Teaching Scheme:

Course – Post B.Sc. B.E. – (Textile Chemical Processing)

Programme Part: FS of Post B.Sc. B.E – I

Code Teaching Total

Subject Scheme of Teaching
No. (Hrs/week)
L T P Total Theory Practical
Paper Duration Marks Term
(Hrs) work,
viva
101 Elementary of Economics 2 - - 2 1 2 50 - 50
102 Organic Chemistry 4 - - 4 1 3 100 - 100
103 Mathematics-I 4 2 - 6 1 3 100 - 100
104* Textile Manufacture-I 2 - - 2 - - - - -
Chemical Industry &
105 4 - - 4 1 3 100 - 100
Process Calculation
106 Electrical Engineering 2 - 2 4 1 2 50 25 75
107 Technical Analysis-I - - 6 6 - - - 50 50
108 Workshop - - 4 4 - - - 50 50
Total 18 2 12 32 5 - 400 125 525

Programme Part: SS of Post B.Sc. B.E – I

Code Teaching Total

Subject Scheme of Teaching
No. (Hrs/week)
L T P Total Theory Practical
Paper Duration Marks Term
(Hrs) work,
viva
201 Mathematics–II 4 - - 4 1 3 100 - 100
202 Physical Chemistry 4 - - 4 1 3 100 - 100
Generation Transmission
203 2 - 2 4 1 2 50 25 75
of Mechanical Power
204* Textile Manufacture-II 2 - - 2 1 3 100 - 100
205 Engineering Drawing-I - - 6 6 - - - 50 50
206 Chemistry of Fibres 4 - - 4 1 3 100 - 100
207 Technical Analysis-II - - 6 6 - - - 50 50
Total 16 - 14 30 5 - 450 125 575
* The examination in the Subject Textile Manufacture-I & II will be held at End of 2nd
Semester
Programme Part: FS of Post B.Sc. B.E – II

Code Teaching Total

Subject Scheme of Teaching
No. (Hrs/week)
L T P Total Theory Practical
Paper Duration Marks Term
(Hrs) work,
viva
Chemistry of
301 4 - - 4 1 3 100 - 100
Intermediates & Dyes.
302 Engineering Drawing-II - - 6 6 1 2 50 - 50
Fluid Flow & Heat
303 4 - - 4 1 3 100 - 100
Transmission
304 Material Technology 2 - - 2 1 2 50 - 50
A) Application of Colour
305 Harmony 2 - - 2 1 2 50 - 50
B) Colour Physics
306 Technology of Dyeing - I 3 1 - 4 1 3 100 - 100
307 Technology of Printing – I 3 1 - 4 1 3 100 - 100
308 Tintorial Chemistry - - 6 6 - - - 100 100
Total 18 2 12 32 7 - 550 100 650

Programme Part: SS of Post B.Sc. B.E – II

Code Teaching Total

Subject Scheme of Teaching
No. (Hrs/week)
L T P Total Theory Practical
Paper Duration Marks Term
(Hrs) work,
viva
A) Applied Mechanics
401 4 - - 4 1 3 100 - 100
B) Strength of Materials
402 Physics 4 - - 4 1 3 100 - 100
Chemical Engineering-
403 4 - - 4 1 3 100 - 100
operations.
Technology of Bleaching-
404 2 - - 2 1 2 50 - 50
I
405 Technology of dyeing-II 3 1 - 4 1 3 100 - 100
406 Experimental Dyeing-I - - 6 6 - - - 100 100
Chemical Engineering-
407 - - 6 6 - - - 50 50
Lab.
408 Applied Mechanics Lab - - 3 3 - - - 50 50
Total 17 1 15 33 5 - 450 200 650
Programme Part: FS of Post B.Sc. B.E – III

Code Teaching Total

Subject Scheme of Teaching
No. (Hrs/week)
L T P Total Theory Practical
Paper Duration Marks Term
(Hrs) work,
viva
Chemical Process
501 2 - - 2 1 2 50 - 50
Economics
502 Industrial Management 2 - - 2 1 2 50 - 50
503 Technology of Printing-II 3 1 - 4 1 2 100 - 100
Analysis of Testing of
504 2 - - 2 1 2 50 - 50
Textile
Chemistry & Application
505 2 - - 2 1 2 50 - 50
of Textile Auxiliaries
506 Seminar - 3 - 3 - - - 50 50
507 Dye House-I - - 9 9 - - - 100 100
508 Experimental Dyeing-II - - 6 6 - - - 100 100
Instrument Method of
509 - - 6 6 - - - 100 100
Analysis
Total 11 4 21 36 5 - 300 350 650

Programme Part: SS of Post B.Sc. B.E – III

Code Teaching Total

Subject Scheme of Teaching
No. (Hrs/week)
L T P Total Theory Practical
Paper Duration Marks Term
(Hrs) work,
viva
Technology of Bleaching
601 4 - - 4 1 3 100 - 100
& Finishing-II
Instrumentation & Process
602 control chemical reaction 4 - - 4 1 3 100 - 100
Engineering
Fiber Structure & Theory
603 4 - - 4 1 3 100 - 100
of Dyeing
604 Project - - 10 10 - - - 125 125
605 Dye-House-II - - 9 9 - - - 100 100
Instrumentation & Process
606 - - 3 3 - - - 25 25
control Lab.
Total 12 - 22 34 3 - 300 250 550
 DEPARTMENT OF TEXTILE CHEMISTRY
FACULTY OF TECHNOLOGY & ENGINEERING.
THE MAHARAJA SAYAJIRAO UNIVERSITY OF BARODA.

