7.2.

13
i
AOAC Official Surplus Method 920.23i
Zinc Aresnite
Pesticide Formulations

Total Arsenious Oxide

Final action
Surplus 1965

4.051, 10th ed.

Method I. (17)

(a) Weigh 2 g sample and transfer to beaker.

Dissolve in 80 mL HCl (1 + 4), wash into 200 mL vol.
flask, and dil. to vol. Thoroly mix soln and filter thru
dry filter. Transfer 25 mL aliquot to 500 mL
erlenmeyer, add 20 mL HCl, and dil. to 100 mL. Heat
to 90E and titr. with std KBrO3 soln, 922.03(c) (See
7.1.05). Or,
(b) Proceed as in (a) without heating soln.

4.052, 10th ed.

Method II.

Proceed as in 4.029, using appropriate Zn salt, ZnCl2

or ZuSO4, for blank detn.

Reference: J. Assoc. Offic. Agr. Chemits 5, 33(1921);

392(1922)

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