OptiDist User Manual

OptiDist™
USER MANUAL
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Document number 8001-004-01E

IB number ---
Contents OptiDist User Manual
Date November 30, 2011
Revision 2.00A
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Table 1.1 Revision History

Revision Date Description
2.00A November 30, 2011 General update
OptiDist™
Copyright
Copyright © 2011, by Petroleum Analyzer Company, L.P.
All rights reserved.
All text, graphics, design, and other works contained herein are the copyrighted
works of Petroleum Analyzer Company, L.P. (hereinafter referred to as PAC).
Any redistribution or reproduction of any materials contained herein is strictly
prohibited without the express written permission of the copyright holder.
The PAC trademark, the PAC service mark, PAC’s logo trademark, PAC division’s
trademarks, PAC product’s trademarks, and PAC’s distinctive colour trademark as
used on its instruments and in these materials, are trademarks or service marks or
registered trademarks or registered service marks of PAC in the U.S. and other
countries and are its sole and exclusive property.
MS Windows, MS Windows XP, and MS Windows Professional are registered
trademarks of Microsoft Corp.
Other trademarks contained within these materials are the property of their
respective owners.
Information
The information contained within these materials is subject to change without
notice. PAC makes no warranties or guarantees, either expressed or implied in
these materials, including the warranty merchantability or fitness for a particular
purpose. At any time, PAC may modify these materials, its instruments or its
programs without notice and subsequent versions of these materials may contain
different information.
These materials could contain technical inaccuracies and/or typographical errors.
PAC does not assume responsibility for the accuracy of any translation of these
materials.
This manual contains confidential and proprietary information. The information

contained within these materials is the property of PAC. This manual and all
information disclosed herein shall not be used to manufacture, construct, or
fabricate the goods disclosed herein; shall not be exploited or sold; shall not be
copied or otherwise reproduced in whole or in part and shall not be revealed or
disclosed to others or in any manner made public without the express written
permission of PAC.
About PAC
PAC is an international manufacturing and service organization with a portfolio
that spans petroleum, petrochemical, biofuels, environmental, food and beverage,
pharmaceutical and industrial analysis solutions.
PAC provides advanced scientific apparatus and testing equipment for laboratory
process, on-line and field use from small to the largest enterprise businesses.
PAC offers analytical solutions for a wide variety of applications, including:
chromatographic systems and detectors, elemental, laboratory, and on-line
process instruments, software applications, and spectroscopy.
Many automatic analyzers bearing the PAC brand are recognized for increasing
test precision, boosting laboratory efficiency and reducing costs.
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Table of contents
1 General information
1.1 Policy statement ..................................................................................................................... 2
1.2 Standard limited warranty of PAC .......................................................................................... 3
1.2.1 Limited warranty ......................................................................................................... 3
1.2.2 Limitations on PAC liability ......................................................................................... 7
1.2.3 Compliance ................................................................................................................ 8
1.3 Software license ..................................................................................................................... 9
1.3.1 Grant of license .......................................................................................................... 9
1.3.2 Description of other rights and limitations .................................................................. 9
1.3.3 Upgrades.................................................................................................................. 10
1.3.4 Copyright .................................................................................................................. 10
1.3.5 Dual-media software ................................................................................................ 10
1.3.6 U.S. Government restricted rights ............................................................................ 11
1.4 Assumptions ......................................................................................................................... 11
1.4.1 Good Laboratory Practice ........................................................................................ 11
1.4.2 The standards of laboratory safety........................................................................... 11
1.4.3 Electronic device ...................................................................................................... 11
1.5 Return policy......................................................................................................................... 12
1.5.1 Returned product warranty determination ................................................................ 12
1.5.2 On-site repair............................................................................................................ 12
1.5.3 Inspection ................................................................................................................. 12
1.5.4 Information ............................................................................................................... 13
1.6 Disposal................................................................................................................................ 14
1.7 Documentation ..................................................................................................................... 15
1.7.1 Document validity ..................................................................................................... 15
1.7.2 Document storage .................................................................................................... 15
1.7.3 Language ................................................................................................................. 15
1.7.4 Typographical and authoring conventions................................................................ 15
2 Safety
2.1 Certifications......................................................................................................................... 18
2.2 Warning pictograms.............................................................................................................. 19
2.3 Caution pictograms............................................................................................................... 20
2.4 Note pictograms ................................................................................................................... 21
2.5 Tip pictograms ...................................................................................................................... 21
2.6 Environmental protection...................................................................................................... 21
3 Introduction
3.1 Intended use......................................................................................................................... 24
3.2 Intended audience ................................................................................................................ 24
3.3 Product overview .................................................................................................................. 24
3.4 Applicable standard methods ............................................................................................... 25
3.5 Benefits and features............................................................................................................ 26
3.6 General Scope...................................................................................................................... 27
3.7 Terminology.......................................................................................................................... 27
3.8 List of abbreviations.............................................................................................................. 28
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3.9 Nameplate ............................................................................................................................ 28

3.10 Specifications........................................................................................................................ 29
4 Description
4.1 Views of the OptiDist™......................................................................................................... 32
4.1.1 Front view left ........................................................................................................... 32
4.1.2 Front view right ......................................................................................................... 33
4.1.3 Rear view ................................................................................................................. 34
4.1.4 Connection ports ...................................................................................................... 34
4.2 Description of the OptiDist™front ......................................................................................... 36
4.3 Distillation flask heater assembly.......................................................................................... 37
4.3.1 Overview .................................................................................................................. 37
4.3.2 Self-positioning flask heater platform ....................................................................... 38
4.3.3 Heating regulation .................................................................................................... 38
4.3.4 Heating element ....................................................................................................... 39
4.3.5 Flask cooling ............................................................................................................ 39
4.3.6 Safety features ......................................................................................................... 39
4.3.7 Distillation flask......................................................................................................... 40
4.3.8 Distillation flask stopper............................................................................................ 41
4.3.9 Vapor temperature probe ......................................................................................... 42
4.4 The receiving chamber ......................................................................................................... 43
4.4.1 Overview .................................................................................................................. 43
4.4.2 Receiver cylinder ...................................................................................................... 45
4.4.3 Condenser tube regulation ....................................................................................... 46
4.4.4 Cooling unit .............................................................................................................. 46
4.5 Safety features ..................................................................................................................... 48
4.5.1 Emergency stop button ............................................................................................ 48
4.5.2 Passive safety - receiver liquid spillage trap ............................................................ 48
4.5.3 Alarms ...................................................................................................................... 48
4.5.4 Automatic fire extinguisher system........................................................................... 49
4.6 Optional parts ....................................................................................................................... 51
4.6.1 Ambient temperature probe...................................................................................... 51
4.6.2 Optional 125 ml and 200 ml automatic dry point detection kit .................................. 51
4.6.3 Optional kit for “10 % (V/V) Distillation Residue” with 200 ml................................... 53
4.6.4 Optional external PC control: HLIS-32® or ALAN® ................................................. 53
4.6.5 Optional external data management software: PDS™............................................. 54
4.6.6 Optional status indicator beacon .............................................................................. 54
4.6.7 Optional built-in printer ............................................................................................. 54
4.6.8 Optional external printer ........................................................................................... 55
4.6.9 Optional bar code reader.......................................................................................... 55
4.6.10 Optional “Doctor Box” ............................................................................................... 55
4.6.11 Optional VOC control ............................................................................................... 56
4.7 Access levels ........................................................................................................................ 57
4.8 The Man Machine Interface (MMI)........................................................................................ 59
4.8.1 Touch-screen ........................................................................................................... 59
4.8.2 Features of the touch-screen ................................................................................... 59
4.8.3 Precautions for the touch-screen ............................................................................. 60
4.8.4 The virtual keybord and keypad ............................................................................... 60
4.8.5 The Welcome screen ............................................................................................... 62
4.8.6 The Run / Start & Display screen ............................................................................. 63
4.8.7 The New Test main menu ........................................................................................ 66
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5 Installation
5.1 Technical specifications and requirements........................................................................... 70
5.2 Care in Unpacking ................................................................................................................ 70
5.3 Installation of the OptiDist™ ................................................................................................. 71
5.4 Main power connection......................................................................................................... 71
5.5 CO2 gas connection ............................................................................................................. 72
5.6 OptiDist™/ PC Connection ................................................................................................... 72
5.6.1 Optional external PC control .................................................................................... 72
5.6.2 Connection with RS 232C serial link ........................................................................ 72
5.7 Flask stopper holder ............................................................................................................. 72
5.8 Temperature probe connection ............................................................................................ 73
5.8.1 Pt100 vapor temperature probe ............................................................................... 73
5.8.2 Ambient temperature probe...................................................................................... 73
5.9 125 ml and 200 ml automatic dry point kit and holder .......................................................... 73
5.9.1 Installation of the automatic dry point kit and holder ................................................ 73
5.9.2 Adjustment of the vapor probe in the dry point stopper............................................ 74
5.10 Installation of the status indicator beacon ............................................................................ 75
5.11 VOC Control Option Connection .......................................................................................... 75
5.12 Connection of an optional external printer............................................................................ 75
5.13 Connection of the optional bar code reader ......................................................................... 75
5.14 Power-On procedure ............................................................................................................ 76
5.14.1 Switch on the OptiDist™ .......................................................................................... 76
5.14.2 PAC addresses screen............................................................................................. 76
5.14.3 Heat exchanging liquid (level checking and recommendations) .............................. 76
5.14.4 Self diagnostic screen .............................................................................................. 76
5.14.5 OptiDist™ calibration................................................................................................ 76
6 Operation
6.1 Preparation ........................................................................................................................... 80
6.1.1 Basic preconditions .................................................................................................. 80
6.1.2 Safety ....................................................................................................................... 80
6.1.3 Sampling, storage and sample conditioning according to ASTM D86 ..................... 81
6.1.4 Clean the devices..................................................................................................... 84
6.1.5 Preparation of the OptiDist™ and accessories ........................................................ 86
6.1.6 Set-up of the distillation flask and the receiving cylinder.......................................... 88
6.1.7 Set up the receiving chamber temperature .............................................................. 90
6.1.8 Scan the volume in the receiver cylinder.................................................................. 91
6.2 Measurements...................................................................................................................... 93
6.2.1 Start modes .............................................................................................................. 93
6.2.2 Start procedure - run a distillation test.................................................................... 108
6.2.3 Residue measurement ........................................................................................... 110
6.2.4 Displaying and printing of results ........................................................................... 111
7 Database management
7.1 The Results database......................................................................................................... 114
7.1.1 Displaying of results ............................................................................................... 114
7.1.2 Printing of results.................................................................................................... 117
7.1.3 Transmitting of results ............................................................................................ 117
7.1.4 Modifying of results ................................................................................................ 119
7.1.5 Creating of a new optimized product...................................................................... 121
7.1.6 Removing of results................................................................................................ 122
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7.2 The Products database....................................................................................................... 123

7.3 The QC (Quality Control) sample database........................................................................ 135
7.3.1 Displaying the spreadsheet format of the QC sample database ............................ 135
7.3.2 Displaying the graphic format of the QC sample database .................................... 137
7.3.3 Removal of a test from a QC sample database ..................................................... 138
7.3.4 Modification of specified results in a QC sample database .................................... 139
7.3.5 Removal of a QC sample database ....................................................................... 139
7.4 The Messages database .................................................................................................... 140
7.5 The OptiDist™ Parameter database................................................................................... 142
7.6 The service functions of the Parameter database .............................................................. 148
7.7 The Reports profile database ............................................................................................. 151
7.8 The Operator database....................................................................................................... 158
7.8.1 Displaying the list of prestored Operator names .................................................... 158
7.8.2 Add a new operator name to the list of prestored operators .................................. 159
7.8.3 Remove an operator name from the list of prestored operators............................. 160
7.9 The Standard test methods database................................................................................. 161
7.9.1 List of standard test methods ................................................................................. 162
7.9.2 List of ASDM D1078 / D850 compounds................................................................ 165
7.10 The Calibration database.................................................................................................... 168
7.10.1 Introduction............................................................................................................. 168
7.10.2 Calibration of the barometric pressure ................................................................... 170
7.10.3 Vapor probe calibration .......................................................................................... 171
7.10.4 Vapor probe circuit calibration ................................................................................ 174
7.10.5 The service button of the vapor probe circuit calibration ........................................ 177
7.10.6 Calibration of the volume measurement system .................................................... 178
7.10.7 The service button of the volume measurement calibration ................................... 183
7.10.8 Temperature correction table ................................................................................. 184
7.10.9 Calibration of the heater temperature..................................................................... 189
7.10.10 The service button of the heater temperature calibration ...................................... 190
7.10.11 Calibration of the optimizer .................................................................................... 191
7.10.12 The service button of the optimizer calibration ...................................................... 192
7.10.13 Calibration of the touch screen .............................................................................. 194
7.10.14 Refuse the test start............................................................................................... 196
7.10.15 Calibration ticket printing ....................................................................................... 196
7.11 Diagnostic functions............................................................................................................ 197
7.12 The About main menu ........................................................................................................ 199
7.13 Backup and Restore ........................................................................................................... 201
7.14 Firmware update................................................................................................................. 203
8 Diagnostic functions
8.1 Frequency of measurement checks.................................................................................... 206
8.2 Displaying current readings ................................................................................................ 207
8.3 Measurement checking procedures.................................................................................... 209
8.3.1 Barometric pressure measurement ........................................................................ 209
8.3.2 Vapor temperature measurement circuit ................................................................ 209
8.3.3 Heating element temperature measurement .......................................................... 210
8.3.4 Condenser bath temperature measurement .......................................................... 210
8.3.5 Receiving chamber temperature measurement ..................................................... 211
8.3.6 Volume measurement of the receiver cylinder ....................................................... 211
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8.4 Various individual component diagnostic functions ............................................................ 212

8.4.1 Activate the diagnostic mode ................................................................................. 212
8.4.2 Diagnostic of the distillation flask heating block ..................................................... 214
8.4.3 Diagnostic of the volume measurement ................................................................. 215
8.4.4 Diagnostic of the condenser bath circuit ................................................................ 216
8.4.5 Diagnostic of the receiving chamber ...................................................................... 218
8.4.6 Diagnostic of the cooling unit: the exchanger......................................................... 221
8.4.7 End of diagnostic.................................................................................................... 221
8.5 Connection and use of the “Doctor Box” ............................................................................ 221
8.5.1 Introduction............................................................................................................. 221
8.5.2 Checking of the operation of supply circuits........................................................... 222
8.5.3 Checking and measuring voltages ......................................................................... 224
9 Maintenance
9.1 Reminder on frequency of measurement checks and calibration....................................... 226
9.2 Routine maintenance.......................................................................................................... 226
9.3 Disassembling/Reassembling of the OptiDist™ housing ................................................... 228
9.3.1 Disassemble/Reassemble the housing of the distillation flask heater assembly.... 228
9.3.2 Disassembe/Reassemble the main housing of the OptiDist™............................... 228
9.4 Check and replace wear and tear parts.............................................................................. 229
9.4.1 Check the coils of the heating element .................................................................. 229
9.4.2 Replace the heating element.................................................................................. 230
9.4.3 Check and replace the condenser/distillation flask silicone tube ........................... 230
9.4.4 Check and replace the receiver cylinder rubber cap .............................................. 231
9.4.5 Check and replace the stopper seals ..................................................................... 231
9.4.6 Check and replace the stopper tip.......................................................................... 232
9.4.7 Replace the vapor temperature probe.................................................................... 232
9.4.8 Replace the dry point thermocouple....................................................................... 232
9.5 Drain the receiving chamber spillage trap .......................................................................... 233
9.6 Servicing the cooling system .............................................................................................. 233
9.6.1 Check the coolant level - filling............................................................................... 233
9.6.2 Clean the condenser of the cooling unit ................................................................. 235
9.7 Testing the fire extinguisher solenoid valve and flame detector......................................... 235
9.7.1 Frequency of tests.................................................................................................. 235
9.7.2 Test procedure ....................................................................................................... 235
9.8 Connection of an external fire alarm device ....................................................................... 236
10 Alarm treatment
10.1 Alarm processing................................................................................................................ 240
10.2 Alarm displaying and stopping............................................................................................ 240
10.3 Alarm review....................................................................................................................... 240
10.4 List of alarm messages and troubleshooting ...................................................................... 241
11 List of accessories
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General information OptiDist™
1 General information
UM_2.00A_EN 1
OptiDist™ General information
1.1 Policy statement

The instructions given herein cover generally the description, installation,
operation, and/or maintenance of subject equipment. PAC reserves the right to
make engineering refinements that may not be reflected in this manual. Should
any questions arise which may not be answered specifically by these instructions,
they should be directed to PAC for further detailed information and technical
assistance.
Your satisfaction and safety are important to PAC, and a complete understanding
of this equipment is necessary to attain these objectives. As the eventual user of
this apparatus, it is your responsibility to understand its proper function and
operational characteristics.
This manual should be read thoroughly and all users should be given adequate
training before attempting to place this instrument in service. Awareness of the
stated cautions and warnings, and compliance with recommended operating and
maintenance parameters are important for safe and satisfactory operation.
This apparatus should be used only for its intended operation; alterations will void
the warranty.
2 UM_2.00A_EN
1.2 Standard limited warranty of PAC

This Standard Limited Warranty applies to products manufactured and sold by
Petroleum Analyzer Company, L.P., Walter Herzog GmbH, Instrumentation
Scientifique De Laboratoire SAS, A.C. Analytical Controls B.V., and A.C.
Analytical Controls Asia Pacific Pte Ltd. (hereafter each or any of them referred to
as "PAC").
1.2.1 Limited warranty
1.2.1.1 Warranty
For each product sold, PAC offers to the original owner ("Buyer") a limited
warranty against failure to conform to the product specifications or any defects in
material and workmanship for a period of
i twelve (12) months from the date of installation of the product or
ii eighteen (18) months from date of invoice,
whichever is less (the "Initial Warranty"). If a failure to conform to specifications or

a defect in materials or workmanship is discovered within the Initial Warranty
period, Buyer must promptly notify PAC in writing, which notification, in any event
must be received no later than 14 months from the date of installation of the
product. Within a reasonable time after such notification, PAC will correct any
failure to conform to specifications or any defect in materials or workmanship, or in
lieu of such repair, and at its sole option, shall replace the product, F.O.B. PAC's
city of shipment or refund the purchase price, less a reasonable reduction in such
purchase price as determined by PAC. In no event shall PAC be liable for
consequential or special damages, or for transportation, installation, adjustment or
other expenses, which may arise in connection with such products or warranty
claim. Products and parts sold by authorized PAC Distributors are covered by the
Distributor's terms and conditions.
During the Initial Warranty period, PAC offers a limited warranty on each part or
product repaired or replaced by a PAC service person for a period ending the later
of
a the remaining term of the Initial Warranty of the product or
b ninety (90) days from the date of repair or replacement,
whichever is longer. After expiration of the Initial Warranty period, PAC offers a
ninety (90) day limited warranty on each part or product repaired or replaced by a
PAC service person. PAC further warrants that the products and parts it sells will
conform to PAC's written specifications therefor. The foregoing limited warranties
cover parts and labor only and PAC does not warrant and will not reimburse the
Buyer for any other costs relating repairing or replacing the product at issue. The
foregoing limited warranties apply only to the repair or replacement of defective
parts and/or products and such determination will be in the sole discretion of PAC.
The limited warranties of this Section 1.2.1.1. Warranty are further subject to those
warranty exclusions set forth in Section 1.2.1.3. Limited warranty exclusions.
UM_2.00A_EN 3
1.2.1.2 Aftermarket
The use of third party parts in the operation or maintenance of the product or
repairs or servicing by unauthorized service personnel immediately voids all
further warranty obligations of PAC. PAC genuine consumables are sold on an as-
is basis and have no warranty beyond being shipped in good working order.
1.2.1.3 Limited warranty exclusions

