Versión : 5

Informe de Análisis : 9604 Fecha : 23/06/2020

Muestra : MEDIKIT (CAÑAMO)

Datos del cliente

Empresa : RODRIGO FAGUNDEZ

Datos de la muestra

Forma farmacéutica : EXTRACTO

Principio activo : CANNABINOLES (THC;THCa;CBD;CBDa), CADMIO, PLOMO, ARSENICO, MERCURIO

Cantidad declarada : %CANNABINOIDES, METALES PESADOS

Lote : 1 Vencimiento : No aplica

Fecha de recepción : 26/05/2020

Presentación : Estuche de silicona

Descripción : Extracto

Metodología de ensayo

Ensayo Descripción Procedimiento

DOSIFICACIÓN HPLC DAD - DOSIFICACIÓN > HPLC > DOSIFICACIÓN HPLC DAD MAK-CANAHP-001
CANNABINOLES
(THC;THCa;CBD;CBDa)
ABSORCIÓN ATÓMICA DE LLAMA DOSIFICACIÓN > ABSORCIÓN ATÓMICA > ABSORCIÓN MAK-CANAHP-001
- CADMIO ATÓMICA DE LLAMA
ABSORCIÓN ATÓMICA DE LLAMA DOSIFICACIÓN > ABSORCIÓN ATÓMICA > ABSORCIÓN MAK-CANAHP-001
- PLOMO ATÓMICA DE LLAMA
ABSORCIÓN ATÓMICA DOSIFICACIÓN > ABSORCIÓN ATÓMICA > ABSORCIÓN MAK-CANAHP-001
GENERACIÓN DE HIDRUROS ATÓMICA GENERACIÓN DE HIDRUROS (TRAZAS)
(TRAZAS) - ARSENICO
ABSORCIÓN ATÓMICA DOSIFICACIÓN > ABSORCIÓN ATÓMICA > ABSORCIÓN MAK-CANAHP-001
GENERACIÓN DE HIDRUROS ATÓMICA GENERACIÓN DE HIDRUROS (TRAZAS)
(TRAZAS) - MERCURIO

Inicio análisis : 01/06/2020 Fin análisis : 22/06/2020

Resultados de análisis

Ensayo Descripción Cumple

DOSIFICACIÓN DE Resultado : CBDs=43.7% / THCs=3% NA
CANNABINOLES Especificaciones : NA
(THC;THCa;CBD;CBDa)
DOSIFICACION DE CADMIO Resultado : ND <=0.0001 ug/g Si
Especificaciones : <=2.9 ug/g
DOSIFICACION DE PLOMO Resultado : 0.47ug/g Si
Especificaciones : <=4.2 ug/g
DOSIFICACION DE ARSENICO Resultado : 0.14ug/g Si

Revisado / Aprobado por : Director Técnico Q.F Mauricio Silvestri Suárez

FIRMA :
Digitally signed by: MAURICIO JOSE SILVESTRI SUAREZ
Reason: Informe muestra nro: 9604.
Location: C:\Users\msilvestri\Desktop\firmas electronicas
Date and time: 7/13/2020 2:47:35 PM
Los valores asignados en este informe sólo corresponden a las muestras ensayadas. El muestreo y transporte de las muestras lo realiza el cliente. Este informe
de ensayo no podrá ser reproducido total o parcialmente, sin la autorización del Laboratorio Kemia.
Av. Gral. Rivera 2023 Montevideo - Uruguay CP 11200 +(0598) 2 402 63 66 / +(0598) 2 401 19 96 www.kemia.com.uy laboratorio@kemia.com.uy
Informe muestra nro. 9604.Página 1 de 27
 Versión : 5

Informe de Análisis : 9604 Fecha : 23/06/2020

Muestra : MEDIKIT (CAÑAMO)

Especificaciones : <=7.0 ug/g

DOSIFICACION DE MERCURIO Resultado : <=0.002 ug/Kg Si
Especificaciones : <=1.4 ug/g

Av. Gral. Rivera 2023 Montevideo - Uruguay CP 11200 +(0598) 2 402 63 66 / +(0598) 2 401 19 96 www.kemia.com.uy laboratorio@kemia.com.uy

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Instrument:EQA_073 Sequence:cannabis 06062020

Chromatogram and Results

Injection Details
Injection Name: STD 2PPM Run Time (min): 29.04
Vial Number: GA1 Injection Volume: 20.00
Injection Type: Calibration Standard Channel: UV_VIS_1
Calibration Level: 1 Wavelength: 270
Instrument Method: THC-THCa-CBD-CBDa Col3um Bandwidth: 4
Processing Method: Basic Quantitative Dilution Factor: 1.0000
Injection Date/Time: 05/jun/20 16:11 Sample Weight: 1.0000

