oeezere nu zo POCCMIACKOE ATEHTCTBO lo IATEHTAM 4 TOBAPHBIM SHAKAM ® RU"? 2 182 330" C2 ©) MK” G O41 N 21/73, 33/28 (2) ONVCAHVE V3OBPETEHMA K NATEHTY POCCUMCKON SEQEPALINN (21), (22) Sanexa, 96104910728, 13.03.1996 (24) fara wevana efoto narenra: 13.03.1998 (43) Hora ny6ruaunn sasow: 10.01.2000 (48) Hara nyénmayyn: 10.05:2002 (68) Counor: US 3825945 A, 23.07.1974. SU 431451 1K, 05.08.1974, SU 1770902 A1, 23.10.1992. US 44449887 A, 15.05.1904 (98) Anpec ana nepencis 664003, r Vipnyrex, yn. Kapna Mapxca, 1, AY, paresis oven (71) Sasenrens: HaywHo-nccnenosarensoxnit wHoTATYT Inpmeniagwoi cbwaunn np MipKytcKoM rocynmaepcuTere IK "BAIIKAST" (72) Vso6perarens: Anxnmos A.B. Aporoe B.., Sapy6mn B.7., Kasmnpos A.J], Moposos B.H., Tonpesos A.M., Crynaes 0A. (73) MarekrooBnagarens: ‘ApoKos Bukrop FpxropLeens, SapyOmn Banewtan Nasnioows, Kaaunpos Anexcavap [mmTpHeens, Mloapeaoe Anoxcolt Muxalinoows, Cxyaaen Opi Awarpweans (64) CNOCOB ONPEAENEHMA XAPAKTEPUCTHK M/KPOMPHMECE METAMNOB B CMASO4HbIX MAGIIAX, TOMIMBAX MW CTELIMATIBHEIX KAKOCTAX 67) VaoGperenne orHocwTon x obnacta akanmTMveckon xHMAM. [JIA ueMepeHHA xapaKTep/cTHK v KOHYeHTpayun MeTANTECKOR NpwMech, HaxopmuJevcn @ |nge oTAEnHEK Vacty, aHaNvaMpyeMunh — OBkeKT B® pacnbinesiom supe nonaerca 8 ninasky Tasosoro paspaa armoccbepHora AaaneHAA TaKOR —cxOpocreNe, TO6H MACTHUbL eTannmecron —rpvMect —BXORUNIM—B akanmTuseckyio soHy locnenoBaTaNsHo nO ‘onHOA, NoaroroeneHHylo npoby AononMinrensHo PacteopaioT 8 OpraHinvecKom pacraopuTene, OnpaRenniot KonwwecTao wacTAy & HEKOAKOH W PacrRopeHHolH npoGax, no COCTHOUIEHKO Hx konwectaa onpepensior — KoocbebaynenT, OueHMBALOW\NA KavECTEO PaGoTAIOI\er Macha, pn eTOM cpeAHAA paamep Yacray OYeKHEaGT No pacnpegenennie vacTay, nanyHeHHOMy MDM BHANMe —PACTEOPEHHOA NBOOkI, MC YETOM Konnecrea vacray MuKponpHMeDeR HK ‘onamaxTHore cocTaka onpemAnsicr yponette \aHoca OTAeMHE YOROB MELIMH # WEXAHMMOS, Texnmvecknt pesynbtaT - g0aMOxHOCTe ‘2kenpeccHoro onpeneneus KoMyeHTpauMl, epenwero paawepa, KonMvecTea wacTMy sneMexTHor® cocTaea KaXROM WacTHys! 3 TAbN 2182330 c2 RUoeezere nu zo RUSSIAN. AGENCY FOR PATENTS AND TRADEMARKS: (2) ABSTRACT OF INVENTION ® RU"? 