SYLLABUS & BREAK UP OF LECTURES FOR

POST B.SC. B.E. (TEXTILE CHEMICAL PROCESSING)
1ST SEMESTER:-
THEORY.

SUBJECT: ELEMENT OF ECONOMICS (2 hours/Week)

The Subject Matter of Economics. Wants and Their Satisfaction Exchange Markets,
Demand and Supply, Prices.

The Nature of Production, Specialisation. Factors of Product Land & Labour & Capital.
Increasing & Diminishing Return. Load Wages, Interest and Profits. Competition and
Monopoly.

The Nature and Function of Money. The Forms of Money. The Banking System and
Money Market.
SUBJECT: ORGANIC CHEMISTRY (4 hours/Week)

Characteristic of the Chemical Bonds. Conjugated Bonds. Shapes of Molecules-

Conformation and Stereochemistry. Physical Properties and Molecular Structures.
Chemical Reactivity and Molecular Structure. Dynamics of Organic Reaction –
Nature of Ionic Reaction.

Reaction Energies and Equilibrium, Reaction Rates and Transition State Theory,
Laboratory Study of Reaction.

Intermediates in Organic Reaction- Their Formation, Stability Reaction.

Nucleophilic Substitution. Nucleophilic Addition. Elimination Reaction.
Electrophonic Addition at Multiple Bonds. Electrophonic Substitution in Aeromatic
Compounds. Heterocyclic Compounds. Molecular Rearrangements. Oxidation and
Reduction. Radical Reaction. Polymerization Reaction. Literature of Organic
Chemistry.
SUBJECT: MATHEMATIC- 1 (4 hours/Week)
(2 hours/Tutorial)

Logarithms, Scale, Slide Rule. Nomo grams. Fitting Of Emperical Equation to

Observed Data: - Two and Three Constants.

Determine and Solution of Equation.

Graphical Methods of Solution of Equation.

Evaluation of Derivation and Integrals.

Elementary Probability, Error and Random Sampling.

Application of Differentiation, integration, reduction Formula. Differentiation
Equation: First Order, Higher Order with Constant Co-Efficient.
SUBJECT: TEXTILE MANUFACTURING-1 (4 hours/Week)

The Cotton Fibre. Preparation of Cotton for Spinning. A Brief Survey Of Machines
Used For Performing The Operations Of Opening, Cleaning and Carding.
Preparation For and Principles Involved In Combing. Theory of Drafting and a Brief
Study of Mechanism Of Draw Frames, Speed Frames, Ring Frames And mule.

Classification of Yarns and Fabrics and Their Chief Characteristics. General Survey of
The Main Warp Preparatory Processes Employed for The Preparation Of Grey,
Mono-Colour and Stripes And Warps.
SUBJECT: CHEMICAL INDUSTRY & PROCESS CALCULATION (4 hours/Week)

Chemical Industry:-

(A) Fuels, Combustion and Utilities:-

Proximate and ultimate analysis of Coal, Calorific value, fuels. Specifications for fuel
oils, types of gaseous combustion of solid, liquid and gaseous fuels, control
combustion. Treatment of water for various industrial uses, introduction to different
utilities.

(B) Chemical Process: -

Salient features of basic chemical industry, present state of chemical industry in

India. Outlines of the manufacture of basic inorganic chemicals such as Sulphuric
Acid, Caustic, Soda, Soda Ash, Ammonia and Nitric Acid (with an emphasis raw
materials and product specifications).

Outlines of the manufacture of olefins, acetylene, and alkyl benzenes. Manufacture of
intermediates such acetaldehyde, acetic acid, acrylonitrile, ethylene oxide, phenol,
phthalic anhydride, vinyl chloride and fatty Acid.

Process Calculations:-

Systems of units, stoichiometry and composition relations. Material balances. The

use of ideal gas law and vapour Pressure solubility and heat capacity data. Humidity
and solvent recovery.

Thermo chemistry & Energy balances. Material & energy balances for a few typical
processes.
SUBJECT: ELECTRICAL ENGINEERING (2 hours/Week)

Electric currents & their effects. Ohm’s: law, resistance. Insulators, conductors, units.

Self inductance, mutual inductance, capacitance, motion of a conductor in a
magnetic field. A.C. Circuits - sinusoidal and current, R.M.S. value. Simple A.C.
Circuits containing inductance, capacitance and resistance in series. Power in
Circuits.

Three phase system of voltages and currents. Star and de - connections. Power it
three phase circuits.

D.C. Generations -principle of working, typos of generator; their characteristics.

D.C. Motors - principles of working, types of motors and the: characteristics, starting
method and speed control.

Transformer - principle of working.

A.C. Alternators - principles of working.

A.C. Motors - induction motor and syneroneus motor. Principle of working and their
special features.

Comparision of the above mentioned types of motors as regard their starting and
running characteristics, speed control, & their suitability for various drive,
Specifications of mach Electrical tariff

 Engineering Laboratory:- (3 hours/Week)

Electrical Engineering:-

Measurement of Armature and field resistance, Load tests on -transformer D.C.