Chromatogram

Integration Results
No. Peak Name Retention Time Area Height Relative Area Relative Height Amount
min mAU*min mAU % %
1 CBD 11.197 36.695 181.083 50.67 55.05 0.0019
2 THC 15.390 35.723 147.848 49.33 44.95 0.0020
Total: 72.417 328.931 100.00 100.00
No. Peak Name Retention Time Area Height Relative Area Relative Height Amount
min mAU*min mAU % %
1 CBDa 7.340 16.931 97.542 48.99 52.56 0.0020
2 THCa 11.767 17.626 88.029 51.01 47.44 0.0020
Total: 34.557 185.570 100.00 100.00

Chromeleon (c) Dionex

CANNABIS DAD/Integration Version 7.2.9.11323

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Chromatogram and Results

Injection Details
Injection Name: STD 40PPM Run Time (min): 33.00
Vial Number: GA2 Injection Volume: 20.00
Injection Type: Calibration Standard Channel: UV_VIS_1
Calibration Level: 2 Wavelength: 270
Instrument Method: THC-THCa-CBD-CBDa Col3um Bandwidth: 4
Processing Method: Basic Quantitative Dilution Factor: 1.0000
Injection Date/Time: 05/jun/20 17:13 Sample Weight: 1.0000

Chromatogram

Integration Results
No. Peak Name Retention Time Area Height Relative Area Relative Height Amount
min mAU*min mAU % %
1 CBD 11.120 598.397 2986.312 50.20 54.01 0.0382
2 THC 15.357 593.575 2542.500 49.80 45.99 0.0376
Total: 1191.971 5528.812 100.00 100.00
No. Peak Name Retention Time Area Height Relative Area Relative Height Amount
min mAU*min mAU % %
1 CBDa 7.183 283.817 1446.550 50.16 50.25 0.0381
2 THCa 11.650 282.017 1432.316 49.84 49.75 0.0370
Total: 565.833 2878.865 100.00 100.00

Chromeleon (c) Dionex

CANNABIS DAD/Integration Version 7.2.9.11323

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Instrument:EQA_073 Sequence:cannabis 06062020

Chromatogram and Results

Injection Details
Injection Name: STD 80PPM Run Time (min): 33.00
Vial Number: GA3 Injection Volume: 20.00
Injection Type: Calibration Standard Channel: UV_VIS_1
Calibration Level: 3 Wavelength: 270
Instrument Method: THC-THCa-CBD-CBDa Col3um Bandwidth: 4
Processing Method: Basic Quantitative Dilution Factor: 1.0000
Injection Date/Time: 05/jun/20 17:47 Sample Weight: 1.0000

Chromatogram

Integration Results
No. Peak Name Retention Time Area Height Relative Area Relative Height Amount
min mAU*min mAU % %
1 CBD 11.213 1273.696 6053.012 50.46 53.35 0.0818
2 THC 15.437 1250.390 5292.734 49.54 46.65 0.0796
Total: 2524.086 11345.746 100.00 100.00
No. Peak Name Retention Time Area Height Relative Area Relative Height Amount
min mAU*min mAU % %
1 CBDa 7.310 587.841 2564.936 49.51 46.90 0.0793
2 THCa 11.787 599.559 2903.564 50.49 53.10 0.0791
Total: 1187.400 5468.500 100.00 100.00

Chromeleon (c) Dionex

CANNABIS DAD/Integration Version 7.2.9.11323

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Instrument:EQA_073 Sequence:cannabis 06062020

Chromatogram and Results

Injection Details
Injection Name: STD 100PPM Run Time (min): 33.00
Vial Number: GA4 Injection Volume: 20.00
Injection Type: Calibration Standard Channel: UV_VIS_1
Calibration Level: 4 Wavelength: 270
Instrument Method: THC-THCa-CBD-CBDa Col3um Bandwidth: 4
Processing Method: Basic Quantitative Dilution Factor: 1.0000
Injection Date/Time: 05/jun/20 18:20 Sample Weight: 1.0000

Chromatogram

Integration Results
No. Peak Name Retention Time Area Height Relative Area Relative Height Amount
min mAU*min mAU % %
1 CBD 11.183 1493.970 6697.157 50.06 51.92 0.0961
2 THC 15.413 1490.340 6201.440 49.94 48.08 0.0949
Total: 2984.310 12898.597 100.00 100.00
No. Peak Name Retention Time Area Height Relative Area Relative Height Amount
min mAU*min mAU % %
1 CBDa 7.317 696.935 2384.138 49.51 42.69 0.0940
2 THCa 11.750 710.699 3200.356 50.49 57.31 0.0938
Total: 1407.634 5584.494 100.00 100.00

Chromeleon (c) Dionex

CANNABIS DAD/Integration Version 7.2.9.11323

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Chromatogram and Results

Injection Details
Injection Name: STD 2PPM Run Time (min): 33.00
Vial Number: GA1 Injection Volume: 20.00
Injection Type: Calibration Standard Channel: UV_VIS_1
Calibration Level: 1 Wavelength: 270
Instrument Method: THC-THCa-CBD-CBDa Col3um Bandwidth: 4
Processing Method: Basic Quantitative Dilution Factor: 1.0000
Injection Date/Time: 06/jun/20 06:45 Sample Weight: 1.0000

