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Article

Journal of Reinforced Plastics


and Composites

Deformation analysis of short glass 30(16) 1367–1372


! The Author(s) 2011
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DOI: 10.1177/0731684411426203
injection-molded plastic parts jrp.sagepub.com

B. Sikló1, K. Cameron2 and J.G. Kovács1

Abstract
The warpage of injection-molded plastic parts is a complex problem being affected by different technological parameters,
material properties, and mold design. Hence, the description of the deformation is difficult as well. This article presents
the effect of fiber content and mold temperature difference on the deformation of polypropylene parts. Based on the
measurement results, a linear approximation and a calculation method are shown, which can be used to jointly determine
the ideal fiber content and mold temperature difference to produce undeformed plastic parts.

Keywords
warpage, corner effect, injection molding, deformation, injection mold, mold temperature

Many studies have tested the deformation of unfilled


Introduction
thermoplastics.14–19 Akay and Ozden14 analyzed poly-
Injection molding is a high-speed technology to form carbonate and acrylonitrile butadiene styrene and con-
plastic parts.1–6 The effectiveness of the technique, and cluded that the examined specimens injection molded
therefore the quality of the product which can be with a temperature difference between the two mold
achieved, depends on the use of adequate process set- halves have resulted in the final part curving toward
tings and suitable mold construction used to eliminate the hotter side of the mold. Tang et al.15 using acrylo-
different kinds of failures.7–10 The occurrence and min- nitrile butadiene styrene plates for deformation analyses
imization of warpage in injection-molded plastic parts analyzed how melt temperature, filling time, packing
provides a big challenge for mold designers and technol- pressure, and packing time affect warpage. It has been
ogists. At the design stage of an injection mold, it is concluded that the deformation was mostly influenced
required to take into consideration the physical effects by melt temperature, followed by packing time and
ruling in the cavity. These effects will determine the packing pressure.
dimensional accuracy and form stability of the part. Also, Jansen et al.16 analyzed the warpage of speci-
The use of non-optimal technological settings results mens made of amorphous polycarbonate. Plate-like and
in an unequal shrinkage causing warpage in the part. L-shaped specimens (Figure 1(a)) were used in the inves-
The main causes of this variation in shrinkage (resulting tigation to study the effect of holding pressure and mold
deformation) can be material properties, mold and part temperature. The experiments showed that the deforma-
design, or process settings. This deformation can be tion increased along with the increased temperature dif-
attributed to three causes: anisotropic shrinkage, orien- ference between the mold halves, furthermore that at
tation effect, and non-uniform cooling.11–13 Anisotropic
shrinkage means the presence of variation in the shrink- 1
Department of Polymer Engineering, Budapest University of Technology
age from region to region in the part. Orientation effect and Economics, H-1111 Budapest, Hungary.
2
is the difference in shrinkage parallel and perpendicular University of the West of Scotland, Almada Street, Scotland.
to the material orientation direction, mainly occurring
in fiber-reinforced thermoplastics. The third is caused Corresponding author:
J.G. Kovács, Department of Polymer Engineering, Budapest University of
by the temperature gradient through the thickness of Technology and Economics, H-1111 Budapest, Mu00 egyetem rkp. 3.,
the part generated by unequal core and cavity temper- Hungary
atures. This is called non-uniform cooling. Email: kovacs@pt.bme.hu

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1368 Journal of Reinforced Plastics and Composites 30(16)

Figure 1. Specimen geometries with their injection locations for deformation measurements used by (a) Jansen et al.,16 (b) Ammar
et al.,17 and (c) Mlekusch.22

