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    US9410042B2

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    (2) United States Patent Chavan et al 'US009410042B2 (10) Patent No.: US 9,410,042 B2 (45) Date of Patent: ‘Aug. 9, 2016 6 oy 2 Cy © ay @) (66) (n 3) G0) Mat. 30, 2012, oy 2) (8) 66) PROCESS FOR OBTAINING CARBON BLACK POWDER WITH REDUCED SULFUR. CONTENT Applicant: Aditya Birla Science and Technology Company Ltd., Mumbai, Maharashtra aN) Inventors: Sandeep Vasant Chavan, Mumbai (IN): Harshad Ravindra Kink, Mumbai (IN); Shobhit Gupta, New Delhi (IN) Assignee: Aditya Birla Science and Technology Company Led., Mumia (IN) Notice: Subject to any disclaimer, the term ofthis pateat is extended or adjusted under 35 USC. 1540) by 0 days Appl. No: 140989,438 PCT il: Mar. 28,2013 PCT No $371 (Ol. @)Date PCTIN2013/000208 Sep.30, 2014 PCT Pub, Nos WO2013/175488 PCT Pub, Date: Now. 28, 2013, Prior Publication Data US 201510056127 A Feb. 26, 2015 Foreign Application Priority Data o low MuM2012 Incl. cose 156 case 148 us.cl. CPC. CO9C 1/56 (2013.01); COC 148 (2013.01): ‘COLP 2002/88 (2013.01); COIP 200680 201301) (2006.01) (2006.01), Fleld of Classification Seareh cee cose 1/56 See application ile for complete search history. References Cited US. PATENT DOCUMENTS Losger A 121033, Rud Logie A “FI934 Vose 248659 A 71948 Brandon 286819 A 11/149 Chenck BSte77 A 'RINS0 Howmet al 2507S A L191 Hemera deossoe A798? Ady eal, 2oroot A 121082 Shale 268230 1953. Amold etal. dean A $1953. Mamon tal 2oones A 121984 Poter BS1S02 A 101987 Gosser ta 2SGG7SL A 121958. Zimmerschicd ea 2866752 A 1DI9S6 Zimmerchid et 2oontal A "9198 Maye al 25139 A198) Hanston! Yow A "6961 Kenny Zoot A T1961 Higa ctal Sioot912 A 101961 Kaneko ets A "196% Kimbstin Iota A 131968 Webster et a R"TH968. Greenaval A $1967 ‘Steed eta S 51967 ‘Tee R168 Heimtich etal ‘A ‘S196 Rivinet al S41970 Wallace at A S4970 Apoyes SSenyo7 A D197 asker YeI7S30 A LLISTL Riewe eta Si0.oae Binge etal a Tone a 2 Shick 8 ‘ams tl a Shite Lassi & Kohn Aisles & Win eta S778 A Beatdon Je ta (Continved) POREIGN PATENT DOCUMENTS. ow 30127 A 4/2002 ow uasi33s A 32004 (Continued) (OTHER PUBLICATIONS Firs Office Action sued om Jal, 27 2015 by the State allt Propety Office o the People's Republic of China for Chinese Patent Application No. 2013800202280, which was leon Ms. 28, 2013, ad published as CN104334650 on Feb. 4, 2015 (Inventor Cavan tal Applicant Aditya Bila Selnce and Technology Co. Ltd: (only translation provided) (9 pages) Tneraionl Search Report an Writen Opinion mailed on an 4 2014 by the bythe International Searching Authority for Interna tional Patent Application No, PCT IN203 000208, which sled fon Mat 28, 2013 and published as WO 2013/17S488 on Nov. 28. 2013 (Tnsenioe—Chavanetal; Applicant —Adiya Birla Seience snd Technology Co. Lids pes) Iernationl Preliminary Repor on Patentability isso Oct. 1.2014 by the Intoratonal Scarchiag Authority for Intemational Patent ‘Application No. PCTIN2013 000208, which was Hed oa Mar-28, 2015 and published as WO 2015175488 om Now 28, 2015 (iver: CChavanetal; Applicant Aditya Bila Scienceand Technology Co. LuLs pages). (Continved) Primary Examiner — Stoatt Hendrickson (74) Attornes, Agen, or Firm — Ballad Spahe LLP on ABSTRACT Te present disclosure relates to process for obtaining car- bon black powder sith a sulfur content of ess than 0.07%. The process includes step of reacting carbon black powder with @ sulfur content of 1-2% with an alkuli metal or salt thereon. ud media sta temperature inthe range of 100° (C-10-380° C. and pressure in the range af 1010500 psig. It ound that in accordance with the process of the present isclosure, the sulfur content was rediced substantially fro ‘that of about 1.25% to that of 0.05%, resulting in about 96% desulfurization, nel 1 No Drawings US 9,410,042 B2 Page 2 66) 3816301 A847 800 ‘oos.sz4 Sones 109538 20779 133350 7612 ‘ivs.se S2ase9s 4377009 Sue asian 4837980 sero 9s 65 £40130 Aosaass Sansa S510? Sirr99 