Shunt motor. Induction motor. Characteristics. of D.C. Generators. A.C. Series
Circuit.
SUBJECT: TECHNICAL ANALYSIS -I (6 hours/Week)

Optics of the microscope, use of microscope for identification of fibres. Cross-

section of fibres, their preparation and examinations under the microscope.
Examination of faults. Use of Polarized Light. Photomicroscope, colour matching
with comparator and tintometer. Measurement of colour with
Spectrophotometers and colorimeters. Measurements of brightness & luster.

Analysis of water, soaps and Textile Auxiliaries. Students will be encourage to
use various instruments during the course of the above analytical Works.

,
SUBJECT: WORKSHOP (4 hours/Week)

Use and setting of hand tools commonly used in fitting, filing and carpentery.
Practice in preparing simple jobs in fitting, filing and carpentery. Use of dies for
cutting pipe threads. Jointing and fittings of pipes. Introduction to simple
machine tools Practice in simple machining operations.
 POST B.Sc. B.E. TEXTILE CHEMISTRY (1ST YEAR)
2nd SEMESTER:-
THEORY.

SUBJECT: MATHEMATICS-2 (4hours/Week)

Practical differenciation; change of variable, transformation of Laplace's Equation.

Simple, double and trible integrals, line intrigal, stoke and Gaus's theorems,
equation of heat flow.

Simple furier series with application to solution of 1 dimentional unsteady and.2
dimentional steady state of heat flow.

Statistics, standard distribution with simple applications Dimensional Analysis.
SUBJECT: PHYSICAL CHEMISTRY (4 hours/Week)

Basic concepts of heat work and energy, Equations of state, heat capacities.
Properties of thermodynamic, systems. Thermo chemistry The Laws of
thermodynamics. Statistical treatment of heat capacity and entropy Free energy and
chemical potentials. Fugacity and Activity. The equilibrium constant and free energy
charges in chemical Reaction.

Application of phase rule to 2-component and 3 - component systems. Theory of
indicator, the Measurement and control pH, electrometric methods of analysis,
strong and weak electrolytes. Debye Huckel theory.

Adsorb ion of solid surfaces. Gibb’s adsorption isotherm. Types of isotherm for
various adsorption processes. Langmuir and BET isotherm and its applications.
Catalysis and its mechanism. Technical applications of adsorption. Electrical
phenomena at interfaces.

Principles of chemical kinetics, rate equations for simple and complex reactions,
theory of reaction, rates, chain reactions He, rogeneous reactions. Photochemistry,
Lamber and Bees law: The law photochemical equivalence and its applications.
SUBJECT: GENERATION & TRANSMISSION OF MECHANICAL POWER (2 hours/Week)

Brief introduction of laws of thermodynamics. Introduction to air -cycles - otto,

diesel semidiesel, and Brayton Cycles Calculations of work done and power
generated. Representation of the cycles on P -V and T- S diagrams.

Steam engineering -Property of steam and use of steam tables. Steam power plants
and their practical modifications. Elementary description of other types of power
plants, petrol and diesel engines.

Direct energy conversion in study of fuel cells, M.H.D., thermoelectric generation
with their limitations.

Transmission of power – types of drives, group and individual drives their merits
and demerits.

Belt, Chain and gear drives. Calculations of pulley sizes and gear trains, for speed
reduction. Types of bearings - journal, ball and boiler bearings, shaft and couplings.

 Mechanical Engineering :- (Practical)

Study of petrol and diesel engines. Trial on diesel engine, Study of types of drives.
Power plant visits.
SUBJECT: TEXTILE MANUFACTURE –II (2 hours/Week)

Mechanism of plain power loom Timing of the primary and secondary motion of a
loom. A brief survey of the use of dobby and jacquard looms in the weaving of
ornamented fabrics. Fabric construction. Methods of cloth analysis. Principle base
weaves such, as plain, twill, satin, and it’s important. Derivatives, Common cloth
defects, their causes and remedies. System of counting yarns. Calculations
pertaining to warp and weft quantities for fabrics of given types. Healds and reeds
calculations.
SUBJECT: ENGINEERING DRAWING -I (6 hours/Week)

Orthographic projections, first and third angle methods of projection. Conventions A

dimensioning and different sections.

Forms and proportions of screw threads l bolts, nuts, studs, and set screws, locking
devices of nuts.

Rivets and riveted joints, welded joints.

Key shaft couplings, cotter - cotter joint. Simple bearings.
SUBJECT: CHEMISTRY OF FIBRE (4 hours/Week)

Classifications of fibres, occurrence, morphology constitution physical and chemical

properties. and use of natural and cellulosic and protein fibres, raw material
manufacturing process, physical and chemical properties and uses of regenerated
fibres, chemistry, preparation, physical and chemical properties and uses of
important synthetic fibres, important physical properties of fibres, action of various
chemicals, heat, light and micro-organisms on textile: fibres.

