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    «2 United States Patent Bokade ‘US009988337B2 (10) Patent No.: (4s) Date of Patent: US 9,988,337 B2 Jun, 5, 2018 SINGLE STEP PROCESS FOR TH PREPARATION OF BUTYL ACETATE oa (71) Applicant: Council of Seientitic and Industrial Researeh, New Delhi (IN) @ my) Inventor: Vijay Vasant Bokade, Pune (IN) Council of Scientific and Industral Research, New Delhi (IN) Assignee (*) Notice: Subject to any disclaimer, the term of this patent is extended or adjusted under 35 USC. 154) by 0 days. days, an @y 66) Appl. No: 18/810,882 PCT Filed: Sep. 9, 2018 PCT No, 371 (XD, @) Date: PCTAN2015/050108 Mar. 10, 2017 (87) PCT Pub Nos 020161038629 PCT Pub, Date: Mar, 17, 2016 9) Prior Publication Data US 201710283361 AI Oot. 5, 2017 G0) Foreign Application Priority Data Sep. 10,2014 N) 2585/DEL/2014 (1) Incr, core 6702 core 673 Us.cL cc (C07C 67703 (2013.01) Field of Classification Search (2006.01), (2006.01), 2) (58) tion file for complete search history. 5) References Cited US. PATENT DOCUMENTS, LaMAUL A 71980. Martina FOREIGN PATENT DOCUMENTS “ wo Isr WO-2016038629 2205 32016 (OTHER PUBLICATIONS Ali, Sami H, ea, “Potential biobelaive from renewable sources—Kinetc sty of formation of butyl acetate by eteroge cous catalyzed trasesterication of styl actate with butanol ‘Bioresource Technology. vol. 102, Issue 21, Nov. 201, pp. 10004. 10103, (Nex. 2011), 10004-10103, Fischer, Emil etal, "Darsollung der Ester, European Journal of Inorganic Chomisty, 2863), Oct-Dec. 1898, 3252-3288 [English translation), (Det. 1895). 2 pas. Ghesi, Grose TF, ct al, "Biodiessl prtstion via ethytic transection with base ooites".Quim, Nova, 35(1), 2012, 119-13 [sith English translation), (2012), 119-123 Mat, R, etal, “Caalytie Studies of Borex HZSM-S Zeolite for Mesiane Conversion o Higher Hyaloesibons, Journal of Chem cal and Natural Resources Engineering, Special Faiion: 146-182, “Caalytc Applicaton of Hydrophobic Properties of HighsSilia. Zeolites i. Esefiction of Acetic Acid With TButanol, Studies in Surface Seiene and Catalysis, vol. 2, 98S, Pp. 208-211, a. 7, 2008), 208.211 Opava i, “Tomoestrifation of Esters such as hy Acetate with Aleobols Over Moudeite Type of Zeolite H-Z-HMS" Ballin of ‘Tokyo Guhagei University Sect IV 2004, 56, 53-56, (2008), 53-56, ‘Wang, tn, et al, “Preparation and use of heteropotyacid cult ‘arte on dealuminized superstable gamma zeolite, English ran Inton of Chinese Publication No. 1543253, publishol Feb 23 2005, Feb. 23, 2008.2 pas. rang, Fumi, oa, "Caalytie performances of hetropay com- eins sport om deniminae wtb Yeoh for fig hse esteiation”, Chi Ser B (2006) 4902), 140-14, (Apr 2006), 140-17, Jernatonal Application No, PCT/IN201S'0S010S,latenationl Seareh Report and Written Opinion dated Jan, 2, 2016", Jan 21 2010), 9 pas. ‘Yule, Cong, “An Overview on Syatheic Methods of a-Baryl Acsat”, Fu Chem. Bull, 2012.18) 336359, 2012), 386397 Primary Esaminer — Clinton & Brooks

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