Other than the warranties set forth in Section 1.2.1.1. Warranty, PAC disclaims
any and all express or implied warranties, including but not limited to the warranty
of merchantability, fitness for a particular purpose and non-infringement of the
intellectual property of others. Provided, however, this Intellectual Property
Warranty shall apply to the product only so long as Buyer
i does not modify the product, combine the product with other elements or use
the product in a practice or a process, and such modification, combination or
practice of which the product forms a part is the subject of such claim or
allegation of infringement and
ii uses the product under ordinary conditions and for their intended purposes.
PAC makes no warranty, express or implied, as to the design, sale, installation or

use of its products. PAC's warranties will not be enlarged by, nor will any obligation
or liability of PAC arise due to PAC providing technical advice, facilities or service
in connection with any product. PAC disclaims any and all other warranties and
representations and PAC provides no warranty on the oral representations made
by its personnel while they are undertaking Services for Buyer.
There is no warranty by PAC with respect to any product’s:

i uninterrupted or error-free operation;
ii actual performance, other than the product's capability to meet PAC's
specifications therefor;
iii removal or installation from a worksite or process;
iv electronic components or associated accessories (including without limitation
circuit boards and integrated circuits);
v maintenance (including without limitation gasket and seal replacements,
adjustments, minor repairs and other inspection requirements, preventative or
otherwise);
vi use under inappropriate conditions or not in accordance with operating
instructions; or
vii use in connection with the operation of a nuclear facility.
There is no warranty for products determined to be, in PAC’s sole discretion,

damaged or impaired as a result of:
A misuse, neglect or accident;
B improper application, installation, storage or use;
C improper or inadequate maintenance or calibration;
4 UM_2.00A_EN
D operation outside of the published environmental specification;

E improper site preparation or maintenance;
F unauthorized repairs or replacements;
G modifications negligently or otherwise improperly made or performed by
persons other than PAC;
H Buyer-supplied software or supplies;
I use in conjunction with or interfacing with unapproved accessory equipment;
J use of ABC-style or dry powder fire suppression agents; or
K leaked sample materials.
To the extent a PAC product is used in connection with the operation of a nuclear
power facility, Buyer agrees to indemnify and hold PAC harmless from any and all
actions, claims, suits, damages and expenses arising from such use. PAC
provides no warranty on the oral representations made by its personnel while they
are attempting to assist Buyer in the operation of a product. This Standard Limited
Warranty does not apply to items consumed by the products during their ordinary
use, including but not limited to fuses, batteries, paper, septa, fittings, screws,
fuses, pyrolysis, dryer or scrubber tubes, sample boats, furnaces or lamps.
This warranty is valid only if genuine PAC parts, consumables and standards are
used in PAC products.
1.2.1.4 Resale products

Resale products are goods (that are sold with PAC's products) which are not
manufactured by PAC and which are supplied as an accommodation to Buyer.
PAC MAKES NO WARRANTY FOR RESALE PRODUCTS, EITHER EXPRESS
OR IMPLIED, INCLUDING WARRANTIES OF MERCHANTABILITY AND
FITNESS FOR A PARTICULAR PURPOSE. THE SOLE WARRANTY SHALL BE
THAT OF THE RESALE PRODUCT MANUFACTURER.
Buyer agrees that PAC has no liability for resale products beyond the services
within PAC's direct control necessary to reasonably discharge the above stated
responsibility and that PAC shall not be liable for delays caused by resale product
manufacturer. PAC does not warrant products it does not manufacture except to
the extent the warranty of the manufacturer of the product at issue passes through
or is otherwise assigned to PAC. Buyer further agrees that Buyer's SOLE AND
EXCLUSIVE REMEDY for PAC's breach of the stated responsibility shall be
limited to the difference between the resale product manufacturer's price to PAC
and PAC's price to Buyer for resale products.
.
UM_2.00A_EN 5
1.2.1.5 Expenses on non-warranty work

All repairs or replacements by PAC after the expiration of any applicable limited
warranty period will be performed in accordance with PAC’s standard rate for parts
and labour. Further, if upon PAC’s inspection and review, PAC determines the
condition of the product for which a warranty claim is submitted is not caused by a
defect in PAC’s material and workmanship, but is the result of some other
condition, including but not limited to damage caused by any of the events or
conditions set forth in Section 1.2.1.3. Limited warranty exclusions, Buyer shall be
liable for all expenses incurred by PAC to conduct the inspection and review of the
product.
1.2.1.6 Exclusive remedy

The limited warranty contained herein constitutes Buyer's exclusive remedy with
respect to products sold by PAC and PAC's liability shall be exclusively limited to
the written limited warranty specified herein. No employee, representative or
agent of PAC is authorized to either expressly or impliedly modify, extend, alter or
change any of the limited warranties expressed herein to Buyer.
1.2.1.7 Procedure and costs

All limited warranty claims must be made in writing promptly following discovery of
any failure to conform to specifications or any defect in materials or workmanship.
Buyer must hold products for inspection by PAC. If requested by PAC, Buyer must
send the product to PAC for inspection. Any such returns by Buyer will be at
Buyer’s expense and Buyer will remain liable for any loss of or damage to the
product during such product’s transportation to PAC. No products will be sent to
PAC for inspection unless PAC has authorized Buyer to do so.
1.2.1.8 Terms and conditions

PAC’s General Terms and Conditions are incorporated herein by reference and
Buyer accordingly agrees to be bound by the terms thereof.
6 UM_2.00A_EN
1.2.2 Limitations on PAC liability
1.2.2.1 General
Buyer agrees that in no case shall PAC be liable for any special, incidental,
consequential, or punitive damages based upon any legal theory whether or not
such damages are foreseeable. Such damages include, but are not limited to, loss
of profits, loss of savings or revenue, loss of use of the product or any associated
equipment, cost of capital, cost of any substitute equipment, facilities or services,
downtime, the claims of third parties including customers, injury to property and,
unless precluded under applicable state law, bodily and personal injury. PAC's
total liability for any and all losses and damages arising out of any and all causes
whatsoever including, without limitation, defects in the product(s), services,
software, or documentation supplied or breach of this agreement, shall in no event
exceed the purchase price of the applicable product(s). Buyer agrees these
limitations on PAC’s liability are reasonable and reflected in the amounts charged
by PAC for its products.
1.2.2.2 Buyer Data

If any data supplied by Buyer, whether in the form of Buyer specifications or
pursuant to any purchase order or other documentation, proves to be inaccurate,
any warranties or other related obligations of PAC relying thereon will be void.
1.2.2.3 Force majeure

This Standard Limited Warranty does not cover and PAC shall not be liable for
either direct or consequential damage caused, either directly or indirectly, as a
result of:
i any act of God, including but not limited to natural disaster, such as floods,
earthquakes, or tornadoes;
ii damages resulting from or under the conditions of labor disputes, strikes or
riots, insurrection, civil commotion or war;
iii damages or improper operation due to intermittent power line voltage,
frequency, electrical spikes or surges, unusual shock or electrical damage;
iv accident, fire or water damage, neglect, corrosive atmosphere or causes other
than ordinary use;
v failure of supplies or transportation, or governmental action; or
vi any other causes beyond Seller's reasonable control.
1.2.2.4 Limitation on warranty claims

Prior to any obligation of PAC to perform any limited warranty service as set forth
herein, Buyer must have:
i paid all invoices to PAC in full, whether or not they are specifically related to
the product at issue; and
ii notified PAC of the limited warranty claim within sixty (60) days from the date
Buyer knew or had reason to know of the defect.
UM_2.00A_EN 7
1.2.3 Compliance
1.2.3.1 General
These Warranty Terms are subject to change without notice. PAC also retains the
right to modify these warranty terms in order to comply with policy or laws
governing warranty issues in states or countries having specific remedies differing
or additional to those described within this document.
1.2.3.2 Severability
If any one or more of the provisions or subjects contained in the Agreement shall
for any reason be held invalid, illegal, or unenforceable, it shall not affect the
validity and enforceability of any other provisions or subjects.
8 UM_2.00A_EN
1.3 Software license

This End-User License Agreement (“EULA”) is a legal agreement between you
(either an individual or a single entity) and the manufacturer (“PC Manufacturer”)
of the computer system (“COMPUTER”) with which you acquired or installed the
Sulfacert software product(s) identified above (“SOFTWARE PRODUCT” or
“SOFTWARE”).
If the SOFTWARE PRODUCT is not installed into a new computer system, you
may not use or copy the SOFTWARE PRODUCT. The SOFTWARE PRODUCT
includes computer software, the associated hardware and media, any printed
materials, and any “on-line” or electric documentation. By installing, copying, or
otherwise using the SOFTWARE PRODUCT, you agree to be bound by the terms
of this EULA.
If you do not agree to the terms of this EULA, PC Manufacturer and PAC are
unwilling to license the SOFTWARE PRODUCT to you. In such event, you may
not use or copy the SOFTWARE PRODUCT and you In such event, you may not
use or copy the SOFTWARE PRODUCT, and you should promptly contact your
local PAC representatives for return of the unused product(s) for a refund.
The SOFTWARE PRODUCT is protected by copyright laws and international

copyright treaties, as well as other intellectual property laws and treaties. The
SOFTWARE PRODUCT is licensed, not sold.
1.3.1 Grant of license
This EULA grants you the following rights:

• Software
You may install and use one copy of the SOFTWARE PRODUCT on the
COMPUTER. A license for the SOFTWARE PRODUCT may not be shared or
used concurrently on different computers.
• Back-up Utility
If PC Manufacturer has not included a back-up copy of the SOFTWARE
PRODUCT with the COMPUTER, you may use the back-up utility, if included
with the SOFTWARE PRODUCT, to make a single back-up copy of the
SOFTWARE PRODUCT. You may use the back-up copy solely for archival
purposes. After the single back-up copy is made, the backup utility will be
permanently disabled.
1.3.2 Description of other rights and limitations

• Limitations on Reverse Engineering, Decompilation and Disassembly
You may not reverse engineer, decompile, or disassemble the SOFTWARE
PRODUCT, except and only to the extent that such activity is expressly
permitted by applicable law notwithstanding this limitation.
• Separation of Components
The SOFTWARE PRODUCT is licensed as a single product. Its component
parts may not be separated for use on more than one computer.
UM_2.00A_EN 9
• Single COMPUTER
The SOFTWARE PRODUCT is licensed with the COMPUTER as a single
integrated product. The SOFTWARE PRODUCT may only be used with the
COMPUTER.
• Rental
You may not rent or release the SOFTWARE PRODUCT.
• Software Transfer
You may permanently transfer all of your rights under this EULA only as part
of a sale or transfer of the COMPUTER, provided you retain no copies, you
transfer all of the SOFTWARE PRODUCT (including all component parts, the
media and printed materials, any upgrades, this EULA and, if applicable, the
Certificate(s) of Authenticity), and the recipient agrees to the terms of this
EULA. If the SOFTWARE PRODUCT is an upgrade, any transfer must include
all prior versions of the SOFTWARE PRODUCT.
• Termination
Without prejudice to any other rights, PAC may terminate this EULA if you fail
to comply with the terms and conditions of this EULA. In such event, you must
destroy all copies of the SOFTWARE PRODUCT and all of its component
parts.
1.3.3 Upgrades
If the SOFTWARE PRODUCT is an upgrade of a component of a package of
software programs which you licensed as a single product, the SOFTWARE
PRODUCT may be used and transferred only as part of that single product
package and may not be separated for use on more than one computer.
1.3.4 Copyright
All title and copyrights in and to the SOFTWARE PRODUCT (including but not
limited to any images, photographs, animations, video, audio, music, text and
“applets,” incorporated into the SOFTWARE PRODUCT), the accompanying
printed materials, and any copies of the SOFTWARE PRODUCT, are owned by
PAC or its suppliers. The SOFTWARE PRODUCT is protected by copyright laws
and international treaty provisions. You may not copy the printed materials
accompanying the SOFTWARE PRODUCT.
1.3.5 Dual-media software

You may receive the SOFTWARE PRODUCT in more than one medium.
Regardless of the type or size of medium you receive, you may only use one
medium that is appropriate for your single computer. You may not use or install the
other medium on another computer. You may not loan, rent, lease, or otherwise
transfer the other medium to another user, except as part of the permanent
transfer (as provided above) of the SOFTWARE PRODUCT.
10 UM_2.00A_EN
1.3.6 U.S. Government restricted rights

The SOFTWARE PRODUCT and documentation are provided with RESTRICTED
RIGHTS. Use, duplication, or disclosure by the Government is subject to
restrictions as set forth in subparagraph (c)(1)(ii) of the Rights in Technical Data
and Computer Software clause at DFARS 252.227-7013 or subparagraphs (c)(1)
and (2) of the Commercial Computer Software-Restricted Rights at 48 CFR
52.227-19, as applicable. Manufacturer is PAC, L.P., 8824 Fallbrook Drive
Houston, TX 77064, USA.
For the limited warranties and special provisions pertaining to your particular
jurisdiction, please refer to the software product printed materials.
1.4 Assumptions
1.4.1 Good Laboratory Practice

Refer to Good Laboratory Practice or GLP as a system of management controls
for laboratories and research organizations to ensure the consistency and
reliability of results - as outlined in the Organisation for Economic Co-operation
and Development (OECD) Principles of GLP and national regulations.
GLP applies to non-clinical studies conducted for the assessment of the safety of
chemicals to man, animals and the environment. The internationally accepted
definition reads:
• Good Laboratory Practice (GLP) embodies a set of principles that provides a
framework within which laboratory studies are planned, performed, monitored,
recorded, reported and archived. These studies are undertaken to generate
data by which the hazards and risks to users, consumers and third parties,
including the environment, can be assessed for pharmaceuticals (only
preclinical studies), agrochemicals, cosmetics, food additives, feed additives
and contaminants, novel foods, biocides, detergents, etc.
GLP helps assure regulatory authorities that the data submitted are a true
reflection of the results obtained during the study and can therefore be relied
upon when making risk/safety assessments.
1.4.2 The standards of laboratory safety

Refer to the standards of laboratory safety, wearing appropriate gloves, glasses
and clothing to handle materials safely.
1.4.3 Electronic device

Refer to the standards of manipulating an electronically / electrical device and
electrical current safely.
UM_2.00A_EN 11
1.5 Return policy

No product may be returned, whether in warranty or out of warranty, without first
obtaining approval from PAC. No replacements will be provided nor repairs be
made for products returned without such approval. A return authorization number
must accompany any returned product. The buyer will pay for the expense of
returning the instrument to PAC for service. The status of any product returned
later than 30 days after the issuance of a return authorization number will be
subject to review.
Products may not be returned that are contaminated by radioactive materials,
infectious agents, or other materials constituting health hazards to PAC's
employees.
1.5.1 Returned product warranty determination

After PAC’s examination, warranty or out-of-warranty status will be determined. If
a warranted defect exists, the product will be repaired at no charge and shipped
pre-paid back to the buyer. Warranty repairs do not extend the original warranty
period.
If an out-of-warranty defect exists, the buyer shall be notified of the repair cost. At
such time, the buyer must issue a valid purchase order to cover the cost of the
repair and freight, or authorize the products to be shipped back as is, at the
buyer’s expense. Failure to obtain a purchase order number approval within
fifteen days of notification will result in the products being returned as is, at the
buyer’s expense.
1.5.2 On-site repair

If a PAC product cannot be made functional by telephone assistance or by
installing replacement parts, and cannot be returned to PAC for repair, the
following policy applies.
PAC will provide an on-site field service representative in a reasonable amount of
time, provided that the customer issues a valid purchase order to PAC covering all
transportation, subsistence, and prevailing labour costs, including travel time,
necessary to complete the repair. For warranty field repairs, the customer will not
be charged for the cost of transportation, labour, or materials. If service is
rendered at times other than normal work periods, then special service rates may
apply.
1.5.3 Inspection
This system was thoroughly inspected and carefully packed before leaving our
factory. Responsibility for its safe delivery was assumed by the carrier upon
acceptance of the shipment. Claims for loss or damage sustained in transit must
be made upon the carrier by the recipient as follows.
1.5.3.1 Visible loss or damage

Note any external evidence of loss or damage on the freight bill or express receipt,
and have it signed by the carrier’s agent. Failure to adequately describe such
external evidence of loss or damage may result in the carrier’s refusing to honour
your damage claim. The form required to file such a claim will be supplied by the
carrier.
12 UM_2.00A_EN
1.5.3.2 Concealed loss or damage

Concealed loss or damage means loss or damage, which becomes apparent
when the merchandise is unpacked and inspected. Should concealed loss or
damage occur, make a written request for inspection by the carrier’s agent within
15 days of the delivery date, then file a claim with the carrier since the damage is
the carrier’s responsibility.
By following these instructions carefully, we guarantee our full support of your
claim to be compensated for loss from shipping damage.
CAUTION
DO NOT - for any reason - return the instrument without first
obtaining authorization.
1.5.4 Information
In any correspondence to PAC, please supply the data from the nameplate,
including catalogue number and serial number.
/i
Catalog number:
Serial number:
Purchase date:
UM_2.00A_EN 13
1.6 Disposal
Correct disposal of Waste Electrical and Electronic Equipment in
the end-of life
Applicable in the European Union and other European countries with
separate collection systems.
This product is designed for exclusive professional use by commercial

companies. This marking shown on the product or its literature, indicates that it
should not be disposed with other household wastes at the end of its working life.
To prevent possible harm to the environment or human health from uncontrolled
waste disposal, please separate this from other types of wastes and recycle it
responsibly to promote the sustainable reuse of material resources.
Business users should contact the producer or the importer and check the terms
and conditions of the purchase contract. If you have a separate agreement with
your producer or your importer on the end-of-life disposal in a way that you will
care for disposal by your own, would you please ensure an environmentally sound
disposal according to the legal regulations for electric and electronic waste
equipment in your country.
This product should not be mixed with other commercial wastes for
disposal.
The above WEEE-symbol is the official marking for equipment under the WEEE-
scope. In some EC-Member states "pure B2B equipment" is not necessarily
marked with the waste bin-symbol. To provide a homogenous EC-wide procedure,
PAC however uses the marking in all EC-Member states.
14 UM_2.00A_EN
1.7 Documentation
1.7.1 Document validity

This manual has been prepared with great care, in compliance with the relevant
regulations, and based on PAC’s experience and latest knowledge.
The information in this document is therefore valid and correct at the moment of
release of this version. (The version number is indicated on the front page of this
manual). However, changes and improvements may be made to this document at
any time and without prior notice.
This document is only complete in conjunction with all other system-related
documents.
1.7.2 Document storage

This document is part of the apparatus that is described in it, and must be kept in
a safe place near the apparatus.
This document must be accessible at all times.
1.7.3 Language
The source language of this manual is English.
As a translation may be inaccurate or imprecise, the original source text will be
legally binding and shall prevail in the case of any difference between the source
text and any translation.
1.7.4 Typographical and authoring conventions

• Hardware buttons that can be pushed, software buttons that can be clicked in
the Human Machine Interface (HMI) of software applications, menu
commands that can be selected, and data that can be entered via a keyboard,
are indicated in the font as shown in the following example:
Click OK.
• Combined menu selections in the HMI are indicated by the ‘>’ symbol, e.g.
Select File > Save As.
• File names and texts in the HMI are indicated in the font as shown here:
The menu Temperature of the Weather screen appears.
• E-mail and internet addresses are indicated as in the following example:
sales@paclp.com.
• Lists and enumerations without prescribed order are always preceded by
bullets (like this list).
• Steps in a procedure, which must be performed in consecutive order, are
always numbered.
• Abbreviations are defined upon their first use in a document (except in a title).
• Throughout this manual, PAC L.P. and its subsidiaries are referred to as
‘PAC’.
UM_2.00A_EN 15
• Throughout this manual, PAC automatic laboratory equipment (or device, unit,
or apparatus) is referred to as the ‘instrument’.
• Throughout this manual, the complete analysis system is referred to as ‘the
system’.
16 UM_2.00A_EN
Safety OptiDist™
2 Safety
UM_2.00A_EN 17
OptiDist™ Safety
2.1 Certifications
The system and its components have been designed with safety in mind. The
design applies to the use, the conditions and the instructions described in the
documentation. The system
• Is CSA/cCSAus approved.
• Has been tested and found to comply with the limits for a Class A digital
device, pursuant to Part 15 of the FCC rules.
• Meets the requirements of the European Directives concerning health,
hygiene and safety. The standards applied are listed in the “CE Declaration of
Conformity”.
For a copy of the corresponding declarations, please consult the Service

Organization of PAC (see back page).
If the user makes changes or modifications that are not expressly approved by
PAC, PAC reserves the right to void the user’s authority to operate the equipment.
During performance or routine maintenance, the system operator may be exposed

to potentially dangerous chemicals, temperatures, electrical voltages and/or other
hazards. In order to reduce the personal risk involved, the following guidelines are
established. These requirements are within accepted standards for general
analytical laboratory operation.
WARNING
Failure to follow the instructions and procedures contained in this
manual could result in death or serious injury.
The instructions and procedures must be performed by qualified
and trained personnel only.
Do not perform installation or maintenance operations or proce-
dures outside the scope of this manual.
Please refer to the corresponding Material Safety Data Sheet (MSDS) for each
PAC-supplied product and also reference the corresponding MSDS that is vendor-
supplied for each sample and standard utilized with the product for the established
safety requirements and government safety and disposal standards.
18 UM_2.00A_EN
Safety OptiDist™
2.2 Warning pictograms

