593078409871 ft^2
shell and tube
lbm/jam
23269.2508316354
10953.7768596457
Tube (Panas)
Jumlah tube (n) 98
OD 3/4 in = 0.0625
ID 0.482 in = 0.04016666667
ft BWG 10
Pitch 0.938 in,SQ
Pass 2
A't 0.182 in^2 = 0.01516666667
PREHEATING
uida dingin Tu

ap
ft^2

10953.7768596457 lbm/jam Gp
0.083333333333333 ft^2
131445.322315748 lb/jam ft^2

˚F Pada Tc
lb/ft.jam µ organik
ft D
Rep
131445.322315748
0.03798
162.217

Dari buku kern fig.24 hal 834 diperoleh j
jH

˚F Tc
Berdasarkan yaws 1999, halaman 552 d
btu/jam ft ˚F K
Berdasarkan yaws 1999, halaman 78 dip
btu/lb ˚F Cp
lb/ft.jam µ organik
0.03798 ⅓ Cp X µ
0.018861 K
Øv = µ/µw = 1
9. Menghitung hi
⅓ µ 0.14 hi =
µw
0.897108451532505 1 =
10. Menghitung hio

hio
hio x ho
hio + ho
382.709284837395 x 92.29079942058
382.709284837395 + 92.29079942058
74.3590306904852 Btu/jam ft^2 ˚F
n preheting :
qp 343,848.7806
Up X (Δt)p 17876.4872065985
= 19.2346950857552 ft2
URFACE = Ac = 14.
ft2
1430.2732822038 40888.3423997704
298.98624
141.54035 Btu/jam ft^2 ˚F
1
+ Rd
Uc
1 rd
141.54035
0.007065123271947
0.707701735347383
steam
158,639 1
0.0013 fig 29
reheat zone
16 19.2346950857552
298.98624
1.02932872423726 ft
N+1 12L/B
2.47038893816943
0.045833333333333 2
0.403267 ft
1 ft
1
f x (Gs^2) x Ds' x (N+1) /(5.22x10^10 x ID x s x Os) 3
0.057511399752452 psi
1.64926422927361 psi
2.71032191157727 psi 4
Va
Va^2
2 x g'
1.64326187051715
2
0.02551648867
NGAN steam di shell
Panas laten
Td Lambda (Kj/mol) Lambda (KJ/kgmol)
473 34.15371167905 34153.7116790546
474.74 K
444.5 K
R 1.10578695171 R=(T1-T2)/(t2-t1)
S 0.16733485475 S=(t2-t1)/(T1-t1)
Ft 0.96 FT=fig.13 hal;328
311.31296 K delta T 230.791439304 delta T=lmtd/ft
338.66 K
Menghitung LMTD vaporizing

Fluida Panas (˚F) Fluida Dingin (˚F) Selisih (˚F)
392 Suhu tinggi 149 243
338 Suhu rendah 149 189
54 Selisih 0 54
2. ∆t LMTD = ∆t2 - ∆t1

ln (∆t2 /∆t1)
= 54 ˚F
ln 7 ˚F
= 214.870273742 ˚F
qp qv
 42318.61568197 btu/jam.°F
t t
2535982.807 btu/jam
42318.616 btu/jam.°F
59.92594 °F
ft
ft
ft
enghitung Flow Area (a)

= 0.00516087963 ft^2
Nt x at/ 144 x n
enghitung mass velocity

= W 23269.2508316354 lbm/jam
ap 0.00516087962963 ft^2
= 4508776.11987732 lb/jam ft^2
ynold Number (Rep)

= 124.583 ˚F
= 0.944747905192 lb/ft.jam
= 0.0402 ft
= D x Gp
µ
= 0.0402 4508776.11987732
0.944747905192447
= 191,694 191.601
enentukan Heat Transfer

buku kern fig.24 hal 834 diperoleh jh =
= 450
enghitung Thermal Konduktivity

= 124.583 ˚F w/mK
= 0.01886 btu/jam ft ˚F
= 0.4469 btu/lb ˚F
= 0.94475 lb/ft.jam
⅓ 0.446872654987 0.944747905192447 ⅓
= 0.01886
= 2.818263576086
enghitung hi Øv = µ/µw = 1
asarkan kern 1950, persamaan 6.15a halaman 114 diperoleh:
jH k Cp X µ ⅓ µ
D K µw
450 0.01886 2.81826357608554 1
0.0402
595.50199923 Btu/jam ft ˚F
Menghitung hio
asarkan kern 1950, persamaan 6.5 halaman 111 diperoleh:
= hi ID
OD
= 595.5019992283 0.040166666666667
0.0625
= 382.7092848374 Btu/jam ft ˚F
design overall coeficient

Surface / lin ft of tube (Ao) = 0.1963 table10
Total surface ( A koreksi) = L X Nt a''
= 307.7984 ft2 28.5954
Ud= Q 2535982.80692037
A. Δt 307.7984 59.92594
137.488095071235 Btu/jam ft^2 ˚F
Rd Uc-Ud 141.54035 137.48810

Uc.Ud 141.54035 137.48810
SUMMARY
Uc 141.54035 Btu/jam ft^2 ˚F

Ud 137.488095071 Btu/jam ft^2 ˚F
fluida
TUBE
For Ret 191,694
f 1.2E-05 fig 26
s 0.762166
G 4508776.119877
L 16
n 2
Ds 0.0402
Ot 1
ΔPt = 1 f . G^2 . Ln
2 5,22 . 10^10 . Ds .s. Ot
ΔPt = 2.442490502884 psi
Gt 4,508,776 V^2/2g' 0.02551648867

0.267831408693
∆P = ∆Pt + ∆Pn eq. 7.47

2.710321911577 psi
∆P < 10 psi LIQUID
= Ga
x ρ
3600
= 4,508,776
x 762.1657
3600
= 1.643261870517 fps
1.64326187051715 625
X
x 32.2 144
GAS
KOMPONEN
HCL
(CH3)2O
CH3CL
CH3OH
H2O
densitas
Komponen
CH3OH
H2O
ch3cl
hcl
dme
viskositas gas (microp