low holding pressure the plates warped toward the hot injection-molded polypropylene part. They showed
side, while at high holding pressure they warped toward that the addition of 2 weight percent (wt%) of carbon
the cold side. nanotubes reduced the warpage of the parts by 55%
Ammar et al.17 used a specimen with four corners compared to the unfilled ones.
(Figure 1(b)) for their warpage measurements. It was The aim of our research was to analyze the effect of
concluded that two phenomena caused the deformation the material and of the asymmetrical cooling on the
of the part: the first was the asymmetrical cooling and deformation of injection-molded plastic parts on a
the second was the spring forward effect. The spring specific specimen.
forward effect was generated in fiber-reinforced poly-
mers due to the higher thermal expansion coefficient in
the thickness direction of the component. The deforma-
Experimental
tion around the corner and the deformation of the plane In this study, the warpage of specific specimens injection
surfaces were distinguishable. Using fiber-reinforced molded of unfilled polypropylene and with polypropy-
polypropylene in their experiments, with an equal lene-reinforced with glass fiber of different weight con-
mold temperature in both mold halves, they recorded tent (10, 20, and 30 wt%) were examined. The matrix
a significant angle deformation of 3 and 5 . A temper- (Borealis, HD120MO) and the glass fibers were mixed
ature difference of 40 C between the two sides of the on a Brabender Plasticorder twin-screw extruder, and a
mold caused an angle variation of about 1.5 . Brabender pelletizer was used to produce pellets from
Other studies dealt with the warpage of fiber- the extrudate. From these materials, special V-top speci-
reinforced thermoplastic parts.20–24 Kikuchi and mens (Figure 2) were injection molded on an Arburg
Koyama20 studied the orientation of fiber-reinforced Allrounder 320 C 600-250 injection-molding machine.
polymer, being the main cause of the occurring warp- The sides of the V-top specimen close an angle of 90 ,
age. They used glass-reinforced polyamide in their anal- and the warpage caused by the technological or other
yses and made a conclusion that in a case of uniform parameters can be described as a change of this angle.
orientation there were not any deformations, while non- The specimens were injection molded with a special two-
uniform orientation caused warpage on the specimens. cavity mold. The mold has changeable and variable
In another study,21 they distinguished different defor- inserts making it possible to alter the layout of the
mation modes of a circular disk made of PA66-GF33, runner system (one directional or bidirectional cavity
namely bowl-like, saddle-like, and waves on the circum- filling) and to inject with different gate types (standard
ference of it. gate at the front of the edge, standard gate at the mid-
Mlekusch22 analyzed the effect of glass fiber on the dle of the edge, film gate along the whole edge).
warpage of corner-like geometries (Figure 1(c)) using The stationary side of the mold contains changeable
polyamide as the matrix material. He concluded that cavity inserts allowing a variation of the part’s wall
the warpage difference between the reinforced and the thickness. The wall thickness can be chosen as either
non-reinforced polymer appeared due to the orthotropy 1 mm or 2 mm. The specimens were injection molded
caused by the fibers and their alignment. He also con- with a thickness of 2 mm using film gate type. For the
cluded that the deformation increased with increasing highest precision of the control, temperature and pres-
fiber volume fraction. sure sensors were incorporated in the core and cavity of
Prashantha et al.25 analyzed the effect of multi- the mold. To evaluate the warpage of the V-top speci-
walled carbon nanotubes on the deformation of an men, special image analysis software was used.

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Sikló et al. 1369

In the experiments, the effect of glass fiber content The effect of fiber content can be clearly seen on
and the alteration of the temperature of the movable Figure 3. The addition of more fiber (while maintaining
and stationary mold side (30, 50, and 70 C) were ana- both core and cavity temperatures of 50 C) resulted in a
lyzed. The rest of the technological parameters were smaller deformation occurring, hence a larger final clos-
kept constant. The holding pressure was 300 bar, the ing angle. It is also observable that a decided difference
melt temperature was 230 C, the holding time was 5 s, appeared in the deformation change along the relative
the injection rate was 50 cm3/s, and the cooling time was edge length (Figure 2) using different fiber weight content
15 s. The switchover to holding pressure took place in the material. The use of more glass fiber in the material
when the end-of-the-cavity pressure sensor reached the attenuated the warpage of the specimens.
25 bar. Along with the fiber content, the mold temperature
had an important influence on the deformation of the
parts. Figure 4 shows that the alteration of the moving
Results and discussion
mold side’s temperature (while maintaining the station-
With design of experiment, it was proved that both the ary mold side’s temperature at 50 C) changed the warp-
temperature difference and glass fiber content influenced age of the specimens independently from the used
the deformation of the V-top specimen significantly holding pressure. Increasing the differential mold tem-
compared to the other studied parameters like injection perature resulted in an increase in deformation due to a
rate, melt temperature, and holding pressure.26 reduction in the closing angle.
Analysis of the effects of the application of various
holding pressures alone (Figure 5) showed that it pro-
duced a minor variation on the warpage when the poly-
propylene (PP) was unfilled, with this effect reducing
and eventually disappearing with the increased percent-
age of glass fiber content.
Contemplating the results as the function of the
moving mold side’s temperature (Figure 6) and the sta-
tionary mold side’s temperature, it can be seen that the
closing angle along the relative edge length showed
mainly a decreasing tendency, and the degree of its
change was influenced by the glass fiber content of the
material. In the case of setting a higher mold tempera-
ture in the moving mold side, the deformation was sig-
nificantly influenced by the glass fiber content. Whereas
using a higher mold temperature in the stationary mold
Figure 2. V-top specimen. side, there were not any dominant differences between

Figure 3. The effect of glass fiber content on the closing angle as a function of the relative edge length of the specimen (both core and
cavity temperatures of 50 C).

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1370 Journal of Reinforced Plastics and Composites 30(16)

Figure 4. The influence of the holding pressure on the closing angle as a function of moving mold side’s temperature (PP, PP-GF30, the
stationary mold side’s temperature is 50 C).

Figure 5. The effect of holding pressure on the deformation at a relative edge length of 50%.

the specimens’ deformation made from material with Equation (2):


different weight content.
Based on the results of measurements taken, the clos-  
Ts Ts
ing angle along the edge length of the parts made of ¼   f1   L þ f2  L þ i1  þ i2
Tm Tm
glass fiber-reinforced polypropylene can be character- ð2Þ
Ts Ts
ized with a linear approximation opposing a correlation þ g1   L þ g2  L þ j 1  þ j2
of 98% as in Equation (1): Tm Tm

      Where f1 ¼ 0.00209 /(%wt%), f2 ¼ 0.00289 /


Ts Ts Ts (%wt%), 
g1 ¼ 0.08511 /%, g2 ¼ 0.13576 /%,
L; ; ¼ A ;  L þ B ; ð1Þ
Tm Tm Tm i1 ¼ 0.007821 /wt%, i2 ¼ 0.04713 /wt%, j1 ¼ 2.53355 ,
 

and j2 ¼ 82.16 are constant parameters.


