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ASTM D638-2014 Standard Test Method For Tensile Properties of Plastics
ASTM D638-2014 Standard Test Method For Tensile Properties of Plastics
INT.ltHA OOH.IJ.
Designation: 0638 1
Derechos do autor de ASTM lntemat1onal.
Reproducción distribuida por FONDONORMA
bajo licencia ASTM.
Tell: (0212) 201,77,11 Fu: (0212)
201.77.17
flin \ldnd<1nl has b,·t11 e1¡,pnA·t,I fvr us,· b_\ ugtnnt.t of thl' U.S Ot•purtmn1t uf Otfemr.
2
For refcrcnccd ASTM !tLandards. v1su Lhc ASTM wcb!<tllc. www Olilm.org. or
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Plasucs and 1, thc drrect responvrbuny of Subcomrmuee D::!O 10 on Mechamcal ASTM Sta11dards volume míormauon. rcfcr to lhc stnndard'!t Document Summa.ry
Properues Current ediuon approved Dec. 15. 2014. Pubhched March 2015 pagc on thc ASTM web!t1tc
Origrnally approvcd m 1941 L:H,l prevtcus edition approved m 2010 a� 0638 'Thc last approvcd vcrs1on oí th1s h1,toncal M.anda.rd l.!i refcrcnccd
• 10. DO1: on
10.1520/D0638-14 www.astm.org.
•A Summary oí Changes section appeurs al the end oí this standard
Copyright OASTM lnternauonal 100 Barr Harbor Onve. PO Box C700. Wesl Conshohocken. PA 19428•2959 Umt8d Stales
• 0 6 3 8 -1 4
E83 Pracuce for Vcrificauon and Classification of been seriously questioned. The exact stress-strain characteristics of plastic
Exten materials are highly dependenl on such factors as rate of application
of
someter
Systcms
E 132 Tc,1 Mcthod for Poisson ':, Rano at Room "'Availnble írom American National Stnndards Institutc (ANSI). 25 W. 43rd St.,
Ternpcrature 4lh Floor. Ncw York. NY 10036. hup.//www.:msi.org.
E69 l Pracucc for Conducting an lnterlaboratory Study
to
Determine the Precision of a Test Method
2.2 ISO Standard:"
ISO 527-1 Determination of Tensile Propcrties
3. Terminology
3 .1 Definicions-Detinitions of terrns applying to this
test method appear in Terrninology D883 and Annex A2.
2
�@f 0 6 3 8must
-14
rneet at least Class C (Practice E83) requirements, which
respcct 10 the -tationary rncmbcr, Thi, velocity " 10 include a fixed strain error of 0.001 strain or :t 1.0 % of
be rcgulated n, spcciticd in Sccuon 8. the
5 . 1 . 5 Load lndicator-s-r« suuublc loud-indicating mecha índicated strain, whichever is
greater.
rusrn capable of sho« 111g thc 101nl tcnsrlc loud curricd by
thc
1c,1 spccuncn whcn hcld b) the grips, This rncchnnism shnll
be csxcntially free of inertia lug al thc spccified rute of
tcsung und shall indicare thc load with nn accurucy of
:t 1 % of thc indicated valuc, or bcttcr, Thc accurncy of the
testing rnachinc shnll be vcrilicd in accordancc with
Practices E4.
3
.. 0 6 3 8 - 1 4
t---------
LO---------i
"TYPES 1, 11, 111 & V
�...-rr,.......,� ___,f �
-l j.T
l
o
LO
1YPE IV
"rtuckness. T. shall be 3 2%: 0.4 mm (O 13 .:t O 02 1n.) lar all types ol moldad speclmens, and lar other Types I and II spec.mens where possibíe 11 specirnens
are machlned
from sheets ar platas, thIckness, T, shall be the thlckness ot Ihe sheet ar plata provtded thís does not exceed the range stated lar the mtended specimen
type Far sheets of nomlnal trucknass greater than 14 mm (0.55 1n.} lhe speclmens shaU be machIned to 1 :1: o 4 mm (O 55 :1: o 02 In.) in th1Ckness. lor use
w1th the Type 111 specmen. Far ◄
sheets of nomlnal th1ckness between 14 and 51 mm (O 55 and 2 In.) approxnnatety equal amounts shall be machlned lrom each surface For thicker sheets
both surfaces o! the specunen shall be machmed. and the locaUon ol the spectmen wrth relerence to the ongmat thIckness of the sheet shall be noted Tok!
rances on thIckness less than
14 mm (O.SS In.) shall be tnose standard lor the grade ol matenal tested
8For the Type IV soecimen. the interna! wtdth ol lhe narrow secucn ol the die shall be 6 00 :1: o 05 mm (O 250 :1: O 002 m.} The drmenstooe are essent1ally !
hose of Die
C ln Test Methods 0412
oYne Type V speclmen snau be machmed ar die cut to lhe drmenstcne shown, ar moldad In a mold whose cavrty has mese dunensions The dImens10ns shatt
be:
W = 3 16 : O 03 mm (O 125 : 0.001 1n ),
L • 9.53 : o.os mm (0.375 : 0.003 m.).
G = 7 62 :1: O 02 mm (O 300 :1: 0.001 In.). and
R = 1 2 . 7 : O.OS mm (O 50 0: O 003 In.)
The other tolerances are lhose In the table
"SupportJng data on the mtroducucn of the L specrmen al Test Method 01822 as rhe Type V speclmen are avallable from ASTM Headquarters Request AR
020-1038
E"fhe lolerances al the w1dth al lhe center Wc: shall be ...o 00 mm, -0.1 O mm ( +0.000 In., -0.004 m.) compared wrth Wldth W at other parts ot the reduced
secUon Any
reoucuen 1n W at lhe center shall be gradual, equa11y on each srde so that no abrupI changes m dlmenston resulL
FFor moldad specimans. a draft of not over 0.13 mm (0.005 I n) Is allowed lar eII11er Type I ar II specimens 3 2 mm (O 13 1n ) ln tmckness See diagram below and
thls shall be taken mto account when catculallng wIdth o! !he specunen Thus a typlcal sectlon ol a moldad Type I specimen. having lhe maxlmum a11owable drah,
could be
as follows
Goverall w1dths greater lhan the meumum mdicated are used lar sorne matenals Jn arder to avoid breaking In the gnps
'"'Overall lengths greater than the mlnlmum mmcated are used lar sorne malenals ro avold breaklng in the gnps ar 10 sausty speoat test reqwrements
'Test marks ar 1mtIal extensometer span.
