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SPE

Society of Petroleum Engineers

SPE 20729

Influence of Matrix Shrinkage and Compressibility on Gas


Production From Coalbed Methane Reservoirs
s. Harpalani, U. of Arizona, and R.A. Schraufnagel, * Gas Research Inst.
'SPE Member

Copyright 1990, Society of Petroleum Engineers Inc.

This paper was prepared for presentation at the 65th Annual Technical Conference and Exhibition of the Society of Petroleum Engineers held in New Orleans, LA, September 23--26, 1990.

This paper was selected for presentation by an SPE Program Committee following review.of information contained in an abstract sUb~ilted by the author(s). Contents of the paper,
as presented, have not been reviewed by the Society of Petroleum Engineers and are subJect to correction by the author(s). The matenal, as presen!ed: does not necessanly reflect
any position of the Society of Petroleum Engineers, its officers, or memberS. Papers presented at SPE meetings are subject to publication review by Edltonal Co~mlttees of the Society
of Petroleum Engineers. Permission to copy is restricted to an abstract of not more than 300 words. illustrations may not be copied. The abstract should contain conspicuous acknowledgment
of where and by whom the paper is presented. Write Publications Manager, SPE, P.O. Box 833836, Richardson, TX 75083-3836. Telex, 730989 SPEDAL.

ABSTRACT

The effect of methane desorption on gas flow through is in the form of compressed gas in pore spaces. In
coal was investigated. Adsorption/desorption isotherms coalbed reservoirs, the major quantity of gas is stored
were established for coal samples. Permeability of in adsorbed form, and the gas available for flow is the
cylindrical samples to different gases was measured at desorbing gas. The second maj or difference is the
simulated jn-situ conditions in a triaxial stress field. presence of the natural fracture (cleat) system in
Gas pressure-permeability-desorption relationship was coalbeds. Thus there are two main phenomena involved:
established for helium, methane and carbon dioXide. desorption followed by diffusion of gas towards the
Related experiments measured coal compressibility, and cleats, and ·Darcian flow of gas and water in the cleats.
volumetric changes of coal matrix with methane adsorptionFlow of methane in solid coal is subjected to two distinct
and desorption. processes: desorption of gas, and reduction in pressure.
Both these factors affect permeability of coal, and hence
The hypothesis that desorption of methane shrinks coal production of gas.
matrix, and results in increased permeability was
confirmed. The increase in matrix permeability with An experimental study - preliminary in nature - was
reduction in pressure from 1000 psi to atmospheric was carried out to investigate the effect of these two factors
highest for carbon dioxide (the most adsorptive gas), - desorption and pressure - flow characteristics of coal.
on the order of a factor of five for methane, and A brief description of the background that led to this
non-existent for helium. The corresponding volumetric study, experimental work, a discussion of the results
shrinkage of coal matrix on desorption of methane was and their significance, are presented in the following
0.6%. When measured values of compressibility and sections.
shrinkage were used as input parameters into a reservoir
simulation model, 60% more gas was produced over a five
year period. BACKGROUND

Decline in Pressure
INTRODUCTION
Once production from a coalbed methane reservoir starts,
Simulation of coalbed methane reservoirs and predicting the reservoir pressure starts declining. This decrease
long-term gas production is a complex process. The in pressure - although it takes place at a very slow
number of variables involved is large, and information rate - increases the effective stress. This increase
concerning these parameters and variation in their values in effective stress results in lower permeability. Stress
over the life of a producing reservoir is not well dependency of permeability has been studied by several
quantified. Knowledge of conventional gas reservoirs researchers in the past l • 2 • In general, compressibility
is not very useful due to the fundamental differences declines with increase in stress although there is
between sandstone reservoirs and coalbed methane res- insufficient data to explicitly define the relationshi p 3.
ervoirs. In conventional reservoirs, primary storage With large compressibility values such as those measured
at Rock Creek site in Alabama, a pressure drawdown of
only 300 psi - an increase in effective stress of 300
psi - can reduce the permeability by half or more 4 • This
References and Illustrations at end of paper dynamic changing of reservoir properties makes it
important to use proper pore volume compressibility

