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Test Kits for Lubricating Oils
Instruction Manual
Interpreting Results
Water in Oil Test
TBN Test
Salt Water Determination
Insolubles Loading
Viscosity Test
TAN Test
Parker ee ENGINEERING YOUR SUCCESS.
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Viscosity Comparison
Take samples of used and new oil
and allow to stand for at least 1 hour.
It is very important that both
samples are at the same
temperature.
Place the Viscosity Stick on a flat,
level surface.
Add 5ml of used oil to one reservoir.
Add 5ml of new oil to the other
reservoir.
Tilt the Viscosity Stick so that it rests on the angled base
and allow the oil to run down the channels. When the
new oil reaches the mid point on the scale, return the
Viscosity Stick to the horizontal.
MA-K15685-KW Issue 1
Scanned with CamScannerExamine the point reached by the used oil:
If the used oil has not reached the scale then the
viscosity is higher than recommended.
If the used oil has over run the scale then
the viscosity
is lower than recommended.
New oil
Used oil
Used oil viscosity high.
Scanned with CamScannerSalt Water Determination
MA-K15686-KW Issue 1
Add 2ml of Reagent H to the test tube.
Shake the oil sample and draw off 5ml
using the syringe provided. Add this to
the test tube, replace the cap and
shake vigorously.
Place the tube upright in hot water
and allow to stand for 1 hour until the
water settles out of the oil sample.
Take one test pad from the box and
replace the lid. Handle the test pads
by the edges to avoid contaminating
the surfaces with sweat.
Puncture an area 10mm in diameter
10 to 15 times with the pin provided.
Flush a pipette with Reagent H.
Place the tip in the water layer in the
test tube.
Squeeze the bulb gently and draw
off a sample of the water into the
pipette.
Scanned with CamScannerB Remove the pipette and wipe off any
oil and return a few drops of water
to the test tube.
Place the next drop of water onto
the prepared test pad.
oo Allow the pad to stand for 5 minutes.
Examine the pad:
If there is no yellow colour, or
only a very faint yellow patch
appears, the contamination is
fresh water.
If a large yellow patch
appears, the contamination is
salt water.
6 | A positive result should always be checked by testing
another pad.
Scanned with CamScannerReset
Control
Screen Button
Battery guaranteed
for 5 years Buttons to
(or 5000 tests). action screen
options
Press Right hand button to switch cell on.
Cell will auto power off after 6 minutes inactivity.
Press TBN to switch between WATER/TBN mode.
Select oil desired for test by pressing OIL.
If oil is not found, or if you have a new oil, follow
TBN Setup instructions on previous page.
TBN TEST TBN TEST
Name=Oil Type 1 Name=Oil Type 2
New TBN=46 New TBN=42 Name=Oil Type 1
Last TBN=27.3 Last TBN=24.9 TBN is relative
WATER OIL NEXT] |WATER OIL NEXT to new oil
NEW-test new oil
LLY’ JY, RRS NeW.
BACK NEW NEXT
=
Press NEXT to continue
MA-K16800-KW Issue 3
Scanned with CamScannerBefore starting the test:
Make sure the inside of the cell is clean and dry
(pay particular attention to the seal).
Begin test by following on screen instructions.
Name=Oil Type 1 NB: Use TBN Reagent C. The
4)Add reagent to amount of oil used changes with
lowerline the new oil TBN range.
2)Add XXml oil
3)Replace lid
BACK START|P
Replace lid and press START to begin test.
Please make sure that you use the correct amount of reagent
and oil. Failure to do this could cause the cell to become
over-pressured and damaged.
s 4
Scanned with CamScannera 6 |
sie cell To cancel the test
until graph
ha hed CANCEL for
seconds.
CANCEL - hold 5 sec
45
31 :
= Agraph will be plotted during the
test time (120 seconds).
—= .
CANCEL - hold 5 sec
Name=Oil Type 1 Yo i i
id ur results will be displayed after
New EN the graph has been plotted.
Used TBN = 36
NEXT|P> Press NEXT to return to first screen.
After finishing the test:
Immediately after every test, thoroughly clean the cell paying
particular attention to the O ring and sealing faces, there should
be no reagent residue left in these areas. Where applicable, the
agitator will also require cleaning. Use a lint-free rag or tissue
and a mild solvent (e.g. Reagent A or IPA).
Do not use water or water based cleaners!