-When selt-11ghtemng gnps are used, lar hIghly e,ctens1ble polymers. the d1stance between gnps wIH depend upon the types ol gnps used and may not be cnucal
11
mainta1ned umlorm once chosen.
1
12 83 mm, max
••••• (O.SOS In.) -····
,.-0.13 mm, max
(0.005 In.)
12 70mm
(0.500 In.)
FIG. 1 Tenslon Test Speclmens lor Sheet, Piste, and Molded Plastlcs
4
• D638-14
ness. Th1, groovc shall consist of a straight section 57.2 mm
(2 25 m.) in lcngth wuh a radius of 76 mm (3 in.) at each
end joining II to thc outsrdc diamctcr. Stecl or brass plugs
having diameters such that thcy w1II fil snugly insidc thc
1
tubc and having a lcngth equal to the full jaw lcngth plus 25
mm ( 1 in.)
89 mm, mln. shall be placed in thcpreven!
ends of the spccirnens to
(J.S0 In.) crushing. They can be located convcnicntly in the tubc by
+-o
separating and supporting them on a thrcaded metal rod.
Details of plugs and test assembly are shown in Fig, 2.
6.3 Rigid Rods-The test specimen for rigid rods shall be as
shown in Fig. 3. The length, L, shall be as shown in the
SI mm, mln.
(2.00 m.) table in Fig. 3. A groove shall be machined around the
specimen at the center of its length so that the diameter of
�7�,"!,mRad. the machined portian shall be 60 % of the original nominal
1n.) diameter. This groove shall consist of a straight section 57 .2
Machlne to mm (2.25 in.) in length with a radius of 76 mm (3 in.) at each
L
S7mm end joining it to the outside diameter.
60o/oof
(2.2S In.)
Onglnal 6.4 Ali surfaces of the specimen shall be free of
Nominal
-} -1ommRad . Wall Thidmess visible ñaws, scratches, or imperfections. Marks left by
R.S. (3.00 In.) coarse rna chining operations shall be carefully removed with a
l
SI mm, mln.
1.6 mm
Rad. (0.063
fine file or abrasive, and the filed surfaces shall then be
smoothed with abrasive paper (No. 00 or finer). The finishing
sanding strokes shall be made in a direction parallel to the
In. )
long axis of the test specimen. Ali flash shall be removed from a
molded specimen, taking great care not to disturb the
molded surfaces. In machining a specimen, undercuts that
would exceed the dimensional tolerances shown in Fig. I shall
�89
_I_
be scrupulously avoided. Care shall also be taken to avoid
other common machining errors.
6.5 lf it is necessary to place gage marks on the specimen,
this shall be done with a wax crayon or lndia ink that will
mm, mln.
not affect the material being tested. Gage marks shall not
be scratched, punched, or impressed on the specimen.
6.6 When testing materials that are suspected of anisotropy,
duplicate sets of test specimens shall be prepared, having
their
DIMENSIONS OF TUBE SPECIMENS
long axes respectively parallel with, and normal to, the
Standard lenglh,
Lenglh of Radial Total Calculaled suspected direction of anisotropy.
L,
Nominal Wall ot Specimen to
Sections, Min1mum
Be Ttuckness
2R.S Lenglh ol Specirnen
Used lar 89- 7. Number of Test Specimens
mm
(3 s-m.) JawsA 7 . 1 Test at least fi ve specimens for each sample in the
mm(ln.) case
0.79 ('hz) 13.9 (0.547) 350 (13 80) 381 (15) of isotropic
354 (13.92) 381
381 (15)
1 2(1/,e)
1.6 (1/..) 1917.0 (0.670)
6 (0.773) 356 (1402) (15)
2.4 (fu) 24.0 (0.946) 361 ( 1420 ) 381 (15) 7.2 For anisotropic materials, when applicable, test five
3.2 (1/,) 27.7 (1.091) 364 (14 34) 381 (15) specimens, normal to, and five parallel with, the principie
4.8 (1/,a) 33.9 (1.333) 370 (14.58) 381 (15)
6.4 (¼) 39 O (1 536) 376 (14 79) 400 (15.75) axis of an isotropy.
380 (14.96) 400 (15 75)
7.9 W••l 43.5 (1.714)
7.3 Discard specimens that break at sorne flaw, or that break
9.5 ('V,) 47.6 (1.873) 384 (15.12) 400 (15.75)
11 1 (7/,a) 51.3 (2.019) 388 (15.27) 400 (15.75) outside of the narrow cross-sectional test section (Fig. 1 ,
12.7 ('h) 54 7 (2 154) 391 (15.40) 419 (16.5)
dimension "L"), and make retests, unless such flaws constitute
a variable to be studied.
AFor Jaws greater than 89 mm (3.5 1n.). the standard lenglh shall be lncreased
by twlce the lenglh ol the jaws mlnus 178 mm (7 1n.) The standard length . Non l�Before testing, aH transparent specimens should be inspected
permns a shppage of approxlmalely 6 4 lo 12 7 mm (0.25 lo O 50 1n.) 1n m a polanscope. Those which show atypical or concentrated strain
each ¡aw wh1le mamtalnlng the maxlmum lenglh of lhe ¡aw grip panerns should be rejected, unless the effects of these residual strains
constitute a variable to be studied.