171
Page 2 ItlFLUENCEOF MATR IX SHR INKAGE AND COMPRESS IBILITY :>t"'l: ZU/Z'j

ON GAS PRODUCTION FROM COALBED METHANE RESERVOIRS

values when attempting to analyze long-term production the relative permeability effect alone. There appears
data, or where reservoir drawdowns are large. It is to be an additional parameter influencing permeability
equally important to have a good understanding and of coal and its variation over the life of a producing
knowledge of how this value varies over the life of a reservoir.
producing reservoir.
The purpose of this work was to investigate if there is,
Another major impact of pressure variation on perme- in fact, a variation in the volume of coal in the matrix
ability is the Klinkenberg effect increase in as gas is depleted, and its impact on permeability. This
permeability with decrease in pressure. The phenomenon paper describes the experimental study carried out to
is ascribed to slip flow at the solid- gas boundaries monitor variations in permeability with desorption, and
wi thin the pores and capillaries. When a gas is flowing the corresponding volumetric strain of coal matrix.
along a solid wall, the layer of gas next to the surface Grain compressibility was also determined. Finally, the
is in motion with respect to the solid surface. In other results of a sensitivity analysis are presented where
words, if the wall has a zero velocity, then the velocity the experimental results were used in a set of simulation
of the gas layer in the immediate vicinity of the wall runs using a coalbed methane simulator to predict gas
has a finite value, resulting in a higher gas flowrate production from coalbeds.
than expected5 • The application of Darcy's law to gas
flow in low permeability formations, therefore, requires EXPERIMENTAL WORK
a correction for this gas slippage - or the Klinkenberg
- effectB. This correction takes the form of a slippage Specimen Preparation
factor, b, in the Klinkenberg equation.
Two primary types of experiments are discussed in this
paper: permeability experiments, and coal matrix volu-
............ ( 1 ) metric s train experiments. For these experiments,
cylindrical specimens were needed. As a part of initial
sample characterization work, adsorption/desorption
The apparent permeability, k, is approximately a linear experiments were conducted and proximate analysis of the
function of the reciprocal of mean pressure. The function samples was carried out. For this part, powdered samples
is an approximation, and the factor b is not a constant. were needed.
It increases with increasing gas pressure and decreases
with increasing water saturation5 ,B. Figure I shows the
Fresh coal samples from gassy coal seams in the Piceance
Klinkenberg effect for a core sample of porous rock.
and Black Warrior basins were obtained. Using these
The intercept of the line on permeability axis indicates
lumps of coal, powdered coal samples were prepared in
the permeability of the media to a single incompressible
the Mineral Processing Laboratory at the University of
fluid.
Arizona. Pieces of coal were first crushed in a jaw
crusher to reduce the size to approximately one cm.
Although the Klinkenberg effect is found to be true for These were then ground in a ball mill for half an hour.
most rocks, several researchers have reported unusual Powdered specimen was sieved into different size groups
effects produced by coal. A non-linear relationship and used for adsorption/desorption isotherms. To measure
between the two (reciprocal of mean pressure' and permeability, and monitor the volume of the coal matrix,
permeability), and a negative slope have been reported 7 ,B. specimens one and a half inches in diameter were used.
Considering that a gas reservoir undergoes changes in It was decided to keep the L/D ratio (L is the specime~
pressure and saturation during depletion, the effect of length, and D the diameter) as close to two as possible.
slippage varies throughout the life of the reservoir. Hence the length of the specimen was close to three
It can have a significant positive impact on permeability
inches. These specimens were prepared using a coring
of coal and long-term gas production.
machine and a surface grinder.
Desorption of Gas
Adsorption Characteristics
The primary means of gas storage in coalbeds is by In order to enable the flow of gas due to free gas alone
adsorption of methane molecules on coal surfaces. When to be distinguished from the flow due to free and desorbing
subjected to pressure drawdown, desorbed gas moves by gas, adsorption/desorption experiments were carried out.
diffusion through the extremely low permeability coal Porosity of the sample was first determined using the
matrix in order to reach the natural fracture (cleat) helium expansion method. Using the correction for gas
system in coal. Once in the cleats, gas and formation compressibility, the compressed gas component was
water flow in the cleat system which has a high calculated. Following this, the adsorption isotherm was
permeability relative to the matrix. Based on the above established using methane. The procedure, used by the
mechanisms involved, several models have been developed authors in a previous study, is described in detail in
for predicting methane production from coal seams. An
a prior publica~ion 13. After the highest pressure in
excellent review of the various models has been presented
in recent publications 9 ,10,ll. the adsorption experiment was reached, desorption
isotherm was established for decreasing gas pressure
from 1000 psi to atmospheric. Figure 2 shows the quantity
As production continues and reservoir pressure declines,
of gas adsorbed, along with the free gas content, for
the cleats may contract - similar to contraction of pore
one coal sample.
space in conventional reservoirs - causing a decrease
in permeability. On the other hand, the coal may contract Since the primary objective of tllis research study was
due to gas depletion causing an increase in permeabil- to establish conclusive evidence of the relationship
ity 12. To date, enough information is not available to between desorption and permeability, the effect of the
determine the changes in permeability with decreasing adsorptive affinity was investigated. Hence, carbon
pressure. Production data, however, indicates that dioxide was used as adsorbate and the experiment was
permeability variations can not be fully explained by repeated. Carbon dioxide was selected because it is