A warning pictogram denotes a dangerous situation that, if not avoided, will result
in serious injury or death. The following warning pictograms can be found in the
manuals and on the apparatus.
WARNING
General warning
WARNING
Danger of high voltages: shock hazard, electrocution hazard
WARNING
Fire hazard
WARNING
Explosion danger: release of pressure hazard
WARNING
Hot surfaces present: burn hazard
WARNING
Cold surfaces present: freeze hazard
WARNING
Danger to jam hands or feet
WARNING
Pinch danger
UM_2.00A_EN 19
OptiDist™ Safety
WARNING
Wedge present
WARNING
Sharp edges present
WARNING
Dangerous fluids and gases
2.3 Caution pictograms

A caution pictogram denotes a situation that, may result in injury or damage. The
following caution pictograms can be found in the manuals and on the apparatus.
CAUTION
General caution
CAUTION
Biohazard
CAUTION
Recycling
CAUTION
Wear a gas mask!
CAUTION
Wear protective gloves!
20 UM_2.00A_EN
Safety OptiDist™
CAUTION
Wear safety glasses!
2.4 Note pictograms

A note pictogram denotes a recommendation that, if not followed, may result in
minor damage. The following note pictogram can be found in the manuals.
NOTE
General note
2.5 Tip pictograms

A tip pictogram denotes a recommendation that can help in understanding how to
operate or service the apparatus. The following tip pictograms can be found in the
manuals.
TIP
General tip
TIP
Read the Service Manual
2.6 Environmental protection

Please observe all local regulations and recommendations for the disposal,
recycling or environmentally friendly processing of parts and materials that have
been used or replaced during installation, operation, and maintenance tasks.
UM_2.00A_EN 21
OptiDist™ Safety
22 UM_2.00A_EN
Introduction OptiDist™
3 Introduction
UM_2.00A_EN 23
OptiDist™ Introduction
3.1 Intended use

The apparatus that is described in this document has been designed and is
intended to determine boiling range characteristics of various commercially
available petroleum products, light and middle distillates at atmospheric pressure
under appropriate conditions.
Any other use or modification of the apparatus without written agreement from
PAC will be regarded as noncompliant: PAC will not be liable for any possible
resulting damage or injury, and the warranty will be voided.
The apparatus may only be operated and serviced by trained qualified authorized
persons.
The operator must refrain from any operation that can affect the safety of the
system and of persons. The operator is always required to ensure that the
apparatus is in proper condition when it is operating.
3.2 Intended audience

This document is intended for customer personnel that installs, sets up, calibrates
and operates the instrument in order to perform analyses, that does preventive
maintenance on the instrument, and that maintains its internal database.
The content of this document must be read, understood and observed in all points
and by each person responsible for the preparation, the transport, the storage, the
installation, the operation, and the maintenance of the instrument, before starting
to work with and on the instrument.
3.3 Product overview

The new PAC OptiDist™ is an automated and user-friendly distillation analyzer
born of a combination of customer feedback and over eighty years combined
experience of the companies Walter Herzog and ISL in designing and
manufacturing automatic distillation equipment.
According to strict guidelines and protocols described in these standard test

methods, a given volume of sample is distilled under appropriate conditions
according to its group or class. During the analysis, temperature, volume of
condensate and time are precisely and systematically recorded. The resulting
data is used to determine the materials distillation (or volatility) characteristics.
Test results are commonly expressed as percent evaporated or percent recovered
(according to the sample group) versus corresponding temperature.
Utilizing advanced technology and a high quality design, the OptiDist™ allows
laboratory analysts of all skill levels to perform automatic atmospheric pressure
distillations, which comply with consensus group standard test methods, on a wide
variety of liquid hydrocarbon materials. Typically, these distillations are used to
characterize the tendency of a hydrocarbon fuel to vaporize. Vaporization
characteristics are a critical measure of overall fuel safety and performance.
The instrument offers several modes of operation that employ the power of
automation to significantly increase test productivity (sample throughput) while
also improving repeatability and reproducibility. In all modes, a large graphical
24 UM_2.00A_EN
touch screen interface provides guidance regarding instrument set up and

standard test method requirements that can prove ideal for new or untrained staff
that have small exposure to the distillation test procedure. Each mode is designed
to operate with minimal test programming, while supplying quick, reliable boiling
range characteristics of a product often giving results in compliance with a wide
range of standard methods from the first analysis.
Simple, straightforward operation involves selecting a sample ID or a product from

pre-stored lists following the group in which the sample falls and pressing the
“Start” button when a distillation flask filled with test specimen is placed on the
instrument. No special programming of test conditions is required. To determine
the optimal heating curve, the OptiDist™ employs the unique optimizer
technology. The optimizer technology assures perfect repeatability of distillation
conditions without a compromise on safety. Results are automatically corrected for
barometric pressure and stored to permanent memory. Immediately following test
completion, the OptiDist™ provides a user-customizable report and as pre-
programmed by the user or upon demand, prints and/or transmits results to a
LIMS.
For fast and reliable quality control, analyzed samples can be instantaneously
compared to specifications programmable in the pre-stored product for in spec /
out-spec control. Up to 200 products can be preprogrammed and saved. Thus,
analysts can instantaneously see the information on how obtained results match
to pre-programmed typical specifications, i.e. typical temperature vs. volume or
volume vs. temperature, for fast product quality evaluation. The instrument can
automatically generate a Pass/Fail quality statement providing a detailed report.
The OptiDist™ can be operated as a stand-alone distillation unit. lt also can be

networked with up to thirty with the HLIS®, ALAN® or PDS™ PC software, while
each unit operates independently from the others. The PC connected to the
OptiDist™ plays the role of a central data collection and management server.
Sophisticated safety features include a built-in fire extinguisher system, traceable

automatic calibrations, continual self-monitoring and that helps meet increasing
safety and quality assurance requirements.
3.4 Applicable standard methods

/i
Table 3.1 Applicable methods

Standard method Remark
IP123 British standard method
IP 195 British standard method
ISO 918 International standard method
EN ISO 3405 International standard method
DIN 51751 German standard method
NF M07-002 French standard method
JIS K2254 Japanese standard method
UM_2.00A_EN 25
Standard method Remark

ASTM D86 US Standard method (group 0 to 4)
ASTM D850 US Standard method
ASTM D1078 US Standard method
3.5 Benefits and features

• Accurately determine boiling range characteristics of various commercially
available petroleum products, light and middle distillates at atmospheric
pressure under appropriate conditions.
• Easy to use mistake proof unit:
- Quick connection for distillation flask
- Self positioning heater lift
- Automatic heater base plate detection
- Sensor to detect if the condenser tube is cleaned
• Enhanced control of the sample preparation
• One button straight forward operation
• Superior test precision from the first analysis
• Measurement of the charge volume
• Sophisticated safety features
- Fire extinguisher
- Volatile Organic Components (VOC) control option
• Advanced MMI (touchscreen) contributing to a trouble-free operation
• Large graphic color touch screen with solvent proof protection
• Versatility (Standards ASTM, DIN, EN, etc.)
• Enhanced quality features
• Automatic system validation and calibration using user-defined parameters
• Password protection ensures only authorized changes are made to system
settings
• Stand alone or networked
• Maximized throughput
• Networking capability via external PC with HLIS®, ALAN® or PDS™ software
• Critical operating parameters such as heating and detector temperatures
monitored remotely with HLIS® & ALAN® or PDS™ Network software or
locally by the touchscreen
• Internal or external printer
• Customized printer reports
• Small foot print
26 UM_2.00A_EN
• Enhanced optics
• 24-bit high-resolution A to D converter
3.6 General Scope

The fully automatic OptiDist™ distillation analyzer of PAC has been designed to
determine quickly and with high precision boiling range characteristics of various
commercially available petroleum products, light and middle distillates at
atmospheric pressure under appropriate conditions.
OptiDist™ runs unknown products without preprogramming often-yielding results
in compliance with a wide range of standard methods (as listed in Table 3.1.
Applicable methods) from the first analysis.
The operator can also run:

• Tests in manual mode by replacing the temperature probe with the standard
specified liquid in glass thermometer
• Non-standard tests which do not correspond with any of the above-mentioned
standard methods with customer defined temperature profiles for the
condenser bath temperature and with customer defined distillation rate in the
range of 2 to 10 ml/min.
It is not intended for products containing an appreciable quantity of residual

material that cannot be distilled at atmospheric pressure without thermal
decomposition.
Application is limited to samples having a boiling range between 20 °C (68 °F) and
450 °C (842 °F).
3.7 Terminology
/i
Dry Point (DP): Thermometer reading observed when the last drop of liquid evapo-
rates from the lowest point in the distillation flask. Drops or films of liq-
uid on the side of the distillation flask are disregarded.
Final Boiling Point (FBP) The maximum thermometer reading obtained during the test. Usually
occurs after the evaporation of all liquid from the bottom of the distilla-
tion flask. Also known as Maximum Temperature.
Initial Boiling Point (IBP) The temperature at the instant the first drop falls from the lower end of
the condenser tube.
Per Cent Residue % volume of residue left in the distillation flask (measured in accord-
ance with the standard in a 5 ml graduated cylinder).
Corrected temperature Temperature reading as describe above corrected for barometric pres-
reading sure at 101,3 kPa.
Per Cent recovery The volume measured at the end of the distillation if after a 2-minute
interval two successive observations agree (measured in accordance
with standard method).
Percent total Recovery The combined percent recovery and residue in the distillation flask. To
get percent loss deduct percent total recovery from 100.
Thermometer reading The temperature of the vapor measured in the neck of the distillation
flask below the vapor tube.
UM_2.00A_EN 27
3.8 List of abbreviations

/i
°C Degrees Celsius
°F Degrees Fahrenheit
AN Application Note
CI: Cetan index
DI: Driveability (or distillation) Index
DP Dry Point
FBP Final Boiling Point
hPa hecto Pascal (1 hPa = 1 mbar)
IBP Initial Boiling Point
ICM Installation and Configuration Manual
ID Identity - Identification
IM Interface Manual
K Degrees Kelvin
kPA kilo Pascal (1 kPa = 10 mbar)
LCD Liquid Crystal Display
LED Light Emitting Diode
LIMS Lab Information Management System
mA milliamps
MM Maintenance Manual
mmHG millimeters of mercury column
MMI Man Machine Interface
OM Operator Manual
P/N Part Number
PAC Petroleum Analyzer Company, L.P.
PM Process Manual (System Description)
QC-DB Quality Control Database
SM Supervisor Manual
SPM Site preparation Manual
SS System Specification
Temp. Temperature
TFT Thin Film Transistor
VOC Volatile Organic Components
3.9 Nameplate
The nameplate is located on the rear of the OptiDist™ housing.
28 UM_2.00A_EN
3.10 Specifications
/i
Distillation Rate 2 to 10 ml / min, programmable

Note: The OptiDist™ automatically stores the heating rate that can be
shown on the display during the test.
Equipments
User interface • Large graphic TFT-LCD (Thin Film Transistor Liquid Crystal Display)
color touch-screen with solvent-proof protection
Heating system • Low mass and low voltage, self-positioning heating system
• Unique Optimizer function for fully automatic initial heat settings and
heating regulation
• Detectors for heater plate, vapor probe and centering device
Condenser system • Temperature range from 0 °C to 65 °C (32 °F to 149 °F)
• Programmable constant temperature, temperature ramping or special
temperature profile
• Instantaneously ready at switch on
Receiving chamber • Temperature range from 0 °C to 40 °C (32 °F to 104 °F)
• Programmable constant temperature, temperature ramping or special
temperature profile
• Instantaneously ready at switch on
• Compatible with 100 ml and 200 ml receiver cylinders
• Detectors for "receiver cylinder in place" and "door open"
Cooling system • CFC free cooling unit
• Factory sealed cooling circuit with mono ethylene-glycol and water 50/
50 base mixture as heat exchanging liquid (must be ordered from
PAC)
Safety • Built in fire extinguisher with 2 fire sensors
Connectivity External links:
On the right side:

• USB A: Connection of an optional external printer or bar code reader
or a memory device (USB key) for data transfer and firmware update
• 25-pin connector: Doctor Box connection (optional accessory)
At the rear (on the left top):

• RS 232C serial port: connection to LIMS with user-customizable com-
munication protocol (CTS, ENQ, ACK, XON, XOFF)
• RJ45: Ethernet connection for networking with HLIS® or ALAN® soft-
ware, data transfer and firmware update
• USB A: Connection of an optional external printer or bar code reader
or a memory device (USB key) for data transfer and firmware update
• 4-pin DIN connector: Connection of the optional status indicator bea-
con
• 3-pin DIN connector: Connection of the optional ambient temperature
sensor
At the rear (on the left bottom):

• Hose nozzle. Inlet connection for extinguisher gas source
UM_2.00A_EN 29
Measurements
Vapor Temperature • Range : 0 °C to 450 °C (32 °F to 842 °F)
• Accuracy: Pt 100 IEC 751 probe Class A
• Built in calibration memory with 10 point calibration table and auto-
matic probe ID detection; calibration history; optional calibration certif-
icate
Sample Volume • Optical measuring system compatible with samples producing smoke
in the receiver
• Range: 0% to 103% of charge volume
• Resolution: 0,03 ml (internal)
• Accuracy: ± 0,1 ml
Ambient Pressure • Built-in pressure sensor
• Range: 70 to 110 kPa (500 to 800 mmHg)
• Calibration: Single point against reference barometer
Condenser Bath Tem- • Measuring instrument: Incorporated IC temperature sensor (Inte-
perature grated Circuit)
• Range: 0 °C to 65 °C (32 °F to 149 °F)
• Accuracy: ± 0,5 °C at 25 °C (± 0,9 °F at 77 °F)
Receiving Chamber • Measuring instrument: Incorporated IC temperature sensor (Inte-
Temperature grated Circuit)
• Range: 0 °C to 40 °C (32 °F to 104 °F)
• Accuracy: ± 0,5 °C (± 0,9 °F)
Heating element tem- • Thermocouple K
perature
Optional equipments • Built-in printer
• External printer
• Barcode reader
• External status indicator
• Ambient temperature sensor
• Automatic dry point kit for 200 ml
• Automatic dry point kit for 125 ml
• Option for reduced VOC emission
• Crude oil testing capability
• 200 ml test kit for 10% bottom residue
• Doctor Box
• CRM reference materials
30 UM_2.00A_EN
Description OptiDist™
4 Description
UM_2.00A_EN 31
OptiDist™ Description
4.1 Views of the OptiDist™
4.1.1 Front view left
A
B
C
D
K
E
J
F G
OptiDist™ – Front view left

A Wire support
B Vapor temperature probe connector
C Dry point sensor connector
D Flask stopper holder
E Flask heater enclosure door
F Flask heater assembly cooling fan
G Automatic positioning lever for the flask heater platform
H Spillage trap
I Receiving chamber door
J Door latch
K Touch-screen
L Built-in printer (optional)
32 UM_2.00A_EN
4.1.2 Front view right
E
D
B C
OptiDist™ – Front view right

A Power-on light
B Emergency stop button
C USB B connector for connection of a PC
D USB A connector for connection of an external printer or a bar code reader or a USB key
E 25-pin connector for connection of the optional Doctor Box
F Main power switch
UM_2.00A_EN 33
4.1.3 Rear view
J
A
I
B
C
H
D
E
F
OptiDist™ – Rear view

A RS232C connector
B RJ45 Ethernet connector for connection to the network
C USB A connector for connection of an external printer or a bar code reader or a USB key
D 4-pin DIN connector for connection of the optional status indicator beacon
E 3-pin connector for connection of the optional ambient temperature sensor
F Power supply (mains) cable
G VOC outlet (optional)
H Fire extinguisher gas source inlet connector
I Rear panel cooling fan
J Fire emergency signal series contact grommet
4.1.4 Connection ports

The following connections are available:
At the front of the OptiDist™, above the distillation flask heater platform (from top
to bottom)
• 8-pin DIN socket connector: Connection of the sample vapor temperature
probe
• 5-pin DIN socket connector: Connection of the optional automatic dry point
detection kit
34 UM_2.00A_EN
At the rear of the OptiDist™, on the left top (from top to bottom)
• RS 232C serial port: Connection to a LIMS with user-customizable
communication protocol (CTS, ENQ, ACK, XON, XOFF)
• RJ45 Ethernet connector: Connection of the unit to the OptiDist™ network
• USB A connector: Connection of the optional external printer or bar code

reader
• 4-pin DIN connector: Connection of the optional status indicator beacon
• 3-pin DIN connector: Connection of the optional ambient temperature sensor
At the rear of the OptiDist™, on the left top (from top to bottom)
• Hose nozzle: Fire extinguisher gas source connection
On the right side of the OptiDist™

• 25-pin connector: Connection of the optional Doctor Box
• USB A connector: Connection of an USB memory stick for software updating
and data transfer (results, products, etc.)
• USB B connector: Connection of a PC
UM_2.00A_EN 35
4.2 Description of the OptiDist™front

The front of the OptiDist™ can be divided into three major parts.
Three major parts of the OptiDist™

A The distillation flask heater assembly
B The receiving chamber (as the condensate recovery area)
C The touch-screen or Man Machine Interface (MMI)
During a distillation run, the Central Processing Unit (CPU) of the OptiDist™
controls and monitors the operation of the overall system by means of a user
designated distillation product program and data received from the heating block,
the condenser bath and the receiving chamber.
36 UM_2.00A_EN
4.3 Distillation flask heater assembly
4.3.1 Overview
B J
C I
D H
E G
Distillation flask heater assembly

A Flask stopper attachment device
B Fire extinguisher injection slots for CO2 gas injection
C Self-positioning flask heater platform
D Base plate
E Cooling fan of the flask and flask heater assembly
F Lever of the automatic positioning device of the flask heater platform
G Door
H Heating element
I Opening for optimizer
J Opening of the first fire detector
The distillation flask heater assembly, located to the left of the touch-screen,
breaks down as follows:
UM_2.00A_EN 37
• Distillation flask heater assembly enclosure door (G) for protection of the
operator from accidents and against air drafts draughts.
The distillation flask enclosure has a transparent glass door, at the front for
easy access to and inspection of the distillation flask. The transparent door
has been specially selected for its resistance to heat and shocks.
• A distillation flask stopper attachment device (A) assures that the distillation
flask is well positioned in the distillation flask heater platform (C).
• Two fire extinguisher injection slots (B) (one above and one under the heating
element). CO2 gas injection spray is triggered by two flame detectors (J)
situated on the internal right side of the distillation flask heater assembly
enclosure, above and under the heater platform.
• A fan (E) at the bottom of the distillation flask heater assembly is positioned
for rapid cooling of the distillation flask. For increase distillation flask cooling
efficiency the distillation flask heater platform (C) is automatically released in
low position at the end of test run for a better air distribution. This is performed
by energizing an electromagnet at the rear of the distillation flask heater
platform releasing the automatic positioning device of the heating platform.
The lower part of the distillation flask heater platform is hidden by housing,
while the upper part is easily accessible by opening the transparent door (G)
for placing the distillation flask.
4.3.2 Self-positioning flask heater platform

The flask heater platform features a manually activated automatic distillation flask
positioning capability that helps eliminate most common operator errors as they
relate to test setup and pre-test operations.
The Automatic Positioning Device of the Flask heater platform and the Flask
Stopper assures proper and repeatable flask positioning and improves heating
efficiency and analysis repeatability.
The manually activated lever of the automatic positioning device of the heater
platform is used to lower or to raise the heater platform:
• Lower the flask heater platform positioning lever and the flask heater platform
comes in contact with the flask bottom (high position).
• Pull the flask heater platform positioning lever towards the top to release the
flask heater platform (low position) for flask insertion or removal.
A base plate or flask support board with centered hole, diameter 32 mm (1 1/4 in.),
38 mm (1 1/2 in.) or 50 mm (2 in.) is placed on the heater platform. The heater
platform is equipped with a base plate identification sensor that allows
confirmation that the right base plate is used according to the product group
selected and that the flask and base plate are well positioned.
4.3.3 Heating regulation