A + B T + CT2
KOMPONEN
HCL
(CH3)2O
CH3CL
CH3OH
H2O
viskosit
∆t LOG 10 VISKOSITAS L
∆t2 KOMPONEN
∆t1 HCL
∆t2 - ∆t1 (CH3)2O
CH3CL
Qv CH3OH
9,269,266.9828 Kj/jam H2O
8,785,689.3243 btu/jam
qv
∆t LMTD 40888.3423997704 btu/jam.°F
Komponen
H2O
Total
Komponen
CH3OH
H2O
TOTAL
konduktivit
Komponen
CH3OH
H2O
Total
konduktivi
Komponen
H2O
Total
kg/jam lbm/jam
Laju alir fluida ding8443.81374808734 18615.400665308
tc = t1 + t2
2
= 149
2
= 149
= 338.66
Menentukan viskositas vapourizer
tube = vapour
Pada, T = 149
µ = 0.01104
0.0267207367042
Dari uku Kern tabel 10 hal.843, spesifikasi tube

OD
BWG
ID
Flow area per tube (
Surface per in ft (Ao
Panjang tube
Pitch
Nt = A / (L.Ao)
Dari uku Kern tabel 9 hal.842, spesifikasi HE di
Shell
ID
B
Pass
Shell ID dari fig.28
A koreksi = Nt x L x
Ud Kor. = Q / (A kor.
C' = pitch - OD
Bagian tube (steam)
A't
At = (Nt*A't)/(144*
Gt = Wt/At

aa = ID
= 0.06193055555556 ft^2
Nt x at/ 144 x n

Ga = W 18615.400665308
aa 0.0619305555556
= 300585.07465849

Pada Tc = 149
µ air pendingin = 0.02672 lb/ft.jam
De = 0.04016666666667 ft
Rea = De x Ga
µ
= 0.04016666666667 300585.07465849
0.02672
= 451,840

jH = 900

Tc = 149 ˚F
Cp = 0.3549 btu/lb ˚F
µ air pendingin = 0.02672 lb/ft.jam
Cp X µ ⅓ 0.354859 0.02672
K = 0.01113
= 0.94788122951851
9. Menghitung ho
h0 = jH k Cp X µ
De K
= 900 0.0111 0.9478812295185
0.04016666666667
= 236.4685771312 Btu/jam ft ˚F
10. Menghitung Clean Overall Coefficient (Uv)

Uv = hio x ho
hio + ho
= 382.7092848374
382.7092848374
= 146.15948921796
11. menghitung luar area yang di buruhkan preheting :

Av = qv
Uv X (Δt)v
Check of maksiumum flux
Av 279.75154140554
m2
A= Ac
A koreksi
298.98624
= 287.99679160036
Flux = Qv 8,785,689.3243
A 287.996791600358
= 30506.2055569062 BTU/JAM.FT2
0.0002082337375
Vapouruzer
1 Res 451,840
f 0.001 fig 29
SG 0.972692
2. LENGHT OF VAPORTION ZONE
Lv= L - Lp
14.97067127576 ft
3. No. Of crosses N+1 12L/B

35.9296110618306
4G 300585.0746585 lb/jam ft^2

Ds 1 ft
ID 0.040166666667
Os 1
ΔP v = f x (Gs^2) x Ds' x (N+1) /(5.22x10^10 x ID x s x Os)

1.591752829521 psi
S
cp gas ( j/mol.K)
A B C D E
29.244 -0.0012615 1.121E-06 4.9676E-09 -2.4963E-12
34.668 0.070293 0.0001653 -1.7675E-07 4.9313E-11
27.385 0.026036 0.0001032 1.0887E-07 3.1642E-11
40.046 -0.038287 0.00024529 -2.1679E-07 5.9909E-11
33.933 -0.0084186 2.9906E-05 1.7825E-08 3.6934E-12

A * B^-(1-T/Tc)^n
Td a b n Tc
64.7000 0.2720 0.2719 0.2331 512.5800
100.0000 0.3471 0.2740 0.2857 647.1300
-23.7000 0.3582 0.2611 0.2869 416.2500
85.0500 0.4413 0.2696 0.3187 324.6500
-24.5000 0.2639 0.2633 0.2806 400.1000

A + B T + CT2
A B C
-9.118 5.55E-01 -1.11E-04
-4.276 3.03E-01 6.35E-05
-1.374 3.86E-01 -4.87E-05
-14.236 3.89E-01 -6.28E-05
-36.826 4.29E-01 -1.62E-05

A B C D
-1.515 1.95E+02 3.07E-03 -1.38E-05
-7.4844 5.84E+02 2.78E-02 -4.04E-05
-7.3473 8.54E+02 1.95E-02 -2.35E-05
-9.0562 1.25E+03 2.24E-02 -2.35E-05
-10.2158 1.79E+03 1.77E-02 -1.26E-05
18.01500 4968.55552 275.80103 1.00000 156.9287
4968.55552 275.80103 1.00000 156.92872
viskositas fluida masuk (dingin)

32.04200 10544.21242 329.07473 0.99822 0.39014
18.01500 10.55477 0.58589 0.00178 0.53430
50.05700 10554.76719 329.66062 1.00000 0.92444

KG/JAM XI K XI . K
10544.21242 0.999 0.06801 0.067938
10.55477 0.001 0.63802 0.000638
10554.7671851092 1 0.068576 W/(M.K)

0.0396224915217 BTU/FT.JAM.F

KG/JAM XI K XI . K
4968.55552 1 0.03264 0.032643
4968.55551507546 1 0.032643 W/(M.K)

0.0188605735069 BTU/FT.JAM.F
+ 149
˚F
K
˚F = 338.6600 K
cP
lb/ft.jam
u Kern tabel 10 hal.843, spesifikasi tube direncanakan sebagai berikut

3/4 in
10
0.482 in
0.182 in^2
0.1963 ft^2
16 ft
0.938 in, tringular
67.3691665849054 = 98 Nt = Jumlah tube, dibulatkan ke atas (hal.842)
u Kern tabel 9 hal.842, spesifikasi HE direncanakan sebagai berikut
Tube
12 in Jumlah tube 98
5 in OD 3/4 in =
1 ID 0.482 in =
0.55 BWG 10
307.7984 ft^2 Pitch 0.938 in square
4.64678595536493 Pass 2
0.1875 A't 0.182 in^2
ube (steam)
0.182 in^2
0.083333333333333 ft2
279231.009979625 lb/ft2.jam
VAPORIZING
ft^2
lb/jam ft^2
Øv = µ/µw = 1
⅓ µ 0.14
µw
1
x 236.468577131202
+ 236.468577131202
Btu/jam ft^2 ˚F
8,785,689.3243
31405.3294582351
279.751541405537 ft2
307.7984
ft2 26.7558 m2
cp cair ( j/mol.K)
KOMPONEN A B C D
HCL 73.993 -0.12946 -7.898E-05 2.6409E-06
(CH3)2O 48.074 0.56225 -0.0023915 4.4614E-06
CH3CL 11.381 0.62328 -0.0024353 3.8333E-06
CH3OH 40.152 0.31046 -0.0010291 1.4598E-06
H2O 92.053 -0.039953 -0.00021103 5.3469E-07
ws) g/ml
303.0000 k
0.7828 782.8067 0.787
1.0230 1023.0130 1.027
0.9028 902.8000 0.913
0.7673 767.3262 0.796
0.6472 647.1724 0.655

