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Experiment No. 5
Analysis of Ash
I. OBJECTIVES
RESULTS (g)
Initial Weight Sample Weight After Ignition
Trial % ASH
(Crucible) Weightdw (Sample + Crucible)
1 25.0636 0.6973 25.2430 25.2431 25.73%
2 20.3538 0.7177 20.5441 20.5439 26.51%
3 22.8509 0.7258 23.0304 23.0342 24.73%
Average 25.65%
25.2430 − 25.0636
= × 100 23.0304 − 22.8509
0.6973 = × 100
20.5441 − 20.3538 0.7258
=25.73% = × 100
0.7177 =24.73%
=26.51%
DISCUSSION
In this experiment, the observer first places the crucible containing sample into a 650 oC oven for 6 hours. When the
sample is completely ashed the observer puts the crucible into a desiccator to cool it off for 30 minutes. After cooling it
off the observer weighs it off and records the data. The purpose of this experiment Is to determine the inorganic
materials that are left off in the sample.