172
SPE 20729 S. Harpalani and R.A. Schraufnagel Page 3

known to be more adsorptive than methane. However, the suggested by the International Society of Rock Mechanics
experiment could be carried out only up to 500 psi. (ISRM) , four strain gauges were used on the specimen
Beyond this pressure, the results were difficult to surface - one each for axial and radial strains, 1800
interpret. Either carbon dioxide liquefied, or there apart. The strain gauge wires were passed between two
was a chemical reaction between coal and carbon dioxide. rubber a-rings, with the space in between completely
Figure 3 illustrates the difference between desorption sealed with rubber cement. The specimen was then placed
isotherms for carbon dioxide and methane. in the sample container, the wires were connected to the
strain indicator, and the container was closed. The
Permeability Experiments setup is shown in Figure 5. The zero readings were
recorded and the specimen was evacuated for several
Permeability was measured using cylindrical specimens hours. Gas pressure was then increased to 100 psi with
at simulated in situ conditions in a triaxial stress helium. After the readings on the strain indicator
field. The experiments concentrated on studying the stabilized, they were recorded. The procedure was
flow behavior with changes in gas pressure (permeability repeated for pressure increments of 100 psi until 1000
and pressure relationships). Since desorption takes psi was reached. Gas pressure was then decreased in
place when the gas pressure is reduced below the similar steps. At the end of this part of the experiment,
desorption pressure, decreasing pressure - associated the specimen was evacuated and the entire procedure was
with desorption - only is emphasized in this paper, alon~ repeated using methane. After each pressure change the
with the Klinkenberg interpretation of the results (liP apparatus was left for 8 to 10 hours, since desorption
vs permeability plots). is an extremely slow process and it took a long time for
the readings on the strain indicator to stabilize.
The experimental setup to measure permeability is shown
in Figure 4. A triaxial cell was modified by drilling EXPERIMENTAL RESULTS
holes through the upper and lower platens to provide gas
inlet and exit ports. The synthetic rubber sleeve in Permeability Variations
the cell sealed off the cylindrical surface of the coal,
from an annulus of oil which was pressurized using a Using the measured flowrates during the experiments,
hydraulic pump. A compression testing machine was used permeability of coal samples was calculated using Darcy's
to apply the axial stress. Gas was supplied via a law for steady state isothermal flow of a gas through
regulator and pressure gauge to the top of the cell and porous media. A complete gas pressure-permeability
was collected at the downstream end. The flowrate was relationship was thus established. Figure 6 shows the
measured using bubble flowmeters. results of one experiment carried out at a hydrostatic
stress of 1500 psi (10.34 MPa). Permeability started
The specimen was inserted into the cell, and the setup increasing below 450 psi (3.1 MPa) and continued to rise
arranged as shown in the Figure 4. A small axial load, sharply until the pressure dropped to 50 psi (0.34 MPa)
and confining pressure was applied to the specimen to 'and the experiment was complete.
seal the rubber membrane against the specimen surface.
Both stresses, axial and confining"were then increased As mentioned in the previous section, the effect of
gradually and simultaneously until the desired stress desorption of methane on permeability of coal was further
level was reached. The gas pressure at the upstream end confirmed by using different gases, with substantially
was then increased. Once flow of gas was established, different adsorptive affinity for coal. Figure 7 shows
'the setup was left for several hours for the flow to the variations in permeability of the sample to the three
stabilize. After flow reached equilibrium, flowrate was gases used for decreasing gas pressures. These results
measured. Gas pressure at the inlet end was then increased clearly point out that the permeability increase with
and the procedure repeated. After reaching approximately reducing pressure is highest for carbon dioxide, on the
1000 psi, the gas pressure was decreased in similar steps order of a factor of five for methane, and non-existent
until the flowrate became too low to be measured. The for helium, suggesting that the change in permeability
stress was then released and the triaxial cell removed is not only a function of desorption, but the degree of
from the testing machine. desorption as well.