SR.NO NAME OF TOPIC NO. OF

LECTURE
1 Introduction to textile fibres their Classifications 02

2 Occurrence, constitutions, physical and chemical properties. and 08

uses of natural cellulosic fibres such as cotton, flax, ramie etc.,
3 Occurrence, constitutions, physical and chemical properties. and 08
uses of natural protein fibres such as wool, silk etc.,
4 Raw material and complete manufacturing process, physical and 05
chemical properties and uses of regenerated fibres such as viscose
rayon, polynosic, cellulose acetate etc..
5 Raw material and complete manufacturing processes such as 15
polymerization, spinning, drawing etc, physical and chemical
properties and uses of important synthetic fibres such as polyester,
nylon, acrylic, polypropylene, polyethylene, polyvinyl alcohol etc.
6 Action of various chemicals, heat, light and micro-organisms on 02
textile fibres.
Total 40
SUBJECT: TECHNICAL ANALYSIS-II (TEXTILE CHEMISTRY) (6hours/Week)

Analysis of chemicals such as alkalies, acids, oxidizing agents, reducing agents,

mordants, salts etc. used in textile processing.

Analysis of fibre blends, estimation of size and resins as well as other finishes on
fabrics.
 POST B.Sc. B.E. TEXTILE CHEMISTRY (2nd YEAR)
1st SEMESTER:-
THEORY.

SUBJECT: CHEMISTRY OF INTERMEDIATES & DYES (4 hours/Week)

Classification of dyes according to chemical structure a] according to application.

Systematic treatment of the chemistry of synthetic dyes. Colour and chemical
constitution. Chemical structure and substantively of dyes. Action of light on dyes
and dyed fabrics.

SR.NO NAME OF TOPIC NO. OF

LECTURE
1 Introduction to dyes, colours & pigments 02
2 Classification of dyes according to various means 04
3 Colours theories 04
4 Chemical structure & their relationships with various properties 06
5 Action of light on dyes and dyed fabrics 02

6 Properties and synthesis of intermediates and dyes of various 22

classes.
Total 40
SUBJECT: ENGINEERING DRAWING -II (6 hours/week)

Bearings and supports, Stuffing - stuffing boxes, pipes and pipe connections, valves,
measure vessel components. .such as heads and nozales, flanges etc. and methods of
attachment. Process equipment.
SUBJECT: FLUID FLOW & HEAT TRANSMISSION (4 hours/Week)

Fluid Flow: - Nature of fluids. Viscosity. Measurement of differential pressure.

Laminar and turbulent flow. Laws governing fluid flow. Characteristics of highly
viscous Newtonian and non -Newtonian materials. Methods of measurement of flow
rate of fluids. Calculation, of power required to pump fluids. Pipe fittings, pumps,
blowers, compressors and vacuum pumps. Storage and handling of Fluids.

Heat Transfer: - Mechanism of heat transfer by conduction convection and
radiation. Applications of the principle. of heat transfer -to performance of
equipment such As heat exchangers, condensers jacketed kettles and coils,
Evaporation. Refrigeration.
SUBJECT: MATERIAL TECHNOLOGY (2 hours/Week)

Mechanical properties of materials and their variation with temperature. Various

methods. Of improving the strength of materials. Failure Of materials, under service
conditions.

Heat treatment of steels. Steels in chemical industry. Polymer materials:
Elastumers'and plastomers, Polymers as substitute for metals.

Ceramic materials and retractories. Inorganic glasses and their properties.

Carbides and graphite composite materials, cement, concrete, Olay & wood.

Corrosion: Forms, mechanisms, rate factors, inhibition, prevention and testing.
Corrosion behavior of some common metals and alloys. Metallid plastic and other
protective coatings.

Factors that determine the choice of materials of construction.
SUBJECT: APPLICATION OF COLOUR HARMONY & COLOUR PHYSICS (2 hours/Week)

(A) Application of Colour Harmony:-

Decorative effect arising from technical processes on fibrous materials. Bases of

ornament. Colour effect. Harmonies and contrast. Types of patterns used for
different purposes. Distinctive features of the more important styles of ornaments.

(B) Colour Physics:

The nature of light and colour. Laws of light absorption, Spectrophotometry.

Subtractive and additive methods colour measurement. Colour specification by
trichromatic systems. CIE co-ordinates. Dominant wavelength and purification
Instruments for colour measurement. Colour tolerance and colour difference
formulae. Modern computerized methods of colour matching.
SUBJECT: TECHNOLOGY OF DYEING –I (3 hours/Week)
(1 hours/Tutorial)

History of dyeing, General Considerations of the application of different classes-of

dyes to important textile fibres.

Dyeing of natural cellulosic fibres such as cotton, line, jute with direct, basic,
reactive, sulphur, azoic, vat, solublised vat, indigo, aniline black, pigments etc. After -
treatments of dyed fibres, Dyeing of natural poteineous fibres such as a silk and
wool with acid, basic, pre-metallised acid, chrome, direct, reactive, azoic and vat
dyes, Dyeing of regenerated fibres such as viscose rayon and cuprammonium rayon
with direct, basic, sulphur, azoic, vat and solublised vat dyes, Dyeing of acetate (di
and tri-acetate) rayon with, disperse dyes, logwood black Azoic Dyes and Vat Dyes.