2 182 330" C2 SOM” & O41 N 21/73, 33/28 (21), (22) Application: 98104910128, 13.03.1998, (24) Effective date for property rights: 13.03.1998 (43) Application published: 10.01.2000 (48) Date of publication: 10.05.2002 (98) Mail address {664003, g.Irkutsk, ul, Karla Marksa, 1, IGU, patentny) otde! (64) PROCEDURE DETERMINING CHARACTERISTICS OF MICROIMPURITIES IN LUBRICATING OILS, FUELS AND SPECIAL LIQUIDS, (67) Abstract FIELD: analytical chemistry, SUBSTANCE analyzed object in atomized form is fed into plasma of gaseous discharge of atmospheric pressure wih such rate that particles of metal impurity entered analytical zone in Sequence one by one to measure haractersties and concentration of metal impurity inthe form of individual aticles. Prepared specimen is additionally dissolved in organic solvent, number of paficies is found in inital and dissoved Specimens and factor evaluating quality of (71) Applicant: Nauchno-issledovatelski institut prikladno) fziki pr Irkulskom gosuniversitete, AUK *BAJKAL" (72) Inventor, Alkhimov A.8., Drokov V.G., Zarubin V P., Kazmirov AD. , Morozov V.N., Podrezov AM., Skudaev wo. (73) Proprietor: Drokov Viktor Grigorevich, Zarubin Valentin Paviovich, Kazmirov Aleksandr Dmitrievich, Podrezov Aleksej Mikhailovich, Skudaev Juri Dmitrievich ‘operating oll is determined by relation of their numbers, Average size of particles is evaluated by distribution of particles obtained during analysis of dissolved specimen, Level of wear-out of individual Units of machines and mechanisms is determined with due account of number of particles of microimpurties and their elementary composition. EFFECT. possibilty of proximate determination of concentration average size, number of particles and elementary composition of each particle. 8 tbl 2182330 c2 RUocezesrz nu zo Veo6pereHine orHocwTon x o6nacTa aHANATUYOCKOR XMM, a MMOHHO K ecnenoaahinio anamvsy Marepvanos c oMoW\BIo oMTANeCKAX MeTORES aHaNWaa, MOXeT HaliTA NpAMeHEHNE ANA ONpenENeHAR xapakreprcrHk MeTANNHUECKHK NpMMeCe! B PasnisHix cneunanbHsbe MMEKOCTAN, TAKIN KaK eMasoNHie Macha, TonmWea W mMapaeTMNecKAe >xnnxooTw, creneHi wsHooa ABHraTeNe”, MALIN W Mexannawos, AINA OleHKA KavecTBA cMasoNoro Macna, 8 TpHEoTornwecix vocnenoaannnx Venecren cnocos onpeneneni conepxannn menesa 8 paGoraouyyx macnax jt), Crioco6 ‘ocHoBaH Ka ‘orcbvnsTposbisanian Conepxaujeroca & acne wacTHy xenesa wepes HOrocnoMM unbTpyOUIAA MaTepKAN Nocnenyiouleh NpoBEPKOR MarHATHSK cBOHCTE cbanstpyioujero Mareprana nw nowoum somgercTen® MarHATHOTO none MnO acnpenenehinia xenesa Mexzy cnoRMM cbunerpyiowet neperoponkn cynaT 0 AvcnepcHooTa Yacriny Menesa VsaecTel criocoO onpenenenns crenehn sarpraveHWocT eMasoNeX —Macen 12! 