To confirm that the observed changes in permeability Coal Matrix Volume Variations
were, in fact, due to desorption of gas, pressure-
permeability relationships were established for three Figure 8 shows the changes in volumetric strain (t>V IV)
different gases with significantly different adsorptive with increasing and decreasing pressure for helium and
characteristics. The experiment was first conducted methane. For helium, the volume of coal matrix decreased
using helium since it is weakly adsorptive - almost with increasing gas pressure. Grain compressibility of
non-adsorptive. The specimen was then flushed with coal, as calculated from Figure 8, is approximately 9
methane for six hours and the experiment carried out x 10- 10 per psi. The hysteresis between increasing and
using methane. Finally, the experiment was repeated decreasing gas pressures is due to the slightly plastic
using carbon dioxide - the highly adsorptive gas. nature of coal. With methane, the matrix volume increased
linearly with pressure. At 1000 psi, the matrix volume
Matrix Volumetric Strain Experiments was swollen by 0.6%. When gas pressure was reduced, the
decrease in volume was non-linear, and there was a
The volumetric changes in the coal matrix, associated residual swelling when the pressure was reduced to
wi th changes in gas pressure, were measured independently atmospheric.
of the permeability. It was necessary to keep the pressure
within the specimen, and all around it, equal at all
times to ensure that the void volume in the specimen
remained constant with changes in pore pressure. In
other words, pressure gradient had to be avoided for
these experiments. Following the standard procedures