SR.NO NAME OF TOPIC NO. OF

LECTURES
1 History of dyeing & general Considerations of the application of 02
different classes of dyes to important textile fibres
2 Dyeing of natural cellulosic fibres such as cotton, line, jute with 14
direct, basic, reactive, sulphur, azoic, vat, solublised vat, indigo,
aniline black, pigments etc. and their after –treatment processes
3 Dyeing of natural protein fibres such as a silk and wool with acid, 10
basic, pre-metallised acid, chrome, direct, reactive, azoic and vat
dyes
4 Dyeing of regenerated cellulosic fibres such as viscose rayon and 08
cuprammonium rayon with direct, basic, sulphur, azoic, vat and
solublised vat dyes
5 Dyeing of acetate (di and tri-acetate) rayon with disperse dyes, 06
logwood black, azoic colours and vat dyes
Total 40
SUBJECT: TECHNOLOGY OF PRINTING-I (3 hours/Week)
(1 hours/Tutorial)

Preparation of Fabrics for printing, Printing procedure covering dissolving of

dyestuffs, preparation of printing paste, thickening agents etc. for printing of various
fabrics. Selection, of thickening agents and dyestuffs for printing. Formulation and
properties of printing pastes. Brief introduction to different methods of printing and
styles of printing. Methods of printing such as blocks, screen and roller printing;
Styles of printing such as direct, discharge, resist and conversion styles of printing
Printing of cotton fibres with direct, basic, sulphur, mordant aniline black, pigment
and azoic colours in different styles.

SR.NO NAME OF TOPIC NO. OF

LECTURE
1 Preparation of fabrics for printing 02

2 Ingredients of printing (including thickeners) and preparation of 08

printing paste
3 Introduction to different styles of printing such as direct, discharge, 03
resist, conversion etc.
4 Methods of printing such as blocks, stencil, screen and roller 03
printing.
5 Printing of cotton fibres with direct, basic, sulphur, mordant, aniline 24
black, pigment and azoic colours in different styles.
Total 40

Practical: - PRACTICAL WILL COVER THE ABOVE SYLLABUS.

.
SUBJECT: TINTORIAL CHEMISTRY

Identification and estimation of intermediates and dyes in substance.

 POST B.Sc. B.E. TEXTILE CHEMISTRY (2nd YEAR)
2nd SEMESTER:-
THEORY.

SUBJECT: APPLIED MECHANICS & STRENGTH OF MATERIALS (4 hours/Week)

(A) Applied Mechanics: - Equilibrium of Rigid Bodies : equations of equilibrium, F.B.

Diagram technique, application to simple problems, solution of trusses. Friction: laws of
friction, co-efficient of static and dynamic. friction, application to only statics problems like,
bedges, brackets, brakes, ropes, inclined Plaines t screw jacks etc.,Properties of area:
Centroids and moments of inertia and simple and composite elements. Graphics. Graphical
methods employed to solve problems listed above; simple lifting machines M.A., V.R., and
efficiency of simple machines like, pulley blocks, inclined planes, screw jacks, Crabs, worm
wheel, law of a machine.

(B) Strength of Material:- Simple stress - strain theory. Study of tension. Compression,
impact, hardness test aroltfer mechanical properties as creep, fatigue only descriptive
treatment. - Factor of safety. Relation between elastic constants. - B.M.:AS.F. Diagrams
Importance, sign convention, diagrams for simple loading, relation -between the quantities
Theory of simple bending. Distribution of direct stresses. Eccentric loading. Deflection of
beams only simple cases.

Torsion of circular shafts. Stresses in shafts transmitting power. Columns and struts,
Statement of Eulor's and Rankin’s empirial formulas.

Welded joints. Thin cylinders subjected to pressure. Thick cylinders Lame's formulae
without derivation. Pressure vessel components - shell, head & nozzles. Stresses due to
internal pressure.
SUBJECT: PHYSICS (4 hours/week)

(1) Introduction to Quantam Mechanies:-

Dual aspects of light, dual aspects of matter,De Broglie's hypothesis, experimental

verification of the hypothesis , Schrödinger’s equation for the hydrogen atom and its
solution, Behr’s discrete energy states for the hydrogen atom, quantum numbers. N,
1 and m, atomic Orbital. And their description, Heisenberg's uncertainty principle
and probability interpretation of wave functions, practice in box problem in
quantum m/c.

(2) Molecular and Valence (Quantam Mechanical Treatment):-

Molecular formation and chemical bond, molecular orbital and valence bond
approaches, Quantam mechanical description Of the H 2 ion and H 2 molecule.

Quantam mechanical characteristics of the covalent bond, localized bonds, hybird
orbital. Directed valence and saturation property of valence.

Electronic Structure of Conjugated Systems:-

The Huckel approximation, application to the butadience molecule, charge density,

'bond orders, Polarizabilities, bond lengths, delocalization energies, spin densities
and effects of substitution on spin densities

(3).Interatomatic And Intermolecular Forces: -

Types of such forces and their origin. Classification of solids according to the type of
force binding the constituents

403. Chemical Engineering Operations :- (4 Hours/week)

Definition of unit operations. Size reduction and analysis. Mixing, Selection of

agitators Filtration .and centrifugining. Distillation. Absorption. Types of columns
and their Performance characteristics. Extraction. Adsorption. Humidification and
dehumidification. Drying Crystallization.
SUBJECT: TECHNOLOGY OF BLEACHING –I (2 hours/week)

Removal of natural and added impurities from vegetables, and animal fibres, and,
fabrics sizing, desizing, scouring and bleaching of cotton, Different types of
bleaching agents and optimum conditions for various operations Impurities in wool
and process for their removal, scouring, carbonizing and bleaching Of wool
Machinery for bleaching in loose state, package from as well as batch and
Continuous handling of .fabrics.