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OTABKGHEK MeTANITOR & Nacrayax —MMKpoNpHWecA lO BenwAAHe wnynscos: ” rpanypo8oustam xapakreprcriwam, pw arom ana caTHanoe, saperucrpyposanisn onHOBpaMeHHO Ha KAKZOM kakane, onpenensior cooTHOWeHMe Mace cooTeererayiouyex weTannos, no KoTOpOMy ¢ yueTOM cTexvoMerpMveCKoro coOTHOWeHAA MeTanios ycTaHaanveawr cocTaB vacTAYt, PaccMuTIBaioT KOTMECTBO YaCTAy OTARNbHBIK Nweponpumece, conepxanne eranna 8 Vacrayax waHooa ¥ cpeaHn AraMeTp vaCriM, No KoTopsiM onpegenAicT ypoReHs waHOCA Bninxaliuinkt aHanorom agnserca cnocos onpenenekii® pacnpegenenia vacray 80 Bseck 8 TascotpasHoh —qncnepcHoh opene lo Paswepan, a TaKKe WaMepeHAA KOHKeHTpALWN Yacrmy /4/. 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KpoMe Toro, cuMMTANNAUMOHHEIA aHanws NosaonAeT onpenenmTs cvameckve cosnmieHna vacTay pasnnwHeix weTannos (haKnens! HARP), KoTopsie senaiorca pononHnTenbHeimM NowsHaKaIA NpH noysnoBOh AnarMocTaNe. Cnocoé ocywecrennerca cnenyoun ‘6pasow: 2182330 C2 RUocezesrz nu zo Cro6paniyio npoby vecnepyeMoro wacna ‘6ueMoN 20-50 wn TwaTeNMsHo NepeMeUIMBAOT © MoMOUIbIo ynbrpasayka wnn MexaHnecKoR Moularin, NoMewaior 8 craKal YeHTpHCbyrA UseTpHebyrupyior & TeveHie 60 wa Np acroTe: ‘Bpauenia 4000 oGiwinn. Llewrpacpyrmposanven oTAensIOT YacTHUb! MeTanna, HveIoUInE Gonee eeiconyo —mnoTHocrs»=— oT —sweranina, acrkopeHworo a Mache M HaxoARWerOcR a MonekynapHoR dopke. B ocanox BtinanaoT Tonio MaCTHUS! MeTanNOB, aHOCOHHEK —B 2xnoKooTe WaeHe. Merarnit NpHcanoK, B TOM Menem nerKoHoHNanpyeMbe, ocTaIoTER 8 BepKHeM roe, KOTOPSIA YaaneTcA no OkOHWaHNA UeHTPHCbyTHpOBAHUR. BepxHini cro Macha, He conepxaulMiA Wacra\ npamecd, Yyaansior naneTiOA. NpyNeM yaanATe HyKHO TAK, UroGs! He saxBarvTe aolleneHH ocanOK COcTABHE KAK MOKHO MeHBUIe Macna 8 cTaKaHe Sarem 8 cTaxaH onwaaior abiOpaHHbih PasGasurens, 8 KOTOpOM —_oTayTCTByOT BHANMOMPYEMLS onleMeHTel, Ha KOTOPOM Nprorasnvearn oOpasysi cpasHeHna, cvect TwjarenbHo nepewewnaaior Ww chsaoT —B euKocT® ana ananna TpeaeapurensHo nogroroeneHHyio npoBy & oMoWBIoyslsTpasayKoBorO pacnkurwrens Apespauaior 8 MenkonMonepcHBIA son PacniunaTens paGoraer 8 TaKom pexNMe, WTO Vactmysi —nocrynaiot == nnaamy ocnenoBarensHo No OnHO!, MonyeHHeiA sone, COcTORUAA Ws KaneM’ xMRKOCTH MW YaCTHi, weTanios, noToKON TpaHcoprApyioulero rasa HenpepsisHo saysaeroa 8 nnasMy rasoBoro pasprna CBY niiasworpoHa yrKnoHHOrO Tana, Tenneparypa Koropom cocrasnser oan 5200 K lpm nonanawnn vactHyb! & nnasMy oa Harpesaeter, vonapseroA v1 nony\eHmeh |TOMHIH Nap BooByAKNATCA, Te. NpoAexoRAT fcntska (CuMATANNAYAR) YacTAYs!. CkOpOCT RocTynneHaR avannsHpyeMOR npobk Ba6paa vo pacvera, WroSsi VacTMys! MeTanna uponpumect —noctynana 8 nsasMy ocnenosarentsHo jpyr sa