Chromatogram

Integration Results
No. Peak Name Retention Time Area Height Relative Area Relative Height Amount
min mAU*min mAU % %
1 CBDa 7.267 82.984 480.461 51.12 57.00 0.0024
2 CBD 11.117 40.739 199.721 25.10 23.70 0.0021
3 THC 15.290 38.596 162.674 23.78 19.30 0.0022
Total: 162.319 842.857 100.00 100.00
No. Peak Name Retention Time Area Height Relative Area Relative Height Amount
min mAU*min mAU % %
1 CBDa 7.270 19.245 108.811 49.22 52.68 0.0023
2 THCa 11.663 19.852 97.744 50.78 47.32 0.0023
Total: 39.097 206.555 100.00 100.00

Chromeleon (c) Dionex

CANNABIS DAD/Integration Version 7.2.9.11323

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Instrument:EQA_073 Sequence:cannabis 06062020

Chromatogram and Results

Injection Details
Injection Name: STD 40PPM Run Time (min): 33.00
Vial Number: GA2 Injection Volume: 20.00
Injection Type: Calibration Standard Channel: UV_VIS_1
Calibration Level: 2 Wavelength: 270
Instrument Method: THC-THCa-CBD-CBDa Col3um Bandwidth: 4
Processing Method: Basic Quantitative Dilution Factor: 1.0000
Injection Date/Time: 06/jun/20 07:19 Sample Weight: 1.0000

Chromatogram

Integration Results
No. Peak Name Retention Time Area Height Relative Area Relative Height Amount
min mAU*min mAU % %
1 CBDa 7.243 1205.478 6113.688 49.80 52.76 0.0396
2 CBD 11.120 614.299 2952.616 25.38 25.48 0.0392
3 THC 15.310 600.699 2520.511 24.82 21.75 0.0381
Total: 2420.476 11586.815 100.00 100.00
No. Peak Name Retention Time Area Height Relative Area Relative Height Amount
min mAU*min mAU % %
1 CBDa 7.243 280.632 1406.977 49.38 49.84 0.0377
2 THCa 11.673 287.661 1415.819 50.62 50.16 0.0378
Total: 568.294 2822.796 100.00 100.00

Chromeleon (c) Dionex

CANNABIS DAD/Integration Version 7.2.9.11323

Informe muestra nro. 9604.Página 8 de 27

Instrument:EQA_073 Sequence:cannabis 06062020

Chromatogram and Results

Injection Details
Injection Name: STD 80PPM Run Time (min): 33.00
Vial Number: GA3 Injection Volume: 20.00
Injection Type: Calibration Standard Channel: UV_VIS_1
Calibration Level: 3 Wavelength: 270
Instrument Method: THC-THCa-CBD-CBDa Col3um Bandwidth: 4
Processing Method: Basic Quantitative Dilution Factor: 1.0000
Injection Date/Time: 06/jun/20 07:53 Sample Weight: 1.0000

Chromatogram

Integration Results
No. Peak Name Retention Time Area Height Relative Area Relative Height Amount
min mAU*min mAU % %
1 CBD 11.090 1320.625 6181.984 50.16 53.15 0.0849
2 THC 15.280 1312.188 5448.585 49.84 46.85 0.0835
Total: 2632.813 11630.569 100.00 100.00
No. Peak Name Retention Time Area Height Relative Area Relative Height Amount
min mAU*min mAU % %
1 CBDa 7.190 608.685 2667.071 49.66 47.50 0.0821
2 THCa 11.633 617.141 2947.359 50.34 52.50 0.0814
Total: 1225.826 5614.430 100.00 100.00

Chromeleon (c) Dionex

CANNABIS DAD/Integration Version 7.2.9.11323

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Instrument:EQA_073 Sequence:cannabis 06062020

Chromatogram and Results

Injection Details
Injection Name: STD 100PPM Run Time (min): 33.00
Vial Number: GA4 Injection Volume: 20.00
Injection Type: Calibration Standard Channel: UV_VIS_1
Calibration Level: 4 Wavelength: 270
Instrument Method: THC-THCa-CBD-CBDa Col3um Bandwidth: 4
Processing Method: Basic Quantitative Dilution Factor: 1.0000
Injection Date/Time: 06/jun/20 08:27 Sample Weight: 1.0000

Chromatogram

Integration Results
No. Peak Name Retention Time Area Height Relative Area Relative Height Amount
min mAU*min mAU % %
1 CBD 11.067 1545.134 6853.890 49.91 51.76 0.0994
2 THC 15.263 1550.558 6388.681 50.09 48.24 0.0987
Total: 3095.692 13242.571 100.00 100.00
No. Peak Name Retention Time Area Height Relative Area Relative Height Amount
min mAU*min mAU % %
1 CBDa 7.190 720.036 2467.427 49.64 43.28 0.0972
2 THCa 11.603 730.445 3233.035 50.36 56.72 0.0964
Total: 1450.481 5700.462 100.00 100.00