SR.NO NAME OF TOPIC NO. OF

LECTURE
1 Preparatory & pretreatment processes such as sizing, desizing, 10
scouring, bleaching, degumming, decatising and souring of natural
fibres such as cotton, wool, silk, jute, ramie, flax etc..
2 Different types of bleaching agents such as hydrogen peroxide, 07
hypochlorite, sodium chlorite, per acetic acid etc, and their optimum
conditions for various operations
3 Machinery for bleaching for different forms of fibres 03
Total 20
SUBJECT: TECHNOLOGY OF DYEING- II (3 hours/Week)
(1 hours/Tutorial)

Development of machines for dyeing textile fibres in various forms such as raw
stock, silver, yarn, fabric etc. Dyeing of polyamide fibres with disperser, acid
chrome, premetallised, basic, direct, reactive, azoic, vat dyes, Dyeing of polyester,
fibres with disperse dyes. Dyeing of texturised fabrics. Dyeing of acrylic fibres.
Dyeing of union and blended fibre fabrics Sequence of processing with flow sheet
for important types of man-made fabrics. Recent developments in dyeing processes
and dyeing machineries. Economy and energy dyeing in dye-house. Maintenance of
dyeing machinery.

SR.NO NAME OF TOPIC NO. OF

LECTURE
1 Development of machines for dyeing textile fibres in various forms 10
such as raw stock, silver, yarn, fabric etc
2 Dyeing of polyamide fibres with disperse, acid chrome, 06
premetallised, basic, direct, reactive, azoic, vat dyes
3 Dyeing of polyester & acrylic fibres with various dyes 10
4 Dyeing of union and blended fibre fabrics 06

5 Sequence of processing with flow sheet for important types of man- 02

made fabrics.
6 Recent developments in dyeing processes and dyeing machineries. 04
7 Economy and energy in dye-house & maintenance of dyeing 02
machineries
Total 40
SUBJECT: EXPERIMENTAL DYEING –I (3 hours/week)

Application of different classes of dyes to all types of textile fibers of assistants

mordants etc. in dyeing. After -treatment of dyed textiles. Dyeing of union fabrics.
Evaluation by comparative dye trials.

 Practical: - will cover the Tech. of Dyeing-I and Dyeing-II

SUBJECT: CHEMICAL ENGINEERING LABORATORY (6 hours/week)

Flow through pipes, coils and fittings. Orifice and venture meters, rotameters. Plate
and frame, rotary, Sweetland and Sparkler filters, Compressors and blow pumps.
Heat transfer from steam to water. And steam to air in tubular and plate heat
exchangers and in condensers. Evaporators. Differencing and steam distillation;
fractional distillation. Drying characteristics, Gas absorption and liquid extraction.
Study of agitated vessels.
SUBJECT: APPLIED MECHANICS LABORATORY (3 hours/week)

Experiments will be based on the theory done in the class.

 POST B.Sc. B.E. TEXTILE CHEMISTRY (3rd YEAR)
1st SEMESTER:-
THEORY.

SUBJECT: CHEMICAL PROCESS ECONOMICS (2 hours/Week)

Factors involved in project cost estimation, methods employed for the estimation of
capital investment. Capital formation. Elements of cost acoounting.Interest and
investment costs, time value of money equivalence. Depreciation methods of
determining depreciation, taxes, some aspects of marketing, pricing policy,
Profitability criteria, economics of. Selecting alternatives. Variation of cost with
capacity, break' even point, Optimum batch sizes, production scheduling etc.
SUBJECT: INDUSTRIAL MANAGEMENT (2 hours/week)

Concept of scientific management in Industry Functions of management, decision

making, planning, organizing, direct-and control. Location of Industry. Materials
management. Inventory control. Management of human resources, selection.
Incentives welfare and safety.
SUBJECT: TECHNOLOGY OF PRINTING –II (3 hours/Week)
(1 hours/Tutorial)

Printing of Indigo, Vat dyes, Indigosols, Reactive, Rapid- fast, Rapidogen, Rapidozols
etc., on cotton in different styles. Pigment printing, Machines used for printing,
Steaming and other methods of print development, after treatment of printing
material, Faults in printing and their prevention and correction. Printing of acetate
rayon, polyester .and. polyacrylic types of fibres with selected types of dyes. Printing
process such as Roller screen, Rotary, Speakled, Foam, Polychromatic and transfer
printing. Printing of blended fabrics, including burn –out, batik and other newly
developed styles of printing. Preparation screen for printing, printing of velvet good.
Carpet printing, Economy in the printing of Textiles.