A + B T + CT2
KOMPONEN A B C
HCL 0.00119 4.48E-05 2.10E-10
(CH3)2O -0.0315 1.50E-04 1.39E-09
CH3CL -0.00185 2.03E-05 7.32E-08
CH3OH 0.00234 5.43E-06 1.32E-07
H2O 0.00053 4.71E-05 4.96E-08

LOG10=A+B [ 1-T/C]^2/7 (yg organik)
KOMPONEN A B C
HCL 0.8045 -2.10E-03 -2.32E-16
(CH3)2O -1.5099 0.9936 4.00E+02
CH3CL -1.7528 1.3686 4.16E+02
CH3OH -1.1793 0.6191 5.13E+02
H2O -0.2758 4.61E-03 -5.54E-06
viskositas vapo
CH3OH 32.04200 10544.21242
H2O 18.01500 10.55477
Xi,f*µ TOTAL 50.05700 10554.76719

156.92872
konduktivitas vapourizer dingin
156.92872 micropoise Komponen KG/JAM XI
0.0157 cP CH3OH 10544.21242 0.999
H2O 10.55477 0.001
Total 10554.76718511 1
Xi,f*µ
0.38944
0.00095
0.39039 CP
CP FLUIDA DINGIN (fluida masuk)

CH3OH 329.07473 0.99822275489 47.90239419745 1.49233068790351
H2O 0.58589 0.00177724511 90.813518048 0.00895908301421
TOTAL 329.6606151953 1 1.50128977091772

0.35856833717493
CP FLUIDA panas (steam)

H2O 275.8010277588 1 33.70626531178 1.87101111916618
TOTAL 275.8010277588 1 1.87101111916618

0.44687265498727
tkan ke atas (hal.842)
0.0625 ft
0.04016666666667 ft
Densitas (fluida dingin) suhu tc 324.9865 k
Komponen massa (Kg/jam) Fraksi (xi) p, Kg/m3 Xi / pi V (m3)
ch3oh 10544.21242 0.999 761.9828 0.00131 13.83786152481
air 10.55477 0.001 1002.5574 0.00000 0.010527843569
TOTAL 10554.7672 1.000 0.00131 13.84838936838
Densitas = 1 ; (∑Xi/ρ) 762.1656861562 Kg/m3 47.5820 lb/ft3
1 kg/m3 0.06243 lbm/ft3
Densitas (fluida panas) suhu Tc 459.6200 k

air 275.801027759 1.000 18.0150 18.01500
TOTAL 275.8010 1.000 18.01500

diketahui
p zat 1 atm p ref
BMZAT * Pzat
spgr   
R * Tre
S= 0.403267
viskositas vapourizing
329.07473 0.99822 110.42306 110.22681
0.58589 0.00178 106.60115 0.18946
329.66062 1.00000 217.02421 110.41627 micropoise

0.0110 cP
vapourizer dingin
K XI . K
0.01927 0.019247
0.02216 0.000022
0.019270 W/(M.K)
0.011133784157507 BTU/FT.JAM.F
CP FLUIDAvapourizing
CH3OH 329.07473 0.998222755 47.5798539526
H2O 0.58589 0.001777245 35.2528195235
TOTAL 329.660615195275 1
KJ/KG.K
BTU/LBM.°F
kj/kg.k
btu/lbm.°F
Densitas shell (fluida dingin) suhu tc
Komponen mOL (KgMOL/jam) Fraksi (Yi) BM
ch3oh 263.25978 0.998 32.0420
air 0.46871 0.002 18.0150
TOTAL 263.7285 1.000
diketahui
tzat 338.6600 k
bm zat 32.01707 g/gmol
p zat 1 atm
BMZAT * Pzat
densitaszat R * Tzat BMzat* Pzat
spgr   
denstasrefrensi BMref * Pr ef BMref * Pr ef
R * Tre
298 k S=
28.964 g/gmol
1 atm
* Rref * Tref
* Rzat * Tzat
ng
(Xi . Cp )/bm
1.482282407154
0.003477818538
1.485760225692 KJ/KG.K
0.354859257611 BTU/LBM.°F
338.6600 k
Xi * Bm
31.98505
0.03202
32.01707
tref 298 k
bm ref 28.964 g/gmol
p ref 1 atm
Pzat
BMzat* Pzat * Rref * Tref

r ef BMref * Pr ef * Rzat * Tzat
0.972692
CD
Kode : C-01
Tipe : SHELL TUBE
Dasar Perancangan
Suhu bahan masuk :
Tekanan masuk :
Laju alir :
Bahan Konstruksi :
1. Data Perhitungan
=
=
Fluida Panas =
=
Th in(T1) =
Th Out(T2) =

=
Tc in(t1) =
Tc Out(t2) =
2. Menghitung LMTD
Fluida Panas (˚F)
428.54 Suhu tinggi
58.0054351539398 Suhu rendah
370.53456484606 Selisih
∆t LMTD =
=
Tc = T1 + T2
2
= 428.54
2
= 243.27271757697
tc = t1 + t2
2
= -247
2
= -161.5

Pada, T = 243.27271757697
µ = 0.0646
0.1564
Pipa = AIR PROSES
Pada, T = -161.5
µ = 0.48995
1.185690

Dipilih = 15
A =
=

kg/jam
OD 1.500 in
BWG 10
ID 1.23 in
Panjang tube 16 ft
Nt = A / (L.Ao) 36.9833526196635 =
Shell
ID 17.25 in
B 5 in
Pass 1
Ud Kor. = Q / (A kor. x ∆t) 14.2243663921783
C' = pitch - OD 0.3750
Bagian tube (steam)
A't 1.19 in^2
At = (Nt*A't)/(144*n) 0.161145833333333 ft2
Gt = Wt/At 192439.281800707 lb/ft2.jam

aa = ID
= 0.421142578125

Ga = W
aa
=

Pada Tc = -161.5
De = 0.123333333333333
Rea = De x Ga
µ
= 0.123333333333333
1.185690
= 4,156

jH = 40

Tc = -161.5
K = 0.037853
Cp = 1.0631
Cp X µ ⅓ 1.06313175959134
K = 0.037853
ho = = 3.21725485137186
= 9. Menghitung ho
= jH k Cp X µ
De K
40 0.037853
3.21725485137186
0.123333333333333
39.497253737348 Btu/jam ft ˚F