Chromeleon (c) Dionex

CANNABIS DAD/Integration Version 7.2.9.11323

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Instrument:EQA_073 Sequence:cannabis 06062020

Chromatogram and Results

Injection Details
Injection Name: BLANCO Run Time (min): 33.00
Vial Number: GA5 Injection Volume: 20.00
Injection Type: Unknown Channel: UV_VIS_1
Calibration Level: Wavelength: 270
Instrument Method: THC-THCa-CBD-CBDa Col3um Bandwidth: 4
Processing Method: Basic Quantitative Dilution Factor: 1.0000
Injection Date/Time: 06/jun/20 09:01 Sample Weight: 1.0000

Chromatogram

Integration Results
No. Peak Name Retention Time Area Height Relative Area Relative Height Amount
min mAU*min mAU % % n.a.
Total: 0.000 0.000 0.00 0.00
No. Peak Name Retention Time Area Height Relative Area Relative Height Amount
min mAU*min mAU % % n.a.
Total: 0.000 0.000 0.00 0.00

Chromeleon (c) Dionex

CANNABIS DAD/Integration Version 7.2.9.11323

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Instrument:EQA_073 Sequence:cannabis 06062020

Chromatogram and Results

Injection Details
Injection Name: E1-1 9604 Run Time (min): 33.00
Vial Number: GB8 Injection Volume: 20.00
Injection Type: Unknown Channel: UV_VIS_1
Calibration Level: Wavelength: 270
Instrument Method: THC-THCa-CBD-CBDa Col3um Bandwidth: 4
Processing Method: Basic Quantitative Dilution Factor: 1150.1656
Injection Date/Time: 06/jun/20 09:34 Sample Weight: 1.0000

Chromatogram

Integration Results
No. Peak Name Retention Time Area Height Relative Area Relative Height Amount
min mAU*min mAU % %
1 CBD 11.107 165.943 792.732 87.06 88.45 11.7634
2 THC 15.263 24.659 103.515 12.94 11.55 1.4934
Total: 190.602 896.248 100.00 100.00
No. Peak Name Retention Time Area Height Relative Area Relative Height Amount
min mAU*min mAU % %
1 CBDa 7.227 231.055 1208.827 94.52 94.55 35.5941
2 THCa 11.643 13.403 69.616 5.48 5.45 1.6636
Total: 244.457 1278.443 100.00 100.00

Chromeleon (c) Dionex

CANNABIS DAD/Integration Version 7.2.9.11323

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Instrument:EQA_073 Sequence:cannabis 06062020

Chromatogram and Results

Injection Details
Injection Name: E1-2 9604 Run Time (min): 33.00
Vial Number: GB8 Injection Volume: 20.00
Injection Type: Unknown Channel: UV_VIS_1
Calibration Level: Wavelength: 270
Instrument Method: THC-THCa-CBD-CBDa Col3um Bandwidth: 4
Processing Method: Basic Quantitative Dilution Factor: 1150.1656
Injection Date/Time: 06/jun/20 10:08 Sample Weight: 1.0000

Chromatogram

Integration Results
No. Peak Name Retention Time Area Height Relative Area Relative Height Amount
min mAU*min mAU % %
1 CBD 11.103 168.853 799.861 87.41 88.53 11.9797
2 THC 15.260 24.331 103.599 12.59 11.47 1.4693
Total: 193.184 903.459 100.00 100.00
No. Peak Name Retention Time Area Height Relative Area Relative Height Amount
min mAU*min mAU % %
1 CBDa 7.223 230.948 1208.865 94.51 94.58 35.5775
2 THCa 11.640 13.423 69.279 5.49 5.42 1.6666
Total: 244.371 1278.145 100.00 100.00

Chromeleon (c) Dionex

CANNABIS DAD/Integration Version 7.2.9.11323

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Instrument:EQA_073 Sequence:cannabis 06062020

Chromatogram and Results

Injection Details
Injection Name: E2-1 9604 Run Time (min): 33.00
Vial Number: GC1 Injection Volume: 20.00
Injection Type: Unknown Channel: UV_VIS_1
Calibration Level: Wavelength: 270
Instrument Method: THC-THCa-CBD-CBDa Col3um Bandwidth: 4
Processing Method: Basic Quantitative Dilution Factor: 1167.6786
Injection Date/Time: 06/jun/20 10:42 Sample Weight: 1.0000

Chromatogram

Integration Results
No. Peak Name Retention Time Area Height Relative Area Relative Height Amount
min mAU*min mAU % %
1 CBD 11.103 161.009 734.401 87.18 100.00 11.5700
2 THC 14.997 23.670 0.000 12.82 0.00 1.4424
Total: 184.680 734.401 100.00 100.00
No. Peak Name Retention Time Area Height Relative Area Relative Height Amount
min mAU*min mAU % %
1 CBDa 7.223 238.702 1253.039 94.38 94.33 37.3454
2 THCa 11.637 14.220 75.386 5.62 5.67 1.8153
Total: 252.922 1328.425 100.00 100.00

