LAPORAN PRAKTIKUM OPERAS! TEKNIK KIMIA (OTK) Il Modul 4 lation Column Selasa, 18 Februari 2021 Disusun Oleh: Nama : Eryanto Dwiki Firdauz NIM 1 102318102 Kelompok 1 CE-6-U Sore Ss V = . . @ = Universitas Pertamina LABORATORIUM OPERAS! TEKNIK KIMIA. PROGRAM STUDI TEKNIK KIMIA. FAKULTAS TEKNOLOGI INDUSTRI UNIVERSITAS PERTAMINA 2021 Scanned with CamScannerRUBRIK PENILAIAN LAPORAN Komponen Laporan Pendahuluan Tujuan Dasar Teori Prosedur Tabel Pengamatan Laporan Akhir Data & Pengamatan Pengolahan Data Analisis Kesimpulan Referensi Tata Bahasa & Kerapihan Nilai Max 100 10 40 10 45 10 Scanned with CamScannerL. Tojen ~ Hencarvian Yom prodvk distlat den wottom devjon mengguaakan welode Teg ro tometer ~ Merenpukan ph Stage Feori fs. denon menggunakir metode. Gmpis Me cabe -Thiele dan mevode matenans forse - Netentvion evel Colin ep sicvney D. Dasse Teo | De ttss: adalah gotv metrde pomsaban camper dalam Fase cuir cate lverdesoven Perbedeon Kecepalan aw vomashon moray Cwoiahétes) baker Dalam dishlesi, Campomn Yat Aan didikvan Selngga menap + den Uap ini Hemdcn didvajaben Kembali ke dalm bene Gicam. et you, menills bie dah Letsh ondeh ofan wenguap Jebe to, Kemian U9R bch alan moniloni profes gorsiginan pads vinden D. dlon Fendentor Shan bored pre Reruochen fase , Uap akan bewkah wenjsd pasa care yey rvcraplic veler Sebigai ds hlak, (mess , vor) oniep kaxja dav dhs Sern gam betor Addie dowen cen menesubton Umpan He dalam Votom ashlesi. Unpn digaesan deypa Steam yoo dhasilien tybiler. Setelak Fercapes Hie didibtyn, mala olen bwoentvk Vag yoy nail, ko alss Volom disttasi. dan Kelor rade, Irtag Helaren vag Usp yoy abaciien Lily didiysteon pada lenteror. Bhar yoy (beady Bibra bolo — dishlee digroston ley ach relwiler Sdhiroys bbe becbenne fate | PAR Behan you, dale tecvaglen divebaitan melahs Ashog worl awa ble dishes Seong ase. (enw, (034) Scanned with CamScannerDistilasi atch adele gksklag yey dilalween aly ball Grebe5s yaee aban dimen olan prelate » dpe hemadion dental Kenteli Waslin CUechlak dan reso). Cade proses ini feed yer akon dinabuigkon ke dalam £66 yyy {Selon Sigenttuen tvguiy wend Solana proses borin» Uap you teat Alm diembuslear Secam Uorkne Oleh vordergor | unnwe memento guodte distilat. Selah Sab cits das Agritng bale ralth vowpust geod de Grok yay Selle bewiuh sebiay vat) unsteady shite). Datla bole lomsaya Uguiatin univ opomss oxy bapsies eet Cay al youd 08) amber 24 Comuennoral brick dishllahon Rade proses dishes Seviny diquralim recllks - Wal ws diwabedten ayer proses diel r 9 Ay | leo ophimel — Schunya deyut resmaiolion prmdvk denn Herwrinn yos Letale baggi Rezlox adlah batl Vondasae yg debian Kembali ke Volom destlaas ada craly ban dite dtmgoe Sete Snatch orden divembn bien Ye dam Ueolon dghlt sebagai regl , Fonts ini debt fetal regio. Scanned with CamScannerMeede yom) $47 digvetan unbat wrenentdren yer Sige tdenl onde dicing: tha, vomponen Cosa Asniaton ) ab metode gragce Mecabe - Thide dan mete Mralemars Fenske. A. Revsamaan Fouke Unhe reverie junlah