Professional Documents
Culture Documents
A
Training Report
On
Fabric Wet Processing Machine & Process
(MI industries Private Limited , Aligarh Uttar Pradesh)
Preface
Training in business organization infuses among students a sense of critical analysis of the
real managerial situation to which they are exposed. My institution has given me opportunity
through this program to be aware of and cope with fast rate changing technology,
management policies, quality and productivity. This is a bold attempt to bridge the gap
between the “world of work” and “studies imparted in the institution”.
This training enable us to apply theoretical knowledge to practical situations, appreciate the
sense of responsibility, importance of discipline, punctuality and the psychology of a worker
and their habits which make us more professional and near to the world of technology and
team work. Industrial training bring out better citizens, better technocrats and better
diplomats out of us.
We were lucky to get an opportunity to work in one of the premier private sector industries,
i.e. MI INDUSTRIES PVT LIMITED ALIGARH The purpose of this training is to gain knowledge
about the industry, methodology, procedures, norms, and also to see the environment of the
industry. I have also focused during the training period on learning about machineries
installed, processing, mechanism and construction of processing devices. We have attempted
to describe both the mechanical and process parameters, as well as the underlying chemistry
behind each process. The major focus in describing the underlying chemistry is the
fiber/chemical interaction; however, where possible, I have provided a brief review of the
appropriate chemistry behind the various classes of chemical auxiliaries. Each part of the
book is subdivided into a part that describes equipment and a part that describes unit
operations. Some attempt is made to describe the stages in sequence, one that a typical
greige fabric may follow. Each dye house has its own character, depending largely on the type
of equipment and type of fabric it processes.
Fabric preparation has been subdivided into singeing, desizing, scouring, bleaching,
mercerizing, and heat setting. Further dyeing of fabric is covered with optimum parameters.
Finishing is broken down into chemical and mechanical. Chemical finishing covers those
treatments that alter the performance of the textile fabric where the chemical is the major
component of the change. Mechanical finishing refers to certain types of mechanical devices
that physically alters the fabric.
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Acknowledgement
We extend our heartfelt gratitude to MI INDUSTRIES PVT LIMITED ALIGARH for recruiting us
in this illustrious Summer Training Program. I Have worked in the concern of 45 days and
prepared my industrial training Report. Under the guidance of training officers, I analyzed
various aspects of Production. This has helped in boosting up my confidence and
determination, Which will help me to face any situation in years to come. FOUR WEEKS
(28Days) training was a great venture where we were reincarnated as a technical Novice. We
were really thankful to all the staff members and working hands in the mill who helped us
generously and assisted us through every bottleneck Guiding us to attain a dexterous
knowledge in textile dyeing sector.We also feel sincere and earnest appreciation for valued
supervision and Guidance from:
Moreover, we thank Mr. Aditya Prakash to be supportive and nurturing throughout the
training
program.
We finally thank you Mr. ASHUTOSH SHUKLA(Unit Head) for helping us during the whole
journey.
INTRODUCTION
Context
Departments.
1. Grey fabric
2. Bleaching
Singeing
Desizing
Scouring
Bleaching
3.Mercerization
4.Dyeing
5.Finishing
6.Dyeing Lab
7.Physical lab.
MI INDUSTRIES CERTIFICATION
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SINGEING OPERATIONS
Key Features :
Applicable for different types of fabric.
Sequencing unit.
Automatic flame width adjustment.
Four singeing positions, centreing devices, flat rollers,
counter rotating scroll rolls.
Double-jet burner.
Complete PLC machine with chemical dosing.
Comes with an optical scanning device
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DESIZING UNIT
Object Of Desizing:
To process to remove the size material applied in weaving section and increase the
absorbency power of the fabric is called resizing.
1.Fabric inlet section- grey fabric are directly feed into the inlet of singeing machine
where the fabric is passed over some free roller guider and expended to ensure open
width with entry here there is a controller pannel to control fabric speed.
2.Cleaning unit -1: fabric passed in cleaning unit fabric cleaned by brusher .