-161.5
-53.0099280404522
11. At tw -53.0099280404522
Øs =(µ/µw)^0,14

= 44.2313747020545
Uc = hio x ho
hio + ho
= 107.8656380308
107.8656380308
= 28.9109179639777

a" 0.3925
Ud Q 1381125.8878
A.delta t 92075.0591862149
15

Rd Uc-Ud 13.9109179639777
Uc.Ud 433.663769459665
SUMMARY
Uc 28.9109179639777 Btu/jam ft^2 ˚F


1 Res 4,156
standar (aor 1000 kg/m3) s 1.14136120679346
Ds' 1.4375

(5.22x10^10 x DE x s x Os)
0.035971855328107
∆P < 10
CD
220.3 ˚C
1 atm
14066.2737 KG/JAM
404762.5417 J/S
1457145.1503 kj/jam
1381125.8878 btu/jam
ALIRAN 15
14066.2737 kg/jam
31010.7884318431 lb/jam
220.3 ˚C = 428.54
14.447463974411 ˚C = 58.0054351539398
AIR PENDINGIN
7631.9181 kg/jam
16825.479281622 lb/jam
-155 ˚C = -247
-60 ˚C = -76

-76 504.54 ∆t2 S
-247 305.00543515394 ∆t1 FT
171 199.53456484606 ∆t2 - ∆t1 delta T
∆t2 - ∆t1
ln (∆t2 /∆t1)
199.53456484606 ˚F
ln 1,0986 ˚F
396.4387 ˚F
+ 58.0054351539398
2
˚F
+ -76
2
˚F
˚F = 391.4527 K
cP
lb/ft.jam
˚F = 164.7800 K
cP
lb/ft.jam
(µ cP<0.5 cP)

Btu/jam Ft^2 ˚F
Qs
UD x ∆t LMTD
1381125.8878
15 x 396.43873769797
232.255454451487 ft^2
kg/jam lbm/jam
7631.9181 16825.479281622
14066.2737 31010.7884318431
lb/jam
Tube
Jumlah tube 39
OD 1.5000 in =
ID 1.23 in =
ft BWG 10
Pass 2
A't 1.19 in^2
eam)
de/fluida dingin
ft^2
16825.479281622 lb/jam
0.421142578125 ft^2
39951.9786304485 lb/jam ft^2
˚F
lb/ft.jam
ft
39951.9786304485
1.185690
˚F 164.78 K
btu/jam ft ˚F
btu/lb ˚F
lb/ft.jam
1.185690 ⅓
0.037853
⅓ µ 0.14
µw
1

39.497253737348 404.77271757697
147.362891768148
F 225.5344 K
F µw=0,56 x 2,42
0.528206 lb/ft.jam
1
eq 6.36
btu/jam.ft2.°F
x 39.497253737348 174.195855507374
+ 39.497253737348 174.195855507374
Btu/jam ft^2 ˚F
ft^2/linft
ft2 21.5772 m2
BTU/JAM
FT.°f
Btu/JAM ft^2 oF

Uc.Ud
Pressre Drop
1
ft2/in2 fig 29
ft
2
12L/B
38.4
x DE x s x Os) 3
psi
liquid 4
cp gas ( j/mol.K)
KOMPONEN A B
HCL 29.244 -0.0012615
(CH3)2O 34.668 0.070293
CH3CL 27.385 0.026036
CH3OH 40.046 -0.038287
H2O 33.933 -0.0084186
densitas
Komponen
HCL
(CH3)2O
ch3cl
CH3OH
H2O
Propane
˚F 495.2024 K
A + B T + CT2
KOMPONEN
HCL
(CH3)2O
CH3CL
˚F 116.9 K CH3OH
˚F 212.66 K H2O
visk
0.253130828670397 S=(t2-t1)/(T1-t1) KOMPONEN
CH3CL
CH3OH
H2O
propane
0.48995
Komponen
HCl
(CH3)2O
CH3CL
CH3OH
H2O
Total
kondu
Komponen
HCl
(CH3)2O
CH3CL
CH3OH
H2O
Total
kondu
Komponen
PROPANE
Total
Tube
0.125 ft L/D 156.09756097561

0.1025 ft

ap = 0.161145833333333 ft^2

Gp = W 31010.7884318431
ap 0.161145833333333
= 192439.281800707

Pada Tc = 243.27271757697 ˚F
D = 0.1025 ft
Rep = D x Gp
µ
= 0.1025 192439.281800707
0.156448222572195
= 126,080

jH = 300

Tc = 243.27271757697 ˚F
Cp = 8.8330 btu/lb ˚F
Cp X µ ⅓ 8.83296471723709 0.1564
K = 0.008105302873517
= 5.5450137456324
9. Menghitung hi
hi = jH k Cp X µ
D K
= 300 0.008105302873517 5.5450137456324
0.1025
= 131.543461013171 Btu/jam ft ˚F
10. Menghitung hio

hio = hi ID
OD
= 131.543461013171 0.1025
0.125
= 107.8656380308 Btu/jam ft ˚F
11. At tw 225.5344 K
Øt =(µ/µw)^0,14 1

= 174.195855507374 btu/jam.ft2.°F
X 44.2313747020545
+ 44.2313747020545
35.2745495564088
0.032077657723887
For Ret 126,080

f 0.00013 fig 26
s #NUM!

(5.22x10^10 x ID x s x Ot)
= #NUM!
Gt 192,439 V^2/2g' 0.005

#NUM!
∆P = ∆Pt + ∆Pn eq. 7.47

#NUM! psi
∆P 1,5 - 2 psi GAS

s ( j/mol.K)
(A + B T + C T2 + D T3 + E T4 ) CAIR
C D E KOMPONEN
1.121E-06 4.9676E-09 -2.4963E-12 HCL
0.0001653 -1.7675E-07 4.9313E-11 (CH3)2O
0.0001032 1.0887E-07 3.1642E-11 CH3CL
0.00024529 -2.1679E-07 5.9909E-11 CH3OH
2.9906E-05 1.7825E-08 3.6934E-12 H2O
PROPANE
A * B^-(1-T/Tc)^n
Td a b n Tc
85.0500 0.4413 0.2696 0.3187 324.6500
-24.5000 0.2639 0.2633 0.2806 400.1000
-23.7000 0.3582 0.2611 0.2869 416.2500
64.7000 0.2720 0.2719 0.2331 512.5800
100.0000 0.3471 0.2740 0.2857 647.1300
-188.0000 0.2215 0.2774 0.2870 369.8200
A B C
-9.118 5.55E-01 -1.11E-04
-4.276 3.03E-01 6.35E-05
-1.374 3.86E-01 -4.87E-05
-14.236 3.89E-01 -6.28E-05
-36.826 4.29E-01 -1.62E-05