Chromeleon (c) Dionex

CANNABIS DAD/Integration Version 7.2.9.11323

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Instrument:EQA_073 Sequence:cannabis 06062020

Chromatogram and Results

Injection Details
Injection Name: E2-2 9604 Run Time (min): 33.00
Vial Number: GC1 Injection Volume: 20.00
Injection Type: Unknown Channel: UV_VIS_1
Calibration Level: Wavelength: 270
Instrument Method: THC-THCa-CBD-CBDa Col3um Bandwidth: 4
Processing Method: Basic Quantitative Dilution Factor: 1167.6786
Injection Date/Time: 06/jun/20 11:16 Sample Weight: 1.0000

Chromatogram

Integration Results
No. Peak Name Retention Time Area Height Relative Area Relative Height Amount
min mAU*min mAU % %
1 CBD 11.100 158.916 732.163 87.19 100.00 11.4120
2 THC 14.993 23.348 0.000 12.81 0.00 1.4183
Total: 182.263 732.163 100.00 100.00
No. Peak Name Retention Time Area Height Relative Area Relative Height Amount
min mAU*min mAU % %
1 CBDa 7.220 238.830 1252.942 94.40 94.33 37.3655
2 THCa 11.633 14.165 75.301 5.60 5.67 1.8068
Total: 252.994 1328.243 100.00 100.00

Chromeleon (c) Dionex

CANNABIS DAD/Integration Version 7.2.9.11323

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Instrument:EQA_073 Sequence:cannabis 06062020

Chromatogram and Results

Injection Details
Injection Name: STD 2PPM Run Time (min): 33.00
Vial Number: GA1 Injection Volume: 20.00
Injection Type: Calibration Standard Channel: UV_VIS_1
Calibration Level: 1 Wavelength: 270
Instrument Method: THC-THCa-CBD-CBDa Col3um Bandwidth: 4
Processing Method: Basic Quantitative Dilution Factor: 1.0000
Injection Date/Time: 06/jun/20 20:52 Sample Weight: 1.0000

Chromatogram

Integration Results
No. Peak Name Retention Time Area Height Relative Area Relative Height Amount
min mAU*min mAU % %
1 CBD 11.063 49.111 243.782 52.02 55.24 0.0027
2 THC 15.227 45.294 197.520 47.98 44.76 0.0026
Total: 94.405 441.302 100.00 100.00
No. Peak Name Retention Time Area Height Relative Area Relative Height Amount
min mAU*min mAU % %
1 CBDa 7.233 22.723 133.403 49.18 52.97 0.0027
2 THCa 11.603 23.481 118.420 50.82 47.03 0.0028
Total: 46.204 251.823 100.00 100.00

Chromeleon (c) Dionex

CANNABIS DAD/Integration Version 7.2.9.11323

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Instrument:EQA_073 Sequence:cannabis 06062020

Chromatogram and Results

Injection Details
Injection Name: STD 40PPM Run Time (min): 33.00
Vial Number: GA2 Injection Volume: 20.00
Injection Type: Calibration Standard Channel: UV_VIS_1
Calibration Level: 2 Wavelength: 270
Instrument Method: THC-THCa-CBD-CBDa Col3um Bandwidth: 4
Processing Method: Basic Quantitative Dilution Factor: 1.0000
Injection Date/Time: 06/jun/20 21:25 Sample Weight: 1.0000

Chromatogram

Integration Results
No. Peak Name Retention Time Area Height Relative Area Relative Height Amount
min mAU*min mAU % %
1 CBD 11.050 626.505 3080.838 50.09 53.79 0.0400
2 THC 15.227 624.236 2646.488 49.91 46.21 0.0396
Total: 1250.741 5727.326 100.00 100.00
No. Peak Name Retention Time Area Height Relative Area Relative Height Amount
min mAU*min mAU % %
1 CBDa 7.183 285.855 1461.805 49.46 49.86 0.0384
2 THCa 11.583 292.046 1469.783 50.54 50.14 0.0384
Total: 577.901 2931.587 100.00 100.00

Chromeleon (c) Dionex

CANNABIS DAD/Integration Version 7.2.9.11323

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Instrument:EQA_073 Sequence:cannabis 06062020

Chromatogram and Results

Injection Details
Injection Name: STD 80PPM Run Time (min): 33.00
Vial Number: GA3 Injection Volume: 20.00
Injection Type: Calibration Standard Channel: UV_VIS_1
Calibration Level: 3 Wavelength: 270
Instrument Method: THC-THCa-CBD-CBDa Col3um Bandwidth: 4
Processing Method: Basic Quantitative Dilution Factor: 1.0000
Injection Date/Time: 06/jun/20 21:59 Sample Weight: 1.0000