3.Singeing unit:after passing cleaning unit then fabric comes into contect of flame for
4.Cleaning unit 2: after singeing unit then fabric comes into brushing for cleaning .
5.Desizing unit: finally the fabric is passed thow desizing unit it’s content dezinging
liqour for desizing wetting agent squesting agent enzyme acetic acid is required.
After desizing fabric comes into batching unit & rotation for 8-12 hour.
Wetting agent: it is use to increase the wettibility of textile Substrate & dye in water is
easy to penitration and obtain smooth Paste.
Sequesting: It is used to minimize the impact of hardness of the Water.
Soaping agent: it is used to antifomic agent and increase the penetration of wetting
agent.
TEGEWA solution is also used for the identification of starch. For making this solution
potassium iodide 10 g of KI (100%) in 100 ml of water is added with 0.6358 g of iodine
(100%) and shake this well to disslove iodine crystals. Then make it up to 800 ml using
distilled water and finally make it up to 1000 ml with ethanol.
Classification of Enzyme :
Fabric speed
Concentration.
BLEACHING OPERATIONS:
Object:
Removal of coloured impurities.
Removal of the seed coats.
Minimum tendering of fibre.
Technically reliable & simple mode of operation.
Low chemical & energy consumption.
Increasing the degree of whiteness.
To increase dye affinity.
To ensure level dyeing property.
To make the fabric suitable for the next subsequent process.
Key Features
Machine section:
1.Batch Section.
2.J-scray
3.Pre Washing Section
4.Steamer
5.Post Washing Section
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LOT
INLET J SCREW
BREAK ROLLER
PRE WASHER
APPLICATOR
PRE ZENTAL
STREAMER
POST WASHER
ACID TANK
VDR
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J SCREW
BATCH
Inlet J-Scray:- It is to collect the fabric during batch changing to avoid machine
Stoppage by using tensioner roller, pressure roller and compensator.
Washer:
To Wash Of The Starch & Other Impurities From Desized Fabric By Using Hot Water.
Bleaching Steamer:
Steamer is an important process in every Pretreatment process.
Steam allows fast energy transfer directly into fibre.
During the bleaching process it is necessary to expose the fabric to sensitive but effective
treatment.
We satisfy the need of a successful process cycle by means of machine technology that offers a
safe guiding of material, which is adapted to the fabric and which is essential in the application
of chemical, the steam conditioning and the dosing technology.
Our bleaching range perform the bleaching process in optimum conditions that guarantee a
fabric of corresponding degree of whiteness and high degree of absorbency.
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PROPERTIES:
Inlet section with inclined cloth guiding.
Middle section with vertical cloth guiding.
Drive via perforated pulling roll and pendulum compensator.
Spray nozzle for cleaning and rapid cool down.
Housing in self supporting segment construction mode.
Temperature control through cloud control.
Guiding roller in high quality execution with a high concentricity.
Minimal cloth tension due to frequency controlled drives.
Prevention of creases by small distances between the guide rollers. (1000mm)
CONCEPT
Bleaching steamer consist of section with tight strand fabric guiding and roller bed.
In tight strand section the fabric which has been impregnated with the bleaching liquor is
heated up as the requirements and on roller bed we maintain sufficient dwelling time for
reaction purpose.
Brief specifications
Dwelling suction pulling device, plaiter, reversing drum for planting on roller bed.
Roller bed with driven pulling rollers
Exist section with sensible blade.
By pass device for the roller bed.
Technical data
Field of application
Bleaching liquor application in font of the Steamer in the pretreatment range.
Dye liquor /Chemical application in front of steamer in dyeing range .
Cold bleaching.
Technical Data
Outlet unit: To collect the fabric during batch change to avoid machine stoppage
And provide perfect out batch of fabric without any crease.
About H2O2
Hydrogen peroxide is a clear colorless liquid miscible with water at available in various
strength,from 3 to 90℅ . The strength of commercial solution is generally express in term of
The Volume of oxygen which they are capable off yielding. 10 volume being equivalent to 3.04
℅ Hydrogen Peroxide.