FIG. 2 Diagram Showing Location of Tube Tension Test
spect
mens in Testing
8. Speed of
Machine Testing
8.1 Speed of testing shall be the relative rate of motion
of the grips or test fixtures during the test. Toe rate of motion
machining shall be 60 % of the original nominal wall of the driven grip or fixture when the testing machine is
thick-
running
5
o D638-14
TABLE 1 Deslgnetlons for Speed ol Testlng"
Nominal
-t-
mm/mm- mln
(lnAn mln)
-
500 (20) et 10 % 10
IV 50 (2) • 1 0 % 1.5
500 (20) et 10 % 15
L
Machlne to
mm 60%of
(2.25 in.) Original Nominal "Select the lowest speed that produces ruptura In 0.5 to 5 mm for !he
i..._ & ¿ Dlameter speclmen geomelry be1ng used (see 8 2).
-+R
"rhe 1ni11al rate ol stralning cannot be calculated exacliy for dumbbell-
E
�
�
shaped
R . S. E;; "see Termlnology 0883 Jo, del1n1t1ons.
12.00 in.)
the speed is not specified, use the lowest speed shown in
Table I for the specimen geometry being used, which
gives rupture within 0.5 to 5-min testing time.
8.3 Make modulus determinations at the speed selected
for the other tensile properties when the recorder
89 mm, min.
response and resolution are adequate.
(3.50 in.)
_ 9. Conditioning
9. 1 Condirioning-Condition the test specimens in accor
6
• 0638-14
narrow section. For ali other specimens. measure the actual often desirable to also calculate, in a similar manncr, thc
width of thc ccnter pon ion of the specimen to be tested, corresponding tensile stress at yield or tensile stress at
unlcss it can be shown that the actual width of the specimen
break and repon it to three significan! figures (see Note
is the same as that of the die within the specimen
A2.8).
dimension tolerances given in Fig. 1 .
10.1.4 Meas ure the diarneter of rod specimens, and 11.3 Elongarion values are valid and are reponed in cases
the inside and outside diameters of tube specimens. to the where uniforrniry of deformation within the specimen gage
nearest length is present. Elongation values are quantitatively relevan!
0.025 mm (0.001 in.) at a minirnum of two points 90º and appropriate for engineering design. When non-uniforrn
apart; malee these measurements along the groove for deformation (such as necking) occurs within the specimen gagc
specimens so constructed. Use plugs in testing tube Iength nominal strain values are reponed. Nominal strain
specimens, as shown in values are of qualitative utility only.
Fig. 2. 11 . 3 . 1 Percent Elongation-Percent elongation is the
10.2 Place the specimen in the grips of the testing machi ne, change in gage length relative to the original specimen gage
taking care to align the long axis of the specimen and the Iength, expressed as a percent. Percent elongation is calculated
grips with an imaginary line joining the points of attachment using the apparatus described in 5.2.
of the grips to the machine. The distance between the ends 1 1 . 3 . 1 . 1 Percent Elongation at Yield-Calculate the
of the gripping surfaces, when using flat specimens, shall be percent
as indicated in Fig. 1. On tube and rod specimens, the location elongation at yield by reading the extensión (change in gage
for the grips shall be as shown in Fig. 2 and Fig. 3. Tighten Iength) at the yield point. Divide that extensión by the original
the grips evenly and firmly to the degree necessary to gage length and multiply by 100.
prevent slippage of the specimen during the test, but not to 1 1 . 3 . 1 . 2 Percent Elongation at Break-Calculate the
the point where the specimen would be crushed. per
cent elongation at break by reading the extensión (change in
10.3 Attach the extension indicator. When modulus is gage length) at the point of specimen rupture. Divide that
being
extension by the original gage length and multiply by 100.
determined, a Class B-2 or better extensorneter is required (see
5.2.1). 11 . 3 .2 Nominal Strain-Nominal strain is the change in
grip separation relative to the original grip separation
NOTE 11-Modulus of materials is detennined from the slope of the expressed as a percent. Nominal strain is calculated using
linear portion of the stress-strain curve. For most plastics, this
the apparatus described in 5.1.7.
linear portion is very srnall, occurs very rapidly, and must be
recorded automati cally. Toe change in jaw separation is never to be 1 1 . 3 . 2 . 1 Nominal srrain at break-Calculate the
used for calculating modulus or elongation. nominal strain at break by reading the extensión (change
10.4 Set the speed of testing at the proper rate as required in grip separation) at the point of rupture. Divide that
in extensión by the original grip separation and multiply by 1
Section 8. and start the machine. OO.
10.5 Record the load-extension curve of the specimen. 1 1 . 4 Modu/us of Elasticiry-Calculate the modulus of
elas ticity by extending the inirial linear portion of the
10.6 Record the load and extensión at the yield point (if
load extensión curve and di viding the ditfereace in stress
one exists) and the load and extension at the moment of
corre sponding to any segment of sectioa on this straight line
rupture.
by the corresponding ditference in strain. Ali elastic modulus
NOTE 12-lf it ,s desired to rneasure both modulus and Iailure values shall be computed using the average original cross-
properties (yicld or break, or both), it may be necessary, in the case of sectional area in the gage length segment of the
highly extensible materials, to run two independent tests. The high
specimen in the calculations. The result shall be expressed in
magnification extensornetcr nonnaJJy used 10 determine properties up to
the yield point may not be suitable for tests involving high extensibility. pascals (pounds force per square inch) and reponed to three
lf allowed to remain attached to the specimen, the extensometer could be significant figures.
pennanently damaged. A broad-range incremental extensometer or hand
rule technique may be needed when such rnaterials are taken 10 1 1 . 5 Secant Modulus-At a designated strain, this shall
rupture. be calculated by dividing the corresponding stress (nominal)
by the designated strain. Elastic modulus values are preferable
11. Calculation and shall be calculated whenever possible. However, for
1 1 . 1 Toe compensation shall be made in accordance rnaterials where no proportionality is evident, the secant
with Annex A 1, unless it can be shown that the toe region value shall be calculated. Draw the tangent as directed in A 1 .3
of the curve is not due to the take-up of slack, seating and Fig. A 1.2, and mark off the designated strain from the
of the specimen, or other artifact, but rather is an authentic yield point where the tangent line goes through zero stress.