SR.NO NAME OF TOPIC NO. OF

LECTURE
1 Printing of indigo, vat, Indigosols, reactive, rapid fast, Rapidogen, 16
and Rapidozols dyes on cotton fabric in different styles
2 Pigment printing 02

3 Machines used for printing, steaming, other development 06

procedures and after treatment of printing material
4 Faults in printing and their prevention and correction 01

5 Printing of acetate rayon, polyester and polyacrylic types of fibres 06

with selected dyes
6 Printing process such as Roller screen, Rotary, Speakled, Foam, 04
Polychromatic and transfer printing
7 Printing of blended fabrics, including burn out, batik and other 03
newly developed styles of printing
8 Preparation screen for printing, printing of velvet good, carpet 02
printing and economy in the printing of textiles
Total 40
SUBJECT: ANALYSIS AND TESTING OF TEXTILES (2 hours/week)

Objects of Testing, Testing of raw materials and finished products, Process control,
various specifications, Sampling and statistical analysis of the results, Control on
conditions of testing, Qualitative and quantative analysis of fibres in textiles,
Determination of physical properties such as density, permeability, moisture regain,
abrasion resistance, breaking, bursting and tear strengths,.thermomel insulation
value, shrinkage of textiles etc.

Estimation of size content, wax content, non cellulosic matter, whiteners,
absorbency at various stages of cotton processing, Assessment-of degradation of
textiles during processing, Testing of dye printed materials for fastness to light,
washing, crocking, perspiration, rubbing , sublimation etc.

Analysis of resin finished materials for add-on, nitrogen contents, formaldehyde-
content, wrinkle recovery angle, durable press finished, chlorine retention, soil
release, soil redeposition etc. pilling resistance, flame resistance, glow resistance,
resistance 'to attack by micro-organisms. Special test for woolens, synthetic fibre
materials and Knitted textiles.

SR.NO NAME OF TOPIC NO. OF

LECTURE
1 Objects of testing, and quality control of incoming materials 02
2 Process control & quality control of pretreatment processes 03
3 Process control & quality control of dyeing & printing processes 05
4 Process control & quality control of finishing processes 04
5 Qualitative and quantative analysis of fibres in textiles. 04
6 Determination of physical properties such as density, permeability, 06
moisture regain, abrasion resistance, breaking, bursting and tear
strengths, thermoses insulation value, shrinkage of textile fibres
7 Assessment-of degradation of textiles during processing. 02
8 Testing of dyed & printed materials for various fastness properties 05
9 Analysis of resin finished materials for add-on, nitrogen contents, 07
formaldehyde-content, wrinkle recovery angle, durable press
finished, chlorine retention, soil release, soil redeposit ion, pilling
resistance, flame resistance, glow resistance, resistance to attack by
micro-organisms etc.
10 Special test for woolens and synthetic fibres knitted textiles 02
Total 40
SUBJECT: INSTRUMENTAL METHOD OF ANALYSIS (IMA) (6 hours/Week)

Measurement of fastness properties of dyed material as Light Fast Washing

Fastness, Sublimation Fastness, Perspiration. Fastness Colour measurement by
Speotrophotometrio Method. Blend Analysis. Measurement of dyes impurities by
Chromatographic methods. Spectrophotometric Method Measurement of pH of
dyeing system. Dye analysis by Conduotometric method Potantiometric Method.
Polographic Met Computer colours Matching. Crease Recovery Angle Etc.
SUBJECT: CHEMISTRY & APPLICATION OF TEXTILE AUXILIARIES (2 hours/Week)

Nomenclature, Functions and Classification of textile auxiliaries such as, wetting

agents, detergents, protective colloids, leveling agents, dye fixing agents, proofing
agents etc., used in textile processing, Surface active non surface active auxiliaries.
The ionic nature of these auxiliaries such as anionic, cationic, nonionic and
amphoteria. Preparation and chemistry of these products Chemistry of textile
auxiliaries qualitative and quantitative evaluation of auxiliaries.

SR.NO NAME OF TOPIC NO. OF

LECTURE
1 Nomenclature, characteristics, functions and classification of textile 04
auxiliaries
2 Surface active & non surface active auxiliaries. 02
3 The ionic nature of these auxiliaries such as anionic, cationic, 08
nonionic and amphoteric, their preparation, characteristics & uses
4 Qualitative and quantitative evaluation of auxiliaries 06
Total 20
SUBJECT: Seminar (3 hours/Week)

Every student will be required to prepare critical review on an advanced topic

assigned to him and submit it in the foam of a standard typed report. The student
will also be required to make an oral presentation of the review.
SUBJECT: DYE HOUSE – I (9 hours/week)

Singeing, Desizing, Scouring and Bleaching of cotton. Bleaching of coloured goods.

Mercerization of yarn and cloth. Dyeing of loose cotton, cheeses, hanks and fabric in
different' machines. Single and multi coloured printing. Printing with different
Styles. Finishing of textiles to obtain different effects .including crease-resistance,
water-repellency, flame-repellency, modification of feel, luster, softness etc.
SUBJECT: EXPERIMENTAL DYEING – II (9 hours/week)

Matching of compound shades. Identification of fibres & dyes on fibres.

Determinations of fastness of dyeing and prints.
 POST B.Sc. B.E. TEXTILE CHEMISTRY (3rd YEAR)
2nd SEMESTER:-
THEORY.

SUBJECT: TECHNOLOGY OF BLEACHING & FINISHING –II (4 hours/week)

Scouring and bleaching of man-made fibres fabrics Scouring and bleaching of

blended fibre fabrics. Thermosetting of synthetic fibre fabrics.