Assay :
The sample is diluted with sufficient water to get a one volume solution. A solution of 2gm of
potassium iodide in 200 ml of water is mixed with 30 ml of sulphuric acid ( 1:2) and the mixture
cooled. After which 10 ml of the diluted peroxide solution is slowly run in and the flask allowed
to stand for about 5 minutes to complete the reaction. The iodine liberated is titrated with 0.1
N sodium thiosulphate using starch indicator.
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Reaction:
2nd method
The assays may also be carried out by titration with potassium permanganate. 10ml of the
diluted peroxide solution is added and the mixture titrated with 0.1 N KMnO4.
Reaction:
Acidity:
25 ml of the diluted solution is titrated with 0 . 05 N sodium Hydroxide using
phenolphthalein indicatot.
The acidity of commercial sample should not exceed 1.5 ℅ expressed as sulphuric
acid.
caustic soda is in the form of lumps,pellets stick chips etc. it rapidly abzorb water
and carbon dioxide from and Is very corrosive to animal and vegetable tissues.
Assays:
About 4g of the sample, accurately weighed, is dissolve in carbon dioxide free
distilled water, and made up to 1liter . A 50 ml aliquot is titrated with 0.1N
Hydrochloric acid first in the presence of phenolphthalein till the pink colour is
discharge and then in the presence of methyl orange till an orange tint is
produced.
Reaction :-
NaOH + HCl -----------NaCl + H2O
Hydrogen Peroxide
Sodium Hydroxide
Wetting Agent
Sequestering agent
Stabilizers
H2O2 is an oxidizing agent which is used largely for cellulose fibre bleaching.
H2O2 is also used for protein fibre such as wool, silk-bleaching etc. In H2O2
bleaching, H2O2 releases hydrogen ion (H+) and per hydroxyl ion (HO2-). Here, PH
level is maintained 10.7 – 10.9.
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Per hydroxyl ion is released for alkalinity of hydrogen per-oxide solution. This per
ion bleached the textile materials. H+ ion has no bleaching action. It maintains PH
level.
(HO2-) + Colored materials = Bleached materials + H+
H2O2 is normally unstable, moreover Cu, Ni, Fe, etc. catalyst decomposes H2O2
and produces H2O and O2.
2H2O2 + Catalyst → 2H2O + O2
The produced O2 has no bleaching action. So, bleaching ability can be reduced if
water contain Cu, Ni, Fe, etc ion, then H2O2 catalytically decomposes and reduces
bleaching ability. So, all the above matters should be considered in H2O2
bleaching.
.Acetic Acid
Acetic acid is a colorless and corrosive liquid with pungent smell of its own. It is
miscible with water, alcohol and ether in all proportions. Acetic acid is used in
garment industry for dyeing purposes.
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Citric Acid
Citric acid is in the form of colorless, translucent crystals or a white granular to
fine crystalline powder. It is used as sequestering agent, as mordanting agent in
dyeing and cleansing agent for boiler water.
Formic Acid
Formic acid is a colorless and pungent smelling mobile liquid. It is miscible with
water, alcohol and ether in all proportions. It acts both as an acid and as reducing
agent due to presence of both carboxylic and aldehyde group. Formic acid is used
in dyeing wool and cotton fabrics.
Sodium Silicate
Liquid alkaline Sodium silicate is mostly used in garment industry as a fixing agent
and for rendering the garments fire proof.
Common Salt
It is used as to exhaust dyeing with direct and reactive dyes.
Magnesium Chloride
It is a colorless, crystalline deliquescent substance soluble in water. It is used in
textile and garment industry for sizing, dressing and filling of cotton and woollen
fabrics, for thread lubrication or carbonization of wool.
Tatar- Emetic
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Zinc Chloride
It is a white deliquescent solid exceedingly soluble in water. The concentrated
aqueous solution of zinc chloride dissolves cellulose.