material response. The stress to be used in the calculation is then determined
J 1.2 Tensile S1re11gth-Calculate the tensile strength by
by dividing the load extension curve by the original average
dividing the max.imum load sustained by the specimen in cross-sectional area of the specimen.
newtons (pounds-force) by the average original cross-sectional 1 1 . 6 For each series of tests, calculate the arithmetic
area in the gage length segment of the specimen in square mean of ali values obtained and repon it as the "average
metrcs (square inches). Express the rcsult in pascals (pounds value" for the particular property in question.
force per square inch) and repon it to three significant 1 1 . 7 Calculate the standard deviation (estirnated) as follows
figures as ten si le strength at yield or tensile strength and repon it to two significant
at break, whichever term is applicable. When a nominal figures:
yield or break
load Iess than the rnaximurn is present and applicable, it
is s= Y(LX 2
- nX ')!{n - 1 )
(1)
7
• 0638-14
"hcrc: TABLE 3 Tensile Stress at Break, 103 psi, for Elght Laboratorles,
1·
= csurnated standard Five Materlals"
'(
= deviation, value of single Mean s, SR 1, IR
observation, Polypropylene 2 97 1 54 1.65 437 4.66
= number of observations, and Cellulose acetate butyrate 4 82 o.osa 0.180 O 164 0.50
92 13
x= Acryhc 9.09 O 452 O 751 1 27
aríthmetic mean of the set of observations. 20.8 0.233 O 437 0.659 1 24
Glass-remíorced polyester
1 1 .8 See Annex A I for information on toe compensation. Glass-re1nforced nylon 23.6 0.277 0.698 0.784 1.98
11.9 See Annex A3 for lhe determination of Poisson 's ""Tens1/e strength and elongat1on at break values obtaioed for
Ratio. unrelnforced propylene plasncs generally are h1ghly variable due to
lnconsrstencies In necklng
12. Report or "drawmg• of the center sectton of the test bar Since tenslle strenglh
and elongatlon at y¡eld are more reproducible and relate In most cases to the
1 2 . 1 Repon the following information: practica! usetulness of a molded part, they are generally recommended for
speciñcatlon
1 2. 1.1 Complete identification of the material tested, purposes.
includ ing type, source, manufacturer' s code numbers,
form, principal dimensions, previous history, etc.,
1 2 . 1.2 Method of preparing test specimens, TABLE 4 Elongatlon al Break, %, for Etght Laboratories,
Five
1 2 . 1 . 3 Type of test specimen and dimensions,
MaterialsA
1 2 . 1 .4 Conditioning procedure used,
Mean s, SR 1, IR
1 2 . 1 . 5 Atmospheric conditions in test room, Glass-ramtorced polyester 3 68 0.20 2 33 O 570
1 2 . 1 . 6 Number of specimens tested: for 6.59
anisotropic materials, lhe number of specimens tested and Glass-relnforced nylon 3 87 O1O 2 13 0.283
6.03
the direction in which lhey were tested, Acryllc 13.2 2.05 3.65 5.80
1 2 . 1.7 Speed of testing, 10.3
12.1.8 Classification of extensometers used. A Cellulose acetate butyrate 14 1 1.87 6.62 5.29 18.
7
description of measuring technique and calculations Polypropylene 293 o 50 9 119.0 144.0 337
O
employed instead of a mínimum Class-C extensometer
system, "'Tenslle strenglh and elongat,on at break values obtalned for
unrelnforced propylene plastics generalty are h,ghly variable due to
1 2 . 1 . 9 Tensile strength at yield or break, average value, mconststencíes 1n necking or "drawlng" of the center secnon of the test bar.
and standard deviation, Slnce tenslle strength and elongatlon al y1eld are more reproducible and relate
in most cases to rhe pracncal usefulness ol a molded part, they are generally
1 2 . 1 . 1 O Tensile stress at yield or break. if recommended for specmcatlon
applicable. purposes
average value, and standard deviation,
1 2 . 1 . 1 1 Percent elongation at yield, or break, or
nominal strain at break, or ali three, as applicable,
average value, and standard deviation, 13. 1 . 1 Tables 5-8 are based on a round-robin test
1 2 . 1. 1 2 Modulus of elasticity or secan! modulus,
average conducted by the polyolefin subcommittee in 1988,
valu é , and standard deviation, involving eight polyethylene materials tested in ten
1 2 . 1. 1 3 If measured. Poisson •s ratio, average value, laboratories. For each material, ali sarnples were
stan dard deviation, and statement of whether there was molded at one source, but the individual specimens
proportion ality within the strain range, were prepared at the laboratories that tested them. Each
1 2 . 1 . 1 4 Date of test, and test result was the average of five individual deterrninations.
1 2 . 1 . 1 5 Revision date of Test Method D638. Each laboratory obtained three test results for each
material. Data from sorne laboratories could not be used for
5
13. Precision and Bias various reasons, and this is noted in each table.
1 3 . 1 Precision-Tables 2-4 are based o□ a round-robin 13.1.2 Tables 9 and 10 are based on a round-robin
test conducted in I 984, involving five materials tested by test conducted by lhe polyolefin subcommittee in 1988,
eight laboratories using the Type J specirnen, ali of nominal involving lhree materials tested in eight laboratories. For
0.125-in. thickness. Each test result was based on five each material, ali samples were molded at one source,
individual determinations. Each laboratory obtained two test but the individual specimens were prepared at the
results for laboratories that tested thern, Each test result was the
each material. average of five individual determina tions. Each laboratory
obtained lhree test results for each material.