After entering the group number, the optimal distillation conditions for every
sample run are assured by a unique Heating Optimizer function of the analyzer.
Backed by leading research and advanced technology, the OptiDist™ heating
system typically allows method compliant results from the first run. Without
38 UM_2.00A_EN
preliminary trials and manual adjustments, the operator selects the test method,
enter the samples distillation group and starts the distillation by just pressing the
Start button.
Heater temperature monitoring and advanced mechanical design of the oven
assures excellent repeatability of distillation conditions in complete safety. Any
dependence on the heating element aging or on flask conditions are eliminated.
The optimized heating protects flask material from critical overheating improving
flask life-time and preventing against potential fire.
4.3.4 Heating element

The heating element is a low mass and low voltage element, adjustable from 0 to
600 Watts. It is mounted on a self-positioning heater platform that assures proper
and repeatable positioning of the heating source thereby improving heating
efficiency and analysis repeatability.
The heating element is a wrapped wire resistor that is embedded in a reflective
shield that helps minimize energy losses. This mechanism also enables a direct
flask contact assuring effective energy transfer to the liquid specimen. Approved
flasks of all distillation types (100, 125, 200 and 250 ml) can be utilized without a
need for heater element modification or reconfiguration. A thermocouple in the
center of the heating element provides precise temperature control and helps
protect the flask material from critical overheating.
In case of failure of the heating element, the user will be alerted by an alarm.
4.3.5 Flask cooling

A fan assures the cooling of the heating element and flask. The cooling has been
improved by automatically releasing the heating platform towards the bottom at
the end of test and guiding the air around the flask. Doing this allows a fast
preparation for the next run: flask cooling and readiness for the next test do not
take more than 10 minutes. The reference temperature is permanently monitored
at cooling (vapor and heater temperature). The operator is alerted when he can
safely remove the flask by the green color of the status bar in the Run / Start &
Display Screen or the green light of the Status Indicator Beacon (available as
option accessories). This safety threshold parameter is programmable by the user
allowing deciding the accepted level of safety.
4.3.6 Safety features

The flask heater assembly includes a sophisticated automatic fire extinguisher
system as standard equipment, ready for connection to an external gas supply.
This system, specially developed for the OptiDist™ System, enables flame
detection and the injection of CO2 in less than a 1 second.
UM_2.00A_EN 39
4.3.7 Distillation flask
C B
Distillation flask
A Flask neck
B Vapor tube sealing ring
C Vapor tube
The distillation flask provided is made of heat resistant glass and meets standard
specifications. Its capacity depends on the used standard method.
The distillation flask is equipped with a sealing ring on the distillation flask vapor
tube to ensure an airtight connection to the condenser.
Use only original PAC distillation flasks as replacement parts.
You have to use different sizes of the distillation flask according to the different
distillation standards. See the spare parts list.
40 UM_2.00A_EN
4.3.8 Distillation flask stopper
Distillation flask stopper

A Stopper attachment device
B Threaded probe sealing device (compression nut)
C Attachment device for the flask
The distillation flask stopper assembly provides a quick, reproducible and

pressure tight seal between the distillation flask neck and the vapor temperaure
probe. The vapor temperature probe is automatically centered in the proper
distillation flask neck location.
Additionally, the distillation flask stopper assembly is equipped with an attachment
device that holds the distillation flask in a way that enables an automatic self-
positioning of the distillation flask in the distillation flask heater platform.
The detection of the right position of the distillation flask when the distillation flask
heater platform is in the run test position allows the test start. The operator is
alerted by the green/red color of the status bar in the Run /Start & Display screen
or the green/red light of the optional status indicator beacon.
A liquid in glass thermometer for analysis in manual distillation test mode can
replace the vapor temperature probe.
An automatic dry point detection kit can likewise replace the distillation flask
stopper (the type of sensor is automatically recognized by the system).
UM_2.00A_EN 41
4.3.9 Vapor temperature probe
Vapor temperature probe

A Vapor temperature probe
B Distillation flask stopper
C Flask stopper holder
The vapor temperature probe is a Pt100 IEC 751 platinum probe class A with
built-in memory chip including probe correction values. This means the OptiDist™
automatically recognizes the probe and imports data at plug-in avoiding the need
to enter manually probe correction values and probe ID. Up to 5 calibration points
can be memorized (2 calibration points as standard).
Insert the probe wiring through the wire support atop the distillation flask heater
assembly and install the vapor temperature probe terminal plug into the connector
socket located on the top of the OptiDist™ above the distillation flask heater
platform. When not in use the temperature probe should be placed in the probe
holder atop the unit.
Before the distillation test, the vapor temperature probe must be inserted into the
distillation flask so that the probe is centered into the distillation flask: this is
ensured by the stopper assembly; and the depth of the vapor temperature probe
in the distillation flask must be precisely adjusted. To help the operator to position
the vapor temperature probe with a perfect repeatability, the stopper holder has
been specially designed as a gauge.
42 UM_2.00A_EN
4.4 The receiving chamber
4.4.1 Overview
A O
B N
C M
L
K
J
E
F I
G H
Receiving chamber overview

A Receiving chamber door, made of transparent Plexiglass®, equipped with a rubber sealing
buffer ensuring that the chamber is airtight when the door is closed avoiding humidity
condensation
B Bottom end of the condenser tube
C Drip tip attached to the condenser tube
D Ventilation fan for homogeneous temperature distribution
E VOC exhaust
F Receiver temperature probe
G Graduated cylinder stand
H Spillage trap with 200 ml capacity
I Inlet of cooling liquid connected to the heat exchanger
J Heat exchanger connected to the cooling system including a heating plate
K Door latch
L Movable optical fork for detection of the graduate receiver and level follower
M Fixed optical fork for detection of the first drop of condensate
N Rubber collar, automatically positioned on the top of the receiver when inserted
O Door position detector (open/closed)
The receiver cylinder is placed in a constant temperature air circulation chamber

for the distillate recovery. This automatically regulated chamber called “receiving
chamber” is located under the touch screen. Its function is to ensure the prediction
of true liquid temperature in the receiver cylinder at the moment of volume
measurement.
UM_2.00A_EN 43
The regulation capability of the receiving chamber starts from 0 °C to 40 °C (32 °F

to 104 °F) and is accurate to the nearest ± 1 °C when setpoint ≤ 30 °C (86 °F) and
to the nearest ±2 °C after the IBP when setpoint > 30 °C (86 °F). It can be
regulated during run at programmable single setpoint temperature, according to
the recovered volume or the vapor temperature and in standby at selected
temperature.
An alarm is triggered if the receiving chamber temperature exceeds 50 °C (122 °F)
and if the door is opened during test impacting proper temperature regulation in
the chamber and resulting in an error in volume measurement. Proper cylinder
placement is assured by a special guide.
The OptiDist™ continually monitors the recovered volume recorded as percent
recovery. For this, the receiving chamber is equipped with an automatic optical
measurement system with a movable part which detects the first drop of
condensate (IBP) according to standard requirements and measures the sample
volume retained into the receiver cylinder to the nearest 0,1 ml. The transmission
device of the measurement system called the “level follower” is located on the
external right side of the receiving chamber. When in its role of level follower
detector, the movable optical fork is powered by a stepping motor. When the
OptiDist™ is in standby, the level follower is typically in the upper position.
The presence of the receiver cylinder is checked at test starting. If the receiver
cylinder is present, the level follower checks that it is empty and prevents from test
starting if not.
The level follower can also measure the sample charge volume in the receiver
cylinder; the sample volume retained in the receiver cylinder immediately after the
receiver cylinder is put in place (the value is reported and used as check list
criteria avoiding dead volume) and, at the end of test, the residue by transferring
the distillation flask bottom to the receiver cylinder containing recovery. The
software calculates the difference in measured volume (Recovery 1 - Recovery 2)
and reports it as residue.
Both receiving chamber and volume level measurement system have corrosion
proof design preventing from corrosive vapors and humidity condensation when
operated at sub-ambient temperatures.
A ventilation system is located under the receiving chamber preventing from
excessive evaporation loss of distillate from the receiver cylinder during the run
with light material. This system, the VOC control (available as option accessories)
should be connected with a tube to an appropriate ventilation system.
44 UM_2.00A_EN
4.4.2 Receiver cylinder
Receiver cylinder
A Receiver cylinder
The receiver cylinder provided with the OptiDist™, also called receiver or
graduated cylinder, meets standard test method specifications. The receiver
cylinder is used to
• measure the volume of the material to be distilled (exactly 100% by volume)
for the sample preparation
• for distillate recovery.
After the material is poured into the distillation flask, the receiver must be
positioned in the receiving chamber. The drop plate allowing the distillate to run
down the wall of the receiver is fixed directly to the end of the condenser tube
assuring it is not forgotten before test starting and it is well positioned. The
receiver stand positioning at the bottom of the receiving chamber assures the right
position of the receiver so that the drip tip automatically touches the wall of the
receiver.
If the glass cylinder is replaced after damage, take care that the glass cylinder is
completely on the base to ensure that the 100% volume mark is positioned
properly inside the cylinder (= 180 mm).
NOTE
A 200 ml receiver cylinder is available as optional accessories for
ASTM D189 tests. No re-calibration of the system is needed
between tests with 100 ml and 200 ml receiver cylinders; the stand-
ard method selected in the distillation product determines the cali-
bration scale.
UM_2.00A_EN 45
4.4.3 Condenser tube regulation

The condenser tube is made of corrosion proof stainless steel and meets all test
standard definitions. The upper end of the condenser tube projects into the upper
part of the flask heater assembly while the lower portion of the condenser tube
projects into the receiving chamber.
The drip tip is attached to the condenser tube end to ensure the operator will not
forget it thus avoiding improper volume measurement and a bad distillation rate
regulation. The position of the receiver cylinder stand allows the drip tip to
systematically touch the wall of the receiver cylinder assuring the proper and
repeatable receiver cylinder and drip tip positioning.
Condenser tube cleaning is systematically verified before starting a test. A sensor
installed on the condenser tube automatically detects the passing of the specially
constructed pull-through cleaning swab that is supplied with the analyzer. A new
test can then begin when indicated by the green/red color of the status bar in the
Run / Start & Display screen or the green/red light of the Status Indicator Beacon
(available as option accessories).
If the condenser temperature exceeds 35°C (95°F) during a test, the condenser
tube is kept warm until it is cleaned to facilitate the removal of any waxy residue.
The condenser tube is set in a thermostatically controlled bath that is directly
connected to the cooling system. On the other hand, the condenser tube can be
equipped with an optional boost heater allowing heating of the condenser tube
from 0 °C to 50 °C (32 °F to 122 °F) within less than 3 minutes.
The condenser bath regulation capability starts from 0 °C to 65 °C (32 °F to 149°F)
complying with the specifications for the standard methods referred to at the
beginning of this manual. The delay to start the first test of the day at ambient
temperature (30°C/86°F) is only a few minutes. No delay is required to start next
test with any different group. The condenser bath temperature stability and
uniformity comply as defined by the corresponding standard test method.
The automatic temperature regulation allows various set points: Programmable
single set point temperature, programmable proportional heating ramp with start
and end temperature, condenser step profile with start temperature, condenser
end temperature, vapor temperature where change starts.
The condenser calibration opening, to the right of the probe holder on the top of
the analyzer is for insertion of a thermometer for control of the temperature
measurement circuit of the condenser bath temperature probe.
4.4.4 Cooling unit

The receiving chamber and condenser bath temperature are regulated by
circulation of a heat exchanging liquid in closed circuits. A heat exchanger
provides the interface between the heat exchanging liquid and the air in the
receiving chamber.
A cooling unit and a heat exchanger are used for rapid cooling of the heat
exchanging liquid. Temperature regulation is by means of an electrical flow-
through heater.
In this manual the overall system will be referred to as the "COOLING SYSTEM",
while "COOLING UNIT" is used when referring to the actual cooling device, or
"cold source".
46 UM_2.00A_EN
Once the OptiDist™ is switched on, a continuous pump operation ensures

circulation of the heat exchanging liquid in the main circuit and in the condenser
bath closed circuit. An intermittent (on-demand) pump ensures circulation of the
heat exchanging liquid in the receiving chamber closed circuit.
Hydro fluorocarbon is used as cooling gas in the cooling unit respecting the
environment (HFC R134A). The cooling unit is factory filled and sealed.
The heat exchanging liquid used in the cooling system is a base mixture
composed of mono ethylene-glycol and water. The cooling system circuit is factory
filled through a reservoir equipped with a level sensor. If the heat exchanging
liquid level in circuit is insufficient, the power supply to the "power consuming
devices" is cut off by a security system inhibiting the temperature regulation and
the pumps.
NOTE
The heat exchanging liquid level in the cooling system may have to
be serviced about every two years. The system will be alerted by
the level sensor of the reservoir and the failure alarm “Low cooling
liquid level” will be triggered.
The procedure for filling the cooling system is explained in the maintenance
manual.
The heat exchanging liquid supplied by PAC has been specially studied and
developed. Its thermal capacity, its viscosity at the working temperature, its anti-
corrosive and anti-foaming properties are particularly important for the correct
operation and preservation of the circuits.
NOTE
The heat exchanging liquid must be ordered at PAC (see the spare
parts list). It is important to use coolant provided by PAC for correct
operation of your OptiDist™, as its properties are particularly com-
patible with the application.
In case of problem in the cooling circuit, the circuit must be drained before
replacing any part (call for a qualified technician).
UM_2.00A_EN 47
4.5 Safety features

To prevent damage to the OptiDist™ and its various devices, the system has a
number of built-in safety functions.
4.5.1 Emergency stop button

An emergency stop button is on the front of the OptiDist™, allowing to stop rapidly
the test currently running in case of emergency.
4.5.2 Passive safety - receiver liquid spillage trap

If some liquid was spilled into the receiving chamber due to receiver breakage, the
liquid will be recovered in a liquid spillage trap protecting instrument components
from damage. The liquid trap has a capacity of 200 ml and can be easily drained.
4.5.3 Alarms
No parts of the OptiDist™ at dangerous voltages are accessible by the operator
(EN 61010-1).
Alarms are accompanied by a discontinuous audio alarm,. They remain visible as
long as the default persists; even if the alarm has been acknowledged.
Alarms warn the operator in the event of a malfunction whether the OptiDist™ is in
test or idle:
• Detection of a default during the test run:
- Opening of the receiving chamber door for example
• Component failure detection
• Detection of a safety state (either absolute or fixed by the user)
WARNING
Generally when the alarm buzzer is triggered, the operator must
display the cause and ensure that safety features are working cor-
rectly.
Failure alarm detection has at least one of the following consequences:

• A test cannot be started
• A test in progress is stopped
When a test is stopped the following occurs (if a power supply cutoff has not been
occurred before):
• The distillation flask heater is switched off
• The level follower goes to the upper or standby position
• The distillation flask cooling starts up
• The receiver chamber temperature is regulated to the standby value
(configured in the service parameters)
48 UM_2.00A_EN
• The bath condenser temperature is regulated to its standby value (configured

in the service parameters)
• The status bar indicating the state of the unit becomes red and indicates
"Error"
4.5.4 Automatic fire extinguisher system

The OptiDist™ distillation flask heater assembly is equipped with an automatic
built-in fire extinguisher system that is based on two enhanced ultraviolet
detectors located on the right side of the enclosure, above and under the heater
platform. This system is made up of two injection slots located above and under
the heating element in the distillation flask heater assembly. This enables flame
detection in less than a tenth of a second and the injection of the extinguisher gas
through two slots in less than one second later. Extinguishing takes between 2
and 4 seconds.
CAUTION
A fire extinguisher must always be available in the laboratory. If a
flame has been extinguished with CO2 gas, we strongly advise to
open the windows to air the laboratory.
When a fire is detected, the system injects extinguisher gas into the distillation
flask heater assembly, switches the only power consuming devices off and emits a
continuous loud alarm. Faults can be displayed on the screen by activating the
Message main menu: “Fire Detection” will appear. Switch off the unit to stop the
alarm.
NOTE
A serial contact is provided to connect the fire emergency signal to
an external “fire” alarm device.
NOTE
The gas supply is connected externally at the rear of the Opti-
Dist™.
NOTE
In order to make sure of the good working order of the system, it is
advised regularly testing the flame detector and the control sole-
noid valve of the CO2 inlet.
Time between controls depends on the OptiDist™ environment. The user and the
service personal will determine the ideal interval according to their observations
and their experience.
UM_2.00A_EN 49
CAUTION
If a flame has been detected and extinguished, the system must be
tested again.
WARNING
Repairs should only be carried out by a qualified technician.
WARNING
If one of the failures does not trigger the power supply off automati-
cally, switch off the main power and disconnect the OptiDist™ from
the mains.
50 UM_2.00A_EN
4.6 Optional parts

The OptiDist™ can be equipped with following optional parts:
4.6.1 Ambient temperature probe

An optional temperature probe is available as accessory for the measurement of
the ambient temperature where the OptiDist™ is installed. This temperature can
help with the unit diagnostic and can be used to adjust the receiver temperature to
the ambient temperature.
4.6.2 Optional 125 ml and 200 ml automatic dry point detection kit
The dry point sensor must be installed in the distillation flask so that the point of
the sensor rests exactly at the center of the lowest point at the bottom of the
distillation flask. This is ensured by the specific stopper.
The automatic dry point sensor (DP sensor) consists of a long stainless steel
jacket with a thermocouple at the lower end to detect temperature differences.
NOTE
The type of dry point sensor (125 or 200 ml) is automatically recog-
nized at plug in by the OptiDist™.
NOTE
Boiling stones should not be used with the automatic dry point
detection kit.
4.6.2.1 Adjust the vapor temperature probe in the dry point stopper
Vapor temperature probe location and fixing
procedure in the dry point stopper: A
1. Loosen the threaded probe-sealing
B
device (compression nut) (B).
2. lnsert the vapor temperature probe (A)
through the threaded nut opening
3. Position the adjustment gauge (C) C
supplied against the dry point stopper.
4. Adjust the depth of the vapor temperature D
probe (A) so that the probe tip just
touches the bottom of the corresponding
notch.
5. Tighten the threaded compression nut until the vapor temperature probe (A) is
securely fixed at the proper depth.
6. Confirm that the vapor temperature probe (A) is properly sealed in place by
grasping the metal sheath at the probe base and applying a gentle twisting
motion.
UM_2.00A_EN 51
The vapor temperature probe should be securely fixed in position and not be
easily moved.
lf the vapor temperature probe is not held securely, repeat the adjustment
procedure.
52 UM_2.00A_EN
4.6.3 Optional kit for “10 % (V/V) Distillation Residue” with 200 ml
The optional kit available to get the 10% Distillation Residue for Carbon Residue
measurement with 200 ml consists of
• a 200 ml receiver cylinder
• a drip tip expansion
• a 250 ml distillation flask
4.6.4 Optional external PC control: HLIS-32® or ALAN®

The OptiDist™ is equipped as standard with a fast Ethernet interface allowing
connecting and networking stand-alone units either with the HLIS-32®
management software (Herzog Labor Information System) designed by Herzog or
with the ALAN® management software (Automatic Laboratory Analyzer Network)
designed by ISL.
NOTE
The Alan® and HLIS-32® kits are optional hardware and software
packages (see the spare parts list).
Refer to the corresponding software Installation and Getting
Started Manual for requirements and instructions.
These two software are multitasking software suitable for use with 32-bit system
such as Windows©. They allow several OptiDist™ to be connected to the same
PC. Besides multi-OptiDist™s results retrieving and database management (and
according to the OptiDist™ type: run control, alarms displaying, internal
parameters management, etc.), ALAN® and HLIS-32® software allow transmitting
results directly to a LIMS (Laboratory Information Management System).
Each program comprises several modules. The main program operates as the
control center. This component of the software makes the functions available with
all types of respective brand units in the same way. The OptiDist™ specific
program module can thus be added to the main program if already installed in
your laboratory.
• PC software centralizes the

- result database
- LIMS protocols
- printer protocols
• PC software assures
- printout (launched from the unit or PC)
- link with legacy network software
- link with LIMS
• The unit
- manages dialogue with PC in real time
- sends results to PC
UM_2.00A_EN 53
4.6.5 Optional external data management software: PDS™