Temporary and durable, mechanical and chemical, conventional and special finishes,
Finishing Agents like stiffeners, binders, weighting agents, softeners, optical
brighteners etc, Machines used for finishing shearing, cropping, opening, damping,
calendering etc„ drying of textile materials Physical and chemical aspects of
mercerization of cotton; Determination of efficiency of mercerization and factors
affecting it, machinery used for mercerizing of blended fibre fabrics, Other finished
based on. Swelling of cotton Anti-shrink finishes Finishes for importing wrinkle
resistance wash and wear and durable-press properties of fabrics, soil release
finishes, finishes based non coating, laminating finishes for improving the resistance
of textile fabric to fibre, micro-organism-weathering etc.

Water proofing and water repellent finishes, anti felting and other finishes for wool
chemical Modification and grafting of textiles. Finishes of Blended fibre fabrics.

SR.NO NAME OF TOPIC NO. OF

LECTURE
1 Scouring and bleaching of man-made fibres & their blends. 10
Thermosetting of synthetic fibres
2 Temporary and durable, mechanical and chemical, conventional and 03
special finishes.
3 Finishing agents like stiffeners, binders, weighting agents, soil 04
release, softeners, optical brighteners etc,
4 Machines used for shearing, cropping, opening, damping, 04
calendaring, drying of textile materials
5 Physical and chemical aspects of mercerization of cotton. 06
Determination of efficiency of mercerization and factors affecting it,
machineries used for mercerization
6 Special finishing treatment like swelling of cotton, anti-shrink 04
finishes, finishes for importing wrinkle resistance, wash and wear
and durable-press properties of fabrics
7 Finishes based on coating, laminating for improving the resistance 02
of textile fabric to micro-organism & weathering
8 Water proofing and water repellent finishes, anti felting and other 04
finishes for wool. Chemical modification and grafting of textiles
9 Finishes of blended fibre fabrics. 03
Total 40
SUBJECT: INSTRUMENTATION & PROCESS CONTROL CHEMICAL REACTION
ENGINEERING (4 hours/week)

 Instrumentation & Process Control :-

Control loop and its components. Instruments for measurement of typical -process
control variable such as, temperature, pressure, level, flow etc., Static characteristics
of measuring instruments. Transmission, indication and record of process variables.

Characteristic, of on-off, proportional, integral and derivative modes of control.
Working mechanism of typical tneumatic and electronic controller. Control valve
selection. Dynamic behavior of processes showing capacity lag, transfer lag and
distance -velocity lag.

Closed - loop performance of feedback systems and choice of controller settings.
Control system. Structure with typical example.

 Chemical Reaction Engineering :-

Classification of industrial reactors. Kinetic interpretation of experimental data
using batch and flow reactors for homogeneous, reactions. Conversion and yield
Comparision in reactors. Heat effects in batch and back mix reactors. Choice of
temperature program. Influence of physical factors on hyferogenous reaction
rates with emphasis on reactor scale -up considerations for fluid -fluid and fluid -
fluid -solid systems.
SUBJECT: FIBRE STRUCTURE & THEORY OF DYEING (4 hours/Week)

Fine structure of various fibres, Determination of crystalline and non -crystalline

regions and orientation of fibres, important physical methods for investigating
fibre structure important characteristics in a polymer to make it fibre foaming,
Fibre structure related to spinning and drawing of man-made fibres,
Determination of molecular weight of textile fibres, swelling and solublisation of
fibres. Relation of fibre structure of important physical properties of fibres such
as density, moisture regains elasticity etc.

Physical chemistry of dyeing important textile fibres, factors affecting
equilibrium absorption and kinetics of dyeing, nature of absorption, isotherms,
affinity of dyes, heat of dyeing, entropy changes during dyeing and nature of dye
fibre bonds.

SR.NO NAME OF TOPIC NO. OF

LECTURE
1 Fine structure of various textile fibres. 04
2 Determination of crystalline and non crystalline regions and 05
orientation of fibres
3 Important physical methods for investigating fibre structure 02
4 Important characteristics in a polymer to make it fibre foaming 02
5 Fibre structure related to spinning and drawing of man-made fibres 02
6 Determination of molecular weight of textile fibres, swelling and 04
solublisation of fibres
7 Relation of fibre structure to important physical properties such as 04
density, moisture regains, elasticity etc.
8 Physical chemistry of dyeing of important textile fibres & factors 10
affecting equilibrium absorption and kinetics of dyeing.
9 Nature of absorption isotherms, affinity of dyes, heat of dyeing & 07
entropy of dyeing
Total 40
SUBJECT: PROJECT WORK AND ORAL (6 hours/Week)

Every student will be required to submit the project report in a typed standard form
on a topic set by one or more teachers. The object of the project work is to test the
ability of the student to tackle and investigational problem in his field of
specialization. Every student will be oral examined in the subject incorporated in his
project report.
SUBJECT: DYE HOUSE-II (9 hours/Week)

Dye-House Syllabus of Semester-V to be continued (Page NO.11& Sr.No.7)

SUBJECT: INSTRUMENTATION & PROCESS CONTROL LAB (3 hours/Week)

Experiments based on theory done in the class.

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