173
Page 4 INFLUENCE Of MATKIX ~HKINKA~t ANU ~UM~Kt~~IDILI IT

ON GAS PRODI,JCTI ON FROM COALBED ~IETHANE RESERVO IRS

DISCUSSION OF RESULTS The interesting feature of the above equation is its


similarity to the Klinkenberg Equation, with one extra
Effect of Desorption term. At low gas pressure, the first term in the equation
dominates although this is the combined effect of
Figure 9 demonstrates the relationship between desorption desorption and Klinkenberg phenomena. At high gas
and permeability for methane. Once desorption - which pressures, the third term is dominant resulting in higher
is significant below 600 psi (4.14 MPa) starts, permeability. To better understand the relationship,
permeability starts increasing. The initial decrease the results were plotted as a function of liP, where P
in permeability above the desorption pressure - prior is the mean gas pressure. Figure 14 shows the plots for
to desorption - is due to cleat compression which impedes two experiments carried out at hydrostatic stress levels
free gas flow. Figure 10 shows the same relationship of 1100 psi and 2000 psi. For the 1100 psi experiment,
for carbon dioxide. Since carbon dioxide is highly there is a minimum permeability, with its value increasing
adsorptive, the permeability rises continuously as the in either direction - increasing and decreasing pressure.
gas pressure decreases. The initial decrease in This might be due to variation in the value of the
permeability to carbon dioxide is not observed because slippage factor b. At 2000 psi, the sample behaves more
the maximum gas pressure (of a little less than 600 psi) like a typical rock with the permeability rising
is significantly below the desorption pressure, and the continuously as gas pressure is reduced - except for the
flow of carbon dioxide is accompanied by desorption for initial flat portion of the plot. The initial deviation
the entire experiment. The results also indicate that from the usual Klinkenberg phenomenon is minimized and
the increase in permeability of coal to carbon dioxide the flow appears to be primarily capillary flow. Although
is about 30 times, whereas for methane it is approximately experiments were not carried out at stresses higher than
6 times - even though the measured permeability vlues 2000 psi, it is felt that at high stresses the permeability
are fairly low. would increase continuously with reductions in gas
pressure, i. e., the k v s liP line would be a straight
To further confirm that the observed increase in one, at say, 3000 psi. Since pressure in coalbed methane
permeability was due to desorption, one set of experiments reservoirs decreases with depletion of gas, the perme-
was carried out using a back pressure at the downstream ability might go up continuously for reservoirs with
end of the specimen to minimize pressure gradients across high jn-situ stresses. If this can be shown/proved to
the sample. The stepwise gas pressure experiment was be true, the phenomenon would favor methane production
then repeated at a constant gas pressure gradient by from deep coalbeds, e.g., Piceance basin.
changing the pressure at both ends. ~ was constant
throughout the experiment, and mean gas pressure changed, Importance of Coal Matrix Shrinkage
thus giving a mean gas pressure-permeability relation-
ship. In sjtu conditions were better simulated since It has been clearly demonstrated in the preceding sections
very high pressure gradients - as used in the prior that there is a matrix shrinkage phenomenon associated
experiments - are not found in reservoirs even if large with desorption of methane. An outcome of this has been
gradients occur near drawndown production wells. Figure observed in the experimental results where permeability
11 shows the results for pressure gradients of 300, 200, increases when accompanied by desorption. In this
100 and 50 psi. As the gradient was reduced, an section, an analysis is presented to evaluate the
everincreasing permeability with reduced mean gas sensitivity of gas production to coal matrix shrinkage
pressure below the desorption pressure was observed. using the results of the experimental work in a set of
This confirms the effect of desorption on permeability. simulation runs using COMETPC-3D model. Four simulation
runs were made to determine the effect of pore volume
In order to obtain the effect of desorption on matrix and matrix compressibilities on five year gas production.
volume of coal, the volumetric strain wi th helium (grain
compressibility) was subtracted from the volumetric Measured value of matrix (or grain) compressibility was
strain with methane. Figure 12 shows this as 'effective 9xlO- IO per psi. Hence, C p =9xlO- 7 psi-'. Volumetric
shrinkage' due to desorption. The similarity between measurements using methane were incorporated in the
the desorption isotherm and the effective shrinkage plot simulation runs using the concept of a matrix shrinkage
suggests a clear interdependence. compressibili ty, C~14.

Numerical Analysis
......... (3)
Curve fitting exercise was carried out using the
experimental results. The variation in permeability
with decreasing gas pressure, shown in Figure 6, was From the results, the volume of matrix decreased by 0.62%
taken to be the standard relationship. The best fit when gas pressure was reduced by 1000 psi. Therefore,
gave an equation of the form
c' =0.0062=6.2xlO- 6 ·-1 ........ ( 4)
m 1000 pSI
k=3.3+'076+'0206 p2 ............ (2)
P
Unfortunately, pore volume and bulk compressibilities
were not measured as a part of this experimental study.
where P is the gas pressure in 100 psi. Figure 13
compares the modeled results with the experimental Hence, the pore volume compressibility had to be
results. The two are in good agreement. Similar curve estimated. Using the common assumptions in reservoir
fitting for other results gave non-linear, and similar, engineering, even though these have not been proved for
equations with three coefficients. coalbed methane reservoirs, its value was approximated
to be 4.Sx 1 0'5 psi -I, which is a reasonable value 15 • These
values of compressibilities, as used in the simulation
runs, are shown in Table 1. The results of the simulation
runs are shown in Figure 15.

