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  • Bindura University of Science Education Faculty of SCIENCE Chemistry Department

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    Fortune Vushe
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    Place 3.8g of benzoin and 12ml concentrated HNO3 in a 50ml round bottomed flask. Heat the mixture in a fume chamber on a steam bath with occasional shaking for about 1½ hours (or until the evolution of the brown fumes stops). Pour into a stirred mixture of crushed ice and water, filter off the crystalline precipitate with suction and wash it with water (why?). Recrystallize the solid from about 7ml boiling ethanol. Record yield; m.p.; IR and UV of your product. Keep what you do not use in the n

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    FORTUNE-VUSHE-CH204-ASSIGNMENT-2

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    Place 3.8g of benzoin and 12ml concentrated HNO3 in a 50ml round bottomed flask. Heat the mixture in a fume chamber on a steam bath with occasional shaking for about 1½ hours (or until the evolution of the brown fumes stops). Pour into a stirred mixture of crushed ice and water, filter off the crystalline precipitate with suction and wash it with water (why?). Recrystallize the solid from about 7ml boiling ethanol. Record yield; m.p.; IR and UV of your product. Keep what you do not use in the n

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    © All Rights Reserved
    Download as DOCX, PDF, TXT or read online from Scribd
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    9 views5 pages

    Bindura University of Science Education Faculty of SCIENCE Chemistry Department

    Uploaded by

    Fortune Vushe
    Place 3.8g of benzoin and 12ml concentrated HNO3 in a 50ml round bottomed flask. Heat the mixture in a fume chamber on a steam bath with occasional shaking for about 1½ hours (or until the evolution of the brown fumes stops). Pour into a stirred mixture of crushed ice and water, filter off the crystalline precipitate with suction and wash it with water (why?). Recrystallize the solid from about 7ml boiling ethanol. Record yield; m.p.; IR and UV of your product. Keep what you do not use in the n

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    © All Rights Reserved
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    BINDURA UNIVERSITY OF SCIENCE EDUCATION

    Faculty of SCIENCE
    CHEMISTRY DEPARTMENT

    Student Name: FORTUNE MUNYARADZI VUSHE


    REG No: B202612B
    Course Code: CH204
    Course Description: ANALYTICAL CHEMISTRY 2
    Lecturer: DR N. MUCHANYEREYI
    Program: CHEMICAL TECHNOLOGY
    Level: 2.1
    Assignment No: 2

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