Chromatogram

Integration Results
No. Peak Name Retention Time Area Height Relative Area Relative Height Amount
min mAU*min mAU % % n.a.
Total: 0.000 0.000 0.00 0.00
No. Peak Name Retention Time Area Height Relative Area Relative Height Amount
min mAU*min mAU % %
1 CBDa 7.157 645.433 2970.486 49.61 48.05 0.0871
2 THCa 11.573 655.618 3211.757 50.39 51.95 0.0865
Total: 1301.051 6182.243 100.00 100.00

Chromeleon (c) Dionex

CANNABIS DAD/Integration Version 7.2.9.11323

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Instrument:EQA_073 Sequence:cannabis 06062020

Summary
Sequence Details
Name: cannabis 06062020 Created On: 05/jun/20 16:06:01
Directory: Instrument Data\EQA_073\Secuencia Created By: nh
Data Vault: ChromeleonLocal Updated On: 11/jun/20 14:58:19
No. of Injections: 72 Updated By: nh

By Component CBD
No. Injection Name Ret.Time Area Height Amount % Average amount RSD
min mAU*min mAU % %
UV_VIS_1 UV_VIS_1 UV_VIS_1 UV_VIS_1 UV_VIS_1 UV_VIS_1
CBD CBD CBD CBD CBD CBD
31 E1-1 9604 11.107 165.9432461 792.732 11.763 11.681 2.10
32 E1-2 9604 11.103 168.8529879 799.861 11.980
33 E2-1 9604 11.103 161.0092325 734.401 11.570
34 E2-2 9604 11.100 158.916 732.163 11.412

By Component CBDa
No. Injection Name Ret.Time Area Height Amount Average amount RSD
min mAU*min mAU % %
UV_VIS_2 UV_VIS_2 UV_VIS_2 UV_VIS_2 UV_VIS_2 UV_VIS_2
CBDa CBDa CBDa CBDa CBDa CBDa
31 E1-1 9604 7.227 231.0547026 1208.827 35.594 36.471 2.80
32 E1-2 9604 7.223 230.9479622 1208.865 35.577
33 E2-1 9604 7.223 238.7023785 1253.039 37.345
34 E2-2 9604 7.220 238.830 1252.942 37.366

By Component THC
No. Injection Name Ret.Time Area Height Amount Average amount RSD
min mAU*min mAU % %
UV_VIS_1 UV_VIS_1 UV_VIS_1 UV_VIS_1 UV_VIS_1 UV_VIS_1
THC THC THC THC THC THC
31 E1-1 9604 15.263 24.65896837 103.515 1.493 1.46 2.23
32 E1-2 9604 15.260 24.33072743 103.599 1.469
33 E2-1 9604 14.997 23.6704107 0.000 1.442
34 E2-2 9604 14.993 23.348 0.000 1.418

By Component THCa
No. Injection Name Ret.Time Area Height Amount Average amount RSD
min mAU*min mAU % %
UV_VIS_2 UV_VIS_2 UV_VIS_2 UV_VIS_2 UV_VIS_2 UV_VIS_2
THCa THCa THCa THCa THCa THCa
31 E1-1 9604 11.643 13.40272127 69.616 1.664 1.74 4.85
32 E1-2 9604 11.640 13.42269744 69.279 1.667
33 E2-1 9604 11.637 14.21953643 75.386 1.815
34 E2-2 9604 11.633 14.165 75.301 1.807

TOTAL
PPS(%) Component TOTAL % TOTAL (B.S) Component TOTAL % TOTAL (B.S)
9604 - CBDs 43.666 - THCs 2.98 -

Chromeleon (c) Dionex

CANNABIS DAD/Summary Version 7.2.9.11323

Informe muestra nro. 9604.Página 19 de 27

SpectrAA Report. 2:38 PM 6/22/2020 Page 1 of 2
Analyst
Date Started 12:45 PM 6/22/2020 GMT: 3:45 PM 6/22/2020
Worksheet Pb Cd 22062020
Comm ent
Methods Pb,Cd
Computer nam e AA-HP
Serial Num ber:
Nominal Weight = 1.0000 Nominal Volume = 1.0000

Method: Cd (Flam e)

Elem ent - Matrix: Cd -

Instrum ent Type: Flame
Conc. Units: mg/L
Instrum ent Mode: Absorbance
Sam pling Mode: Manual
Calibration Mode: Concentration
Measurem ent Mode: Integrate
Replicates Standard: 3
Replicates Sam ple: 2

Expansion Factor: 1.0

Minimum Reading: Disabled
Smoothing: 7 point
Conc. Dec. Places: 3

Wavelength: 228.8 nm
Slit Width: 0.5 nm
Gain: 63 %
Lam p Current: 5.0 mA
Lam p Position: 2
Background Correction: BC On

STANDARD 1: 0.011 mg/L

STANDARD 2: 0.102 mg/L
STANDARD 3: 1.023 mg/L
Reslope Rate: 50
Reslope Standard No.: 2
Reslope Low er Lim it: 75.0 %
Reslope Upper Lim it: 125.0 %
Recalibration Rate: 100
Calibration Algorithm : Linear
Cal. Low er Limit: 20.0 %
Cal. Upper Lim it: 150.0 %
SIPS: Off