174
SPE 20729 S. Harpalani and R.A. Schraufnagel Page 5

Case 1, where C p = C;" = 0, is used as the basis of should be conducted using large samples, at least three
comparison. A comparison with the results of Case 2 inches in diameter - preferably four inches. Also,
suggests that production can be underestimated by transient testing should be conducted (rather than the
considering the pore volume compressibility and not the steady state tests) for permeability measurements.
matrix shrinkage compressibility. Case 3 shows that
matrix shrinkage compressibility can more than offset 2. Experiments should be conducted to establish a range
the reduction in permeability due to pore volume of compressibility coefficients - pore volume, bulk,
compressibility, and the resulting increase in production matrix and matrix shrinkage - for different coal basins
can be fairly significant. Coal matrix shrinkage is, in the U.S.
therefore, an important parameter and must be considered
together with cleat contraction due to pore volume 3. Klinkenberg phenomenon should be studied in detail
compressibili ty in order to accurately simulate and in order to isolate·the change in permeability due to
forecast long-term gas production from coalbed methane the Klinkenberg effect, and that due to desorption/
reservoirs. However, it should be pointed out that more shrinkage. This is particularly important for methane
laboratory work needs to be carried out in order to recovery from deep coalbeds - systems already developed,
quantify both pore volume and matrix shrinkage com- as well as for future operations.
pressibilities.
NOMENCLATURE
CONCLUSIONS
k permeability
The most important conclusion of this work is that b slippage factor
desorption of gas causes the coal to shrink. The shrinkage P mean pressure
trend with decreasing pressure parallels that of the Cp - pore volume compressibility
desorption trend. The volume of coal matrix shrinks by Cm - matrix (grain) compressibility
approximately 0.5% with a reduction in pressure from 600 Cm* ~ matrix shrinkage compressibility
psi to atmospheric. If the compressibility of grains Vm ~ specimen volume
is taken into consideration, the effective matrix ~Vm - change in the specimen volume
shrinkage compressibility is even higher. For simulation 6P - pressure change
purposes, C;" was taken to be 6.2xlO' o psi-] since volume 00 - infinite pressure
increase was ,62% at 1000 psi. If grain compressibility
C m (-9xlO- 7 ) is included, the
C~=(6.2xlO-o+9xlO-7) psi-' or 7.1xlO- o psi-] and the ACKNOWLEDGMENTS
effect shown would be even more significant.
This work was carried out as a part of the GRI sponsored
The shrinkage of coal matrix causes the permeability to project "Permeability Changes Resulting from Gas
increase significantly once the pressure falls below the Desorption," Contract No. 5088-215-1666. The authors
desorption pressure, thus resulting in higher production wish to thank the GRI for the support. The simulation
of gas. The effect of shrinkage on permeability can be work using COMETPC-3D was carried out by Walter K. Sawyer,
easily visualized by the gas pressure-permeability and the authors are thankful to him for his assistance.
relationship for pressure reduction from 1000 to 50 psi.
Above the desorption pressure, the effect of pore volume REFERENCES
compressibility is dominant and the permeability
decreases. However, once the pressure falls below the 1 Harpalani, S. and McPherson, M.J.: "Effect of
desorption pressure, the effect of matrix shrinkage Stress on Permeability of Coal," Quarterly Review of
becomes dominant resulting in increased permeability. Methane from Coal Seams Technology, Vol. 3, No.2 (1985),
23-28.
The relative change in permeability with desorption is
strongly dependent on the adsorptive affinity of gas for 2 Somerton, W.H. et al: "Effect of Stress on
coal. It is higher for carbon dioxide than for methane, Permeability of Coal," Int. J. of Rock Mechanics, Min.
and non-existent for helium. Sci. and Geo. Abstr., Vol. 12 (1975) 129-145.

The influence of desorption and Klinkenberg effect on 3 Koenig, R.A. et al: "Application of Hydrology to
permeability of coal is complex. In this study, the two Evaluation of Coalbed Methane Reservoirs," final report
effects could not be separated. At high stresses, the submitted to Gas Research Institute, Contract No.
results appear to favor the Klinkenberg effect. 5087-214-1489 (1989).

Also, interesting is the observation that permeability 4 Zuber, M.D. et al: "The Use of Simulation and
is much higher at low pressure gradients. Lowering History Matching to Determine Critical Coalbed Methane
pressure gradients even further might further increase Reservoir Properties," SPE/DOE 16420 paper presented
permeability and show that desorption plays a key role at the 1987 Low Permeability Reservoirs Symposium,
in maintaining, and potentially increasing, permeability Denver.
during the production life of a well.
5 Klinkenberg, L.J.: "The Permeability of Porous
Future Work Media to Liquids and Gases," Drilling and Production
Practice, API (1941) 200-213.
Based on the findings of this' exploratory' work, further
research is desirable in the following areas: .6 Ertekin, T. et al: "Dynamic Gas Slippage: A Unique
Dual-Mechanism Approach to the Flow of Gas in Tight
1. Analyze additional samples from basins where coalbed Formations," SPE Formation Evaluation (1986) 43-52.
methane is an important resource. These experiments