A B C D
-1.515 1.95E+02 3.07E-03 -1.38E-05
-7.4844 5.84E+02 2.78E-02 -4.04E-05
-7.3473 8.54E+02 1.95E-02 -2.35E-05
-9.0562 1.25E+03 2.24E-02 -2.35E-05
-10.2158 1.79E+03 1.77E-02 -1.26E-05
-3.1759 2.97E+02 9.55E-03 -1.88E-05
cP

36.45800 1439.71247 39.48962 0.13635 0.01186
46.06900 0.00000 0.00000 0.00000 0.05009
50.48500 12625.47413 250.08367 0.86350 0.07296
32.04200 0.73642 0.02298 0.00008 0.20082
18.01500 0.35073 0.01947 0.00007 0.23347
14066.27375 289.61574 1.00000 0.56920

KG/JAM XI K XI . K
1439.71247 0.102352086498 -0.01833 -0.001876
0 0 0.03091 0.000000
12625.47413 0.897570625551 0.01770 0.015884
0.73642 5.235364151E-05 0.06693 0.000004
0.35073 2.493430918E-05 0.68079 0.000017
14066.27375 1 0.014028 W/(M.K)

0.0081 BTU/FT.JAM.F

KG/JAM XI K XI . K
7631.9181 1 0.06551 0.065514
7631.9181 1 0.065514 W/(M.K)

0.0379 BTU/FT.JAM.F
0.21827 CP
0.0000 cP
0.528206 lb/ft.jam
HCl 36.45800
(CH3)2O 46.06900
CH3CL 50.48500
CH3OH 32.04200
H2O 18.01500
Total

HCl 1439.71247
(CH3)2O 0.00000
CH3CL 12625.47413
CH3OH 0.73642
air 0.35073
TOTAL 14066.2737
#NUM!
lb/jam 1 kg/m3
ft^2
lb/jam ft^2
w/Mk 391.4527218431 k
0.14
⅓ µ Øt
µw sama
1
µw=1,5 x 2,42
0.021046 lb/ft.jam
eq 6.37
fig 27
cp cair ( j/mol.K)
A B C D
73.993 -0.12946 -7.898E-05 2.6409E-06
48.074 0.56225 -0.0023915 4.4614E-06
11.381 0.62328 -0.0024353 3.8333E-06
40.152 0.31046 -0.0010291 1.4598E-06
92.053 -0.039953 -0.00021103 5.3469E-07
59.642 0.32831 -0.0015377 3.6539E-06
ws) g/ml
303.0000 k
0.7673 767.3262 0.796
0.6472 647.1724 0.655
0.9028 902.8000 0.913
0.7828 782.8067 0.787
1.0230 1023.0130 1.027
0.7984 798.4069 0.493

A + B T + CT2
KOMPONEN A B C
HCL 0.00119 4.48E-05 2.10E-10
(CH3)2O -0.0315 1.50E-04 1.39E-09
CH3CL -0.00185 2.03E-05 7.32E-08
CH3OH 0.00234 5.43E-06 1.32E-07
H2O 0.00053 4.71E-05 4.96E-08

KOMPONEN A B C
HCL 0.8045 -2.10E-03 -2.32E-16
(CH3)2O -1.5099 0.9936 4.00E+02
CH3CL -1.7528 1.3686 4.16E+02
CH3OH -1.1793 0.6191 5.13E+02
H2O -0.2758 4.61E-03 -5.54E-06
Propane -1.2127 0.6611 3.70E+02
Xi,f*µ
0.00162
0.00000
0.06300
0.00002
0.00002
0.06465 MIKROPOISE
0.0646 cP
CP FLUIDA panas
HCL 39.48962 0.13635176484
(CH3)2O 0.00000 0
CH3CL 250.08367 0.86350165503
CH3OH 0.02298 7.93568065E-05
H2O 0.01947 6.72233231E-05
TOTAL 289.615740157785 1
CP FLUIDA dingin
PROPANE 423.642414654455 1
TOTAL 423.642414654455 1
1439.71247 39.48962 0.13635 110.40751 15.05426
0.00000 0.00000 0.00000 67.20663 0.00000
12625.47413 250.08367 0.86350 83.26857 71.90255
0.73642 0.02298 0.00008 70.38340 0.00559
0.35073 0.01947 0.00007 59.10425 0.00397
14066.27375 289.61574 1.00000 390.37036 86.96636

0.0087
0.021046
suhu t2-t1 391.4527 k

Xi / pi V (m3)
0.102 #NUM! #NUM! #NUM!
0.000 415.9854 0.00000 0
0.898 651.3084 0.00138 19.3847875337213
0.000 689.5597 0.00000 0.00106795776068 Densitas = 1 ; (∑X
0.000 936.8672 0.00000 0.00037436768473
1.000 #NUM! #NUM!
Kg/m3 #NUM! lb/ft3
0.06243 lbm/ft3
CP FLUIDA panas
1311.03091447023 4.90321408070364
2202.68553463745 0
1875.36101038452 32.0764055905161
760.784562023096 0.00188419678154
331.260927592098 0.00123610659873
36.9827399746 KJ/KG.K
8.8330 BTU/LBM.°F
CP FLUIDA dingin
80.1888429516568 4.45122636423296
4.45122636423296 kj/kg.k
1.0631 btu/lbm.°F
MIKROPOISE
cP
lb/ft.jam

Xi / pi
air 7631.9181 1.000 1141.3612 0.00088
TOTAL 7631.9181 1.000 0.00088
Densitas = 1 ; (∑Xi/ρ) 1141.361206793 Kg/m3 71.2552
1 kg/m3 0.06243 lbm/ft3

HCl 39.48962 0.13635 36.4580 4.97111
(CH3)2O 0.00000 0.00000 46.0690 0.00000
CH3CL 250.08367 0.86350 50.4850 43.59388
CH3OH 0.02298 0.00008 32.0420 0.00254
air 0.01947 0.00007 18.0150 0.00121
TOTAL 289.6157 1.000 48.56875
BMZAT * Pzat
spgr   
R * Tre
BMZAT * Pzat
spgr   
R * Tre
R 0.08206
tzat 391.4527
bm zat 48.56875
p zat 1
S= 1.2765
k
V (m3)
6.68668082862316
6.68668082862316
lb/ft3
* Rref * Tref densitas zat campuran 1.51198 g/l