The PDS™ software has been designed and is intended to provide data
management features, including the ability to:
• Control and monitor PAC instruments;
• Collect and archive test data;
• Perform and report on test results and trends;
• Provide analysis of collected result data;
• Connect to external Lab Information Management Systems (LIMS).
PDS™ collects test results from your PAC instruments and stores this data in an
SQL database.
With the integrated Online Manager you can define your operation, tests and
instruments. You can also specify users, access privileges and test result
parameters.
The Workbench, a further component of PDS™, communicates with the
instruments: it controls the execution of tests and gathers and analyzes real-time
data.
Each PAC instrument has a PAC instrument plug-in associated with it.
Instrument plug-ins extend the funcionality of the Workbench by providing features
that are specific to the corresponding instrument.
PDS™ comes in two versions:
• a stand-alone version
• a Client-Server version
4.6.6 Optional status indicator beacon

A “instrument status” indicator light is available as optional accessory (see the
spare parts list). It provides information on the OptiDist™ status viewable from
minimum 10m away easily recognizable according to the color of the indicator:
• GREEN : Ready
• GREEN BLINKING : Collecting or sending data (link active with external
source like PC)
• YELLOW : Test is running
• YELLOW BLINKING: Test is done, waiting intervention (residue entry), beep
for 5 sec (configurable)
• RED : Failure (continuous audio alarm)
The status indicator beacon has to be mounted at the rear of the OptiDist™.
4.6.7 Optional built-in printer

A factory installed static thermal dot line printer with tear bar is available as
optional accessory. Distillation data and diverse OptiDist™ internal data can be
rapidly printed on an 80 mm width ticket without need of connection of an external
printer.
54 UM_2.00A_EN
4.6.8 Optional external printer

An external printer is available as optional accessory (see the spare parts list)
allowing all printouts of the results and the quality control database.
NOTE
The printer must support PCL5 emulation language (or above such
as PCL6 or variants such as PCL5e).
See printer documentation provided for explanations on its operation.
4.6.9 Optional bar code reader
Bar code reader
A bar code reader is available as optional accessory (see the spare part list). The
bar code reader allows to enter the sample name or number during test
configuration without spelling mistakes. When connected, the bar code reader can
be activated after selecting the sample name/number field.
4.6.10 Optional “Doctor Box”
Doctor Box 1
UM_2.00A_EN 55
The Doctor Box allows a rapid diagnostic of the OptiDist™ components and
electronic boards without need for OptiDist™ disassembly.
F F1 F2 30A
U BIP 24V FLASK HT
S VOLTMETER
E F3 F4 F5 F6 OUTPUT
S 24V
12V 12V
5V
T
R
5V 3.3V
A RED COND. HT BOOST HT REC . FAN LED
F
F
I 3.3V
C COOL . UNITT COOL . SV
ORANGE
L ADA DOCTOR BOX
I
G DOWN SOL. COND. REC.
H
T
GREEN
FLASK FAN REC . HT VOC PUMP
Doctor Box 2
The Doctor Box can be connected to the 25-pin connector on the right side of the
OptiDist™.
4.6.11 Optional VOC control

The VOC (Volatile Organic Components) control option can be factory installed to
reduce volatile hydrocarbon compound emissions.
The VOC control option is made off a blower with its fixing plate and an outlet
connector to be screwed at the rear of the OptiDist™. This outlet must be linked to
a fume hood.
WARNING
Do not apply vacuum to the VOC outlet.
56 UM_2.00A_EN
4.7 Access levels

Unit configuration and maintenance functions can be password protected.
If a supervisor passwords is entered, only the supervisor has access to important
and/or sensitive operating parameters and functions of the instrument, the access
level 1. The supervisor will have to enter a special password to access these
functions.
If a maintenance password is entered, only qualified technicians have access to
OptiDist™ service parameters, diagnostic and calibration menus, the access level
2. The technician will have to enter a special password to access these functions.
When the OptiDist™ is switched on, it goes to the configured start up access level.
NOTE
When the instrument is shipped, the default passwords are:
• for operator (Level 0): no password
• for supervisor (Level 1): PAC-1
• for maintenance (Level 2): PAC-2
When an access level is confirmed by entering the correct password, it remains

available until a lower access level is explicitly requested or during a time set in
the OptiDist™ internal parameters. If the touch screen does not detect any contact
up to the end of this time, the access level is reset to the level 0 (Operator) (this
time is not taken into account in Diagnostic mode, during a test or during
calibration). The countdown is reset at each contact.
There are three access levels:

• Level 0: Operator level
= Information and basic functions for test running are accessible without
entering a password
• Level 1: Supervisor level
= Level 0 + configuration of the OptiDist™ and test.
• Level 2: Maintenance level
= Level 1 + information and functions for the OptiDist™ diagnostic and
calibration.
Levels 1 and 2 are protected by numeric passwords with 5 characters minimum.

The user must enter the correct password to access to the concerned functions.
NOTE
To change the password, you need to know the previous password.
UM_2.00A_EN 57
NOTE
The system administrator should set-up these passwords during
installation to prevent unauthorized persons from changing the set-
tings of the instrument. In this way, access to important operations
can be restricted to a limited number of persons.
Set-up of the passwords of access levels is covered in the supervisor manual.
58 UM_2.00A_EN
4.8 The Man Machine Interface (MMI)
4.8.1 Touch-screen
The preloaded software provides a LCD touch-screen Man Machine Interface
(MMI) with a large (640 X 480) high-resolution graphic color display .
A number of large area function keys allow short cuts to most frequently used
functions for comfortable operation. User / machine dialogue is carried out via a
virtual keyboard, a virtual keypad and location sensitive graphics located on the
touch-screen.
The system is protected from unauthorized access and entry by various security
levels that allows changes to be made to the system settings only after a valid
password has been entered.
4.8.2 Features of the touch-screen
The touch-screen is equipped with a specially developed controller interface. It

permits the user to:
• Start/Stop a test
• Display the
- actual status information
- distillation curve in general view
- list of existing distillation products
- data base results (maximum 100 results)
- quality control data base (maximum 50 quality control samples with 250
tests)
• Create/modify/save a distillation product in the data base
• Display/acknowledge failures and warning alarms
• Display menus to run
- configuration
- parameter
- calibration
- diagnostics
- service
• Print the results of a distillation run
• Print the results from the database
UM_2.00A_EN 59
4.8.3 Precautions for the touch-screen

• Avoid high temperature and high humidity. Ensure that the storage and
operating temperatures given in the Technical specifications are observed
(Environmental requirements).
• The touch-screen shall be operated within the limits specified in the Technical
Specifiations.
• Water may cause damage or discoloration. Clean any condensation or
moisture from any source immediately.
• Electricity fed to a touch-screen with moisture on its surface may damage it.
Gently wipe off any moisture or let it dry before using the touch-screen.
• The touch-screen is rugged, but can be easily scratched if rubbed or forcibly
touched by hard or pointed objects. Handle the touch-screen with care so as
not to scratch it.
• The touch-screen can be marred by fingerprints, aqueous fluids, starch, oil or
fat. If the screen becomes discolored, gently wipe it with a soft and clean
cloth. The touch-screen material provides high resistance to the most
chemicals and organic solvents encountered in this distillation OptiDist™
environment (acetone, toluene, trichloroethylene, alcohol or the like). Ordinary
glass cleaner can be used to clean the touch-screen or housing.
4.8.4 The virtual keybord and keypad
4.8.4.1 The virtual keyboard

The keyboard appears each time a text entry field is activated to enter a new text
or to modify the one stored.
The virtual keyboard

• ESC: Quit text entry and return to the previous screen
• BCKSP: Removal of the character positioned on the left of the cursor
• ERASE: Cancel complete entry field
• INS: Insertion of a character on the left of the cursor / replacement of the value
above the cursor
60 UM_2.00A_EN
• CAPS: Locking the keyboard in capital letter

• ENTER: Registration of the new text into the corresponding field
• SHIFT: No object
• HOME: Displacement of the cursor at the beginning of the line
• END: Displacement of the cursor at the end of the line
• AZERTY / QWERTY: Modification of the keys order
• DEL: Removal of the character positioned above the cursor
• ALT GR: No object
• < >: Displacement of the cursor to the left / to the right
4.8.4.2 The virtual keypad
Esc 7 8 9 Bcks
Del 4 5 6 Ins
123 1 2 3 ENT
<_ 0 +- . _>
The virtual keypad
The keypad screen is typical for all numerical entry. It appears each time a
numerical entry field is activated to enter a new value or to change settings by
entering the desired numbers by pressing the 0-9 number keys.
• ESC: Quit numerical entry and return to the previous screen
• BCKSP: Removal of the character positioned on the left of the cursor
• DEL: Removal of the character positioned above the cursor
• INS: Insertion of a character on the left of the cursor / replacement of the value
above the cursor
• ENT: Registration of the new value into the corresponding field
• < > Displacement of the cursor to the left / to the right
• + - Commutation of the new value as a negative value
• 123/789: Modification of the numerical keys order
UM_2.00A_EN 61
4.8.5 The Welcome screen

Switch on the OptiDist™
1. Push the Main Power switch on the right side of the OptiDist™ to the up or ON
position.
The small green indicator lamp on front side of the OptiDist™ lights up
indicating the OptiDist™ is powered on and the following operations are
performed:
• A self diagnostic test is started.
• The condenser bath, receiving chamber and cooling system temperatures
are regulated to default values.
• After the self dignostic test has completed, the welcome screen appears:
The Welcome screen
The Welcome screen provides menu buttons at the bottom of the screen allowing
to access to the following screens (from the left to the right):
• The PAC addresses screen to contact us.
• This display remains active until the EXIT button on bottom right is pressed:
Doing this displays the OptiDist™ Run /Start & Display screen allowing
starting a test immediately.
NOTE
The touch screen is factory calibrated but if it is necessary to cali-
brate it again, press five times on the welcome screen (not on the
buttons) to display the calibration screen of the touch screen.
62 UM_2.00A_EN
4.8.6 The Run / Start & Display screen

Initiating a test consists in entering only three parameters:
• The operator name
• The sample name
• The distillation product
These parameters can either be:

• selected in lists pre-configured by the supervisor and stored in the internal
database of the OptiDist™
• or entered manually using the virtual keyboard
Open the Run / Start & Display screen:

1. Press the Exit button on the Welcome screen.
The Run /Start & Display screen opens.
The Run /Start & Display screen for the Operator
UM_2.00A_EN 63
/i
Buttons on the Run / Start & Diplay screen

Displaying of test product parameters prestored in the test product list
Realtime displaying of measurement values in a spreadsheet during a test is run-

ning, such as:
• Volume
• Distillation rate
• actual temperature
/i
The top of the Run / Start & Display screen shows the status of the unit and is always visible
Status field The Status field indicates the state of the unit:
• Green / READY: The OptiDist™ is ready to start a new test
• Yellow / VOLUME SCAN: The OptiDist™ is waiting for a receiver cylin-
der with sample to measure the charge volume of the sample in the
receiver cylinder
• Yellow / START: Checking of test starting conditions
• Yellow / INIT HEAT: Initial heating – The OptiDist™ is searching the IBP
• Yellow / DISTILLATION: The distillation is in progress
• Yellow / FINAL HEAT: The OptiDist™ is waiting for the FBP (from 5 ml
residual liquid in the flask to the FBP)
• Yellow / RECOVERY: After the FBP, the OptiDist™ is waiting for the vol-
ume in the receiver stabilizes
• Yellow / RESIDUE: Expectation of the input of the recovery
PC link: State indicator of the OptiDist™ / Network link
• 9 (green): Network link established
• X (red): Network link not established
Time display Displays the current time
Unit No.: Name or number of the OptiDist™ unit
/i
The centre left of the Run / Start & Display screen is the operation screen
Operator: Selection of the operator name in the operator name list
Note: The operator name is not mandatory for test starting
Sample No.: Entry field of the sample identifying name or number / Selection of a sample
name in the prestored list of sample names
Product: Selection of a test product in the prestored list of test products
Note: Addition of a comment if wanted
/i
The centre right of the Run / Start & Display screen shows the test monitoring diagram
On the left of the • Actual vapor temperature
diagram • Actual temperature of the heating element
In the centre of the • Actual temperature of the condenser tube
diagram
On the right of the • Volume of condensate in the receiver
diagram • Actual temperature of the receiving chamber
64 UM_2.00A_EN
/i
The bottom of the Run / Start & Display screen is the menu bar with main menu buttons
New Test Set-up of a new test
Results Access to the result database
Products Access to the product database
QC Access to the Quality Control database
Messages Access to the alarm messages database
More Access to more main menu options
For access to more main menu options:

1. Press the More button at the bottom right of the Run /Start & Display screen.
The menu bar shows further main menu buttons.
Second screen with main menu options of the Run /Start & Display screen
/i
More main menu options of the Run / Start & Display screen
Param. Access to the OptiDist™ internal parameter database
Reports Access to the report profile database
Operator Access to the operator name list
Standard Access to the standard method database
More Access to more main menu options
UM_2.00A_EN 65
For access to more main menu options:

1. Press the More button at the bottom right of the Run /Start & Display screen
again.
The menu bar shows further main menu buttons.
Third screen with main menu options of the Run /Start & Display screen
/i
More main menu options of the Run / Start & Display screen
Calib. Access to the calibration main menu
Diag. Access to the diagnostic main menu
About Access to the information screen on firmware version, serial numbers of elec-
tronic boards and MMI
Backup Access to the data download and upload main menu
More Returns to the first screen with main menu options
4.8.7 The New Test main menu

The setup of starting modes is mainly dedicated to the Supervisor.
According to the starting mode set by the supervisor, the operator can either use:
• the Start Guide mode, that leads the user step by step
• the Quick Test starting mode, in case of a test series on the same sample
without parameter input
• or he can directly set up and start a test in the Run / Start & Display screen as
shown below
66 UM_2.00A_EN
Open the New Test main menu:

1. Press the New Test button on the Run / Start & Display screen.
The New Test main menu opens.
The Run / Start & Display screen with state indicators of starting conditions
The Run / Start & Display screen is reset and the New Test button turns into
START button allowing a new test to be started when it will be set up and when all
starting conditions will be fulfilled.
The starting conditions with state indicators are displayed on the left bottom above
the Start button on the Run / Start & Display screen.
/i
State indicators of the starting conditions

Receiver: 9 Receiver cylinder well installed in the receiving chamber.
Flask: 9 Flask well installed in the flask heater platform.
Probe: 9 Vapor temperature probe connected to the unit.
Cond. cleaned: 9 Condenser is cleaned.
Base plate: 9 Diameter of the base plate installed (only detected when the flask heater
platform is in high position and a product is selected).
If a condition is not fulfilled, this will be indicated with the following icon “X” in red
next to the condition in question.
UM_2.00A_EN 67
68 UM_2.00A_EN
Installation OptiDist™
5 Installation
UM_2.00A_EN 69
OptiDist™ Installation
5.1 Technical specifications and requirements

/i
Electrical requirements Electrical requirements:

• Mains Voltage: 100-240V / 50-60 Hz
• Power consumption : 1400 W
• Power cable: supplied with the OptiDist™ and corresponding to the
country of sale
Environmental Ambient conditions:
requirements • Operating temperature: 10 °C to 35 °C (50 ° to 95 °F)
• Operating humidity: 80%RH maximum at temperatures up to 35 °C
(95 °F)
• Atmospheric pressure: Constant
• Storing temperature: -20 °C to 50 °C (-4 °F to 122 °F)
• Storing humidity: Less than 95%RH (no condensation)
Space requirements:
• Physical dimensions: 440 mm (W) x 570 mm (D) x 650 mm (H) / (17
x 20.1 x 26 in)
• Weight: 68 kg (188lbs)
• Place the OptiDist™ on a level and flat laboratory bench, free of
vibrations, away from drafts and close to electric mains connections,
CO2 gas supply and communication connections. In any case, the
OptiDist™ location should be draught free and preferably near a
fume hood.
• Leave sufficient space behind the OptiDist™ for cabling access and
for clear ventilation: Allow a minimum clearance of 200 mm (8 in)
around the OptiDist™ for circulation of air for the cooling unit.
• Distance between two units: 200 mm (8 in)
• Protect the OptiDist™ from water and aqueous mists and spray (see
LCD handling precautions further on).
• Protect the OptiDist™ from direct sunlight
Gas requirements • Fire extinguisher gas: CO2 (CO2 inlet at rear)
• Gas pressure at inlet: 7 bars (+/-0.5bars) / 700 kPa (+/-50 kPa)
• Maxi. safe pressure: 10 bars / 1000 kPa
• Flow of gas during flame quenching: 30 to 35 liter/s
• Average volume used for flame extinguishing: 150 liters
• Extinction takes between 2 and 4 seconds
• Fire extinguisher connection: hose nozzle with a compression fer-
rule with inside diameter of 8 mm
NOTE
Testing with the OptiDist™ must be carried out at constant ambient
pressure. Care must therefore be taken to avoid placing the Opti-
Dist™ under an air vent or under a fume cupboard functioning dur-
ing a test.
5.2 Care in Unpacking

Carefully unpack the OptiDist™ and inspect for damage. If equipment damage
exists, keep the equipment, shipping carton and packaging materials and file a
claim with the final carrier. Usually, the carrier will send an inspector to ascertain
liability. Send a copy of the claim to PAC or to your local sales office.
70 UM_2.00A_EN
NOTE
Do not return the OptiDist™ or any part to the factory without fac-
tory authorization.
After unpacking, verify the unit and its accessories as well as any possible
damage sustained in transit, which must immediately brought to the attention of
the carrier so that a statement of damage can be made.
The various parts of the OptiDist™ are carefully verified and tested before
shipping. Nevertheless, it is worth verifying that the equipment received
corresponds to the packing list enclosed.
On taking delivery of the OptiDist™, unpack all these parts.
5.3 Installation of the OptiDist™
CAUTION
Do not put the OptiDist™ in the direct sunlight.
CAUTION
Do not cover the air intake slots of the unit. If you want to set up
many units in rows, be sure that you keep minimum 20 cm distance
(8 inches) between units. Failure to allow sufficient air ventilation
flow can cause instrument damage.
Put the OptiDist™ on a level, flat workbench and not subject to vibrations, near
electrical sockets and near connections to fire extinguisher gas supply. Provide
enough space so that the OptiDist™ can be operated conveniently and for access
to the rear connectors.
Leave sufficient space behind the OptiDist™ for cabling access and for clear
ventilation.
Place the external PC close to the instrument (the length of the Ethernet cable
provided to connect the PC with the OptiDist™ is about 3 m but it is possible to
use a longer one).
5.4 Main power connection

Regarding the connection of the OptiDist™ to its power source, it should be noted
that the analyzer is built to operate from 100 to 240 Volts, at 50 or 60 Hz, in
accordance with the majority of countries where the OptiDist™ is marketed.
The power plug corresponding to the country of sale is supplied with the
OptiDist™.
UM_2.00A_EN 71
5.5 CO2 gas connection

For the specification of the CO2 gas source requirements refer to 5.1. Technical
specifications and requirements.
1. Test the fire extinguisher solenoid valve and the flame detector as described
in the Maintenance Manual. Call for a qulified technician to perform the test.
NOTE
The CO2 connection system is composed of a hose nozzle with a
compression ferrule with inside diameter of 8 mm to connect a rigid
metallic pipe. Adapt a hose nipple on the hose nozzle to connect a
flexible hose if it is necessary.
2. Connect the CO2 gas source to the connector at the rear of the OptiDist™.
It is possible to connect an external fire alarm device to the OptiDist™. Call for a
qualified technician to perform the connection. For connection instructions refer to
the Maintenance Manual.
5.6 OptiDist™/ PC Connection
5.6.1 Optional external PC control

The OptiDist™ can be connected to the ALAN®, HLIS-32® or PDS™ network on a
Server PC via a router through the RJ45 Ethernet connector, which is located at
the rear of the OptiDist™. The OptiDist™ connection to the Router is plug and
play. The OptiDist™ is automatically detected. Connection of the PC to the LIMS
can be done either by RS232 or Ethernet 2 connection (Ethernet 2 connection has
to be done from an IT specialist in the laboratory).
5.6.2 Connection with RS 232C serial link

The OptiDist™ is equipped with an RS 232C serial port enabling the transmission
of data to a LIMS (refer to the Appendix for the connector broaching and the
meaning of the messages).
1. Connect the LIMS to the RS 232C connector at the rear of the OptiDist™.
NOTE
The RS 232C communication mode needs to be configured.
Parameters are accessible from the setup menu of the internal
parameters.
RS232 software and hardware is provided as standard.
5.7 Flask stopper holder