175
Page 6 INFLUENCE OF MATRIX SHRINKAGE AND COMPRESSIBILITY ~ n. "LU I"L 'j

ON GAS PRODUCTION FROM COALBED METHANE RESERVOIRS

7 Gawuga, J.: "Flow of gas through stressed .11 Sawyer, W.K. et al: "Development: and Application
carboniferous strata," Ph.D. Dissertation, University 'of a 3D Coalbed Simulator," CIM/SPE 90-119 paper presented
of Nottingham (1979). at CIM/SPE IntI. Tech. Meeting, Calgary, JcU1e 10-13.

8 Harpalani, S.: "Effect of Gas Pressure on 12 Kamal, M.M. and Six, J .L.: "Pressure Transient
Permeability of Coal," Proceedings, 2nd U. S. Mine Testing of Methane Producing Coalbeds," SPE 19789 paper
Ventilation Symposium, Reno, Sept. 23-25, 1985. presented at the 64th Annual Technical Conference and
Exhibition, San Antonio, October 8-11.
9 King, G.R. and Erteken, T.: "A Survey of
Mathematical Models Related to Methane Production from 13 Harpalani, S. and McPherson, M.J.: "Retentionand
Coal Seams, Part 1: Empirical and Equilibrium Sorption Release of Methane in Underground Coal Workings," Int.
Models," Proceedings, 1989 Coalbed Methane Symposium, J. of Min. and Geol. Engr., Vol. 4 (1986), 217-233.
Tuscaloosa, April 17-19, 125-138.
14 Sawyer, W.K.: Personal Communication, 1989.
10 King, G.R. and Erteken, T.: IIA Survey of
Mathematical Models Related to Methane Production from 15 Harpalani, S.: "Permeability Changes Resulting
Coal Seams, Part II: Non-Equilibrium Sorption Models," from Gas Desorption," final report submitted to Gas
Proceedings, 1989 Coalbed Methane Symposium, Tuscaloosa, Research Institute, Contract No. 5088-215-1666 (1989).
April 17-19, 139-156.

TABLE 1 - PARAMETERS USED IN SIMULATION RUNS AND RESULTS

Case Cp(psi- 1 ) C~(pSi-l) Gas Prodn. Change

1 0.0 0.0 80,400 0.0


(base case)

2 4.5 x 10- 5 0.0 69,100 -14.1%

3 4.5 x 10- 5 6.2 X 10- 6 105,800 31.6%

4 0 6.2 X 10- 6 127,900 59.1%

fOe 1/11/
f5 e /Vl /

~4.0 V
i I /i?~~~~~--;:::±=:=====±:,-1
35 e
1

.•, /
I I

~ 3J~
::
~~ : :::::::;n l!J. Corbon dioxide
e-

Vl

<3 _L-_,L..-....L-"L-.,...L----l_::'"'=---l'_-::'I:::--::'I~:_l::_---l~:_"I:_'
2.5 L..-.....L.'
0.2 0.4 0.6 0.8 1.0 1.2 1.4
Reciprocal mean pressure, ATM- 1

Figure 1. Permeability of core sample to three gases


at different gas pressures.

176
SP.E 2072,9

28
28
Total Gas

24 24
E
E '"
"-
'"
"-
20 E 20
E Adsorbed Gas
-a.
.
.; ,Q
16
Cl 16 0
.
~
. '". .
• Methane
E "
E
~
,: .It.. Carbon dioxide
0 0
> >

Compressed Gas

a 100 200 300 400 500 600 700 800 900 1000
a 100 200 3 a 400 500 600 700 800 900 1000
Gas Pressure, psi
Gas Pressure, psi
Figure 3. Desorption isotherms for the coal sample using methane and
carbon dioxide, 2SoC.
Figure 2. Capacity of coal to hold methane at 25 (Ie (dry sample).

