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  • Inorg... Lab

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    Kiran Yaqoob
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    inorg... lab

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    © All Rights Reserved
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    23 views9 pages

    Inorg... Lab

    Uploaded by

    Kiran Yaqoob

    Copyright:

    © All Rights Reserved
    Download as PDF or read online from Scribd
    Flag for inappropriate content
    of 9
    eon m -didxalato 1 es PA chromate (til). Objective - Prepare cis pottasium dioxalato cliaqua chromate Pomplex. | Apparatus « | : Weighing Balance + Beaker + Bunsen Buyney + Glass sod + Tripect stancl Watch glass + Wire glass Chemicals + 4- Odalic aud Crystals 2 Follasiom ichiomate 3- ethanol . Chemical uation : KacnOe +7 PO" 2420, 2k [¢r<0,)(H0),)- | P ts GO smets 13420 { evolution of C02 ‘the miccture will STEP no 3. anc ~H2O vapour . become deep Now without fooling the liquid , 20m! ethanol Added over this liquicl and tituyate the Content by metallic spatula unifll the Solicl Mass is fymecb. STEP No 4: Now warm the contents untill the product is obtain In the fom of granciay crystal : is The caystad of Cis pollasiom ciotalate chromate dat) | tompler Looks black in the diffuses day light when they are finally weigh , Obsewation and ealeal ations Molecular weight of Kacy0, = (39), +(52). +Ue)> = 18 + 4 4h2 = 24 g mol Pronger clay weight oO K [cx (<.04), (ro). | ile = 34 152 (12x241b x4). + 12 = 34 +S2 + 116 +72 = 33q Mass of fodua « Ley (2204) H20)2] + 2H20 = = nA * molecclar weight = (0-006) (339) mass = 20346 Actual yeild 2 ty Theoretical yeild = 2.024 = Retual yell 0 Fercentage yeild Theoretical yetit = saat xl0O 2-034 spage yeild - 83-68 [> Results : We usé 20,04 and k2CnO7 and then heat it coe So granvlay Crystals of Cis pottasiom dioxalato i) Complex cue obtained _ oe ee A tAllization, also known as flactionad ¢rgs “1S a procedre for puify an inpre ‘Or O Solvent, Te method of purification tg Based cn tre piindple that the solubility Sf most solid incroaes with increased tempesatie”? pound This Means thal as temperature Mhett can be Aissclied in O An impure Compounc oes vst also be Soluble in she solvent), to prep high concentsated solution at + The solution 1s cooled . Decreasing ae solubility of impurities in ee substances being pari fea impure substance than crgstallizes betore te pea vities- Assuming that ‘there was more ‘aes stance dtran there were impurities re sul! G J . substance will crystallize iy patie temperature Causes the salution and to decrease, (Qn be used to pI re ery stauization procedore. OO Sloise, tne ate oF ceatings the \arqe 4re Crystals ave that form Tees oe Se " Dissolve the Solute. ‘in the Solvent :- Ade bolting Solvent a loeakes containing the im pure Compound , Heat the beaker cinct Keep acing Solvent until the selute is complet ely Afssalve 4 | 2- Cool the solution + | The Sclution is Coolect in cren al firs 5 and | then Cooled in an ice beith , Sow coding often eects tO porier Crgstals , Crysted> should §forr ch the ladtem of the beaker he piceess of “seecting” can be used tO cic the formation Shore sales qs mean? adding the pue ciysteat of the compoone! . The pore crystals Ponies sugar a Paeeciite |e Crystaullize ofen , Is POurec though a Buchner funnel. If fov Fason there are no crystals visible . cee fithettion con be performed , vated carbon \¢ added +0 the solution, the mixtue is boiled art 3 fennet eqstem Is usec to chansfer the new mbitere tO 4 new leaker of boiling Solvent. Fitter paper | Ts used tn the funne? to wemove exess easton After this mixtue cocls slowly , there chould | be lowe crystals present . 4- By the sesulting Crystals 4 The Crystals are ned by leaving then Ww the aspirate ane ‘then oy semouing them +o aq ee clich 0 weight a while \on ger ete poitty 9 ey tre ciystab car bee tested ay pertorming Snot, —_ determination? e aT sep 4 by" on Ofte, itl : Aistillation is the ype. st ctistillation Which ‘involves te separation x i miscible Oigsiets > Oney nage mee clistittations and Mitte {5 separated ‘nto tuo happens When the mirttue ts condensation s arts , The Separction if heatect = Certain te mperciture where — fractions of Mothwe start to Voypcurize Tinciple : The basic Principle Sf this type 4 distitaton is thet — dlifferent liquicls bei and 2vdporate at Alifferent tempercitines So when the Wintire is heatea , the wrth Rower beiling poiet start to bon And Cenverted into vapours, Rocedure » Substance First To do fractionad distillottion , there are Kone apparatuses which Qre yequites) for ‘the process ' Froctionating tjlumn is comedt gl Pt the "flosk Heat 1s Quam oe S the temperature

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