Measurem ent Tim e: 2.0 s

Pre-Read Delay: 2s
Flame Type: Air/Acetylene
Air Flow : 10.00 L/min
Acetylene Flow : 2.00 L/min
Burner Height: 0.0 mm

Sample ID Conc mg/L SD Mean Abs Weight Volume

CAL ZERO 0.000 0.0008 -0.0008 1.0000 1.0000

STANDARD 1 -----e -----e 1.0000 1.0000

Informe muestra nro. 9604.Página 20 de 27

 SpectrAA Report. 2:38 PM 6/22/2020 Page 2 of 2

STANDARD 2 0.102 0.0005 0.0367 1.0000 1.0000

STANDARD 3 1.023 0.0040 0.3802 1.0000 1.0000

Abs Linear - Cal. Set 1

0.38

0.30

0.20

0.10
0.00
0.000 0.500 1.023
Cd mg/L

Curve Fit = Linear

Characteristic Conc = 0.014 mg/L
r = 1.0000
Calculated Conc = 0.000 0.101 1.024
Residuals = 0.000 0.000 0.000

Abs = 0.37241 x C - 0.00098

BI52 0.182 0.0005 0.0028 0.5523 10.000
User-entered Dilution
1.0000
9604 -0.082 0.0002 -0.0025 0.4960 10.000
User-entered Dilution
1.0000

Informe muestra nro. 9604.Página 21 de 27

SpectrAA Report. 2:35 PM 6/22/2020 Page 1 of 2
Analyst
Date Started 12:45 PM 6/22/2020 GMT: 3:45 PM 6/22/2020
Worksheet Pb Cd 22062020
Comm ent
Methods Pb,Cd
Computer nam e AA-HP
Serial Num ber:
Nominal Weight = 1.0000 Nominal Volume = 1.0000

Method: Pb (Flame)

Elem ent - Matrix: Pb -

Instrum ent Type: Flame
Conc. Units: mg/L
Instrum ent Mode: Absorbance
Sam pling Mode: Manual
Calibration Mode: Concentration
Measurem ent Mode: Integrate
Replicates Standard: 3
Replicates Sam ple: 2

Expansion Factor: 1.0

Minimum Reading: Disabled
Smoothing: 7 point
Conc. Dec. Places: 2

Wavelength: 217.0 nm
Slit Width: 1.0 nm
Gain: 68 %
Lam p Current: 5.0 mA
Lam p Position: 2
Background Correction: BC On

STANDARD 1: 0.20 mg/L

STANDARD 2: 1.98 mg/L
STANDARD 3: 5.91 mg/L
Reslope Rate: 50
Reslope Standard No.: 2
Reslope Low er Lim it: 75.0 %
Reslope Upper Lim it: 125.0 %
Recalibration Rate: 100
Calibration Algorithm : Linear
Cal. Low er Limit: 20.0 %
Cal. Upper Lim it: 150.0 %
SIPS: Off

Measurem ent Tim e: 2.0 s

Pre-Read Delay: 2s
Flame Type: Air/Acetylene
Air Flow : 10.00 L/min
Acetylene Flow : 2.00 L/min
Burner Height: 0.0 mm

Sample ID Conc mg/L SD Mean Abs Weight Volume

CAL ZERO 0.00 0.0006 -0.0002 1.0000 1.0000

STANDARD 1 0.20 0.0005 0.0085 1.0000 1.0000

Informe muestra nro. 9604.Página 22 de 27

 SpectrAA Report. 2:35 PM 6/22/2020 Page 2 of 2

STANDARD 2 1.98 0.0011 0.0770 1.0000 1.0000

STANDARD 3 5.91 0.0042 0.2168 1.0000 1.0000

Abs Linear - Cal. Set 2

0.22

0.15

0.10

0.00
0.00 2.00 4.00 5.91
Pb mg/L

Curve Fit = Linear

Characteristic Conc = 0.08 mg/L
r = 0.9998
Calculated Conc = -0.05 0.19 2.06 5.88
Residuals = 0.05 0.01 -0.08 0.03

Abs = 0.03662 x C + 0.00151

9604 0.47 0.0009 0.0024 0.4960 10.000
User-entered Dilution
1.0000
9681 0.00 0.0004 0.0017 100.00 10.000
User-entered Dilution
1.0000

Informe muestra nro. 9604.Página 23 de 27

SpectrAA Report. 8:50 AM 6/23/2020 Page 1 of 2
Analyst
Date Started 11:11 AM 6/19/2020 GMT: 2:11 PM 6/19/2020
Worksheet Arsenico 19062020
Comm ent
Methods As
Computer nam e AA-HP
Serial Num ber:
Nominal Weight = 1.0000 Nominal Volume = 1.0000