8
• 0638-14
TABLE 6 TensUe Yleld Elongallon, lor Elght Laboratories, Elght TABLE 10 ElongaUon at Yleld, "'• lor Elght Laboratories, Toree
Materials Materials
Test ValJes Expressed in Pen:ent Ur>ts Mean S,
MalenaJ 5peed,
3 65 0.27 062 0.76
n.nw, Average s, SR Celluose acetate butyrate
1.75
R 4.89
LOPE 20 170 1.26 316 3.52 884 Aayt,c
Polypropylene 8.79 O 0.21
45 0.55
5.86 0 5 9 16.5
127
LOPE 20 1� 6 1 02 2.38 2.86 6.67
LLDPE 20 15.7 1.37 2.85 3.85 7.97
llDPE 20 1 66 1.59 3..30 4.46 9.24 ry
LLDPE 20 11.7 1.27 2.88 3.56 8.08
TABLE 11 Poisson's Ratio Repeatabllity Data lor One Laborato
LLDPE 20 15.2 127 2.59 3.55 7.25 and Two Polypropylene Materials
HOPE 2 9.27 140 2.84 3 91 7.94
HOPE Villles Expressed as a Dmensoooless Raoo
2 9.63 1.23 2.75 3.45 7.71 Malenals
Average Sr r
pp •1 Chord O 412 0.00 0.1)26
PP •1 leasl 0.413 9
0.011 0.032
TABLE 7 Tensile Break Strass, lor Nine Laboratories, Six Squares
Test pp •2 Chord 0.391 0.009
VaAJes Expressed on psi Uruts
Materials Squares
Ma!enaJ Speed,
in.hnin Average s, SR
R
LOPE 20 1592 52.3 74.9 146.4 209.
LOPE 20 66.6 7
1750 102.9 186.4 288.1
LLDPE 127.1 219.0 13.1.4.1 S,is the within-laboratory standard deviation of
LLDPE 20 2840 78.6 143.5 220.2 the average: I, = 2.83 Sr (See 13.1.4.3 for application of
LLDPE 20 1679 4 0 134.3
8 47.0 95.96 131 6 Ir)
LLDPE 20 2660 119. 1 166.3 333.6 465 13.1.4.2 SRis the between-laboratory standard deviation
of
the average: /R=2.83 SR. (See 13.1.4.4 for application of
IR.)
TABLE 8 Tensile Break Elongation, for Nine Laboratories, Slx
Materials 13.1.4.3 Repearabiliry-In comparing two test results
Test for the same material, obtained by the same operator
VaAJes Expressed on Percent Unrts
Matenal Speed. using tbe same equipment on the same day, those test
on./rmn Average s, SR R
results should be judged not equivalent if they dilfer by
LOPE 20 567 31.5 59.5 882
166.6 more than the I, value
LOPE 20 569 61.5 892 172.3 for that material and condition.
249.7
LLDPE 20 890 25.7 113.8 71.9 13.1.4.4 Reproducibiliry-In comparing rwo test results
318.7 for the same material, obtained by different operators using
LLDPE 20 64.4 6.68 11.7 18.7
32.6 dilfer ent equipment on different days, those test results
LLDPE 20 803 25.7 104.4 71.9
292.5 should be judged not equivalent if tbey ditfer by more
LLDPE 20 782 41.6 96.7 116.6 tban the IR value for that material and condition. (This
270.8
applies between different laboratories or between different
equipment witbin tbe same laboratory.)
13.1.4.5 Any judgment in accordance with 13.1.4.3
TABLE 9 Tensile Stress at Yield, 103 psi, lor Eight Laboratories,
and
Toree Materials
13.1.4.4 will have an approximate 95 % (0.95) probability
Mean s, of
being correct,
Polypropylene 3.63 0.161 0.062 13.1.4.6 Other formulations may give somewhat
Cellulose acetate butyrate 0.022 0.227 0.456 different
Al:(,/,>c 5.01 0.317 0.164
0.058 0.642 results.
10.4 0.190 13.1.4.7 For further information on the methodology used
0.067 0.897 in
this section, see Practice E69 l.
13.1.4.8 Toe precision of this test method is very dependent
1 3. 1. 3 Table 11 is based on a repeatability srudy upon the uniformity of specimen preparation, standard prac
involving a single laboratory. Toe rwo materials used were tices for which are covered in other documents.
unfilled poly propylene types. Measurements were performed
by a single technician on a single day. Each test result is 13.2 Bias-There are no recognized standards on which
an individual determination. Testing was run using rwo Type to base an estímate of bias for this test metbod.
B-1 extensom eters for transverse and axial measurements at
14. Keywords
a test speed of
5 mm/min. 14.1 modulus of elasticity; percent elongation; plastics:
13.1.4 In Tables 2 -1 1. for the materials indicated, and Poisson 's Ratio; tensile propenies: tensile strength
for
test results that derived from testing five specimens:
9
• D638-14
ANNEXES
(Mandatory Information)
Al. TOE
COMPENSATION
A l. 1 ln a typical stress-strain curve (Fig, A I . I ) there is elastic modulus can be determined by dividing the stress at
a toe r�gion, that does not represent a property of
¿
the material. lt 1s an artifact caused by a takeup of slack
any point along the line CD (or its extension) by the strain
at the same point (measured from Point B, defined as zero-
and alignment or seating of the specimen. ln order to obtain strain).
correct va�ues of_ such parameters as modulus, strain, and
offset yield point, this artifact must be compensated for A 1.3 In the case of a material that does not exhibit
to give the corrected zero point on the strain or extension any linear region (Fig. A 1.2), the same kind of toe correction
axis. of the zero-strain point can be made by constructing a
tangent to the maximum slope at the inflection point (/-f). This
A 1.2 ln the case of a material exhibiting a region is extended to intersect the strain axis at Point B', the
of Hookean (linear) behavior (Fig. AI.I), a continuation corrected zero-strain point. Using Point B' as zero strain, the
of the linear (CD) region of the curve is constructed stress at any point (G') on the curve can be divided by the
through the zero-stress axis. This intersection (8) is the strain at that point to obtain a secant modulus (slope of Line
corrected zero strain point from which ali extensions or B' G'). For those materials with no linear region, any attempt
strains must be measured, including the yield offset (BE), to use the tangen! through the inflection point as a basis for
if applicable. The determination of an offset yield
point may result in unacceptable error.