thential sage (Io) pada seat tolel copies Creeave 11993) : Nas beotvd/rel 7 (gay \n cag pg ease) MU (ie) Keetermean a Xo; fats mol Lahr bey dt aisha Xe. Fes re\ Light by 4 toftom Ang: geomernc cuaage velatve valatiny, Fed vomgonen Conde hy dewlet don bottom) B. Metode Me- Cave Thiele Metode Medabe- Thide fri menage SFO. Gabwe Coy abie wwalor Laid don Vager CUM) eras tation: Legh = Logi pataran finish haps bal Sly, Gorgon meiode Melabe-thele « 1) Memiuer kurv Kesekmboypr Vag- coir Comsoryn oni Seayaun alti lem poem Yyorg leh vob) Date Keesehinlogpe dapet apunlel, dard oot fora fe bechaspi Literate tertait baie Scanned with CamScanner2), Meat gars openti cecrgying Lonceiny) eee aim ye (Be wt(2 _ Ret aH Reto. eeplx cave ~ Yo Member gars peed (qeune). Keniangin goes bergerg pala fata da feed Genlor 2.2. Wmprantan tape git eed line Aengen Gam ceed. 4). Mem bad ays ogous Sarigpiny - Guns Ini dapat dinet dean woh GRE gerpotorgpn anton feed re dom rech fyi tre dengan WHE xg, S). Memiuat gers Stage yaw dk tual: dei Xy dan boathir pode Xe devopn Wolesan ava Fesetinbapn sreehivig dm ge pees Swspgay Scanned with CamScanner| 6 i ar Guonor 2.3 Reronivan tneontwal Sage dengpn mete Newdabe Thee Unie episients kaom asnles (e,) at Alibng eronyyeatn pocancan Verte Fo: Néeennaal Nachal leeheergan = Mesos nel + umber 0g theorinaal sexe [qute Meat etal punter og piss Scanned with CamScannerIl. W. Alet dan Bolan + Alt V. Baia dishlakon por glat 2. Refrateowetee 3. Teang Rents: 4. Gules vl WML den loome 5. igor betes 6. Botany gergtbvt % Boto| semprot B. Theemameter 5. Ertenmeyer Corn, Keeja 34 3. DSK Gatch dogon Tolel Replies D. Gageen Refrettoweter dan dat G (aston campen ero| don Gir dongan grates mel yoy yer beda - bide . + Gombor. 31 Bakes OisKllehon filet glen Pembater jurva Stade dengon metode Regrattometer Scanned with CamScanner4 Dierecean (avian comprar elmel den air puda ve FAHD INELEr UNE bop Somgel yor re dinat. Kemdan amar dom dicatat wlai indebs aya. 4 Te Vila gage fics mal teadag SMES bor + Dares date yor Upeatls . kewdien Dlsat forva kalibrers gaber mol tevbadeg indas bas Benger wibinar cas dala 1", Bigerde ave pres mol 0-6 B12. Batch dstllatom dampa folsl Replies Dirct fovren 40% gel den air (Aker. Kenden dinateieten Lenton ¥e delom lely G4 + Dive raazac lat dalam Feodnan Bake node dagen tends total Gets, inane Gierad vabe St terttup (setteg raglies gue tds off) ‘ Dinter fouew heater pada pel Sekiya Girton dapat tervagten pada dla Secon Krensten. Keawudion dicntat Gu pada Tr dan Tq sebeln paganbbin Som t Scanned with CamScannerDonbal sempel bsrlet dyn mambuen si solenoid she 54 don dihacka dish Ace tearpery pada foget 0-4 = oe ee ee SS ee Diver wiles indets Los derapa imengguraten regvearte meter dm diterien andy Yaw telah dieu We grate mel disblak mempow tan von $ Prado Langlah Sebelurya . Kenudien Diamb| Sempel Peltor grodect te he Vr | Distoe wiles indets bias Aonjon meryyuroken repratrometer dn diem nila fore wel pode bottom payer mergyveten Kwon Stardosl yore) | tel