MA-K16800-KW Issue 3
Scanned with CamScannerTest Kits, Spares and Reagents
Code
FG-K1-001-KW
FG-K1-003-KW
FG-K1-004-KW
FG-K1-007-KW
FG-K1-008-KW
FG-K1-010-KW.
FG-K2-001-KW
FG-K2-002-KW
FG-K2-003-KW
FG-K1-006-KW
FG-K1-005-KW
FG-K24743-KW
FG-K3-020-KW
AS-K13888-KW
AS-K13889-KW
AS-K13890-KW
MA-K12804-KW
MA-K17478-KW Issue 1
Description
DIGI Water Kit
DIGI Basic Kit
DIGI TBN Kit
al Kit
DIGI Industri
DIGI Field Kit
DIGI Combined Kit
Water in Oil Reagent Pack (50)
TBN Reagent Pack (50)
Insolubles Reagent Pack (50)
ECON Insolubles Test (100)
ECON Salt Test (30)
ECON TAN Drop Test Kit (50)
ECON Viscosity Test
Digital Water Cell
(5 year battery)
Digital TBN Cell
(5 year battery)
Digital Water & TBN Cell
(6 year battery)
Fuel & Lube Oil Training CD
Range
0-125, 0-10%, 0-20%.
1-10,000ppm
Water/Visc/Insols/Salt
5-80 TBN
Water/TBN/Visc/Insols
Water/TBN/Visc/Insols/
TAN
Water/TBN/Visc/Insols/
Salt
qualitative
qualitative
0-6 TAN
go/no go
0-1%, 0-10%, 0-20%,
1-10,000ppm
5-80 TBN
5-80 TBN, 0-1%, 0-10%
0-20%, 1-10,000ppm
Scanned with CamScannerTest Kits, Spares and Reagents cont.
Code Description Range
FG-K1-101-KW EasySHIP DIGI Water Kit 0-1%, 0-10%, 0-20%
1-10,000ppm
FG-K1-102-KW EasySHIP DIGI Water kit 0-1%, 0-10%, 0-20%,
1-10,000ppm
FG-K1-103-KW EasySHIP DIGI Basic Kit Water/Visc/Insols/Salt
FG-K1-107-KW. EasySHIP DIGI Industrial Kit Water/TBN/Visc/Insols
FG-K1-109-KW EasySHIP DIGI Industrial Oil Kit Water/TBN/Insols/Visc
FG-K1-110-KW EasySHIP DIGI Combined Kit Water/TBN/Visc/Insols/
Salt
FG-K2-101-KW. EasySHIP Water in Oil
Reagent Pack (50)
( \
Scanned with CamScannerMA-K15687-KW Issue 4
6
Insolubles Loading
Shake the oil sample bottle to mix the
contents and pour a small volume
into the beaker.
Place a clean filter paper on a level
surface.
Dip the acetate rod into the oil and
allow the first drop to return to the
beaker.
Place the second drop onto the paper
and set aside for 24 hours.
Compare the dried spot with the
examples given on the page below.
Scanned with CamScannerInsolubles % wiw approx.
Light (<0-1) Medium (1-2) Heavy (>2)
|
>
Insolubles
This is indicated by the shade of the spot. A very dark spot
indicates a heavy insolubles loading. If the dispersency is
poor, only the centre of the spot will be dark.
Poor (<1)
Dispersency TBN - mg.KOH approx.
Moderate (1-2)
Good (>5)
Dispersency
This is indicated by the colour change from the centre to
outside of the spot. A distinct colour change indicates
reduced dispersency. (Low TBN is also an indication of
reduced dispersency).
Scanned with CamScannerWater in Oil Test
Control Reset
Screen Button
Battery guaranteed
for 5 years Buttons to
(or 5000 tests). action screen
options
Press Right hand button to switch cell on.
Cell will auto power off after 6 minutes inactivity.
Press WATER to switch between WATER/TBN mode.
Press RANGE to change the required range of the test.
Four test ranges are available:
WATER TEST Range 0 - 10%
Range 0.02 - 1.0%
AERIEST Range 200 - 10,000ppm
IRange=0.02-1.0%
Wseeeaeo oon Range 0 - 20%
ITBN RANGE NEXT| WATER TEST
|Range=200-10,000ppm}
Vv lLast test=000 ‘
TEN RANGE NEXT.
WATER TEST
IRange=0-20%
Last test=0.00%
TEN RANGE NEXT
Press NEXT to continue with chosen range.