Pressure gauge

/ Valve

To strain

indicator

From strain

gauges #2
Go>
Specimen

Hydraulict
System ~ Axial strain Radial strain

gauge #1 gauge #1
Figure 4. Schematic diagram of apparatus for
testing coal permeability.
Figure 5. Setup to monitor changes in the volume of
coal matrix with variations in gas pressure.

7
Hydrostatic Stess: 1500 psi

'U increasing gas pressure


.: 5
'"
N decreasing gas pressure

..,E
0 4
';;

~
.
:<i 3
"E
;;
ll. 2

a 200 400 600 800 1000


Gas Pressure, psi

Figure 6. Variation in permeability of coal to


methane with increasing and decreasing gas pressure.

177
SPE 2072,9

hydrostatic stress: 1500 psi .006


Experiment # 2
helium
.005
~ Mathane cycle
methane .004

:;
.
<l

.OOJ
Experimenl # 1

E- "u Adsorption
N

-.
E
;:;
",
0 D

g
.
f~:::::::~:i;4~0~0~;~6~0~0:::~800:==1:0~0°C:i
:;;
.1
"
E
Q .08
carbon dioxide
-.001 Helium cycle
... .06 Gas PrBSSUrB. psi
.04
Figure 8. Volumetric strain of coal matrix for increasing and
decreasing gas pressure for helium and methane .
.02

.01 0 200 400 600 800 1000


Gas Pressure, psi

Figure 7. Variation in permeability of coal


to helium, methane and carbon dioxide for
decreasing gas pressure.

7 .... adsorbed gas (28-48 mesh)


• adsorbed gas (28-48 mesh)
• permeability (hydrostatic
• permeability (hydrostatic
6 J.O stress: 1500 psi)
stress: 1500 psi)
:;
.., 5 25 2- 2.5 25
E- N

N
E
E E E
", '"
,.
"
0
4 '"
"-
E
0 2.0
"-
E
20

';; .; .;
" ~ "
~
.tl

...
J .tl 15
..,...
:;; 1.5
..,.
0

.
:;; 0

. E
"
E
Q 2 ...Q "
" 1.0 E 10
... E
.=0 .!
0
> >
.5

o o 400 600 8 1000 0


Gas Pressure I psi Gae Pressure, psi

FiRure 9. Variation in adsorbed gas and permeability Figure 10. Variation in adsorbed gas and permeability of
of coal to methane - decreasing pressure only. coal to carbon dioxide - decreasing pressure only.

178
SPE 20 72.9

Hydroslalic siress: 1500 psi .006


Efhclil8 shrinkage
20
.005 Mllhane
-g, 10 ~

8
<i
,. 6
.
o 4 ~
u

'"
D
.'"
2
.
j
>
.001
E
.. I 0
a..
...;2=<OO;.::..-e.......:.4..;OO-=--.-_6~0~0~_~8:0~O_ _=1000
.8
.6
• ap=300 psi
-.001
r Helium

Gas pressure. psi


Mean Gas Pressure, psi Figure 12. Volumetric strain of coal matrix for decreasing gas pressure.

Figure 11. Variation in permeability of coal to


methane with mean gas pressure, at constant
pressure gradients.

8-,----------------,
10
7

~ 8 1130 psi
~6 'K - 3.2692/P + 0.0763 + 0.0206P"
o N
'tJ
~s .,E
u
'E 0

-4
g .;.
=
~
:=3
J:l
D

.'" 2000 psi


o
III

E2
III
.~
a..
a..

0+--,.-.--..--,--,--.--,--,---,.-.---1 .04
o 1 2 3 4 5 6 7 8 9 10 11
1/PfIII pSi-I
Gas Pressure Gradient(P), x100 psi
Figure 13. Experimental and modeled results Figure 14. Variations in permeability of coal
for variations in permeability of coal to with reciprocal of mean gas pressure.
methane.

100

90

POSITIVE EFFECT OF
MATRIX SHRINKAGE
":;:
4-

::E: 70
.;
+'

'"'"
<::
0 NEGATIVE EFFECT OF
:;:; 50 PORE VOLUME
u
COflPRESSIBILITY
"'"s-
0
o..
~
30
'"
<.0

10
o 4
TIME, YEARS
Figure 15. Effect of compressibilities on gas production.

179

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