npyron. Venywette afowHoro napa ¢ noMCWbO owpeHcopa nocrynaeT Ha chexrpansHtit Npw6op. PasnoxeHoe B chemp nanyueHne onmxpomaropore perworpHpyeTcA Ha BLXORE oroywwomirenaian Dpwrenswocrs winynecosvanyweHns Vactay—nponopuvioHanbHa —_apeMeHn HaxoNReMMA wx nnaswe W cocTaenseT 1-10 MC, & aunnutyaa, nvG0 -NNOUIaLe MTEC = enapHaulelicn Mace vactuyts Mostowy. Ha BoKONe — chOTOYMHOKMTeNeA _NpwcyTcrayior ocnenosarensHocrA minyfiscos ashy aunnarya ¥ annTensHocre”. SneKTpHNecKHe wunynsces ¢ @oroyHoxnrene nocrynaior Ha ‘ananoro-uncheo8o — npeoGpasosarens ‘Gpa6artisaioron SBM To cheyvanHum —rpanyaposouene xapakrepycrumam 98M —_onpegenser KonyeHTpaynio Meranna 8 YacrHyax vaHoDA WM KohueHTpauWNo pacraopaHHoro weTanina Tipwep. 1 Men NonroToaneHHor —npoGe akanmenpylor Ha ConepKaHMe — NpAMEcHEK YacTay, “OWeHNBaR pagMep, x cocTas konmuecrao, Cnenyouqwe 1 wn Macna pasGasnaior opranivecknt’ pacrsopuTenem WHTEHCHBHO ACTPRKHEAIOT B TeYeHHE 3 MMH akannanpyior No TOR xe MeTORWKE. fine O6pa6orkmn 1 mn Macha Gepyr 1-2 6 pacteopwrens, 8 KavecTee pactaopaTena Mower Gaia Hononk208ak TerpaxnopsTAnex. Mo 0 6 a 35 “+ oTHOWeHAO wena vacray, ‘sapervcTpHposaHHix nipH aHannge VoKoAHOrO ‘wacna Kk Ywony NacTHy, saperncrpaposannen pn ananae —acna, — obpaGoraHHoro acreopwrenem, onpenennioT KosccbMyieHT, oTpax@ouA KavecTeo wacna, Yem Gonaule RoodhebuueHT, TeM BbuLIe KaveCTEO Macna, T. & Tent Orinke OHO no caon noTpeduTeniscKH kavectaam x HepaGoranweny Macny. Mo ‘aneMeHTHOMy COCTaBY OTAENLHEIK YACTMY. H WK paswepam — coywecrenaor —noysnoByo Awarwocruny aantarened, Tlpnwep. B kavecTes npritepa noyanosoi Avarsocraa’ abnagsnrarenet pacouoTpena ‘warwocraxa psvrarans IC-80. ‘Otoxnectaneraa crow acta co connagann yanos noxasakol 8 Ta6n. 1 Uvebpt! a xnmnvecket cxmaonom snemenTa oxasnBaIoT NPOYEHTHOe cOREPKAHMe 9TOrO sneweura e cnnae, Kax cnenyer vs Ta6n.1, cootas onoxHet act MOKeT RENATECA NpMaHaKOM Toro Wi Horo yana, Tak, B crywae oGhapyxenMa Yacray Tne Fo(Cr 12), voropwe woryr npyHannexaTe: Conswnncrey arperaroa # wacray Tana TiAl, HanGones seporTHa — HevcnpaaHocTe Kownpeceopa, cra @ Macne oOwapyxeHs! Yacrhys! Fo(W 9), Cu2n 34), ACU 5) B KOHyeHTpaynnx NPEBLLAIOUIA oNPEAENeHHOS sHAYEHME, TO IMoKHO caenart BbiBOA 06 usHoCe NojUMNMKOS, Eonh o6vapyxen vacrnybi Tin Mg(Al 8) = He vwonpasnen craprep, Kpowe Toro saeveHo, To ¢ yeennuexnen viatioca 8 Mache YaeninuvaaercA YnonO cnOKHEK acray - HaKnenos. 