0.0015 gr/cm3
* Rzat * Tzat
1.5120 KG/M3
* Rref * Tref
* Rzat * Tzat

k tref 298 k
atm p ref 1 atm
rboiler stripr
Kode : H-02
Fungsi : Menaikkan temperatur umpan REAKTOR dari 248˚C
Tipe : shel and tube
Dasar Perancangan
Suhu bahan masuk :
Tekanan masuk :
Laju alir :
Bahan Konstruksi :
1. Data Perhitungan
Beban Panas (Q) =
=
=

=
Th in(T1) =
Th Out(T2) =
Fluida Dingin = ALIRAN 8

=
Tc in(t1) =
Tc Out(t2) =
2. Menghitung LMTD
Fluida Panas (˚F)
392 Suhu tinggi
392 Suhu rendah
0 Selisih
∆t LMTD =
=
Tc = T1 + T2
2
= 392
2
= 392
tc = t1 + t2
2
= 124.97
2
= 163.985

Annulus = Steam
Pada, T = 392
µ = 0.0163
0.0395
Pada, T = 163.985
µ = 0.31205
0.7552

Fluida Dingin = gases
Dipilih = 50
A =
=

OD 0.750 in
BWG 18
ID 0.652 in
Panjang tube 16 ft
Nt = A / (L.Ao) 339.190325748959 =
Shell
ID 17.25 in
B 5 in
Pass 1
Ud Kor. = Q / (A kor. x ∆t) 102.1658
C' = pitch - OD 0.2500
Bagian tube (steam)
A't 0.334 in^2
At = (Nt*A't)/(144*n) 0.192513888888889 ft2
Gt = Wt/At 641659.005424892 lb/ft2.jam

aa = ID
= 0.149739583333333

Ga = W
aa
=

Pada Tc = 392
De = 0.079166666666667
Rea = De x Ga
µ
= 0.079166666666667
0.039491093143781
= 1,379,952

jH = 230

Tc = 392
K = 0.019676
Cp = 0.449878669779053
Cp X µ ⅓ 0.449878669779053
K = 0.019676
ho = = 0.966531170033359
= 9. Menghitung ho
= jH k Cp X µ
De K
230 0.019676
0.966531170033359
0.079166666666667
55.252038527522 Btu/jam ft ˚F

163.985
168.020350606997
11. At tw 168.020350606997
Øs =(µ/µw)^0,14

= 58.3109883818954
Uc = hio x ho
hio + ho
= 3066.73035948467
3066.73035948467
= 54.2742022132012

a" 0.1963
Ud Q 12026078.3346
A.delta t 240521.566692221
50

Rd Uc-Ud 4.27420221320117
Uc.Ud 2713.71011066006
SUMMARY
Uc 54.2742022132012 Btu/jam ft^2 ˚F


1 Res 1,379,952
standar (aor 1000 kg/m3) s 0.3904
Ds' 1.4375

(5.22x10^10 x DE x s x Os)
19.9697548759178
∆P < 2 psi
rboiler stripr
mperatur umpan REAKTOR dari 248˚C menjadi 350˚C
51.65 C
1 atm
56031.5476 KG/JAM
3524447.7545 J/S
12688011.9163 kj/jam
12026078.3346 btu/jam
46754.5188530827 kg/jam
103075.947353883 lb/jam
200 ˚C = 392
200 ˚C = 392
ALIRAN 8
56031.5476 kg/jam
123528.270474923 lb/jam
51.65 ˚C = 124.97
95 ˚C = 203

203 189 ∆t2 S
124.97 267.03 ∆t1 FT
78.03 -78.03 ∆t2 - ∆t1 delta T
∆t2 - ∆t1
ln (∆t2 /∆t1)
-78.03 ˚F
ln 1,0986 ˚F 0.7078
225.7721 ˚F -0.3456139965793
+ 392
2
˚F
+ 203
2
˚F
˚F = 474.7400 K
cP
lb/ft.jam
˚F = 347.0516 K
cP
lb/ft.jam
(µ < 0,5 cP)

Btu/jam Ft^2 ˚F
Qs
UD x ∆t LMTD
12026078.3346
50 x 225.77210637387
1065.3290 ft^2
kg/jam lbm/jam
56031.54760 123528.270474923
46754.51885 103075.947353883
Tube
Jumlah tube 166
OD 0.7500 in =
ID 0.652 in =
ft BWG 18
Pass 2
A't 0.334 in^2
eam)
de/fluida dingin
ft^2
103075.947353883 lb/jam
0.149739583333333 ft^2
688368.065806803 lb/jam ft^2
˚F
lb/ft.jam
ft
688368.065806803
0.039491093143781
˚F 474.74 K
btu/jam ft ˚F
btu/lb ˚F
lb/ft.jam
0.039491 ⅓
0.019676
⅓ µ 0.14
µw
1

55.252038527522 228.015
3121.98239801219
F 349.3114 K
F µw=0,56 x 2,42
0.026875 lb/ft.jam
1
eq 6.36
btu/jam.ft2.°F
x 55.252038527522
+ 55.252038527522
Btu/jam ft^2 ˚F
ft^2/linft
ft2 98.9723 m2
BTU/JAM
FT.°f
Btu/JAM ft^2 oF
0.001575 Btu/hr ft^2 oF
Rd Uc-Ud 0.0015750400886
Uc.Ud
Pressre Drop
1
ft2/in2 fig 29
ft
2
12L/B
38.4
x DE x s x Os) 3
psi
GAS 4
cp gas ( j/mol.K)
KOMPONEN A B
HCL 29.244 -0.0012615
(CH3)2O 34.668 0.070293
CH3CL 27.385 0.026036
CH3OH 40.046 -0.038287
H2O 33.933 -0.0084186
densitas
Komponen
HCL
(CH3)2O
ch3cl
CH3OH
H2O
˚F 474.74 K
A + B T + CT2
KOMPONEN
HCL
(CH3)2O
CH3CL
˚F 325.2032 K CH3OH
˚F 368.9 K H2O
visk
0 R=(T1-T2)/(t2-t1) LOG 10 VISKOSIT
0.29221435793731 S=(t2-t1)/(T1-t1) KOMPONEN
CH3CL
CH3OH
H2O
VISKOS (steam)
163.1863 micropoise
0.0163 cP