aso — Sebetumyn. | Dives: pergambilan Sengel oR 5 ment Sebayak 1 FAL. Non Mlevteng patel theoahco | plates da Glenn epricancy merpweator 3.2. Dishbe Botch deyan este Refives Bat Pombvaler Youn Semded dogm mettde efaetenetee Repapromeier don dibvatlelr Loven coger Dinopen yy verbo heda Chorel dan ae deagan grabst mal Dye tn mefode — Pawenceran. ae ‘ | Scanned with CamScanner‘ DHeteston fawten camguron Crerel den OF pala alot regrabiowcior ihe Setag Sengel yang Athh dibat - Kemsbon thaws dar denies TTT i eae eee aoe t | Olt gape feats mol terhadap inders 8 den Aagyeaban Scag Vorun Stadeed 3.2.2. Batch dishlfation derape consiank Regls Dat rerayain alat dolom Keadamm boick mode demyor Konig: Ceostent fryes , dieting EFM Lalor Leadon 'oy¢” CEE TTL ILTTEVUEL I § Rlaot Laven 40% etacl dan air Schamak 4 Ser Kemdion dimantten Lenten 2 dalam Baby 4 t Dratue power hater Sehiyye Lect apt tewapean cocoa verstn Keovdion etelal Mencofei Honk Steady SIME, diate feds rake bergen govberdiogan sii (5 FEFWES Ke Kolom dan 15 dalon togk 91) Sekelah 10 merit, Arcatok she geda Tr dom Ty leerden duambil Compt Brrkint pada toyys dan Spel better grit dae vole Yt ri STITT TT AIATTT TUT Scanned with CamScannerFema Men bbiturg jumtth theoabcal plttes Jon celenn Lfsrcieney Menegugtan matode V - Viste Penganaton MeGbe - Thele Al Dis lags Batch dergn Toba ce glues 0 lees peogpan low Sumpe' Kap S mes! Selenyak lokndy Tabel 5.1 Data kurva standar dengan menggunakan refraktometer x (fraksi mol} Volume (mL) Inceks Bias (Nl) Ethanol Air Ethanol 0 25 0 13325 O4 13.375 6.625 13468 025 1a 2B 1.3574 Os 5.89 wal 13625 06 4.26 20.74 1363 07 2.92 22.08 1.3632 O75 2.33 22.67 1.3625 08 179 23.21 13622 1 0 25 1.3592 Scanned with CamScanner‘Tabe|5.2 Data Volatilitas Relat (a) dan Indeks Bias TOTAL REFLUKS i we Tose Teel TT i = St ee = 3 faa eee ee fa = =n aa es} [ae [eel pete thn ae ome Ta we T= | I I TTT Saar oun am Tapes ed ‘abel 4 Dato Volatiita Relat (a) dan Indcks Bias KONSTAN REFLUKS 2:Tabel 5.5 HasilPenentuan Taba Distilash | ay — oe Te Tee fof) | via [sori enw | ie [res | senaal [sas [emmmnns FT aasss | as [sean] snr L eanowy —_[omtmnenss Fr some] ae sol aan (Graf 5.1 McCabe Thiele Total reflux Me-Cabe (Total Reflux) A (GraflS.2 Mecabe Thiele konstapt reflux 3:2 Me-Cabe (Constant Reflux 3:1)Grallk 5.2 McCabe Thiele Konstant reflux 5:2 Mc-Cabe (Constant Reflux 5:1)a . Pengelalan Date A. Pembatan kuna Stander bee baat pres etano | > Fras mol elano | z= mokeml ; mo etenol ; T= etane| mot total mod etewo\ & mel air js air Ol = 0,3 Yi/4e.or 0.7893 /46,07 + 0,59¥. “He, Volome etonol = 6, 626 md Volume aic > tEmL- 6.615 ms 5 (8 3t5 me 4 B. Rersamaan korea Srondar Kurva Standar Metode Refraktometer os ay: Ug ,0¥6 KA — LoON3> Rvs 0, 844d oa y=1S07Gx- 20.197 RF=O.aae Fraksi mol (x) p S ate “Las Ls L345 135 L355 L386 L365 Indeks Bias (N) ce Linear (Series om Linea (Series) C. Peciituran Xo dan Xe * Total Berton (ts ve menit) ¢ Konstan Replux Ss ~ Xo. (15,036 x (341) - 20,137 -Xp- ( tg0% x36) — VIS = 0,3844 = O01 