A B E
NO'Tl!l-
Some chart recorders plot the mirror image of this graph,
NO'Tl! 1-Some chart recorders plot the mirror image of this graph.
FlG. A1.1 Material with Hookean Region
FlG. A1.2 Material with No Hookean Reglen
10
� 0638 -14
11
• D638-14
A2 14 _rare ofsrraining-the change in tensile strain per urut It ,s expressed in force per unit arca. usually megapascals
urne. lt os expressed either a, strain per unit time, (pounds-force per square inch).
usually mctres _per metre (inches per inch) per minute, or N01c A2.8-The expression of tensüe propcrues in terms of
percent elon�a!Jon per umt time, usually percent elongation per thc rmrumum original cross secrion 1� almost universally used m pracuce
In thc case of rnatenals exhibiting high extensibiluy or necking. or
minute. The iruual rate of straming can be calculated from
both (A2.16). nominal stress calculations rnay not be mcamngful beyond
the initial slope of the tensile strain versus time diagram. thc yield pomt (A2.22) due to thc extensive reducuon in cross-sectionat
NOTE A2.5-The imtral rate oí strarmng is synonymous wilh thc area that ensues Under sorne circurnstances II may be desirable to
rate oí crosshead movement divrded by the iruual distance between express the tensile properties per umt of minimum prevailing cross
crossbeads only in a machme wuh constam rate of crosshead rnoverneru secuon These properties are called true tensile properues (that is. true
and when the specimen has a uruform onginal cross secuon, does not tensile stress. etc.),
"neck down." and does not slip m the jaws
A2.20 tensile stress-strain curve-a diagram in which
A2.15 rate o] stressing (nominal)-the chanze in val ues of tensile stress are plotted as ordinales against
tensile stress (nominal) per unit time. lt is expressed in force correspond ing values of tensile strain as abscissas.
per unit area per unit time, usually megapascals (pounds-
force per square inch) per minute. The initial rate of A2.2 I true strain (see Fig. A2.2) is defined by the following
stressing can be equation for &7:
calculated from the initial slope of the tensile stress
(nominal)
versus time diagram. t7= JLdLIL = lnLIL. (A2 1 )
L,
NOTE A2.6-The rrnual rate of stressmg as detenrnned m this
manner where:
has only lirrnted physical sigmficance II does, however, roughly descnbe
the average rate at which the rruual stress (nominal) camed by the test dL = increment of elongation when the disrance between the
specimen is apphed It 1s affected by the elasticity and ñow gage marks is L,
characrensucs of the rnaterials beong tested. At the yield pomo. the rate
of stressing (true) may conunue m have a posiuve value 1f the L. = original distance between gauge marks, and
cross-secuonal area 1s L = distance between gauge marks at any time.
decreasmg
A2. l 6 secaru modulus-the ratio of stress (nominal) to A2.22 yield poi111-the first point on the stress-strain curve
corresponding strain at any specified point on the stress-strain at which an increase in strain occurs without an increase
curve. lt is expressed in force per unit area, usually in
rnegapas cals (pounds-force per square inch), and reponed stress (Fig. A2.2).
NOTE A2.9-0nly materials whose stress-strain curves exhibit a
together with the specified stress or strain. pornt of zero slope may be considered as havmg a yield point.
NOTE A2.7-This measurement 1s usually employed in place of NoTE A2 ) �orne materials exhibit a distinct "break" or dhcontinuity
rnodulus of elasucity rn the case of materials whose stress-strain in the stress-strain curve in the elastic region. To.is break 1s not a
diagram doce; not dernonstrate proporuonality of stress to strain. yield point by defirution. However, this poinr may provc u.seful for
material characterizarion in sorne cases.
A2. l 7 strain-the ratio of the elongation to the gage
length of the test specimen, that is, the change in length per A2.23 yield strengrh-the stress at which a material
unit of original length. lt is expressed as a dimensionless exhibits a specified limiting deviation from the proportionality
ratio. of stress to strain. Unless otherwise specified, this stress will
be the stress at the yield point and when expressed in relation
A2. l 7 . 1 nominal strain at break-the strain at the
to the tensile strength shall be designated either tensile
moment
strength at yield or tensile stress at yield as required in A2.18
of rupture relative to the original grip separation.
(Fig. A2.3). (See offset yield strength.)
A2. l 8 tensile strength (nominal)---the maximum tensile
stress (nominal) sustained by the specimen during a tension
test. When the máximum stress occurs at the yield point
(A2.22), it shall be designated tensile strength at yield. When dL
the maximum stress occurs at break. it shall be designated
t=
tensile strength at break.
� -- ------------J J
- L -------i ,I
A2. l 9 tensile stress (nominal)-the tensile load per unit 4)
area of mínimum original cross section, within the gage
boundaries, carried by the test specimen at any given FIG. A2.2 lllustration ol True Straln Equation
moment.
12
---------�----��----------------�---------�-----------.J
�t' D638 - 1 4 Mlnlmum crosa-secucnat area at any time
Original cross-sectlonal araa
lncrement ol cross-secuonal aree
A Cross-sectlonal area at potnt ol ruptura measured
altor braaklng speclmen
Cross-sectronal area al polnt ol ruptura, measured al the
moment of ruptura
B
,---------------
1
e (!.f
Time
lncrement of time
1 o Tensile stress
1 lncrement ol stress
1 /\o
ºr True tenslle stress
YIELD ªu Tenslle strength at break (nominal)
PO ºur Tensile strength al break (true)
- -- e Stra,n
IN T E (!.e lncrement of strain
, -- ·1
<u Total stra,n, al break
1 Cr True stram
·------- %El
Y.P.