HCl 36.45800 9350.90377
H2O 18.01500 37403.61508
Total 46754.51885

Komponen KG/JAM XI
HCl 9350.90377 0.2
(CH3)2O
CH3CL
CH3OH
H2O 37403.61508 0.8
Total 46754.5188530827 1

Komponen KG/JAM XI
H2O 46754.5188530827 1
Total 46754.5188530827 1
Tube
0.0625 ft L/D 294.478527607362

0.0543 ft

ap = 0.192513888888889 ft^2

Gp = W 123528.270474923
ap 0.192513888888889
= 641659.005424892

Pada Tc = 163.985 ˚F
D = 0.0543 ft
Rep = D x Gp
µ
= 0.0543 641659.005424892
0.755151538607673
= 46,168

jH = 450

Tc = 163.985 ˚F
K = 0.312652117595778 btu/jam ft ˚F
Cp = 1.0468210035447 btu/lb ˚F
Cp X µ ⅓ 1.0468210035447 0.7552
K = 0.312652117595778
= 1.3623281218307
9. Menghitung hi
hi = jH k Cp X µ
D K
= 450 0.312652117595778 1.3623281218307
0.0543
= 3527.68062824157 Btu/jam ft ˚F
10. Menghitung hio

hio = hi ID
OD
= 3527.68062824157 0.0543
0.0625
= 3066.73035948467 Btu/jam ft ˚F
11. At tw 349.3114 K
Øt =(µ/µw)^0,14 #DIV/0!

= #DIV/0! btu/jam.ft2.°F
Densitas (fluida dingin) suhu tc
Komponen mOL (Kg/jam) Fraksi (Yi) BM
HCl 507.17019 0.196 36.4580
(CH3)2O 0.00000 0.000 0.0000
CH3CL 0.00000 0.000 0.0000
CH3OH 0.00000 0.000 0.0000
air 2083.88215 0.804 18.0150
TOTAL 2591.0523 1.000
BMZAT * Pzat
densitaszat R * Tzat BMzat* Pzat * Rref * Tre
spgr   
denstasrefrensi BMref * Pr ef BMref * Pr ef * Rzat * Tz
R * Tre
R
tzat
bm zat
p zat
S=
densitas
For Ret 46,168
f 0.00012 fig 26
s 0.6411

(5.22x10^10 x ID x s x Ot)
= #DIV/0!
Gt 641,659 V^2/2g' 0.0061

0.076120163945357
∆P = ∆Pt + ∆Pn eq. 7.47

#DIV/0! psi
∆P < 2 psi GAS

s ( j/mol.K)
(A + B T + C T2 + D T3 + E T4 ) CAIR
C D E KOMPONEN
1.121E-06 4.9676E-09 -2.4963E-12 HCL
0.0001653 -1.7675E-07 4.9313E-11 (CH3)2O
0.0001032 1.0887E-07 3.1642E-11 CH3CL
0.00024529 -2.1679E-07 5.9909E-11 CH3OH
2.9906E-05 1.7825E-08 3.6934E-12 H2O

A * B^-(1-T/Tc)^n
Td a b n Tc
85.0500 0.4413 0.2696 0.3187 324.6500
-24.5000 0.2639 0.2633 0.2806 400.1000
-23.7000 0.3582 0.2611 0.2869 416.2500
64.7000 0.2720 0.2719 0.2331 512.5800
100.0000 0.3471 0.2740 0.2857 647.1300
A B C
-9.118 5.55E-01 -1.11E-04
-4.276 3.03E-01 6.35E-05
-1.374 3.86E-01 -4.87E-05
-14.236 3.89E-01 -6.28E-05
-36.826 4.29E-01 -1.62E-05
viskositas LIQUID (CP)

A B C D
-1.515 1.95E+02 3.07E-03 -1.38E-05
-7.4844 5.84E+02 2.78E-02 -4.04E-05
-7.3473 8.54E+02 1.95E-02 -2.35E-05
-9.0562 1.25E+03 2.24E-02 -2.35E-05
-10.2158 1.79E+03 1.77E-02 -1.26E-05
507.17019 0.19574 0.02837 0.00555
2083.88215 0.80426 0.38109 0.30649
2591.05234 1.00000 0.40945 0.31205 MIKROPOISE

0.3120 cP
INGIN
K XI . K
0.07500 0.015000
0.65765 0.526117
0.541116 W/(M.K)
0.3127 BTU/FT.JAM.F
panas
K XI . K
0.03405 0.034055
0.034055 W/(M.K)
0.0197 BTU/FT.JAM.F
lb/jam
ft^2
lb/jam ft^2
w/Mk 347.0516 k
0.14
⅓ µ Øt
µw sama
1
µw=1,5 x 2,42
#DIV/0! lb/ft.jam
eq 6.37
347.0516 k Densitas (fluida panas)
YI*BM Komponen mol (Kg/jam)
7.13626 air 2595.310510857
0.00000 TOTAL 2595.3105
0.00000
0.00000 R 0.08206
14.48876 tzat 474.7400
21.62502 bm zat 18.01500
p zat 1
zat* Pzat * Rref * Tref S= 0.3904

ref * Pr ef * Rzat * Tzat
0.08206 L.atm/gmol.K R 0.08206

347.0516 k tref 298
21.62502 g/gmol bm ref 28.964
1 atm p ref 1
0.6411
0.75933054300928 kG/L DENSITAS ZAT 0.759330543009275 g/L
0.0474 lb/ft3
0.759330543009275 kg/M3
Va = Ga
3600
fig 27 = 641659.00542489
3600
= 8.4491071264142
Va^2
2 x g'
8.44910712641416
2 x 32.2
0.131197315627549
cp cair ( j/mol.K)
A B C D
73.993 -0.12946 -7.898E-05 2.6409E-06
48.074 0.56225 -0.0023915 4.4614E-06
11.381 0.62328 -0.0024353 3.8333E-06
40.152 0.31046 -0.0010291 1.4598E-06
92.053 -0.039953 -0.00021103 5.3469E-07
s) g/ml
303.0000 k
0.7673 767.3262 0.796
0.6472 647.1724 0.655
0.9028 902.8000 0.913
0.7828 782.8067 0.787
1.0230 1023.0130 1.027

A + B T + CT2
KOMPONEN A B C
HCL 0.00119 4.48E-05 2.10E-10
(CH3)2O -0.0315 1.50E-04 1.39E-09
CH3CL -0.00185 2.03E-05 7.32E-08
CH3OH 0.00234 5.43E-06 1.32E-07
H2O 0.00053 4.71E-05 4.96E-08