SELECTMETHOD | Dregs 1 to run the test with Reagent B Powder or
= Reag B Powder 2 to test with EasySHIP Paste.
l2= EasySHIP Paste
BACK 1 2
Scanned with CamScannerWhen using EasySHIP Paste
Before starting the test: make sure that the inside of the cell is
clean and dry (pay particular attention to the seal).
EasySHIP Test Reagent must be above 18°c
Always start the test with the highest range selected, when in
doubt about the approximate amount of water in your test oil.
Overpressure can occur if an oil sample is tested with a very high
water content on the low range 0.02-1% (200-10000ppm).
This can cause permanent damage to the pressure sensor.
Shake the bottle of Reagent A thoroughly.
Begin test by following on screen instructions.
NB: The amount of oil used changes
with the range. Always use 20ml
Reagent A (or up to the top line in the
cell).
> Always use gloves when handling
EasySHIP Sachets.
1)Add 20m! ReagA
2)Add All Paste”
3)Add XXml Oil
4)Add Agitator
5)Replace Lid
BACK START
*Squeeze all of the EasySHIP Paste into the centre of the cell
>. LL.
Replace lid and press START to begin test.
Skip next page for the remainder of the EasySHIP test method
@ — yo a
Scanned with CamScannerWhen using Reagent B Powder
Before starting the test: make sure that the inside of the cell is
clean and dry (pay particular attention to the seal).
Always start the test with the highest range selected, when in
doubt about the approximate amount of water in your test oil.
Overpressure can occur if an oil sample is tested with a very high
water content on the low range 0.02-1% (200-10000ppm).
This can cause permanent damage to the pressure sensor.
Shake the bottle of Reagent A thoroughly.
Begin test by following on screen instructions.
NB: The amount of oil used changes
4)Add 20m! ReagA
2)Add XXmi Oil with the range. Always use 20ml
3)Cut ReagB pack Reagent A (or up to the top line in the
4)Place in cell cell).
5)Replace lid
Always use gloves and tweezers
ar
sranu> when handling Reagent B.
BACK
Replace lid and press START to begin test.
Tum page for remainder of test
MA-K17476-KW Issue 3
Scanned with CamScannerShake cell vigorously
until graph To cancel the test
has finished press and hold
CANCEL for 5
CANCEL - hold 5 sec ue
50 Agraph will be plotted during the test
1.47% time
ca (180 seconds for the EasySHIP Test
— and 120 seconds for the Reagent B
CANCEL - hold 5 sec Test).
Test complete Your results will be displayed after
1.52% the graph has been plotted.
Water in Oil
NEXT | > Press NEXT to repeat test.
Please make sure that you use the correct amount of reagent
and oil. Failure to do this could cause the cell to become
over-pressured and damaged.
After finishing the test:
Immediately after every test, thoroughly clean the cell paying
particular attention to the O ring and sealing faces, there should
be no reagent residue left in these areas. Where applicable, the
agitator will also require cleaning. Use a lint-free rag or tissue
and a mild solvent (e.g. Reagent A or IPA).
Do not use water or water based cleaners!
Confidence Test:
Check that the cell is working by conducting a test with no oil
added and add 1 drop of water before starting the test. This
should give a positive result above 0.02%.
l 0 Gq
Scanned with CamScannerTBN Setup
TBN is determined by measuring the pressure build-up in the cell
when a predetermined quantity of oil sample is added to a special
reagent. The amount of sample needed is determined by the cell
measurement processor and is based on the expected TBN.
When using this instrument for the very first time it is necessary to
calibrate it for each of the oil grades to be measured. The cell is
able to hold calibration data for up to seven different oil grades.
The calibration process requires a sample of new oil for each of
the grades to be measured. We recommend you use the oil grade
name as the "Name" during the cell setup process. The cell
should be re-calibrated approximately every six months. The
calibration can be checked by using new oil in the TBN test
procedure, in place of used oil. The ‘test’ TBN should be close to
the new oil TBN.
Press Right hand touch pad to switch cell on.
Cell will auto power off after 6 minutes inactivity.
Press TBN to switch between WATER/TBN mode.
Select the oil to be changed or edited by pressing OIL.
Once oil is selected, press NEXT to continue.
TBN TEST TBN TEST
Name=Oil Type 1
New TBN=46, Name=Oil Type 1
Last TBN=27.3 es TBN is relative
WATER OIL NEXT
to new oil
NEW-test new oil
NEXT-test used
BACK NEW NEXT
v
Press NEW to continue
MA-K15691-KW Issue 1
Scanned with CamScannerPress SETUP, then follow on screen instructions to give
your oil a name and change the new oil's TBN.