Bleaching Powder
It is hypochlorite of calcium and sodium. Bleaching powder on treatment with
small quantities of dilute acid liberates hyopchlorous acid, which can easliy
furnish nascent oxygen and thus acts as an oxidizing and bleaching agent. It is
used for the following purposes:
Potassium Chromate
Potassium chromate is available in the form of lemon yellow crystals with no
water of crystallization. In garment industry it is used as a mordant.
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Potassium Dichromate
It is available in the form of orange red crystals. It is soluble in water. In neutral or
acidic solution, potassium dichromate furnishes nascent oxygen and thus acts as
an excellent oxidizing agent. It is used in garment industry as an oxidizing agent
and as mordant in dyeing.
Potassium Permanganate
It acts as a powerful oxidising agent in neutral, alkaline or acidic solution and
hence used in the garment industry as an oxidising agent.
. Sodium Perborate
Sodium perborate is mainly used as a bleaching agent for a variety of fabrics
namely wool, cotton, rayon, linen etc. It is also used as an oxidising agent and dye
fixing agent.
Sodium Hypochlorite
Sodium hypochlorite liberates hypochlorous acid and thus acts as a powerful
oxidizing and bleaching agent. It is used in textile and garment industry for
bleaching process.
Sodium Hydrosulfite
It is used as reducing and bleaching agent in garment and textile industry.
Sodium Metabisulfite
On heating, it decomposes into sodium bisulfite and sulfur dioxide and hence it is
an important reducing agent. It is used as an antichlor after bleaching garments
with chlorine.
Sodium Sulfite
It forms colorless crystals very soluble in water. It is decomposed by dilute
mineral acids with the evolution of sulfur dioxide. It is used as mild bleaching
agent for silk and woollen fabrics and as an antichlor after chlorine bleach.
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Sodium Sulfide
Its aqueous solution shows and alkaline reaction due to hydrolysis. It is used for
manufacture of sulfur dyes and as reducing agent in garment industry.
. Sodium Thiosulfate
It is also know as hypo. It is a colorless, crystalline and efflorescent substance. It is
used as an antichlor after bleaching garments with chlorine.
Dextrin
It is a modified starch prepared by heat treatment of starch in the dry state, with
or without the addition of small quantities of chemicals. It is a white powder, and
finds extensive use as sizing and finishing agent.
Glucose
It acts as a strong and cheap reducing agent in garment industry.
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The drop in concentration of the dye in the treating solution can then be found
out colorimetrically and the amount of carboxyl groups present in the cellulose
can be calculated in terms of milliequivalent/100 g of dry cellulose. For this
purpose pure methylene blue is required.
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In this study first of all, a calibration curve is obtained with the known
concentration of methylene blue solutions ( 2-16 mg/litre with increment of 2
mg/litre). The curve will be between absorbance and known concentrations of
methylene blue solutions.
After plotting the curve, in the second step, the concentration of methylene blue
solution left after treatment of cellulose is determined using colorimeter. The
concentration of the dye in a solution to be estimated by finding out the
absorbance of a solution at 620 nm wavelength. Following reagents are used in
this study:
When cellulose is bleached i.e oxidised and hydrolysed by treatment with mineral
acid solution , reducing groups are formed. These reducing groups are capable of
reducing an alkaline solution of copper sulphate, when insoluble cuprous oxide is
formed is proportional to the amount of the reducing groups present in the
cellulose sample. This is expressed in terms of Copper Number, which is defined
as a gram of cupric copper reducing to cuprous oxide by 100g of the cellulose
sample under standard conditions of boiling in an alkaline medium.
Take 0.25g of the dry sample in dry test tube in triplicate. For highly
degraded sample, 0.125g of sample may be taken
Mix solution A and B in the ratio of 5:95 and boiled. Take 15 ml of this
solution and add to all the tree test tube. Now each test tube will have
cellulose sample and 15ml of mixture of solutions.
