GRU

DISTIL
Data Praktikum
Larutan etanol 90% 300 ml + CaCl2
Perhitungan Densitas Fase Uap dan Liquid
Massa pikno kosong = 15.7246 gram
Volume pikno = 10 ml
Massa pikno Massa pikno T bottom T distilat ρ ρ
Percobaan
isi distilat isi bottom (°C) (°C) distilat bottom
1 23.7024 24.2944 75 63 0.79778 0.85698
2 23.6499 24.2491 76 63 0.79253 0.85245
3 23.6022 24.2314 76 62 0.78776 0.85068
4 23.5615 24.36 77 63 0.78369 0.86354
Rata-rata 23.629 24.283725 76 62.75 0.79044 0.8559125

Tekanan Parsial T rata (°K) C1 C2 C3 C4 C5

Alkohol Bottom 349.15
73.304 -7122.3 -7.1424 2.8853E-06 2
Alkohol Distilat 335.9

T rata (°C) T1 (°C) T2 (°C) P1 (Mpa) P2 (Mpa) P (Mpa)

Tekanan Parsial
[x] [x1] [x2] [y1] [y2] [y]
Air Bottom 76 - - - - 0.040239
Air Distilat 62.75 62 63 0.021867 0.022885 0.0226305

Po alkohol Po air α
Relative Volatility α
(atm) (atm) campuran
Bottom 0.91241723208 0.3971279 2.2975397
2.3218044
Distilat 0.52404144313 0.2233456 2.3463253
 GRUP R PARALEL A
DISTILASI EKSTRAKTIF

Pembuatan larutan
V alkohol 96% = 281.25 ml
Kebutuhan entrainer CaCl2
CaCl2 = 30.6 gr
Densitas percobaan ke-4
ρ distilat = 0.78369 gr/ml
ρ bottom = 0.86354 gr/ml

Konsentrasi alkohol (30°C)

ρ distilat ρ1 ρ2
Percobaan
[x] [x1] [x2]
Po (Pa) Po (atm) 1 0.79778 0.79555 0.79835
92450.70102581 0.912417 2 0.79253 0.78981 0.79271
53098.51357517 0.524041 3 0.78776 0.78684 0.78981
4 0.78369 0.78075 0.78382
Po interpolasi
(atm) ρ bottom ρ1 ρ2
Percobaan
0.39712794597 [x] [x1] [x2]
0.223345609515 1 0.85698 0.85667 0.85908
2 0.85245 0.85184 0.85426
3 0.85068 0.84941 0.85184
4 0.86354 0.86148 0.86387
 % % % distilat
[y1] [y2] [y]
95 94 94.203571
97 96 96.062069
98 97 97.690236
100 99 99.042345

% % % bottom
[y1] [y2] [y]
71 70 70.871369
73 72 72.747934
74 73 73.477366
69 68 68.138075
Data Literatur
X Y
0 0
0.02 0.192
0.05 0.377 Kurva Kesetimbangan Ethanol-Air
0.1 0.527 (Literatur)
1
0.2 0.656
0.3 0.713 0.8
0.4 0.746 0.6
0.5 0.771
Y 0.4
0.6 0.794
0.2
0.7 0.822
0.8 0.858 0
0 0.1 0.2 0.3 0.4 0.5 0.6 0.7 0.8 0.9 1
0.9 0.912
0.94 0.942 X
0.96 0.959
0.98 0.978
1 1
 Data Percobaan
Xd Yd
0 0
0.1 0.205073 Kurva Kesetimbangan E
Air 0.2 0.367269 (Percobaan)
1
0.3 0.498761
0.8
0.4 0.607515 α
Relative Volatility
0.5 0.698958 campuran 0.6

Yd
0.6 0.77692 Bottom 0.4
2.321804
0.7 0.844177 Distilat 0.2
0.8 0.902792
0
0.9 0.95433 0 0.1 0.2 0.3 0.4 0.5 0.6
1 1
0.9 1 Xd
urva Kesetimbangan Ethanol-Air
ercobaan)

0.2 0.3 0.4 0.5 0.6 0.7 0.8 0.9 1

Xd