NEX
SETI
Name=Oil Type 1
T- calibrate
new oll
UP- change
name/TBN
BACK SETUP NEXT
Vv
EDI
EDIT
Name=Oil Type 1
IT-to change
New TBN=40
TBN-to change
TBN NEXT
v
Vv
NB: This screen only
appears if a new oil
TBN has previously
been entered.
Name=Sil Type 1
UP/DOWN-change
NEXT-move cursor
DOWN UP NEXT
NEXT-to finish
DOWN UP
Name=Oil Type 1
New TBN=H0
UP/DOWN-change
NEXT
Name=Oil Type 1
NEXT- calibrate
new oil
SETUP- change
name/TBN
BACK SETUP NEXT
Press NEXT to
continue.
>
Follow out test instructions as for TBN Test on next page.
Name=Oil Type 1
New TBN=55
Calibrated
>
The cell will confirm calibration after
the graph has been plotted.
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Guide to Interpreting Results
A full laboratory analysis should be considered if any monitored
parameter approaches the relevant limit.
Fuel Oils
Water: <0.1% 0.1-0.25% >0.25% Check centrifuge.
_ Distillate fuel operation, drain ser
tank regularly.
| Water: 20.25% 0.25-0.5% >1.0%
| Residual fuel
ee
Lube Oils
(0.15- ->0.20% Upper limit
0.2% checked against
Sh **-- manufacturers’ da
4 tolerate water
BEWARE!
\ ‘Change | Always monitor TAI
-#/-0,6 | trend as it can fluctu
s the oil ages
MA-K15688-KW Issue 1
Scanned with CamScannerCrank Case Oils
Water in Oil <0.05%
TBN- 2 to 12
| Crosshead TBN
Engines
TBN- Trunk >50%
Piston Engines nominal
| Salt Water 0%
Viscosity 110% -
90%
| nominal
| Insotubles 0.5- 1%
ESF ee
Neti
0.05-0.4% 70.5%
1.751025 <1.75 TBN
TBN or >25
TBN
<50%
nominal
20%
>+/- 20%
>120% nominal
<90%
nominal
1-2% >2%
Check for fresh/salt
water, eliminate leakage
source and batch
centrifuge sump charge.
Partial renewal of
lubricant charge. Check
stuffing box seals for
leakage of high TBN
scavenge drains.
Partial renewal of
lubricant charge.
Take immediate
remedial action.
Partial oil change. Check
for fuel leaks into sump
and fuel pump lubricating
oil supply pressure.
Check centrifuge
operation, stuffing box
seal, piston ring
condition (by
observation/blow down),
Scanned with CamScannerTx feel flea
Enclosed Gears
"Check viscosity
frequently. Check correct
"grade of oil is used for
top up.
| (cSt at 40°C)
: fee Upper limit should be
0.05 = 0.15 - >0.20% checked against
0.15% 0.2% manufacturers’ data.
Some oils cannot
tolerate water -
BEWARE!
Water (%)
~ Always monitor TAN by _
trend as it can fluctuate _
as the oil ages.
Refer to manufacturers | limits.
Turbine Oil
Usa! a, ERIE) ‘Action on Borderline
Ze Oe
[Viscosity — <#1-10% = ee Check viscosity —
(cSt at 40°C) = nom frequently. Check correct
| grade of oll is used for
Ee | top up.
Water (%) | 0.05- 0.15 - >0.20% Upper limit should be
0.15% 0.2% checked against
manufacturers’ data.
Some oils cannot
tolerate water ~
BEWARE!
|
|
|
| <1100 | +10 42.0 Check for water —
contamination at low
\ \ levels,
Scanned with CamScannerCompressor Oil
Test S
Parameter
Always check: —
inter-cooler drains are
operated effectively.
Refrigeration oils cannot
tolerate water at all.
“0.10% High insolubles wi
Pe rapidly foul air delivery
Stern Tube Oils
0.25 305%
- 0.5% 4 ~ levels:
Viscosity § _ >75% <75% - Linked with water:
nominal nominal contamination. Consult
manufacturers of seals
and bearings.
Use the Kittiwake Training Resource CD for guidance on fuels
and lube oils. Help is also available at www. kittiwake.com
"Scanned with CamScanner