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Certificate of Analysis 1.00731.2500 Sulfuric acid 95-97% for analysis EMSURE® ISO Batch K45933231 Spec. Values. ‘Assay (akalimetic) 960-970 % % Colour <10 Hazen Hazen CChlorce (C1 504 om Pom Nitrate (NOs) <02 em Pom Phosphate (PO.) 05 om Pom Ag (Siver) 0010 em Pom ‘A\(Aluminium) 0.050 om Pom [As (Arsenic) 50010 pm Pom ‘Au (Gold) 0050 pom Pom 8 (Boron) 50.050 pm Pom Ba (Barium) 0050 pm Pom Be (Beryl) 0010 om Pom {i (Bismuth) 0050 pm Pom (6a (Calcium) 0.100 em Pom (C3 (Cadmium) 0010 pm Pom C0 (Cobat) 0010 em Pom Cr (Chromium) 0.020 pm Pom cu (Copper) 0010 em Pom Fe (ron) 0.100 pm Pom Ga (Gallium) 50050 om Pom Ge (Germanium) 0.020 pm Pom tn (indium 50050 em Pom (Potassium) 0.100 pm Pom (Lithium) 0010 pom Pom [Mg (Magnesium) 50050 om Pom Mn (Manganese) 0010 pom Pom ‘Mo (Molybdenum) 50.020 om Pom ‘Na (Sodium) 0300 pom Pom INH« (Ammonium) st pom Pom Ni (Nike) <0.020 em Pom Pb (Lead) 0010 pom Pom x (Platinum) 0.100 ppm Pom ‘sa (Tin) 50.050 em Pom ‘5 (Strontium) 0010 pm Pom (Titanium) 50.020 om Pom (Thalia) 0.020 pm Pom (Vanadium) 50010 om Pom Zn Zine} 50.050 pm Pom 2+ ireonium) 50020 om Pom ‘Substances reducing potassium s2 pm Pom permanganate (as SO) Residue on ignition <3 pm <3 Pom Merck KGaA, Frankfurter Strafe 250, 64293 Darmstadt (Germany): +49 6181 72-0 Page 1 of 2 EMD Millipore Corporation -a subsidiary of Merck KGaA, Darmstadt, Germany 290 Concord Road, Bieri, MA 01821, USA, Phone: (978) 715-4321 Certificate of Analysis 1.00731.2500 Sulfuric acid 95-97% for analysis EMSURE® ISO Batch K45933231 Dale of expiry see produc label ISO-Reagent Dale of release (DD.MMYYYY) 16.08.2014 Dr. Reiner Vogt ‘Response laboratory manage ql Conval ‘This document has been produced electronically and is vali without a signature Merck KGaA, Frankfurter Strae 250, 64293 Darmstadt (Germany): +49 6151 72.0 Page 2 of 2 EMD Millipore Corporation - a subsidiary of Merck KGaA, Darmstadt, Germany 200 Concord Road, Bilerica, MA 01821, USA, Phone: (978) 715-4321

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