1. Install the flask stopper holder in the hole provided for this on the top of the
OptiDist™.
2. Then install the flask stopper in the holder.
72 UM_2.00A_EN
5.8 Temperature probe connection
5.8.1 Pt100 vapor temperature probe
1. Connect the vapor temperatur probe to the connector on the front of the
OptiDist™.
2. Insert and adjust the vapor probe in the flask stopper.
3. Pass the vapor probe wire through the wire support.
5.8.2 Ambient temperature probe

The ambient temperature probe is an optional accessory that has to be ordered
separately.
1. Connect the ambient temperature probe to the connector located at the rear of
the OptiDist™.
When connected, the ambient temperatur probe is automatically detected by the

OptiDist™.
5.9 125 ml and 200 ml automatic dry point kit and holder
The automatic dry point kit and holder is an optional accessory that has to be
ordered separately.
The dry point sensor must be installed in the distillation flask so that the point of
the sensor rests exactly at the center of the lowest point at the bottom of the
distillation flask. This is ensured by the specific dry point stopper.
The automatic dry point sensor (DP sensor) consists of a long stainless steel
jacket with a thermocouple at the lower end to detect temperature differences.
5.9.1 Installation of the automatic dry point kit and holder
A Wire support
B Dry point sensor connector C A
C Flask stopper holder
D Dry point stopper
E Dry point stopper holder
1. If the vapor probe is installed in the flask

stopper, loosen the threaded probe
B
sealing device (compression nut) and
remove the vapor probe (do not
disconnect the vapor probe).
2. Remove the flask stopper holder (C) by D E
pulling it upward.
3. Insert the dry point stopper holder (E) on the top of the OptiDist™ behind the
flask heater assembly .
4. Reinstall the flask stopper holder (C) (through the hole of the dry point stopper
holder (E)).
UM_2.00A_EN 73
5. Insert the vapor temperatur probe and adjust the probe length in the dry point
stopper, see 5.9.2. Adjustment of the vapor probe in the dry point stopper.
6. Install the dry point stopper (D) to the dry point stopper holder (E).
7. Connect the dry point sensor to the dry point sensor connector (B) and pass
the wire through the wire support (A).
5.9.2 Adjustment of the vapor probe in the dry point stopper

The figure below shows both, a 125 ml and a 200 ml dry point kit.
A Vapor temperature probe A A
B Threaded probe sealing device (compression nut)
C Adjustment gauge
D Dry point sensor B B

device (compression nut) (B).
C
2. lnsert the vapor temperature probe (A)
through the threaded compression nut
D D
opening.
3. Position the adjustment gauge (C)
supplied against the dry point stopper.
4. Adjust the depth of the vapor temperature
probe (A) so that the probe tip just touches the bottom of the corresponding
notch.
5. Tighten the threaded compression nut until the vapor temperature probe (A) is
securely fixed at the proper depth.
motion.
The vapor temperature probe should be securely fixed in position and not be
easily moved.
lf the vapor temperature probe is not held securely, repeat the adjustment
procedure.
NOTE
The type of dry point sensor (125 ml or 200 ml) is automatically rec-
ognized at plug in by the OptiDist™.
NOTE
Boiling stones should not be used with the automatic dry point
detection kit.
74 UM_2.00A_EN
5.10 Installation of the status indicator beacon

The staus indicator beacon is an optional accessory that has to be ordered
separately.
A Screws supplied
B Support
C Status indicator beacon
1. Install the support (B) with the supplied

screws (A) to the rear of the OptiDist™.
C
2. Insert the status indicator beacon (C) into
the support (B).
B
3. Connect the wire to the status indicator
beacon connector at the rear of the A
OptiDist™.
5.11 VOC Control Option Connection

If the VOC Control option (Volatile Organic Component) is factory installed:
1. Connect an exhaust pipe to the VOC outlet at the rear of the OptiDist™ and
link it to a fume hood.
5.12 Connection of an optional external printer

The external printer is an optional accessory that has to be ordered separately.
1. Connect the external printer to the USB A port on the right side of the analyzer
or to the USB A port at the rear of the OptiDist™.
NOTE
When connected, the external printer needs to be configured in the
OptiDist™ internal parameter settings.
See printer documentation provided for explanations on the opera-
tion.
5.13 Connection of the optional bar code reader

The bar code reader is an optional accessory that has to be ordered separately.
1. Connect the bar code reader to the USB A port on the right side of the
OptiDist™ or to the USB A port (3) at the rear of the OptiDist™.
After activating the sample name/number in the input field, the barcode reader can
be activated to enter the data.
UM_2.00A_EN 75
5.14 Power-On procedure
CAUTION
Once the OptiDist™ has been installed, before switching on, allow
the OptiDist™ to adjust to the ambient temperature in the labora-
tory for 24 hours (especially if the OptiDist™ was stored at low tem-
perature).
5.14.1 Switch on the OptiDist™
1. Push the Main Power switch on the right side of the OptiDist™ to the up or ON
position.
The small green indicator lamp on the front side lights up indicating the
OptiDist™ is powered on and the following operations are performed:
• A self diagnostic test is started.
• The condenser bath, receiving chamber and cooling system temperatures
are regulated to default values.
• After the self dignostic test has completed, the welcome screen appears,
see 4.8.5. The Welcome screen.
5.14.2 PAC addresses screen
1. By pressing the PAC button at the bottom of the welcome screen, the PAC
addresses screen appears giving the list of PAC contacts.
2. Press the EXIT button to return to the welcome screen.
5.14.3 Heat exchanging liquid (level checking and recommendations)

The heat exchanging liquid used in the cooling system is factory filled through a
reservoir equipped with a level sensor. If the heat exchanging liquid level in the
cooling system is unsufficient, the system will trigger the corresponding failure
alarm. If this failure alarm occurs, follow up with the recommendations about the
cooling system in section 9.6. Servicing the cooling system.
5.14.4 Self diagnostic screen

When it is powered-on, the OptiDist™ performs an auto-dignostic test of each
part. This can take a few seconds. In case of failure, a red screen appears
displaying the list of failing parts or supply circuits. To perform a detailed
diagnostic of the parts implicated and its supply, see chapter 8. Diagnostic
functions.
5.14.5 OptiDist™ calibration

Calibration of measurement circuits and measuring instruments is performed by
the factory before the OptiDist™ is shipped.
If any calibrations are necessary, see 7.10. The Calibration database.
76 UM_2.00A_EN
NOTE
The touch screen is factory calibrated but if it is necessary to cali-
brate it again, press five times on the welcome screen (not on the
buttons) to display the calibration screen of the touch screen.
UM_2.00A_EN 77
78 UM_2.00A_EN
Operation OptiDist™
6 Operation
UM_2.00A_EN 79
OptiDist™ Operation
6.1 Preparation
6.1.1 Basic preconditions
CAUTION
Wear safety glasses when handling dangerous chemical such as
solvents.
CAUTION
Wear protective gloves when handling dangerous chemical such
as solvents.
NOTE
Clean the distillation flask, the receiving cylinder and the vapor
temperature probe regularly.
Otherwise the boiling range characteristics are influenced.
6.1.2 Safety
This OptiDist™ has been carefully designed, manufactured and inspected for
quality. It has been equipped with a number of safety features.
However, the use of this OptiDist™ may involve the handling of solvents,
chemicals, and other potentially dangerous flammable, toxic, etc.) materials.
Please exercise caution when handling these materials while operating the
OptiDist™.
• read the manual
• wear proper protective clothing
• perform all suggested service procedures
• use care to prevent accidents
The manufacturer accepts no responsibility for any damage or liability arising from
the use of the OptiDist™.
Use of Non-PAC Products and Accessories. Defects or damage that result from
the use of non-PAC branded or certified products, accessories, software or other
peripheral equipment are excluded from warranty.
NOTE
Use only standard OptiDist™ PAC receiving cylinders. If it is not the
case, the OptiDist™ does not detect the receiving cylinder and the
alarm “No receiver detected” is triggered.
80 UM_2.00A_EN
NOTE
Use duran glass distillation flasks for a maximum heating tempera-
ture of 700 °C to 870 °C.
NOTE
Use quartz glass distillation flasks for a maximum heating temper-
ature of 870 °C to 1000 °C.
6.1.3 Sampling, storage and sample conditioning according to ASTM D86
6.1.3.1 Samples - storage and conditioning
WARNING
Handle all solvents, chemicals and other potentially dangerous
materials with care.
The operator needs to have training about potential hazards,
before operating the system.
NOTE
To obtain accurate and repeatable results, prepare the samples
and the OptiDist™ with particular care as described in the following
sections.
1. Clean and dry all instruments and accessories for use before sampling. See
6.1.4. Clean the devices.
2. Determine the group characteristics of the sample according table 2 of the
ASTM D86 test method.
/i
ASTM D86 table 2

Group charater- Group 1 Group 2 Group 3 Group 4
istics
Sample characteristics: distillate type, vapor pressure:
at 37.8 °C, kPa ≥ 65.5 < 65.5 < 65.5 < 65.5
at 100 °F, ps ≥ 9.5 < 9.5 < 9.5 < 9.5
(Test methods D 323, D 4953, D 5190, D 5191, D 5842, IP 69 or IP 394) distillation:
IBP °C ≤ 100 > 100
IBP °F ≤ 212 > 212
FBP - EP °C ≤ 250 ≤ 250 > 250 > 250
FBP - EP °F ≤ 482 ≤ 482 > 482 > 482
3. Collect the sample at ambient temperature.

4. After sampling close the sample bottle immediately with a tight fitting closure.
UM_2.00A_EN 81
5. For Group 0 and 1:

a. Prechill the sample container and the sample before drawing to the
required temperature as directed by the standard method for the indicated
group.
b. If this is not possible, draw the sample into a container prechilled to the
required temperature in such a manner that agitation is kept to a minimum
6. After sampling close the sample bottle immediately with a tight fitting closure
and place the bottle in an ice bath or refrigerator.
TIP
Referral: Consult table 3 of the ASTM D86 standard test method.
/i
ASTM D86 table 3 Sampling, storage and sample conditioning

Group 1 Group 2 Group 3 Group 4
Temperature of sample °C < 10
bottle
°F < 50
Temperature of stored °C < 10A < 10 ambient ambient

sample
°F < 50A
< 50 ambient ambient
Temperature of sample °C < 10B < 10B ambient or 9 to 21°C above

after conditioning prior pour pointC
to analysis
°F < 50 < 50 ambient or 48 to 70 °F above
pour pointC
If sample is wet resample resample dry in accordance with 7.5.3
D
If resample is still wet dry in accordance with 7.5.2
AUnder certain circumstances, samples can also be stored at temperatures below 20 °C (68 °F).
See also 7.3.2 and 7.3.3.
B If sample is to be immediately tested and is already at the temperature prescribed in table 1, see
7.4.1.1.
C
If sample is (semi)-solid at ambient temperature, see also 10.3.1.1.
D
If sample is known to be wet, resampling may be omitted. Dry sample in accordance with 7.5.2
and 7.5.3.
82 UM_2.00A_EN
6.1.3.2 Sample storage recommendations

• If testing does not start immediately after collection, store the sample at
ambient or lower temperature away from direct sunlight or sources of direct
heat.
• For group 0, 1 and 2:
- Store the sample in a refrigerator to the required temperature as directed
by the standard test method for the indicated group.
- If it is not possible, sample may also be stored at a temperature below 20
°C (68 °F), provided the sample container is tightly closed and leak-free.
TIP
6.1.3.3 Sample conditioning recommendations

Samples should be conditioned to the same temperature than storage.
NOTE
For group 3 and 4, if the sample has solidified during storage, heat
the sample to a temperature of 9 to 21 °C above its pour point prior
to analysis. Then mix it gently prior to opening the sample con-
tainer to ensure homogeneity.
6.1.3.4 Wet samples
CAUTION
Samples of materials that visibly contain water are not suitable for
testing.
If the sample is not dry, obtain another sample that is free from sus-
pended water.
If such a sample cannot be obtained, remove the suspended water
by adding anhydrous sodium sulfate and then separating it from the
drying agent by decanting (see standard method). Note in the
report that the sample has been dried by the addition of a
desiccant.
UM_2.00A_EN 83
6.1.4 Clean the devices
CAUTION
Wear safety glasses when handling dangerous chemical such as
solvents.
CAUTION
Wear protective gloves when handling dangerous chemical such
as solvents.
NOTE
Clean the distillation flask, the receiving cylinder and the vapor
temperature probe regularly.
Otherwise the boiling range characteristics are influenced.
6.1.4.1 Clean the distillation flask

1. Clean the distillation flask.
2. Use only distilled water.
6.1.4.2 Clean the receiving cylinder

1. Clean the receiving cylinder carefully with
a brush and a cleaning cloth.
84 UM_2.00A_EN
6.1.4.3 Clean the condenser

1. Use the supplied condenser cleaner.
2. Inside the receiving chamber, insert the
condenser cleaner into the opening of the
condenser tube.
3. Push the condenser cleaner carefully
through the tube.
4. Pull out the condenser cleaner at the
other end of the tube.
UM_2.00A_EN 85
6.1.5 Preparation of the OptiDist™ and accessories
6.1.5.1 ASTM D86 table 1

/i
ASTM D86 table 1

Preparation OptiDist™ Group 1 Group 2 Group 3 Group 4
Distillation flask ml 125 125 125 125
ASTM distillation thermometer 7C (7F) 7C (7F) 7C (7F) 8C (8F)
IP distillation thermometer range low low low high
Distillation flask support board B B C C
diameter of hole, mm 38 38 50 50
Temperature at start of test
Distillation flask °C 13 - 18 13 - 18 13 - 18 not above
ambient
Distillation flask °F 55 - 65 55 - 65 55 - 65 not above
ambient
Distillation flask support and shield not above not above not above
ambient ambient ambient
Receiving cylinder and sample °C 13 - 18 13 - 18 13 - 18A 13 -ambientA
Receiving cylinder and sample °F 55 - 65 55 - 65 55 - 65A 55 -ambientA
A
See 10.3.1.1 for exceptions
6.1.5.2 Choose and install a base plate
1. Choose the appropriate base plate with centered opening and diameter as
directed by the standard for the indicated group.
TIP
2. Install the base plate on the distillation flask heater platform: position the cut
corner to the right and to the back of the distillation flask heater platform when
you are facing the OptiDist™.
NOTE
When the distillation flask heater is installed and the distillation
flask heater platform will be in elevated or "run" position, the open-
ing diameter of the base plate will be indicated in front of the base
plate state indicator in the starting condition list of the Run / Start &
Display screen.
86 UM_2.00A_EN
6.1.5.3 Adjust the vapor temperature probe in the distillation flask stopper
NOTE
The distillation flask stopper assembly is specially designed for the
precise adjustment of the vapor temperature probe positioning in
the stopper (see below) and so, in the distillation flask.
1. Put the flask stopper assembly in its

holder (C).
A
device (B). B
3. Insert the vapor temperature probe (A)

through the threaded nut opening until it
just touches the bottom of the stopper
assembly holder.
4. Tighten the threaded compression nut
until the vapor temperature probe is
C
securely fixed at the proper depth (vapor
temperature probe tip has very little
contact with bottom of the stopper
assembly holder).
motion.
6. Fix the vapor temperature probe (A) securely in position. It should not be
easily moved.
If the vapor temperature probe is not held securely, repeat the procedure.
7. Connect the vapor temperature probe to the OptiDist™ connector.
NOTE
When the vapor temperature probe is connected to the OptiDist™,
the "Probe" state indicator in the list of starting conditions of the
Run /Start & Display screen becomes green. In the contrary case, a
test cannot start.
NOTE
If a dry point kit is used, refer to manual for the adjustment of the
dry point probe.
UM_2.00A_EN 87
6.1.6 Set-up of the distillation flask and the receiving cylinder

When all accessories needed are installed and the test set-up is completed, the
distillation flask with sample and the receiver cylinder can be installed in the
OptiDist™. The test can only start when the OptiDist™ detects they are in the
correct position.
6.1.6.1 Preparing and inserting the sample and receiver cylinder
NOTE
Be sure that the sample, the receiver, and the distillation flask are at
the temperature specified by the standard test method. Otherwise,
the recovery determination will give incorrect results.
6.1.6.2 Filling the receiver cylinder
1. Fill the receiver cylinder with 100 ml of the material to be distilled.

The bottom of the meniscus must be exactly on the mark drawn on the
receiver cylinder.
6.1.6.3 Filling and installing the distillation flask
1. Put a few boiling stones in the distillation flask to prevent a boiling retardation.
2. Pour the content of the receiver cylinder into the distillation flask.
Be sure that the vapor tube of the flask is pointed upward, otherwise material
could run out through the vapor tube.
NOTE
• Do not use any boiling stones for dry point tests.
• Do not clean the receiver cylinder after pouring the sample
into the flask, or the result will be false!
3. Remove the flask stopper from the stopper holder.

4. Hold it by the flask attachment clips.
5. Press on the attachment clips and insert the stopper into the flask neck so that
the flask vapor tube is lined up with the attachment arm of the stopper.
6. Release the attachment clips.
NOTE
Be sure that the vapor temperature probe has been adjusted
with the stopper assembly holder.
7. Pull the flask heater platform positioning lever to release the flask heater
platform in low position.
8. With your left hand, open the door of the flask heater enclosure door.
88 UM_2.00A_EN
9. With the right hand, position the flask with the stopper in a vertical position in
the flask heater platform:
a. Insert the vapor tube of the flask in the condenser tube opening.
b. Insert the flask stopper attachment device into the attachment device of
the heater assembly.
NOTE
Tightness between the flask vapor tube and the condenser tube
opening is ensured by the vapor tube sealing ring, which prevents
any escape of vapor during the distillation.
1. Close the flask heater enclosure door.

2. Lower the flask heater platform positioning lever for the flask heater platform
raises up it comes in contact with the flask bottom.
Thus, the flask is automatically centered in the hole of the base plate.
NOTE
The diameter of the hole in the base plate and the presence of a
flask in the flask heater platform are parts of the starting conditions
list displayed in the Run /Start & Display screen. These are tested
when the heater platform is in high position. If the diameter of the
hole in the base plate corresponds to the requirements of the
standard test method selected for the sample group to be tested,
the two corresponding fields becomes green and the diameter of
the hole is automatically displayed in front of the “Base plate:” state
indicator.
6.1.6.4 Installing the receiver cylinder
NOTE
Do not clean the receiver cylinder after pouring the sample into the
flask, or the result will be false!
1. Press the door latch to open the door of the receiving chamber.
2. Place the receiver in the receiving chamber:
a. First insert the lower end of the condenser tube into the receiver cylinder;
b. Then position the bottom of the receiver cylinder on the receiver stand. It
is automatically centered when the receiver chamber door is closed.
3. Make sure that the tip of the drop plate touches the front inner wall of the
cylinder so that the drops run down the wall.
If the drops fall freely into the liquid in the cylinder, the volume measurement
will not work properly.
4. Check that the rubber cap has well gone down onto the top of the receiver. If
this is not the case, push down the rubber cap to cover the top of the receiver.
UM_2.00A_EN 89
5. Close the receiving chamber door.
NOTE
The OptiDist™ detects the presence of the receiver in the receiving
chamber: the “Receiver:” state indicator in the starting condition list
of the Run /Start & Display screen becomes green indicating the
receiver is well positioned. In the contrary case, a test cannot start.
6.1.7 Set up the receiving chamber temperature

The receiving chamber temperature has to be the same as the charge
temperature of the sample otherwise the thermal expansion will create a volume
error.
The receiving chamber temperature during the test is normally set up in the
product according to the standard test method and the sample group.
If the sample temperature is not the same as the programmed receiver
temperature, OptiDist™ offers also the possibility to adjust the receiver
temperature to the sample temperature just before the test starts.
NOTE
The manual adjustment of the receiving chamber temperature
before test starting is part of OptiDist™ internal parameters and
can be activated with a level 1-access authorization (Supervisor).
lf the parameter "Adjust receiver at start" is set on "Yes", the operator can set-up
another receiving chamber temperature thän the one set in the product before
starting the test.
In this case, when the New Test button is pressed, a yellow dialog box appears
allowing:
• To enter the desired receiver temperature
• To select the current ambient temperature as receiver temperature if an
ambient temperature probe is connected to the OptiDist™
• To cancel the adjustment procedure by pushing the CANCEL button
1. Enter the desired receiver temperature value in the field right to the text
2. Press the ENTER button to validate.
3. Press the OK button in the dialog box to validate.
1. Or: Press the CANCEL button to use the receiving chamber temperature set
in the product.
2. Or: If an ambient temperature probe is connected to the OptiDist™, press on
the OK button in front of the ambient temperature displayed to use the
ambient temperature as eceiver temperature.
3. Prepare and install the distillation flask with sample and the receiver.
90 UM_2.00A_EN
6.1.8 Scan the volume in the receiver cylinder

The OptiDist™ can measure the charge volume of the sample to be tested before
filling the sample into the distillation flask.
NOTE
The measurement of the charge volume by the OptiDist™ before
test starting is part of OptiDist™ internal parameters and can be
activated with a level 1-access authorization (Supervisor).
If the OptiDist™ internal parameter "Scan charge volume" is set on "Yes", the
OptiDist™ measures the charqe volume in the receiving cylinder and calculates it
to 100% volume for more precise results.
In this case, when the operator presses the New Test button of the Run / Start &
Display screen or after the adjustment of the receiving chamber temperature (if
activated), a yellow dialog box appears indicating the operator can place the
receiving cylinder with sample in the receiving chamber to measure the exact
volume of sample in the receiving cylinder.
NOTE
The New Test button turns into Stop button allowing the operator
aborting the scan.
The Stop button will then turn into Start button allowing starting the
test.
1. Install the receiving cylinder with sample in the receiving chamber.