Where a ( ) is the closing angle, L (%) is the relative
Based on Equation (2), the closing angle will be con-
edge length,  (wt%) is the glass fiber content, Ts/Tm (–)
stant along the relative edge length, if Equation (3) will
is the ratio between the temperature of the stationary
be true:
mold side and the moving mold side, A and B are math-
ematical expressions concerning from the material’s
glass fiber content and from the mold temperature Ts   f 2 þ g2
¼ ð3Þ
ratio. The exposed mathematical expression forms into Tm   f 1 þ g1

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Sikló et al. 1371

Figure 6. The effect of glass fiber content and mold temperature on the closing angle as a function of relative edge length.

Figure 7. Required theoretical glass fiber content and mold temperature difference to enable the injection molding of a non-
deformed specimen.

If the closing angle would be 90 along the relative


edge length, the needed mold temperature difference can
Conclusions
be described as in Equation (4): Under normal circumstances, manufacturing a compo-
nent containing angles, by injection molding, results in a
Ts 90  ð  i2 þ j2 Þ
¼ ð4Þ deformation and warpage of the part. In this article, the
Tm   i1 þ j1
effect of glass fiber content and mold temperature on the
With Equations (3) and (4), a theoretical glass fiber deformation of an injection-molded special V-top speci-
content and a theoretical mold temperature difference men was analyzed. The results showed that the addition
can be determined, which allow the injection molding of of more fiber resulted in a smaller deformation occur-
specimens with a closing angle of 90 along the whole ring, hence a larger final closing angle, closer to that
relative edge length (Figure 7). This is at a fiber content originally intended. It was also concluded that the
of  ¼ 31.04 wt% and a mold temperature ratio of Ts/ higher the moving mold side’s temperature was com-
Tm ¼ 2.29, which corresponds with the measured exper- pared to the stationary mold side’s temperature, the
imental results obtained. larger was the warpage of the part. Both of these

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1372 Journal of Reinforced Plastics and Composites 30(16)

normally independent parameters have to be jointly 9. Kovács JG and Sikló B. Experimental validation of sim-
taken into account, when trying to remove any defor- ulated weld line formation in injection moulded parts.
mation and warpage. Based on the results of the mea- Polym Test 2010; 29(7): 910–914.
surements recorded, the closing angle along the edge 10. Solymossy B and Kovács JG. The examination of weld
line properties in injection molded PP composites. Mater
length was characterized with a linear approximation.
Sci Forum 2008; 589: 263–267.
A theoretical glass fiber content and a theoretical mold 11. Fischer JM. Handbook of molded part shrinkage and warp-
temperature difference was then determined, and in age, 1st ed. Norwich: Plastics Design Library/William
practice proved, which allows the injection molding of Andrew Inc., 2003.
the specimens with a closing angle of 90 along the 12. Subramanian NR, Tingyu L and Seng YA. Optimizing
whole relative edge length. warpage analysis for an optical housing. Mechatronics
2005; 15: 111–127.
13. Shoemaker J. Moldflow design guide. Munich: Carl
Declaration of Conflict of Interests Hanser Verlag, 2006.
This work is connected to the scientific program of the 14. Akay M, Ozden S and Tansey T. Prediction of process-
‘Development of quality-oriented and harmonized induced warpage in injection molded thermoplastics.
Polym Eng Sci 1996; 36(13): 1839–1846.
R+D+I strategy and functional model at BME’ proj-
15. Tang SH, Tan YJ, Sapuan SM, Sulaiman S, Ismail N and
ect. This project is supported by the New Széchenyi Plan Samin R. The use of Taguchi method in the design of
(Project ID:TÁMOP-4.2.1/B-09/1/KMR-2010-0002). plastic injection mould for reducing warpage. J Mater
Process Tech 2007; 182(1–3): 418–426.
Acknowledgments 16. Jansen KMB, van Dijk DJ and Keizer KP. Warpage of
The authors would like to thank Arburg Hungaria Ltd. for the injection moulded plates and corner products. Int Polym
injection-molding machine and to Dr. Tung Pham from Proc 1998; 13(4): 417–424.
Borealis Polyolefine GmbH for the material. 17. Ammar A, Leo V and Régnier G. Corner deformation of
injected thermoplastic parts. Int J Form Proc 2003; 6(1):
53–70.
Funding 18. Oktem H, Erzurumlu T and Uzman I. Application of
This article was supported by the János Bolyai Research Taguchi optimization technique in determining plastic
Scholarship of the Hungarian Academy of Sciences. injection molding process parameters for thin-shell part.
Mater Design 2007; 28: 1271–1278.
19. Kabanemi KK, Vaillancourt H, Wang H and Salloum G.
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