Method: As (Vapor)

Elem ent - Matrix: As -

Instrum ent Type: Vapor
Conc. Units: ug/L

Sam pling Mode: AutoMix

Calibration Mode: Concentration
Measurem ent Mode: Peak Height
Replicates Standard: 3
Replicates Sam ple: 3

Expansion Factor: 1.0

Minimum Reading: Disabled
Smoothing: 7 point
Conc. Dec. Places: 3

Wavelength: 193.7 nm
Slit Width: 0.5 nm
Gain: 69 %
Lam p Current: 10.0 mA
Lam p Position: 1
Background Correction: BC On

STANDARD 1: 1.960 ug/L

STANDARD 2: 3.906 ug/L
STANDARD 3: 9.798 ug/L
Reslope Rate: 50
Reslope Standard No.: 2
Reslope Low er Lim it: 75.0 %
Reslope Upper Lim it: 125.0 %
Recalibration Rate: 100
Calibration Algorithm : Linear
Cal. Low er Limit: 20.0 %
Cal. Upper Lim it: 150.0 %

Measurem ent Tim e: 5.0 s

Pre-Read Delay: 45 s
Vapor Type: Air/Acetylene
Air Flow : 10.00 L/min
Acetylene Flow : 2.10 L/min
Burner Height: 0.0 mm

Sample ID Conc ug/L SD Mean Abs Weight Volume

CAL ZERO 0.000 0.0025 0.0053 1.0000 1.0000

STANDARD 1 -----e -----e 1.0000 1.0000

Informe muestra nro. 9604.Página 24 de 27

 SpectrAA Report. 8:50 AM 6/23/2020 Page 2 of 2

STANDARD 2 -----e -----e 1.0000 1.0000

STANDARD 3 9.798 0.0019 0.0545 1.0000 1.0000

Abs Linear - Cal. Set 2

0.07
0.06

0.04

0.02
0.00
0.000 2.000 4.000 6.000 8.000 9.798
As ug/L

Curve Fit = Linear

Characteristic Conc = -0.187 ug/L
r = 1.0000
Calculated Conc = 0.000 9.798
Residuals = 0.000 0.000

Abs = 0.00502 x C + 0.00534

9604 143.752 0.0017 0.0125 0.4960 10.000
User-entered Dilution
5.0000

Informe muestra nro. 9604.Página 25 de 27

SpectrAA Report. 8:50 AM 6/23/2020 Page 1 of 2
Analyst
Date Started 1:35 PM 6/19/2020 GMT: 4:35 PM 6/19/2020
Worksheet Hg 1
Comm ent
Methods Hg
Computer nam e AA-HP
Serial Num ber:
Nominal Weight = 1.0000 Nominal Volume = 1.0000

Method: Hg (Vapor)

Elem ent - Matrix: Hg -

Instrum ent Type: Vapor
Conc. Units: ug/L

Sam pling Mode: AutoMix

Calibration Mode: Concentration
Measurem ent Mode: Peak Height
Replicates Standard: 5
Replicates Sam ple: 2

Expansion Factor: 1.0

Minimum Reading: Disabled
Smoothing: 7 point
Conc. Dec. Places: 2

Wavelength: 253.7 nm
Slit Width: 0.5 nm
Gain: 43 %
Lam p Current: 4.0 mA
Lam p Position: 1
Background Correction: BC Off

STANDARD 1: 2.11 ug/L

STANDARD 2: 5.34 ug/L
STANDARD 3: 12.21 ug/L
Reslope Rate: 50
Reslope Standard No.: 2
Reslope Low er Lim it: 75.0 %
Reslope Upper Lim it: 125.0 %
Recalibration Rate: 100
Calibration Algorithm : Linear
Cal. Low er Limit: 20.0 %
Cal. Upper Lim it: 150.0 %

Measurem ent Tim e: 2.0 s

Pre-Read Delay: 100 s
Vapor Type: Cold Vapor

Burner Height: 0.0 mm

Sample ID Conc ug/L SD Mean Abs Weight Volume

CAL ZERO 0.00 0.0008 -0.0003 1.0000 1.0000

STANDARD 1 ----- -----e 1.0000 1.0000

Informe muestra nro. 9604.Página 26 de 27

 SpectrAA Report. 8:50 AM 6/23/2020 Page 2 of 2

STANDARD 2 ----- -----e 1.0000 1.0000

STANDARD 3 12.21 0.0028 0.0725 1.0000 1.0000

Abs Linear - Cal. Set 3

0.07
0.06

0.04

0.02
0.00
0.00 5.00 10.00 12.21
Hg ug/L

Curve Fit = Linear

Characteristic Conc = 0.79 ug/L
r = 1.0000
Calculated Conc = 0.00 12.21
Residuals = 0.00 0.00

Abs = 0.00596 x C - 0.00029

9604 -0.96 0.0001 -0.0060 1.0000 1.0000
User-entered Dilution
1.0000

Informe muestra nro. 9604.Página 27 de 27