The volume measurement system automatically detects the presence of the
receiving cylinder and measures the charge volume.
2. If the volume of sample in the receiving cylinder is 100 ±1 ml, the following
message appears: "Charge Volume is ok". Transfer the sample into the
distillation flask.
3. If the volume of sample in the receiving cylinder is not correct (volume of
sample <99% or >101%), the following message appears: "Charge volume
out of range. Try again with 100 ±1 ml".
4. Adjust the volume of sample in the receiving cylinder then put again the
receiving cylinder in the receiving chamber to scan the volume or abort the
procedure by pressing the stop button.
NOTE
When the volume of sample is correct or by aborting the procedure,
the Stop button turns into Start button allowing the operator to start
the test.
5. Prepare and install the distillation flask with sample and the receiving cylinder.
UM_2.00A_EN 91
NOTE
When the vapor temperature probe is connected to the OptiDist™,
the "Probe" state indicator in the list of starting conditions of the
Run /Start & Display screen becomes green indicating this starting
condition is fulfilled. ln the contrary case, a test cannot start.
92 UM_2.00A_EN
6.2 Measurements
6.2.1 Start modes
Select one of the three default start modes:

• Start Guide mode: Set-up and start a new test using the assistence of the
Start Guide.
• Quick Start mode: Start a new test with the Quick Start mode from the Run /
Start & Display screen with the parameters of the last sample tested.
• Normal Start mode: Set-up and start of a competely new test from the Run /
Start & Display screen with the Normal Start mode.
6.2.1.1 Start Guide mode

Go step by step through the start procedure
To perform its first tests, the operator can use the Start Guide mode that will lead
him step by step through the start procedure:
• Parameterize the test
• Check the OptiDist™ preparation
• Check that all accessories are properly installed
This guide allows to understand rapidly the various functionalities offered by the
OptiDist™ interface.
NOTE
The use of the Start Guide is factory activated and can be disabled
in the OptiDist™ internal parameters with a level 1-access authori-
zation (Supervisor).
1. Press the New Test button on the Run / Start & Display screen.
UM_2.00A_EN 93
First screen of the Start Guide mode
NOTE
According to the OptiDist™ internal settings, a dialogue box
appears when the New Test button is pressed for the adjustment of
the receiver chamber temperature during test or for the measure-
ment of the sample charge volume.
NOTE
The Start Guide can be deactivated at any time by pressing the Exit
start guide button but data entered are saved.
1. Press the Continue start procedure button.
94 UM_2.00A_EN
Select an operator name
Second screen of the Start Guide mode - Operator name selection
NOTE
The next screens of the Start Guide mode contain the additional
Back button.
For access to the previous screen of the Start Guide mode press
the Back button.
First, the operator must select an operator name in the list prestored in the unit.
This list also contains the operator names of the last tests performed with the unit
(up to 100).
1. Press on the field corresponding to the operator name desired to select it.
2. Select an operator name in the list prestored in the unit.
3. Press the Continue start procedure button to continue.
NOTE
lf the operator presses the Continue start procedure button without
entering or selecting a name, the operator name of the last test
performed is entered by default.
UM_2.00A_EN 95
Choose the sample name
Third screen of the Start Guide mode - Sample No. selection
Two possibilities are offered to the operator:

1. First possibility: Select the sample name in the prestored list, where up to 100
names of the previous tested samples are listed.
a. Press on the Get Sample List button to display the list of last samples
tested and the list of sample names prestored in the unit.
b. Press on the sample name desired to select it: the sample name is
automatically entered in the Sample No. entry field.
2. Second possibility: Enter the sample name manually by using the virtual
keyboard:
Press on the Sample No. field to display the virtual keyboard. Enter a new
sample name.
NOTE
It is possible to modify the sample name selected: Press on the
Sample No. entry field, the virtual keyboard appears allowing a
manual modification.
.
96 UM_2.00A_EN
NOTE
Passing to the next screen of the Start Guide is only possible if a
sample name or number is entered.
NOTE
lf the operator presses the Continue start procedure button without
entering or selecting a name, the sample name of the last test per-
formed is entered by default.
3. Press the Continue start procedure button to continue.
Select a distillation product
Fourth screen of the Start Guide mode - selection of a distillation product
NOTE
If (in the previous step) the sample name has been selected in the
prestored list, the corresponding product is proposed by default.
1. Press on the Get product list button to display the list of the distillation
products stored in the unit.
2. Select a distillation product in the list prestored in the OptiDist™ (If needed or
if it is the first test since the OptiDist™ switching on).
UM_2.00A_EN 97
3. Press on the distillation product desired to select it: the product name is
automatically entered in the “Product” entry field.
4. Press on the Continue start procedure button to continue.
Conditions fulfilled - Start the test
The last screen of the Start Guide appears:
Fifth screen of the Start Guide mode - test initiating
Data entered previously appear on the left of the screen. Only the state indicators
of starting conditions not fulfilled indicated with the following icon “X ” in red are
displayed to make the reading of the screen easier for the operator.
They indicate that the test cannot be started now.
If cleaning and preparation operations have been already done as recommended

in the chapter “Preparation”, the following starting conditions are validated and
consequently they are not displayed:
• Receiver: Receiver cylinder well installed in the receiving chamber
• Probe: Vapor temperature probe is correctly connected
NOTE
The operator can still prepare the accessories and the OptiDist™
as indicated in the right of the screen.
98 UM_2.00A_EN
NOTE
The diameter of the base plate installed can only be detected when
the distillation flask heater platform is in high position with the distil-
lation flask installed in the heater assembly and a product is
selected.
The distillation flask filled with sample and the receiver cylinder can now be set up
in the OptiDist™.
The operator will be able to start the test when all starting conditions will be
validated: the Start button will appear in the left bottom of the screen.
1. Press the Start button to start the test.
UM_2.00A_EN 99
6.2.1.2 Quick Start mode

Start a new test
In case of a series of test on the same sample type, the Quick test starting mode
allows the operator to start a test from the Run / Start & Display screen without
inputting parameters. The OptiDist™ will use the same set-up than the previous
test. If the distillation group is the same than in the previous test a test can be
started with two button strokes. To use this mode, the test starting mode must be
set on “Quick” mode.
The screen of the Quick Start mode
NOTE
The test-starting mode is part of OptiDist™ internal parameters and
can be modified with a level 1-access authorization (Supervisor).
1. Press the New Test button in the left bottom of the Run / Start & Display
Screen.
When the New Test button is pressed, the operator name, the sample name and
the product used for running the previous test are automatically recalled in the
dedicated field and the New Test button turns into Start button allowing a new test
to be started immediately. The product list is immediately displayed.
If needed, the user can modify all parameters in the same way that in “Normal”
mode.
The OptiDist™ can also be set to increment automatically the sample number. For
this, the “Auto increment sample no.” internal parameter must be set on “Yes”.
100 UM_2.00A_EN
NOTE
If it is the first test since the OptiDist™ is switched on, a product
must be selected.
NOTE
According to the OptiDist™ internal settings, a dialogue box can
appear when the New Test button is pressed for the adjustment of
ment of the sample charge volume. These cases are handled in the
section “Setup of the receiver chamber”.
If cleaning and preparation operations have been already done and correctly
performed, the following starting conditions are validated:
/i

NOTE
during/after the test setup.
NOTE
Diameter of the base plate installed can only be detected when the
distillation flask heater platform is in high position with the distilla-
tion flask installed in the heater assembly and a product is
selected.
NOTE
The operator can still prepare the accessories and the OptiDist™.
1. Prepare and insert the sample and the receiver cylinder.

UM_2.00A_EN 101
NOTE
The Start button of the Run / Start & Display screen, or the New
Test button if the test is initiated from the Start Guide, turns into
Stop button allowing the operator to stop the test at any time.
102 UM_2.00A_EN
6.2.1.3 Normal start mode

Start a new test
For a complete set-up of the test directly in the Run / Start & Display screen
(information of the operator name with sample name/number and selection of the
product) in "Normal" mode, the test-starting mode must be set on "Normal".
Run / Start & Display screen for the operator
NOTE
The test-starting mode is part of OptiDist™ internal parameters and
can be modified with a level 1-access authorization (Supervisor).
1. Press the New Test button in the left bottom of the Run / Start & Display
screen.
The Run / Start & Display screen is reset and the New Test button turns into
START button allowing a new test to be started when it will be set up and
when all starting conditions will be fulfilled.
NOTE
According to the OptiDist™ internal settings, a dialogue box can
appear when the New Test button is pressed for the adjustment of
ment of the sample charge volume.
If cleaning and preparation operations have been already done and correctly
performed, the following starting conditions are validated:
UM_2.00A_EN 103
/i

NOTE
during/after the test setup.
Select the operator name in the prestored list
Selection screen of an operator name

1. Press on the list button in front of “Operator:” to display the list of operator
names stored in the unit (this list also contains the operator names of the last
tests performed with the unit, up to 100).
The list of operator names stored in the unit appears.
2. Press on the desired name to select it and automatically enter it in the
corresponding field.
104 UM_2.00A_EN
Select the sample name in the prestored list by manual entry
Selection screen of sample names with the associated product

1. Press on the list button in front of “Sample No.” to display the list of samples
tested with the unit (up to 100) associated with a test product.
2. Either: Press on the desired sample name to select it and automatically enter
it in the corresponding field.
The associated product is proposed in the “Product” field.
3. Or: Press on the “Sample No.” entry field to display the virtual keyboard to
enter a sample name or number manually and then select the appropriate
product for the sample to be distilled.
The list of last samples tested with the associated product appears.
NOTE
It is possible to modify a sample name selected in the prestored
list: Press on the “Sample No.” entry field, the virtual keyboard
appears allowing a manual modification.
UM_2.00A_EN 105
Select the product in the prestored list

If the operator has entered a sample name manually, he has to select a product in
the list of products stored in the unit.
If the operator has chosen a sample name in the prestored list, he can choose
another product than the one proposed with the sample name selected.
Selection screen of products

1. Press on the list button in front of “Product:” to display the list of test products
stored in the unit.
2. Press on the appropriate product for the sample to be destilled to select it and
automatically enter it in the corresponding field.
106 UM_2.00A_EN
Conditions fulfilled - Start the test

The distillation flask filled with sample and the receiver cylinder can now be set up
in the OptiDist™.
1. Prepare and insert the distillation flask and the receiver cylinder.
NOTE
The diameter of the base plate installed can only be detected when
the distillation flask heater platform is in high position with the distil-
lation flask installed in the heater assembly and a product is
selected.
The operator will be able to start the test when all starting conditions will be
validated.
Add a comment in the “Note:” field

At any time, it is possible for the operator to add a comment that will be stored with
the result.
1. Press on the “Note:” entry field.
The virtual keyboard appears allowing to enter a comment.
UM_2.00A_EN 107
6.2.2 Start procedure - run a distillation test
6.2.2.1 Start the test
NOTE
When the distillation flask will be installed and the distillation flask
heater platform will be in elevated or "run" position, the opening
diameter of the base plate will be indicated in front of the "Base
plate" state indicator in the starting condition list of the Run /Start &
Display screen.
1. Press the New Test button in the left bottom of the OptiDist™ Run /Start &
Display screen then set up the test.
NOTE
According to the configuration of the OptiDist™ internal parame-
ters, the test starting will be done either with the Start Guide or
directly in the Run /Start & Display screen in Normal mode or in
Quick mode.
6.2.2.2 Test progressing after test start

When you press the START button, the OptiDist™ verifies the different test
starting conditions.
If all conditions are fulfilled, the test starts. If the test has been initiated from the
Start Guide mode, the Run / Start & Display screen is automatically displayed. The
message “START” appears in the status bar in the top of the screen and the
OptiDist™ measures the volume of sample that is left in the receiver cylinder. If
this volume is lower than 3%, the OptiDist™ will start the sample distillation.
NOTE
The test can only start if
• all starting conditions, like cleaning operations and proper
installation of appropriate accessories, are fulfilled.
• the receiver cylinder positioned in the receiving chamber is
empty.
NOTE
The test can not start if the condenser tube is not cleaned.
Cleaning is a part of the OptiDist™ internal parameters: parameter
“Show condenser cleaning”.
If another swab than the one provided with the unit is used, test
start refusal can be disabled.
If not all starting conditions are fulfilled, the starting condition(s) not fulfilled will be
indicated in the left bottom of the last screen of the Start Guide.
In case of a normal or a quick test starting, the test starting conditions not fulfilled,
are identified in the left bottom of the Run / Start & Display screen by a cross in a
red box.
108 UM_2.00A_EN
6.2.2.3 Manual test stop

When a test is started, the START button in the left bottom of the Run /Start &
Display screen turns into STOP button allowing the operator to stop the test any
time.
If a test progressing is stopped, a confirmation message appears: “Do you really
want to stop the test”. Confirm the test stopping by pressing on “Yes” or abort the
request by pressing on “Cancel”.
The result will be stored after all in the memory.
6.2.2.4 Distillation phases

• The first distillation phase is the “INITIAL HEAT” phase: the OptiDist™ applies
heating to the sample and thanks to the Optimizer automatically regulates the
heating power during the entire distillation run to meet with the standard test
method requirements.
• The Run / Start & Display screen includes a test-monitoring diagram in which
all readings (temperatures and volume) are displayed in real time allowing the
operator to follow the evolution of the test. The distillation conditions, vapor
temperature, volume, times and rate are reported in real time in a spreadsheet
that can be displayed by pressing the key: on the right. The button turns
into key: allowing displaying again the distillation test-monitoring diagram.
• When the IBP is found, the message becomes “DISTILLATION”.
• The “DISTILLATION” phase is completed when the residual liquid in the
distillation flask is approximately 5 ml, the “FINAL HEAT” phase starts until the
stop condition configured in the product used to perform the test is found
(FBP, Dry Point, etc.). Then the OptiDist™ waits until the volume in the
receiver cylinder stabilizes and starts the COOLING phase in background
(see next section). This phase is called “RECOVERY”.
• If for any reason a problem occurs during distillation, the OptiDist™ will trigger
an alarm and in certain cases, the test will be stopped. A message will appear
indicating the reason.
Whatever happens, the reason for the stopping of the test will be displayed.
6.2.2.5 End of test and cooling
The “COOLING” phase starts in background as soon as the test is completed

when the RECOVERY phase starts:
• The distillation flask heater platform is automatically released in low position to
increase cooling efficiency of the distillation flask and the distillation flask
heater assembly.
• The cooling fan of the heater assembly starts to cool the distillation flask, the
base plate, and the heating element. The cooling phase lasts about 10
minutes. It stops when the vapor temperature is lower than 50 °C.
• The level follower returns to its standby position (upper position).
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WARNING
Let the distillation flask cool before removing it. Check the vapor
temperature displayed in the test-monitoring diagram.
The result is saved in the OptiDist™. If the residue is automatically input by the
OptiDist™, the result is immediately displayed according to the parameters of the
report profile set in the product. The result can also be printed and/or sent to the
PC/LIMS. If the residue should be manually input or measured by the OptiDist™,
a dialogue box appears indicating the procedure to follow.
6.2.3 Residue measurement
6.2.3.1 Automatic input
According to the “Residue measurement” parameter set in the product data base
selected to perform the test, the residue can be:
• Predicted by the OptiDist™ using the optimizer.
• Constant (a default residue is entered in the product)
• None (set in the product)
In this case, the residue is automatically entered at the end of test.
6.2.3.2 Manual input

If the “Residue measurement” parameter is set in the product on “manual”, the
operator has to measure the residue into a 5 ml graduated cylinder to the nearest
0,1 ml.
CAUTION
Wait for the distillation flask is cooled before removing it for the res-
idue measurement. Check the vapor temperature displayed in the
test-monitoring diagram.
A yellow box appears under the test-monitoring diagram at the end of test allowing
entering the residue manually using the virtual keypad.
6.2.3.3 Measured residue by the OptiDist™

If the “Residue measurement” parameter is set in the product on “Delta volume”,
the operator will be able to use the level follower of the receiving chamber to
measure precisely the residue in the distillation flask. At the end of test, a dialogue
box appears asking to the operator to spill the distillation flask residue in the
receiver cylinder.
110 UM_2.00A_EN
WARNING
Wait for the distillation flask is cooled before removing it for the res-
idue measurement. Check the vapor temperature displayed in the
test-monitoring diagram.
1. Spill the distillation flask residue in the receiver cylinder and replace the
receiver cylinder in the receiving chamber.
2. Close the receiving chamber door then press the OK button in the dialogue
box.
6.2.4 Displaying and printing of results

The internal memory the OptiDist™ can store up to 100 test results, that can be
displayed at any time.
The last result of the list is the last test result saved. When the memory is full, the
OptiDist™ automatically deletes the first result saved (the oldest).
Results can be displayed either graphically, as a plot of the distillation, or in a
table, according to standard test method requirements or according to customized
report profile set in the product selected to perform the test. Results also include
specific limits and method limits if set in the profile.
To display and print the test result, refer to 7.1. The Results database.
1. Press the Results button on the Run / Start & Display screen.
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112 UM_2.00A_EN
Database management OptiDist™
7 Database management
UM_2.00A_EN 113
OptiDist™ Database management
7.1 The Results database

The internal memory of the OptiDist™ can store up to 100 test results, that can be
displayed at any time.
The last result of the list is the last test result saved. When the memory is full, the
OptiDist™ automatically deletes the first result saved (the oldest).
Results can be displayed either graphically, as a plot of the distillation, or in a
table, according to standard test method requirements or according to customized
report profile set in the product selected to perform the test. Results also include
specific limits and method limits if set in the profile.
NOTE
• To transmit test results, to modify or to delete them, a level 1
access (Supervisor) or level 2 access (Maintenance) is
required.
• With level 0 access, the operator can only view and print the
test results.
7.1.1 Displaying of results

Open the Results main menu:
1. Press the Results button on the Run / Start & Display screen.
The Results main menu opens.
Screen of the Results main menu
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Buttons on the Results main menu display

Result Modification button: Modify parameters in the result
View button: Displaying of the list of results stored in the internal memory
Graphic result displaying
Displaying of temperature and volume specifications and reference standard

method limits
Displaying of computed values (DI, CI)
Transmit to LIMS button: Sending of the result to the LIMS
Print button: Printing of the results displayed
Exit button: Return to the Run / Start & Display screen
Left/right arrow buttons to scroll through the up to 100 pages with results stored in
the internal memory of the OptiDist™
Scroll through the stored results:

1. Use the left/right arrow buttons at the bottom of the screen to scroll through
the results stored in the internal memory of the OptiDist™.
NOTE
Information displayed is presented by default according to the
parameters of the report profile set in the product used to perform
the test.
The spreadsheet can display different information in each column:

1. Press the headline of each column to scroll through the various possibilities.
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Spreadsheet column headlines of the Results main menu display

Column 1 Volume Report of volumetric readings in percentage of the charge volume
according to standard test methods requirements
User V Customized report of volumetric readings in percentage of the charge
volume according to the report profile selected in the product used to
perform the test
Vol 1% Displaying of volumetric readings at intervals of 1% of the charge vol-
ume
Vol 5% Displaying of volumetric readings at intervals of 5 % of the charge vol-
ume
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Spreadsheet column headlines of the Results main menu display

Column 2 Cor Tmp Displaying of the barometric corrected temperature readings
Obs Tmp Displaying of temperature readings at prescribed percent recovered
Evp Tmp Displaying of temperature readings at prescribed percent evaporated
Column 3 Cor Tmp Displaying of the barometric corrected temperature readings
Evp Tmp Displaying of temperature readings at prescribed percent evaporated
Rate Displaying of the instantaneous distillation rate
Heat Displaying of the temperature of the heating element
Column 4 Rate Displaying of the instantaneous distillation rate
Heat Displaying of the temperature of the heating element
View list of results with tested sample name and corresponding date:
1. Press the View button in the Results main menu.
The following screen appears:
Results screen with list of tested sample names
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Further buttons on the Results main menu display

Remove button: Removal of the highlighted sample no.
Spreadsheet result displaying
Transmit to PC button: Sending database to PC
Return to the Run / Start & Display screen:

1. Press the Exit button to return to the Run / Start & Display screen.
7.1.2 Printing of results
1. Activate the Results main menu.