Mouth of these tubes closed using glass stopper and placed in the boiling
water bath. Along with these three test tubes, also placed three blank test
tubes (only contain solution, No sample) in the boiling water bath. Boiling
continue for three hours.
Cooled above test tubes and content of each test tube filter using Gooch
crucible (Sinterd glass, AG3) and washed with distilled water (now the
colour of solution become red).
The residue in the crucible also treated with first 10 ml and then 5 ml
ferric alum solution (Solution C). The residue also washed with
successively with 10 ml and 5 ml 2N sulphuric acid. All these process are
carried out on each test tube.
The solution so collected is titrated against N/100 ceric sulphate
(Solution-D) using a few drop of ortho-ferrus phenathroline indicator (the
initial red colour of the solution turns Green at the end point).
The blank alkaline copper solution gives a reading of 0.02 ml of N/100
ceric sulphate solution. This blank reading is subtracted from the actual
reading in each case, where the cellulosic sample is treated.
The copper number is calculated from the amount of ceric sulphate
solution consumed (after deducting blank reading) by ferrous sulphate
formed by the reduction of ferric sulphate sulphate by cuprous oxide
deposited on the cellulosic sample during the three hours of boiling.
Where V is the titration reading (ceric sulphate solution) after deducting the blank
reading, N is the normality of ceric sulphate solution and W is the weight of the
bone dry cellulosic sample.
Some Parameters checking on CBR machine
MERCERIZATION
Types of Mercerization
There are different types of mercerization processes is used in
textile for cotton processing.
Chainless mercerization
This method is called roller mercerization. The machine consists
of several stainless rollers and rubber rollers, relatively large in
diameter, tiered zigzags in close contact with each other inside
long holes, designed for immersion in alkaline solutions of
mercerization with low levels. Bound to a limited length of this
type of fabric. Alkaline penetration and fabric swelling in these
early stages, similar devices are used to remove most of the
alkali and to use an open-width soaping machine for further
removal and neutralization.
Chain mercerization
To compensate for the defects of the roller mercerizing
machine, a clip stenter is used for the post-mercerization
treatment after massaging the stenter, where the widthwise
tension is applied but most of the alkali is removed from the
fabric placed on top of the stenter, then the whole alkali is
removed and an open width washing machine is used for
neutralization.
Cold mercerization
The mercerization process takes place at 15 to 18°C with 31 to
35% caustic soda solution with a dwelling time of 50 seconds.
At this stage, cotton swells best but also swells. Fast swelling
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Hot mercerization
The mercerization process takes place at higher temperatures
with 30 to 38 % caustic soda solution, with a dwelling period of
20 to 30 sec. In this process alkali rapidly penetrates the fabric
and improves the core mercerization.
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Expander roller: Remove dirtness and keep the fabrics in level Padder Upperb
padder: made by rubber Check hardness : 80-90%, Lower padder: made by AUTO
Check hardness : 100%
Dancing roller: Tension keeps proper before going on dryer.
Caustic temperature : 35-55’C
Vacume pump(air): Remove water
Padder pressure: 3bar-washing, IMP-1 & IMP-2—3.5bar
IMP-1 :Strong lime with 30’ baume Solid caustic + 28’ baume mercerize oil.
IMP-2 :Here shrinkage is controlled by using caustic and mercerizing oil. Airing
zone: In airing zone = 11 air roller/8 air rollerIn airing zone, fabrics are dried by air
and chemical is added with fabrics.
Gear+chain : Maintain width, control shrinkage in weft And caustic is utilized in
every fibre equally.