Percentage elongatlon
Yield polnt
E Modulus ol etasucity
A & E = TENSILE STRENGTH AT BREAK A2.25 Relations between these various terms may
ELONGATION AT BREAK be defined as follows:
B = TENSJLE STRENGTH AT YIELD o W/A0
ELONGATION AT YIELD or W/A
au W/A 0 (where W ,s break1ng load)
C = TENSILE STRESS AT BREAK our W/Ar (where W Is breaking load)
ELONGATION AT BREAK l!.LA.0 = (L -
LJIL0
D = TENSILE STRESS AT
<u (Lu - L J/L0
YIELD ELONGATION AT <r Í[ dUL=/nUL
YIELD %Et l(L - L JIL,J x 100 0 = e x 100
STRAIN Percent reduction of area (nominal)= [(AJ> -Au)/Anl X 100
FIG. A2.3 Tensile Designations Percent reduction of area (true) = [(A, - Ar)/A ) x TOO
0
Rate of loading = D. W//J.t
Rate of stressing (nominal)= /J.cr//J. = (D. W]/A )//J.t
A2.24 Symbo/s-The following symbols may be used Rate of straining = /J.e//J.t = (/J.L/L )/J.t 0
for the above terms: For the case where the volume of 0
the test specimen does
not
Symbol Term change during the test, the following lhree relations hold:
w Load
l!. W lncrement ol load
L Distance between gage marks al any lime
or= o ( I +t) = ( A2.2)
0L/L 0
13
o D638-14
molding the matenal into the spccirncn shapc to be
E I 0 I : ! Pr ,11,c tur vcní ic 1111111 ot l e lllll' l 1,1111< ,11ul \ tested.
p«1
Non A3.4-When prepanng specimcnv from certain
m, n \ltl!n111�nt l ndct Icnvrlc .111d C11111prL ,11 e \ ,1 rl cornposue larni
) or ,L \ppit,,ltlllll natev ,uch a, wovcn rovmg, or glavs cloth. care must be
exercised m
\1.2.2 ISO Stundard '
ISO S:! · 1 Dct: r1111n-1tlllll ol lbi-ik
Propcrtic-,
\J.3. Tcrminolo�
\3 1 1 D,j11111w111-Defin111on, of tcrm, applymg to th1,
tc,t rncthod appcar in fcrmmology D883 and Anncx A2 of this
<tandard
A3.5. Apparatus
A3.5 1 Refer to 5 . 1 and 5.3 of this standard for the
require
rnents of thc testing machine and
rnicrometers,
A3.5.2 For mcasurcment of Poisson's Ratio use either a
bi-axral cxtcnsomctcr oran axial extensometer in combination
with a transverso extensorncter. They must be capable of
rccordmg axial strain and transverse strain simultaneously. The
cxtcnsornctcrs shall be capable of measuring the change in
strains with an accuracy of 1 % of tne relevan! value or better.
Non, A3.3-Sua,n gagcs are used as an alternauve method to mensure
axial and iransvcrsc strain: howevcr, proper techniques Ior rnounung
vtrain gauge, are crucial to obtaimng accurate data. Consult strain
gauge supphers for mstrucuon and trarnmg ,n theve special
techniques.
A3.6.3 Ali surfaccs of thc spccrrncn shall be free of visrblc ñaws, A3.8. Conditioning
scratchcs, or impcrfccuons. Markv lcft by coarsc rna chining A3.8. I Specimens shall be conditioned and tcsted in accor
opcrations shall be carefully removed with a hne file or abrasivc. and dance with the requrrement shown in Section 9 of this standard.
the filed surfaccs shall thcn be smoothcd wuh abrasive papcr (No.
00 or finer). The ñmshmg sanding strokcv shall be made in a AJ.9. Procedure
direction parallel to the long axis of the test specimen. Ali flash shall
be removed from a molded spccimen, taking great care not to A3.9. I Measure the width and thickness of each specimen
disturb the molded surfaces. In machining a specimen, undercuts to the ncarcst 0.025 mm (0.001 in.) using the applicable
that would exceed thc dimensional tolerances shown in Fig. 1 shall test methods in D5947. Follow the guidelines specified in
be scrupulously avoided. Care shall also be taken to avoid other 1 0 . 1 . 1 and 10.1.2 of this standard.
common A3.9.2 Poisson's Ratio shall be determined a t a speed of
machining errors. 5
mm/min.
A3.6.4 Jf it is necessary to place gage marks on the
specimen, this shall be done with a wax crayon or India ink that will A3.9.3 Place the spccimen in the grips of the testing
not affect the material being tested. Gauge marks shall not be machine, taking careto align the long axis of the specimen and
scratched, punched, or impressed on the specirnen. the grips with an imaginary line joining the points of attach
ment of the grips to the machine. The distance between thc
A3.6.5 When testing materials that are suspected of anisotropy, ends of the gripping surfaces, when using flat specirnens,
duplicate sets of test specimens shall be prepared, having their long shall be as indicated in Fig. 1 . Tighten the grips evenly and
axes respectively parallel with, and normal to, the suspected firmly to the degree necessary to prevent slippage of the
direction of anisotropy. specimcn during the test, but not to the point where the
specimen would be crushed.
A3.7 Number of Test Specimens
14
�------------------------------------------------�----------
�
-0 D 6 3 8 - 1 4
A3.9.4 Attach the biaxial extensorneter or the axial nnd A3.10.1. I For those materials where there is proportionaliry
trnnsverse extensometer combination to the specimen. The of stress to strain nnd it is possible to determine a modulus
transverse extensorneter should be anached 10 the width of of elasticity, a straight line is drawn through each set of
the points
specimen. within the load range used for determination of modulus. and
A3.9.5 Apply a small preload (less thnn 5 N) to the the slopes dt 0
dP nnd dz, / dP. of those lines are deterrnined.
/
s�tmen_ at a crosshead speed of O. 1 mm/mio. This Toe use of a least squares method of calculation will reduce
preload errors resulting from drawing lines. Poisson's Ratio, lµl, is then
"�11 eliminate nny bending in the specimens. calculated as follows:
AJ.9.6 Rebalance the extensorneters 10 zero.
lµI = (A3. I )
A3.9.7 Run the test at 5 mm/min out to a minimum of0.5 (dt/dP}/(dt/dP)
% whcrc:
strai� before re�oving the extensorneters, simultaneously re
cording the stram readings from the extensometers at the de, change in traasverse
same applied force. The precision of the value of
strain, de. change in axial stram, and
Poisson's Ratio will depend on the ournber of data
poirus of axial and transverse strain taken. lt is dP change m applied load;
recomrnended that the data collection rate for the test be ¡µ1 = (dt,)/(dt.) (A3.2 )
a minimum of 20 points per
second (but preferably higher). This is particularly important A3. I 0.1.2 Toe errors that are introduced by drawing a
for rnaterials having a non linear stress to strain curve. straight line through the points are reduced by applying the
least squares method.