KOMPONEN A B C
HCL 0.8045 -2.10E-03 -2.32E-16
(CH3)2O -1.5099 0.9936 4.00E+02
CH3CL -1.7528 1.3686 4.16E+02
CH3OH -1.1793 0.6191 5.13E+02
H2O -0.2758 4.61E-03 -5.54E-06
CP FLUIDA DINGIN
HCL 507.17019 0.195739075148962 68.4055508560075 0.36726203466
H2O 2083.88215 0.804260924851038 89.9488508126272 4.01567282508
TOTAL 2591.052335703 1 4.38293485974

1.04682100354
CP FLUIDA panas
H2O 2595.310510857 1 33.933 1.8835970025
TOTAL 2595.310510857 1 1.8835970025

0.4499
VISKOS AIR Air fase gas (steam)
111.05189 micropoise
0.0111 cP
0.026875 lb/ft.jam

Komponen BM(kg/kgmol) (kg/jam) (kmol/jam) Xi,f
HCl 36.45800 9350.90377 256.48428 #DIV/0!
(CH3)2O 0.00000 0.00000 #DIV/0! #DIV/0!
CH3CL 0.00000 0.00000 #DIV/0! #DIV/0!
CH3OH 0.00000 0.00000 #DIV/0! #DIV/0!
H2O 18.01500 37403.61508 2076.24841 #DIV/0!
Total 46754.51885 #DIV/0! #DIV/0!

suhu Tc 474.7400 k
Fraksi (Yi) BM Yi * BM
1.000 18.0150 18.01500
1.000 18.01500
L.atm/gmol.K
BM * Pt
k V 
RT
g/gmol
atm DENSITAS ZAT 0.462430987405233 g/L
0.0289 lb/ft3
0.462430987405233 kg/M3
L.atm/gmol.K
k
g/gmol
atm
x ρ
x ρ
x 0.0474
fps
625
X
144
KJ/KG.K
BTU/LBM.°F
kj/kg.k
btu/lbm.°F
µ Xi,f*µ
171.20578 #DIV/0!
109.18420 #DIV/0!
127.61832 #DIV/0!
114.11027 #DIV/0!
111.05189 #DIV/0!
633.17046 #DIV/0! MIKROPOISE

#DIV/0! cP
#DIV/0! lb/ft.jam

NM, Ne, Spek

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antoin

P (mmHg) 1 atm 760.0000

T(C) T(K) ln PA° PA°

KESIMPULAN HCL BISA DIPEISAHKAN DENGAN

KESIMPULAN DIMETIL TIDAK BISA DIPEISAHKA

3626.5000 -34.2900 364.0000 257.0000

NA) XA = (𝑃𝑡𝑜𝑡𝑎𝑙 −𝑃𝐵°)/(𝑃𝐴°−𝑃𝐵°)

∑ ἀab / total T𝐴𝐵 22.1478352570522

∑ ἀab / total T𝐴𝐵 1.02766602399052

METANOL (BAHAN BAKU) ch3oh

CAIRAN YANG DIUAPKAN MAX 80% 0.8000

MASSA METANOL (KG/JAM)MASUK REAKTOR F-01 F - 01 = 0.8 ×𝐹𝐹 - 01

(KG/JAM) BAHAN BAKU METANOL FF-01 (80%)

FF-01 (H2O) FF-01 (H2O) = FF -01 (80%) - FF

RECAYCLE (PRODUK BOTOM VAPOURIZER) KG/JAM RC-01 RC - 01 = FF -01 (80%) - F -01

komposisi bottom striper XB (%) PURITY HCL 20.0000

KOMPOSISI FF-02 (HCL) AWAL PURITY HCL 0.3300

INPUT TOP VAPOUR

REAKSI UTAMA mol (kgmol/jam) CH3OH

REAKSI SAMPING mol (kgmol/jam) 2CH3OH

kebutuhan air untuk melarutkan dme

mtil klorda 12626.3444 12626344.4186

f-01=100/(𝑝𝑢𝑟𝑖𝑡𝑦 𝑐ℎ3𝑜ℎ) ×𝑏𝑎𝑠𝑖𝑠

H2O) = FF -01 (80%) - FF-01 (CH3OH)

1 = FF -01 (80%) - F -01

(CH3OH)= KEMURNIAN CH3OH × RC −01

329.6664 8443.9612 263.7331

NERACA KOMPONEN FF-02 (HCL)× XFF-02 (HCL) = F -02 (HCL) ×XF-02(HCL) + B . XB

3039.9971 10716.7663 298.4093

KEMURNIAN HCL TOP 98.5176

NERACA MIXER satu

263.7331 10716.7663 298.4093

562.1424 19160.7275 562.1424

NERACA FLASH DRUM

KEMURNIAN CH3CL 89.6573

KEMURNIAN CH3CL 89.7570

air (L) suhu (c)

KEMURNIAN HCL 99.9713

impurity air impurity air perbandingan mol

UPL (PRODUK BOTOM VAPOURIZER)

RC - 01( CH3OH) 2108.8793

2110.9903 65.9333 80.0000

- 20%B = (1.289020023×33 %) − (1.289020023×97% ) MASSA AIR 158.8643

/𝑌 = ("(1.289020023 ×97%) -(1.289020023×33 %" ))/"30% −20 %)"

54855.5509 2736.9191 16.3434

KEMURNIAN HCL BOTTOM 20.0000

NERACA MIXER satu

NERACA FLASH DRUM

KEMURNIAN CH3OH 8.0425

kelarutan dalam air

46 gram alrut dalam 1027,58982 air

KEMURNIAN CH3CL 99.9928

KPSTS TON/TAHUN 99999.00016

% mol hcl 0.9700

% berat HCl (massa larutan utama/massa larutan ) x 100 %

% berat h2o 1.4824 %

MOL HCL = 𝑀𝑂𝐿 𝑀𝐸𝑇𝐴𝑁𝑂𝐿 𝑋 𝑃𝐸𝑇𝐵𝐴𝑁𝐷𝐼𝑁𝐺𝐴𝑁 𝑀𝑂𝐿 𝐻𝐶𝐿 1.1

Massa HCl = 𝑀𝑂𝐿 HCl 𝑋 BM Metanol

Massa Air = (𝑖𝑚𝑝𝑢𝑟𝑖𝑡𝑦 ℎ2𝑜 𝑦𝑔 𝑑𝑖𝑖𝑛𝑔𝑖𝑛𝑘𝑎𝑛 (3))/(𝑝𝑢𝑟𝑦𝑡𝑦

271.9420 73.4988 26.5012

OUTPUT BOTTOM komposisi komposisi

11.8654 98.4605 1.5395

250.1119 10.2374 89.7626