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Tlpenraraewoe vsoOperesine MoxeT Harn NpvleveHve ana ayarHocTim™ —vaHoca Aawrareneh, WauiMH ww MexansMos 8 MauIMHOcTpooHMY, 8 ABHaMOHHOM, MenesHOROPOAHOM, BORHOM, aBTOMOBNNEHOM Tpancnopre | apyrax —orpacax powiuinesHoors, crown uncbopMayun, IpHARTINe 80 4. Aare 39190,1990 2. Aar.ca, COGP 431481 © 01 N 9128,1973 coop 170902 G ot N 3. SanaKa Po 96102386/25, G 01 N 24/73 1996 r 4 Tlareur CWA 3825345 G 01 J 3/30, G01 2182330 C2 RUocezesrz nu zo NN 15102 1974 F, (npororin) ‘®opmynia uso6perenua: Cnoco6 onpagenenus’ xapaKrepecric mnponpimeceh werannos a cMasoWwek Wachax, TOMWBaX ¥ CheURANeNESK KADKOCTH Ornwaiouion TeM, TO npopBapaTanseo noprorasnisaict npoby, eonaT npoty co cxopocTno, obecrewwBacWeN 6 saRaHHOR Sepomtwocreie pasgensiyio 80 spewenin petwerpauyio cMimarios oF KaNdOM acral SianraepyeMol npvveck, 8 aMie aoposonA myrem paensinesinn @ nnaaorpos Upknostor© Tana, perucrprpyior ommecke rant vanjuenin onvoapeNenvo No 2ayM wna Bone vamepirensnt Kavarna, Kanga a FOTOS acrpoeh Ha avannrieckyie sino ranyuerun 0 6 a 35 ‘opHore MeTanna, npeoGpasytor _onryvecKne ChrHansl 8 sriexTpHeckHe MMyNboss, waMepAOT we, AononHWTeNsHo nogroToENeHKIVIO poy acreopAior @ OpraHnueckom pacraopuTene, onpanenoT KoNMECTEO HACTHY @ HExOAHOH pacTBopeHHoM npoGaAK, no COOTHOUIEHiNO HK Konmect8a onpenensior _KosdebvynedT, OyeHnBAIOWNA KaYECTBO padoTAIoW\ero Macha, ‘pn oToM cpenHni pasmep YacrMy CusHHEaOT No pacnpenenehnio vacTAy, nonyueHHOMy np ‘Hane PACTECPEAHOR NPD, C yNeTOM konmectaa —acTay——_-MUKponpHMeCeR, ‘onemeHTHorO cocTasa YacTHy, onpenenaoT yposels waHoca oTpenbHbK yanos MaulAH Mexannswos, ocyujectanan noyanosyio swarwocrany agniarene” 2182330 C2 RUoeezere nu zo Xaparrepubie npysiaxn wsHoca aBuraresich Ta6amua 1 _ Tio cocrany warepnan _ Arperatél jist Cocras | Craprep | Tou | Kopo6-«a | Komnpe | Kopnyc | Typonua | Maco wacrmu, nun — | upusonos |-ccop | pasa, arpera- pu. To Fe * o 7 > - | Faery * * * . * * [e(Cri9)_| ‘ Fe (Cri * : : Nig | Fe(W9) oF | Cw(Zn34) | * [cuéne) | * Cu(Pb27) . | | Cu(sn7) : Lowat | * [Ale * ‘Al(Cus) | of Mg__| . [MaiAl 9) ) * [Ti oF * _ To wawienam | (FeCu) (FeCu) (FeAl) (FeMg) (FeMg) (FeAg) (TIAL, 7 (Fei) (CuAg) (FeTi) L (FeAl) _ - 2182330 c2 RUoeezere nu zo Ta6smua 2 HapaSorka Neare/ Nee Neate / Nex 2000 0.24 0,02 ‘5700 0,55 0,16 Tieuratens noniea 13 erpos 18 0,05 *Peakoe, s1aBuHHoe yhemimentie "esa wacTH Mem CY 1 _uexoanoe pacTaopentioe 2_wexosnoe pacTaopentioe CY 3 _ncxomH0e Pactnopennioe rae, Ne 4HC0 "ACTHIE NpuMect, C- coneprxarine auemenTa B Macate; K,- Koodipuuutent xapaxtepwsyiouusii yepemenueiii pasmep acta (woxpdmunenr xpyniocta sacra). 2182330 c2 RU