A3.9.8 Make the toe compensation in accordance with
A3.10.l.3 For those materials where there is no proportion
Annex A 1 . Determine the maximum strain (proportional
ality of stress to strain evident determine the ratio of de , I
limit) at which the curve is linear. If this strain is zreater than
0.25 % the Poisson's Ratio is to be determ.ined anywhere in dt0 when ae; = 0.002 (based on axial strain range of 0.0005
this linear portion of the curve below the proportional to
limit lf the material does not exhibir a linear stress to 0.0025 mm/mm) and after toe compensation has beeo made.
strain relationship the Poisson 's Ratio shall be determined lµI = dt,)/0.002 (A3.3)
within the axial strain range of 0.0005 to 0.0025 mm/mm (0.05
to 0.25 %). If the ratio is deterrnined in this manner it shall be AJ.11. Report
noted in the report that a region of proportionality of stress to
A J. 1 1. 1 Report the following information:
strain was not evident.
A3. I I. I. I Complete ideotificatioo of the material tested,
NOTE A3.6--A suitable method for detenninntion of lincarity oí including rype, source. rnanufacrurer' s code numbers, form,
thc stress to strain curve is by m:lking a series of tangent modulus principal dimensions, previous history, etc.,
measurc menlS at differcnt axial strain tevels. Va.lucs equívalenr al each
strain level mdicate lineariry, Va.Jucs showing a downw:ird t.rcnd with
A3. l 1. l.2 Method of prepariog test specimeos,
incrcasing strain level indicatc non lineariry, A3.1 l. l .3 Type of test specimen nnd
dimeosioos. A3. l l. l.4 Conditioning procedurc
AJ.10. Calculation used.
A3. l l. l .5 Atmospheric conditions in test room.
A3. IO. I Poisson 's Ratio-Toe axial strain. t A3. l l. l .6 Number of specimens tested.
indicated by
0
the axial extensorneter, and the transverse strain, i;. indicated A3.l 1.1.7 Speed of testing,
by the traosverse extensometers, are ploned against the A3. l 1 . l .8 Classification of exteosometers used. A descrip
applied tion of measuring technique aod calculations employed.
load. P. as shown in Fig. AJ. l.
12
11
10
w 9
::' 8 --- Axial Strain, Ea
�"'
111
7
6
.fl 5
..:!
o
e"'
4
3 -<J
□
2 □
□
1 □ � Transverse Strain, Et
0---
o
o 1 2 3 4 5 6
Applied Load,
P
AG. A3.1 Plot of Stralns Versus Load for DetermlnaUon of Polsson's Ratio
15
� D638- 14
,\3 1 1 1 9 Poissons ratio, average value. standard on precision and bias cannot be givcn, Because uns test methotl
de, ianon. and staternent of whcther there wa, proponionality
does not contam a round-robin based numerical precisión
"1thm thc stram runge,
and bias statcment, it shall not be used as a referee test
A J . 1 1 . 1 10 Date of test, and
method m case of dispute. Anyone wishing to parucipate m
A3 1 1 1 1 1 Revisión date of Test Method D618.
the develop ment of precision and bias data should contact
\3.12. Precision and Bias the Chairman. Subcomminee D20.1 O Mechanical
Properties, ASTM lnternational, 100 Barr Harbor. We,t
A3 12 1 Precisio11-The repcatabilny standard Conshohocken, PA
deviation ha, been determincd to be the following (see Table 19428.
A3. I .) An atternpt to develop a full precision and bias
statemeru for this A3.13 Keywords
test method will be made at a later date. For this reason, axial strain: Poisson 's ratio; transverse strain
data
16
0 D638-14
TABLE A3.1 Polsson's Ratio Baaed on One Laboratory
Maienal Extensome1er Type Average VA
8
Ve ,e
0 031
Aº
PP Copolymer 2-i)Olnt O 408 O 011
PP Copolymer 4-j)oint o 392 O 010 O 028
PP Homopolymer w,tll 20 "- Glass 2-i)Oint o 428 O 013 O 036
PPHomopolymerw1tll20%Glass 4-j)oont 0 410 001 5 0042
�. • W1lhln labora1ory standard dev,auon lo, the mdrcated matenal. 1t 1s obtamed by hrst poo&1ng the w1th-laboratory standard devia.Uons of !he tes! results from aU lhe
part.ictpat1ng taboratones
S, - {[(S,)'+(S,)'+ +(S,)')in}'ª
2 2) 112
°SR = between-laboratones reoroducibmry, expressed as standard deviaUon S R= [S, + SL
Cr- = wtthln-laboratory cnucat lnterval between two test results = 2 e >e S,
°A = between-laboratones cnucat mterval between two test results = 2 8 x SR
SUMMARY OF CHANGES
Committee D20 has identified the location of selected changes to this standard since the last issue
(0638 - 10)
that may impact the use of this standard. (December 15, 2014)
( l / Revised Note I since changes were made to ISO 527- (3) Made sorne editorial changes.
1, and it is no longer equivalen! to this standard. (4) Moved Tables 2-5 to Section 13 on Precision and Bias.
/2/ Removed pennissive language. (5) Revised Summary of Changes section.
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of lnfnngement of such nghts. are entirely the,r own responsJb1lIty
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and Jf not teveea. eIther reapproved or w1thdrawn Your comments are 1nv1ted either for rev1slon of thIs standard or for addluonal
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heanng you should
make your wews known to tne ASTM Comm,nee on Standards, at the address snown below
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°
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