Tanki : No. of tanki-5These keeps water hot and creates weak line (8baume)
Washing chamber (1-3): Hot wash 90’c
Washing chamber 4: Wash at room temperature
Cylinder dryer temperature : 110=-130’c
Cooling dryer temperature : 25-40’c
Exact roller : Maintain fabrics that, selvedge does not remain straight.Using acid
according to fabric GLM -1. 300+GLM thick- 100% acid, 2. 140-274 thickness-
50% acid + 50% water
Types of mercerizer : 1.cool mercerizer – 18’ baume . But for cool mercerizer
good chellers are needed. 2. Hot mercerizer- 28-30’ baume
Recipe: Sodium Hydroxide (NaOH) – (28±2)º Be (Baume´) 267 gm/l (see note) Steam,
water – As required, Green acid / Nurta acid (32%) – 3-4 % of total water, Wetting
agent- 1-1.5 gm/l,
Compressed air -: As required
Mercerizing Oil (Mercirol QW2F) : 3-4 gm/l
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Tests : Barium activity test, 2.PH, 3. Absorbency , 4. Size chemical Suitable For
All cotton fabric, TC/CVC fabric, Twill Fabric
Flow chart of Mercerization
Fabric inlet
J-Box
Impregnation-1(IMP)
Airing Zone
Impregnation-2(IMP)
Gripping Chain
Stabilizing Compartment
Washing Chamber 1 2 3
Neutralizing chamber
Drying unit
J-Box
↓
Batching
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Fabric inlet for mercerized cotton: Batcher from scouring & bleaching unit is feed
into the inlet of mercerizing range. Where the fabric is passed over some free
roller, guider & expander. Here there is a compensator to control fabric open
width entry.
Airing zone of Mercerizing Machine : Fabric is passed over the Airing zone after
chemical padding. Here there is no application of temperature & pressure. It
involves 4 rollers which are driven by motor. This application is only for drying in
contact of air which facilitates more chemical consumption from next bath
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Gripping chain for mercerized cotton: from Impregnation-2 fabric pass over the
free roller & comes in to chain for gripping. Here the fabric is stretched for control
width. If crease mark is found from previous process, that can also be controlled
by stretching. Here there is an additional option of showering by hot water.
Which ensure proper cleaning & removal of residual caustic.
Dryer for mercerized cotton: After washing & neutralizing for drying process 2
stage vertical cylinder dryer is used. It is heated by steam. For course fabric the
cylinder dryer temperature is around 180-200’c. and for pocketing fabric the
cylinder dryer temperature is around 110-130’c.
Batching : Finally after drying the fabric is ready to dye. It is now rolled in the
batcher for next process.
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Jet dyeing machine is the best example of a machine that circulated both
the fabric and the dye bath. Jet dyeing is used for knitted fabrics. For Terry-
towels soft flow dyeing is use. In jet dyeing machine the fabric is
transported by a high speed jet of dye liquid.As seen in the figure, this
pressure is created by venturi. A powerful pump circulates the dyed bath
through a heat exchanger and the cloth chamber. Cloth guide tube helps in
circulation of fabric.
TECHNICAL DATA:
HYDROEXTACTOR
OPENER
Machine used: BIANCO
Made in: INDIA
Work- opening of hydroextracted fabric which is in rope form .
Sensor present-3
Menzel COMPACTFLOW, a new multifunctional and compact continuous washing line for
Washing after Digital printing and small batches The new machines performance compared to her
Big sister, the MENZEL OPTISPLASH drum washing line, is almost identical besides the
Production capacity. The substantially smaller COMPACTFLOW can be operated economically
Already from 5.000-6.000 production capacity per day. As a comparison; the conventional large
Scale continuous washer requires at least 40.000 Meters a day to be lucrative. MENZEL has
Succeeded to arrange four full washer modules on only four meters or two COMPACTFLOW
Modules, without reducing the machines efficiency. We have designed the COMPACTFLOW
Down to the detail in the aspects of modular concept, an outsourced and modular plug-and-play
Utility-rack and expandability with growing demands of the production. Menzel has also turned the
Aspect of drastically cut down time for erection and commissioning and for linking the machine to
The customers utility delivery points into reality. In sum and substance, considering all those cost
Aspects, the investment in a COMPACTFOW is a worthwhile investment with a comparably short
Return on investment. The goal of fulfilling the technical requirements of processing and the
Performance requirements on all practical relevant washing methods is not only reached but
Outperformed by the new COMPACTFLOW.
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