sbasaat suv sana 1402940 300219 eissnsi5, 630.268 speno8 Sse o90 71809 72413 7278132 7291289 maidsas Tato sma Tse8690 ‘To68635 9.114 2000009684 20020022868 20020169242 20030029777 sonso1so98 aopvo0t29ss sooworo9Kte doogo119199 sonson31s38 2noso0078 aoso14ssas 2n0so1s926L 20060022604 20060210564 20080226049 20080283780 aooro10s7is aovronr79st 20070295640 sonwonosse 2000 0000000 aono.on8isis 2opo0144874| sn100r64067 2owworreT09 201010302326 aowwo14T274 References Cited USS. PATENT DOCUMENTS Bo B al a AL al sume Live List 2i0Ts oles loses roses 1079 Sips Divs A982 Sis Liss 98a vibe Sii987 10.1990 T1991 e999 Stv94 101997 e109 2001 4001 201 2001 2002 2002 $2003 102003 12005 $2006 12 2008 12006 32007 72007 02007 hao? 008 ons 2000 5009 e211 2015 72001 2002 22003 102003 ‘3008 ‘2004 ‘62004 ons 200s ‘ros 9005 22006 9 2006 ro2008 122008 10200? 22007 1008 13009 000 ‘2009 102010 112010 12010 ‘e201 Baird et a Bearden Baink ital Bind tl Bain tl Miasck ea Chang Seamon Miler ea Heredy eal Nongbr et al Mile a inert Nocman ea Tower Delve amass Brons etal Mahim t Bronte a Gore Kocal Rappas (Gunmen Schmid Tose ea Rabon ea Schocker Srinivas Line at ‘Gupta ea Kalas etal. Denitoe cove 56 Dysart a Sehucker Yorke Chava tal. Kawazne ct Mackay eal Kiara Khare hare tal Sinks Sinias el Kanne eta Niedermeie ta Zinnca ct Schucker Bit eal Tach Kumagai tal Nemeth ta Spivey ta Salsetal “Thingeanasampanthar etal Tana Keckler etal. ‘oid Shibata eta Morshoshi ea Soto eta. 20120183387 AL 62012. Munya. aovaupiass? AL V2014 Chavan etal sovanro0si2 AL 102014 Rodiguer ea. POREIGN PATENT DOCUMENTS. ow 3939 872006 wv wors91940 A 3/2009 cw oLdisass A 2008 Ow totssiso7 A 72008 Ow lossus7 A 12014 cw oseisat A 32014 Ow joatsesst A 11 2014 wv Toisseso A 22018, rey Towsi2get A 72015, @ TSI7S55 AL 32006 iP desist AP 12018 iP deaioss AP 22014 iP praia Ad 92014 ip DSL A2_— 22015, iP aooos70 A? 82015, Gh 4103 A U1936 Ga LaTKI90 61977 aK tower” 112014 aK Hoss 112014 D aoidoaiss 10014 »D anisoies? "42013 »D aoisosit 72018 IN sAsMUMBOIL 32014 2 SOON 21975 » Sop14e9 1975 » GLsSIs3 1086 w 2001-501239 41/2001 @ dootssiors A 122001 » dooxsau70 A ‘R003 w 2003-828192 A 92003 @ doossow7 A 3 2005 » doos-tonios A L005 ® domeitest3 A "83000 w “4626802 B22 2011 » foster B2 22011 » 2012010480 A 12012 w ovacsossss A 22014 @ doutsi7ms A 7014 » doissonast A 1018, w doisisiass2 A $2018 wx 201301202 A 52014 Nox aoiaooaors & $2014 Mx aoisooases $3018 RU ao1su7=L LLB 1984 WO WOSSTEDE AL 41998 WO Wosnussa4s “01 Wo WO.0170855 92001 WO WO-2DINDIT AL 6 2002 WO — woomso2Ns9 AZ — 3005 Wo — Wo20707K8I6 AY 72007 WO — Wo2mDSosBq2t AL 52008 WO — Wo2UIT OSD AZ —-K2OIT WO Woosiiz7s4 a2 92012 WO Wo2MI287097 A211 2012 wo 2012 wo 72013 Wo Wo2mig0s9885 AY 42014 (OTHER PUBLICATIONS First fice Acton ase on Doc. 28, 210Sby the State nll Propety Office ofthe People's Republic of China for Chinese Patent Application No. 2013800881012 (lnvenlor—Chava etal Appl ‘i ~ Aya Birla Science Technology Co Li only tamslation provided) page). Final Ofice Action sued on Des, 31, 2015 bythe US, Paes and Trademark Office for US. Appl No. 14353610, which vas ed on Apr21, 2014 and publishes US 20140290852 on Oct 2, 2014 (ventor—Rodiguez eal; Appicant—Aaiya Bila Seience & Technology Co, Lt; (16 pages) Asian, A.V. otal, Vanadium Poroxocompleses as Osidation ‘Catalysts of Sulfur Orzanc Compounds by Hydsogen Peroxide in [BiPhase Systems, Catal. Td, 783 195825 2003) US 9,410,042 B2 Page 3 66) References Cited OTHER PUBLICATIONS Altar, A.. Corcoran W. H, Desulrization of organic slur com Pounds Regenerable and on regenerable oxygen arin, Ind Eng ‘Chem Prod Res Des 172): 10291978). ‘Chen, L- Oxidative Deslfrizaton of Sitaated Gasoline ver “Metal Oxidelnded Molecilr Siew, Chin. J Chem. Fg. SC 520-523 2007), (Collins, FM etal, Oxidative Desulphusistion of Os Vi Hydrogen feteropolyanion Catalyis, J. Mol. Catal A, H1%1-3 307403 997) Doibear GE, Skov E.R. Selestiveoxidationasaroutetopetroeu

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