Aoted X62 (ice «4, e406) - 16,137 = 0.07389 - Xo - (sew Antoine Loy tots A - 6 Tte CF, yy CA" Me) HE tano\ A: F586? To: mr °C Bz 12859 To. 848 °C C: (G3 1 Hs 8 636,907 we P’ a 69,ar He A hc - Ae Bort To: 747°" 3: thao es Te = 84,8 °C C: 128,4u4 Uo - 258,347 wa 0% Se 399,501 kha k= @* . ve } Pholal< lat Protest X lo. tus plo 7 Dis hlasi kez G36, gor ue z Jor bln : 6,854 to, 325 Ka lens UR ANY bons assay lol, su teu Bottom ; Kez 9b2, 4r03 Ur = 95595 top, BU Kela Kou: 39, col Een Ee 30 tor, su ee ; eS ? Tol Replox > Katoine Crmenceri t*) ‘ (ar @/tre) Rr zo q E dane | -Toe 7&7 °C Te: 863°C Rp, 763.9507 Hla CB: tort. os3e Per A fac - R*p. Bir, 3343 Els Ca: 423, 8193 Ela et > Prot 2 Late Prormi = (or gaz ve 4 Dist les ke = 263, 5502 ths 2 PS39b tot, as ke kw _siny2943 Hs - 5, 085 jor, 325 Kes A Bottom Ke- om asus lovuss tor. are ee Kw. A BUTE 4B a96 (ol, gr ha© Long tan Reclu« 3: | * mengari ? > Antoine eg Med 4 €tano | To= 86,9 ‘c Tg: 84,9 ° P*o: (048, 3023 Ela Ca. wnsoss ¥en # pie C80: W760, 664 Ken R782 14, 692 Kee E. ( Graph Me Labbe - Thick Ns lh Go) Feed Line ~ Fetal replys 2p: 01985 — leone tea Re jon 3:1 tee 0,r608 ~ Konstan feflue $1 TF = or 7% . Cpisiensi eolorn “bos Mion wool Natnel - thy z 2 ¥ reflux = 4103 ioole 234,43 % ? 7 Vests repber 3:1: 3 A433 otf = 44 19% f 19% > ; —Moasten t reglue 5:) 2 30207, rool, = 439%) } \ «: CC Roa = Lato ! Chote DV lois sue ele A Oanlas, \ Kes “load. ove = (013453 | 10, BB Kw, AiFeo, 286% 2 (lb, ogat Lol, 3% f Bottom te: _ Wh, $953 zs WW, st Lot. BS lew 2 — 14 659% — 2 0,14567 Ld, BUS * Fomlih Stage ~— Tatl Reflux Me (665 -— enghm4 Reslog 3:\ Ne (85 ~ Rens tent Repos ge] N: |,84Vl Pombahasan ada (rab kom medut " Gatch Dishllakon” iri dengen mela bwkan evsperinen dergon renyveran hypen menennkr Fom pos & eceduk top (iste) " Batch dishlaton Wir Cod © Sebagai alat viemonya Devan den bottom. Pons p keqa bleh distlaken terselut yaily pawschon fran tempore leordosertin peibedon Bik didi atav volo mlites leengoren. {come nen yrs) te Volanliins SRUIBRE diddh yor leek vendal alcar Keeler Sebiani prod dishlek, Sedmaven (empower, yay mempurye valahlites yor leh bey alow kelvar Sebasps Produk bottom . Produe dis Klat 7a) want (ier voreliklas yay Nelle pander menrtier Walen Stine Videleaon yo Lebil, rendob Sibmdinn kon dewpn produ boltora,, Shingo grok degtrlot d%ehvt Sebreps Laghs Fey , Sodahy bn Unive produr loottorn disehut heavy vey - Kem dan prabslwm ka di ini melatvken ebspaimen dawn Higa uoah refbA , yoiv toll replin, eorstent reflux 3, dn vorsten repli Sil. Dan peamerer pag aten divuc Oleh tampeate \olom den inhoks bas Lenten, Daia yy eb dipaoleh das gerstian temebt dept Sislth Many tort grafic don label perk fngan . Combet gfoge Kine Sinden tech dpat dyorleh des ule inders ‘reg laden Crmel -air down fry mol yay berkede body, Borsrkin luna torent , dpenieh persamaon ais Sar pur Ve tS, 096 x 10,139 deren RVs O.B44B . Persamaan gars yor dipervleh dev gage tenet digmban UnME mencaNiton fealeg al pada maging - main prodib dishligs . Pers baan dilatv ben Selome 5-§ wrenit dargen tviven Fendt epereti Mencapei Steady State « Rede meant ASt SS ment » WE Seting Percelam winrar indiags Hendics Steody Site dilihok dex ila indets fies mogny- mary yay Cendewag bensten. Miles inders bis Cereb Kemwdiun dogut dicen Untule wren ing wilai trcles mol pada produk destiled, proiue bottom, den aktren feed, Abn fetepi pada pratime produc bottym men hag len nile wong,| Buchsorton batl geri hanen , avrnlch Sine elorm desta dugat —ditenkirer deny mengcungiion metode Mmatenats faske den mebde gage Me cabe ~ Tide . Araviss qua Stage pale mabey = ener “ | beedasa ton deta dutn yor) dipeccleh dagat dilauden Derg melpde wodemahs — fertice didopat ton dural siege Prde Parohaon telat TEAS 7 Keonsint Taps 3:1, Konstnt rests 5.) mosing - rrasiy “econ enaion , d condi 7907 3.4435 7 30199. Cada bade fale t dep eget decameulten 414 dioording ver dengan | cower af leudaye , Fowstan reps 3:1 46 bons tan t rege 5:1, meni —qumldk Cage lebih ' Sond 7 Hit teseo Period Koren fd vondtss total repr, probe disALor den praht bottom divembulicen Ke abun Kolom . Dan ards otal Tepex dbp ber Unt opanes Volo ARIAS mena \eordrs Steady Srate, Unie menen Ven berapa vm Stage wii doih Gay operas d'shlag — Lemudion dowen Metode Gmpin Ne Cove - Trice didepal ten Jrnlah Stage pada pertobaom tobl Tepe leandtind replas 3:1, eons tent ep Fs mating cwabrg Adapatim Wee) 1105 5 IR. Pade metode MeCate Thiele Cong d m sagen metede TOS Bey Yai pads endeyy tolel Peplvx memitie ueieh Sreye yong lebih vecil, u IMU terse Feindi perena pede merede meeabe Thich ini wena asem@ ben loshin Lagu atic molar buite Laud wasp Varor, (A) eensien Won de, Fes dSewst sebages Constant Mela Over Low (eK4o) Namun Pade keadnan yen Seoenarn ya Kaul lal [Long fen, Sekinggn pertedemn nilai teselye bend.Vil ; Kesimplan Yeamevion : Bordasareen rat new vert felnk dilalyken 1 di dapat tear ame k reper 3:1 |. Neomposigs provox draitot ime ing mating gercoloon toral rege rVesiont ef BG dak Konstent reflex St yaih 01346367 0385 % 0, 2884. Unne Ieemgo SG ere wis Bi), enstent bolton ods maging - mains perebbacn total cops 1 berger vege BN PW S-1 ardalar 9021 7 0.005 7 0016S. 2. Yanloh Saye pada wating wary percoinon dowmm metode waterchY Fesee Padu total veplr , benstent replves Sol, \emshat cope StL yk ty 2) 4105 i 714453; 3,09%%. Den pada metode Mecabe Miele pedo wing maging yaiby UbS ys 1d 7 LBA, 3. Overs {) Column Sfitercy — Phde mating -masng perebbcon folal reflec gy lenge FESIES 7:1, Kongpens refs S31 Seihy 34, AB fo; 19, 1908 G7 43, Hb hh. XI. Re sere & r Sender, Healey and Poper _ Seporatss ny (ro cess, petncig len, 3° edihen ott Wenteot rw). Segeress on ro 28 5 eryineerng Incase mass teanger “gtd edkon, - a) HH, Chan 2006, Pemishen Sere Purcell Alnoho | de manga dergin core dis . ei . Ba Erarpves. Ponronnle : Citeenite Negeri fortranerc, Norv ’ Pain, ond Metey 4 W099, “ Tintern teonihs, Pees en Lslom dhloy ane Cra reprone Pb ike seala industrs Polen beng > Unveemong Swifoaya