Expt No
pate: 12/ Ws 2014 Cage NCE 7/2)
“DETERMINATION OF OIL ConTenT OF SPICES
~_ CLEVENGER APPARATUS
AIM
L To conduct Study m cleven ger appesrat us
| PRIndCIPLE
| \ Eesenkal oth can be. orttaaid nung, mothods Such
| las Solvent extiacton , Superculical fluid exbadion &
| Tmuorwave extiactoon. It 4s smportank to nole that the|
| Teagnid alway bos ab the temperaturc.ab whith 49 Was
| [pour prossuce equals the atmospheuc presturt oY Sunom
| Tundung pressure - for any two urnmusble Liquids, He
lGofal Kumber of mofecule. prusent alone at the Some
[hem peratone - dente the pressure excited ether de by
| [pare Vapour clone - consequently the Vapour pressure
of wheter System enveases that couse to evapo uate
Vessential od haveng tegh booting poont cen & eva
| powrartad with s@am GR akabo Such that thir ombmnid
Vo-pouh Prtss Wie caves eg uals the atmosphenc prcssure
i the manufacture essortleal oxl , zug the me-
[tho of- wale. ditllaton . mateual Lt comple Lely inn
ded ca water and brought ts the bol . The mawn chdsact-
[eesteer of this prowess that thee 1t dusct cantack bet-
nen bolerig wole and _plant matewal. Dustillotion
offes beter Condton for the _ormosi of ol because
the fughaer femperoduat and pressure fluctuaton withit
|
[WATER DISTILLATION
1
+Expt No. .
Date : ba
the wtill snesease ov accolasle the fore of Ad
such a pont that all the wlatde oil entavned vidrin
the plant tusue can be Collected A speual cased, wales
later to the shit afbr the oct has bed Seperated dum
[ab So uk can be avboiled. the prinuple behund sk is to mi
dutteton, sb usa prachie of rctummuig the dutillases
nimige the Losses of oxygenated component s practical adc}
vantages f- wate dédlloteoin are thot the _skib are
inexpensive, tasy to construct and suitable for puld ape-
5 4
Raten
EXPERIMENTAL
the cle uk of a maun tube contauméid
widh Condenser ahd graduated tube widh glass stopcock
4 setuvn tube for the aqeous port of cle Killaloe conn-
ech the botlorn of the measuring tube and man fuky
The 609 Sample 1 bo be placed into a Sand entaack-|
ton fotk soaked widh 250 ml of water. the flask ts fo
he heaped unrig peotorg mantet - the Sample should be
moxed and allowed to boil. Vow the water and extrac -
ted ol Gtk evaporabed . the Vapour Mmucturs condlemed
wun sehr wondenser, ditilale watw and ou Plows
‘nto graduated tube as the oil is imiible wh wailor
uw may be seperated eanly and Start accumutatirig -the|
datil(ale waka rehunung, ‘te flask offer the ol Aas beon
seperated Jom ub, o that rbcan be avboued. -the ou! was
allowed to stand Jor sufpieent Lovie to lear and Jhen
wb llecld weighed.
YF
RESULT: Determmahion of ou Confent by clevenger
apparatus 4s Studeed