2. Display the desired result.
3. Press the Print button to print the result displayed.
Results can be printed in different ways:

• with more or less details
• with the product parameters
• without the product parameters
• the specifications and limits of the standard test method
• with temperature in °C or °F
• with the error messages
All these parameters are set in the report profiles and results are printed according
to the report profile set in the product used to perform the test.
lt is possible to print test result automatically after the end of each test.
7.1.3 Transmitting of results

3. Either press:
a. button Transmit to PC to send the displayed result to a PC or
b. button Transmit to LIMS to send the displayed result to the LIMS.
4. Validate by pressing the OK button.
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Send results to PC
Send results to LIMS
118 UM_2.00A_EN
7.1.4 Modifying of results

3. Press the Result Modification button.
Results database modification screen - modification of results
4. Modify the result data.
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Results database modification screen - storing of modified results

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Buttons on the Database modification screen

Store button: Storing of the modified result
No Store button: Cancel the action without storing
5. Validate by pressing the Store button or quit without validating by pressing the
No Store button.
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7.1.5 Creating of a new optimized product

The OptiDist™ can automatically optimize the initial heat regulation to get perfect
IBP time. This can be achieved by pressing the Create new optimized product
button at the bottom of the Results database modification screen.
3. Press the Result Modification button.
4. Press the Create new optimized product button.
Results Database modification screen - creation of a new optimized product
5. Validate by pressing the OK button or quit without validating by pressing the

Cancel button.
6. Type new sample name or accept the one proposed.
7. Modify the result data if desired.
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Results database modification screen - storing of a new optimized product.
No Store button.
7.1.6 Removing of results

3. Press the Remove button to delete the result displayed.
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Results screen - deleting of results
4. Validate by pressing the Yes button or quit without validating by pressing the
No button.
7.2 The Products database

The Products main menu allows accessing to a database stored in the OptiDist™
in which up to 200 preset distillation products can be stored.
A product consists of a series of parameters and limit values that will act as a
guideline for the distillation test complies with the standard test method and the
group set-up.
Products factory set comply with international standard test methods. With a level
1-access authorization (Supervisor), these products can be displayed and copied
for creation of a new product. Other products can be modified or they can be
deleted.
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NOTE
• To modify, delete, copy and create products, a level 1 access
(Supervisor) or level 2 access (Maintenance) is required.
parameters of the preset products.
Exception:
• A Supervisor with level 1 access can give authorisation to the
operator in the Parameter main menu by setting the Parameter
“Product modif. by operator: = yes”. The operator can then
modify products with the following limitations:
- Product modifications are only effective for one test
- Product modifications will not be stored in the product data-
base
- The operator cannot create new products to be stored in
the database
- The operator cannot delete prestored products from the
database
Open the Products main menu:

1. Press the Products button on the Run / Start & Display screen.
The Products main menu opens.
The first page of the Products main menu
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Buttons on the Products main menu display

Remove button: Removal of the product displayed
Copy button: Creation of a new product by making a copy of the one displayed
Print button: Printing of the parameters of the product displayed
Reports button: Accessing to the list of prestored report profiles
Standard button: Accessing to the list of prestored standard test methods and
D850/D1078 compounds
Left/right arrow buttons to scroll through the eight pages with all parameter settings
for each product.
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Parameters on the first page of the Products main menu display

Product: The name of the product (permanent field) - a maximum of 20 characters can be
used
- Routine The type of the product:
- Calibration • Routine: Product used to run current samples
- Quality • Calibration: Product used to run pure products to calibrate the optimizer.
These products are factory set and cannot be modified or deleted.
• Quality: Product used to run reference samples in order to supervise the per-
formance of the OptiDist™. The specific values of the results obtained
(defined in the specification limits of the product) are also stored in the Quality
Control Database allowing trend analysis
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Parameters on the first page of the Products main menu display

Standard: Selection of the group and the standard test method in the list of prestored stand-
ards. On selection, concerned parameters are checked regarding to the limit val-
ues set in the standard test method selected
Report: Selection of a report profile in the list of prestored reports. The report file deter-
mines the format for displaying of results, printing and sending to the LIMS
Heat control: Selection of the heating mode:
• One-Button Distillation: Automatic heating mode
Selected by default with the ASTM D86 - the heating power is automatically
adjusted using the optimizer so as to respect specifications of the standard
test method selected above.
• One-Button + Offset: Automatic heating mode where the user can change
expected IBP time and 5%-time.
• Manual Distillation: Automatic heating mode with manual measurement of
vapor temperature with liquid-in-glass thermometer. The user can adjust the
initial heat regulation to get perfect IBP-time and 5%-time. He can enter two
heating temperatures and the duration of the first heating level.
• Supported: Selected by default with the ASTM D850 / D1078
The user can adjust the initial heat regulation to get perfect IBP-time and 5%-
time. He can enter two heating temperatures and the duration of the first heat-
ing level.
• Bar. corr.: For ASTM D850 and ASTM D1078 standard test method only
Selection of a compound for the determination of the constants to be applied
for variations in barometric pressure.
1. Use the right arrow button at the bottom of the screen to scroll to the next
page with further product parameter setting options.
126 UM_2.00A_EN
The second page of the Products main menu
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Parameters on the second page of the Products main menu display

Distillation rate: Filled by default with the average of limit values of the standard test
method selected -Uniform average rate of condensation from 5 or 10%
volume to 5 ml residue in the flask.
Condenser temperature: Temperature of the condenser bath
• Constant: Fixed by a set point temperature - Selected by default
and filled by default with the average of limit values of the standard
test method selected
• Linear: Increase of the condenser temperature with recovered
volume (enter a starting and an ending temperature for the
condenser)
• Switching: Modification of the condenser temperature when the
vapor temperature reaches a set value (enter the starting tempera-
ture, the second temperature and the vapor temperature at which
the second condenser temperature must be applied)
Receiver temperature: • Constant: Fixed by a set point temperature - Selected by default
and filled by default with the average of limit values of the standard
test method selected
• Linear: Increase of the receiver temperature with recovered vol-
ume (enter a starting and an ending temperature for the receiver)
• Switching: Modification of the receiver temperature when the vapor
temperature reaches a set value (enter the starting temperature,
the second temperature and the vapor temperature at which the
second temperature must be applied)
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The third page of the Products main menu
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Parameters on the third page of the Products main menu display

FBP detection: Selection of the type of FBP detection:
• Max Temperature: Selected by default with the ASTM D86 – The Final
Boiling Point is detected by a temperature drop. The maximum tem-
perature reading before the temperature drop is then determined and
recorded as the FBP.
• Dry Point: Selected by default with the ASTM D1078 / D850 - End of
test on detection of the dry point (automatic or manual).
• Max. Temp. or Dry Point: End of test on maximum temperature or on
Dry Point (automatic or manual).
• Max. Temp. and Dry Point: End of test with maximum temperature and
Dry Point (automatic or manual).
Automatic final heat Automatic final heat regulation: “Yes” is selected by default in ASTM D86. If
regulation: “Yes”, the OptiDist™ determines the volume for the final heat adjustment
and adjusts the final heating. “No” is selected by default in ASTM D1078 /
D850. If the selection is “No” the user has to enter the volume for last heater
correction and the last heater correction:
• FBP detection at: Set by default at 95% in ASTM D1078 / D850 – Indi-
cation of the volume corresponding to 5 ml residue.
• Final power adjustment: Set by default at 0% in ASTM D1078 / D850 –
Correction of the heating power in percentage (additional power) so as
to respect time specifications between 5 ml residue and the FBP if time
specifications are applicable to the standard method (e.g. ASTM D86).
FBP temperature Set by default at 2 °C. The FBP is detected by a temperature drop (t °C)
drop: usually between 1 and 5 °C. This detection parameter means that any inter-
mediate temperature (< t °C) variations are neglected. The maximum tem-
perature reading (before the temperature drop) is then determined and
recorded as the FBP.
FBP time max: Set by default at 5 min – Set-up of the maximum time between 5 ml residue
and FBP.
Dry point detection: • Automatic: Selected by default – Automatic detection by the automatic
dry point detection kit.
• Manual: Manual detection by the operator by pressing a button
appearing in the Run / Start & Display screen a few minutes before the
expected dry point.
• Learn: The first dry point detection of the sample tested with this prod-
uct will be done in manual mode.
Then the OptiDist™ will automatically calculate the delay and will store
it in the product parameters.
This delay will be used for the following tests in automatic dry point
detection.
Dry point delay: Set by default at 0 s – Time in seconds by which the dry point should be
delayed for automatic detection. This parameter is not effective for the man-
ual detection of the dry point. The parameter is automatically set to zero
when using the mode “dry point learning”. Such a delay for the automatic
detected dry point is necessary for many substances, because the sensor
responds too quickly and the automatically determined dry point differs from
the observed dry point.
Stop at: • %: The test can be stopped at a certain volume.
• °C: The test can be stopped at a certain vapor temperature value.
• --- / IBP / FBP / DP: The test can be stopped when the IBP or the FBP
or the Dry Point is found.
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The fourth page of the Products main menu
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Parameters on the fourth page of the Products main menu display

Recovery detection: • Volume change: Selected by default – Measurement of the recovery
following automatic method - the volume in the receiver cylinder is
observed until this volumes changes by no more than a certain
amount (default set at 0,1 ml) in a certain time (default set at 120s)
• Volume constant: Measure of the recovery following manual method -
the volume in the receiver cylinder is observed at fixed intervals until
two successive observations agree (adjustable parameter)
• Waiting time: Set-up of the waiting time after the FBP
Residue measure- • Prediction: Selected by default with the ASTM D86 – Residue auto-
ment: matically predicted using the Optimizer
• Manual: Selected by default with the ASTM D1078 / D850 – Manual
key-in of the residue after the end of test.
• Delta volume: Use of the level follower to measure the residue after
spilling in the receiver cylinder
• Constant: Use of a default residue automatically entered
• None: None residue
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Parameters on the fourth page of the Products main menu display

Hesitation: “No” is selected by default – Report of the hesitation point with the result.
Decomposition: “No” is selected by default – Report of the decomposition point with the
result.
Oven cool temp.: Temperature to which the flask must be cooled.
NOTE
In the case of the distillation of a QC sample, specifications limits
define the points recorded in the QC sample database.
The fifth page of the Products main menu
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The sixth page of the Products main menu
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Parameters on the fifth and sixth page of the Products main menu display
Spec. limits for defined • Observed: Percent recovered specified
temperatures: • Pressure corrected: Volume specified according to corrected
temperature readings
• Evaporated: Percent evaporated specified
Temperature: Set-up of the defined temperature for accepted minimum and maximum
volume value
Mini vol / Maxi vol: Set-up of the accepted minimum and maximum volume value
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The seventh page of the Products main menu
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Parameters on the seventh page of the Products main menu display

Spec. limits for defined • Observed: Temperature specified according to percent recovered
volumes: • Pressure corrected: Corrected temperature readings specified
• Evaporated: Temperature specified according to percent evapo-
rated
Volume: Set-up of the defined volume for accepted minimum and maximum tem-
perature value for IBP, several percent steps, FBP an DP.
Mini temp / Maxi temp: Set-up of the accepted minimum and maximum temperature value
UM_2.00A_EN 133
The eighth page of the Products main menu
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Parameters on the eighth page of the Products main menu display

Method limits: Setting of limits fixed by the standard test method (filled with default
values when the standard is set in the first screen)
• IBP time: Minimum and maximum time between the first application
of heat and the IBP.
• 5% time: Minimum and maximum time between IBP and 5% recov-
ered (for group 1 and 2)
• 10% time: Minimum and maximum time between IBP and 10%
recovered (for group 0).
• FBP time: Minimum and maximum time from the 5 ml of liquid resi-
due in the flask to the FBP.
• Rate 5% - 15%: Average rate of condensation from 5% - 15% recov-
ered (according to standard test method) to 5 ml residue in the flask
Rate 16% - last corr.: Average rate of condensation from 16%
recovered to the final heat adjustment
• Rate 16% - last corr.: Average rate of condensation from 16%
recovered to the final heat adjustment.
• Loss: Minimum and maximum loss.
134 UM_2.00A_EN
7.3 The QC (Quality Control) sample database

The Quality Control database allows tracking specified results of 50 Quality
Control samples (QC samples) for example, a reference material.
Each QC sample should be run with a different “Quality” type product to be stored
in a specific QC sample database. The specified results are set in the specification
limits of the quality product used to run the QC sample.
Each specified result of all tests of a QC sample (run with the same quality
product) can be displayed in a spreadsheet or under graphic form to show trends.
The minimum and maximum specification limits set in the quality product used to
run the QC sample selected are displayed in the graphic allowing the laboratory
supervisor to easily see if the result is out of range. Thus, using a reference
product or a reference material, the laboratory supervisor can monitor the
deviation of the OptiDist™ and decide when it needs to be recalibrated.
NOTE
• To modify the QC database or to modify a quality product, a
level 1 access (Supervisor) or level 2 access (Maintenance) is
required.
• With level 0 access, the operator can only view and print
parameters and information diplayed on the QC main menu
screen.
7.3.1 Displaying the spreadsheet format of the QC sample database

Open the QC main menu:
1. Press the QC button on the Run / Start & Display screen.
The QC main menu opens.
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The QC main menu - spreadsheet format

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Buttons on the QC main menu display

Remove button on the right of the display: Removal of all QC sample tests from
the QC sample database displayed
QC Parameter button: Visualization of the parameters of the quality product used
to run the QC sample displayed
Print button: Printing of the parameters of the QC-sample displayed
Complete Test Results button: Displaying of the complete result of a test.

Only results defined in the specification limits of the quality product used to run the
QC sample test are stored in the QC sample database but all tests are stored in
the results database. They can be displayed at any time from the QC database
with this button.
Remove button on the bottom of the display under the “Statistics” group : Removal
of one test from the QC sample database displayed
Left/right arrow buttons to scroll through the two pages of the QC main menu.
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Parameters on the QC main menu display

QC sample Name: Selection of the QC sample database displayed
Specification point: Selection of the specific result displayed from the specification limits set in
the quality product used to run the QC sample displayed
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Further information on the QC main menu display

Mini Minimum value accepted for the result specified (volume or temperature)
Maxi Maximum value accepted for the result specified (volume or temperature)
Statistics • Mean: Mean of results obtained for the specific result displayed
• Mini: Minimum value obtained for the specific result displayed among all
tests on the QC sample displayed
• Maxi: Maximum value obtained for the specific result displayed among
all tests on the QC sample displayed
• Std. Dev.: Standard deviation calculated according to the following for-
mula:
where {x1, x2, ..., xN} is the sample and x is the mean of the sample
Green/red colours in The colour of the listed lines and of the value indicates if the result is within
the list or outside of the specification limits:
• Complete line is green: All specified values of the QC sample run are
within the specification limits
• Line is red and only the measured value is green: One or more speci-
fied values of the QC sample run is outside of the specification limits but
the specified value displayed is within the specification limits
To select a QC sample to be displayed:

1. Press on the pull-down menu QC Sample Name and select from the list.
All specified results of all tests performed on a QC sample are stored in a QC

sample database, but only the specified results selected in the pull-down menu
Specification point are displayed per page.
To select the specified value to be displayed:

1. Press on the pull-down menu Specification point and select from the list.
7.3.2 Displaying the graphic format of the QC sample database

The graphic QC sample database includes the same menus and information than
in the spreadsheet QC sample database with in addition, the minimum and
maximum specification limits set in the quality product used to run the QC sample
selected. These limits allow seeing rapidly if the specified result displayed is within
or outside of specifications and underline an eventual deviation of the specified
result.
Open the graphic format of the QC sample database:

1. In the spreadsheet format of the QC main menu display press the right arrow
button.
UM_2.00A_EN 137
The graphic format of the QC sample database opens.
The QC main menu - graphic format
Return to the spreadsheet format of the QC sample database:

1. Press the left arrow button to return to the spreadsheet format of the QC
sample database.

7.3.3 Removal of a test from a QC sample database
1. Display the spreadsheet format screen of the QC sample database.

2. Press the Remove button on the bottom of the screen under the “Statistics”
group: a dialog box appears allowing to indicate the line number of the test to
be deleted.
3. Press on the keying field to enter the number: the virtual keypad appears.
4. Enter the number, then press the ENTER button.
5. Press the OK button to delete the test.
138 UM_2.00A_EN
7.3.4 Modification of specified results in a QC sample database

Specification limits set in the quality product used to run a QC sample define the
specified results recorded in the QC sample database. Specified results can be
added or deleted by modifying the specification limits of the quality product. Refer
to 7.2. The Products database.
NOTE
When a specification of a Quality Product is modified, if a point is
added, it will be recorded in the next quality records. If a point is
deleted, it will be no more available for quality control.
7.3.5 Removal of a QC sample database

To delete a QC sample database, delete the corresponding Quality Product from
the list of prestored products. Refer to 7.2. The Products database
UM_2.00A_EN 139
7.4 The Messages database

The OptiDist™ can register up to 48 different alarm messages. These alarm
messages can be displayed in the Messages main menu.
Open the Messages main menu:

1. Press the Messages button in the Run / Start & Display screen.
The Messages main menu opens.
Messages main menu - alarm display screen
If an alarm occurs, the alarm review is displayed on the alarm diplay screen. In
this case, the status bar on the centre-top of the screen changes from green to red
and indicates “ERROR”.
• To quit the alarm, press the OK button.
• To return to the Run / Start & Display screen, press the Exit button.
Open the alarm history list of the Messages main menu:

1. Press the History button to open the alarm history list.
The alarm history list opens.
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Messages main menu - alarm history list
The alarm history list can store up to 200 alarm messages including date, time,
alarm code and alarm message.
The last alarm message of the list is the last message saved. When the memory is
full, the OptiDist™ automatically deletes the first message saved (the oldest).
• To print the alarm history list press the Print button.
• To exit the alarm history list and return to the Run / Start & Display screen
press the Exit button.
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7.5 The OptiDist™ Parameter database

The Parameter main menu allows accessing to the OptiDist™ internal
parameters. All parameters can be modified by pressing on the corresponding
field: the virtual keypad or the virtual keyboard will automatically appear. In case of
scrolling selection, press on the field to scroll through the various possibilities (flip-
flop selection).
NOTE
• To modify the parameter settings, a level 1 access (Supervisor)
or level 2 access (Maintenance) is required.
• With level 0 access, the operator can only view and print
parameter settings.
Open the Parameter main menu:

1. Press the More button on the Run / Start & Display screen and then press the
Param. button.
The Parameter main menu opens.
The first page of the Parameter main menu
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Buttons of the Parameter main menu display

Print button: Printing of the parameter settings displayed
Left/right arrow buttons to scroll through the five pages with all internal parameter
settings for the OptiDist™.
/i
Unit parameters on the first page of the Parameter main menu display
Start Mode: Selection of the default test-starting mode
• Guided: Set-up and starting of a new test using the Start Guide.
• Normal: Complete set-up and starting of a new test from the
Run / Start & Display screen with the Normal Start Mode.
• Quick: Starting of a new test with the Quick Start Mode from the
Run / Start & Display screen with the parameters of the last sam-
ple tested.
Ambient sensor connected: Measurement of the ambient temperature with the ambient tempera-
ture probe (available as option). If “Yes” is selected and no probe is
connected, an alarm is released indicating the probe is faulty.
Adjust receiver at start: Request to enter the desired receiver chamber temperature which
should be the same as the charge temperature of the sample
Pressure Unit: Selection of the pressure measurement unit used by default (hPa,
kPa, mBar, Bar, mmHg or psi).
Autoincrement sample no.: Last sample number is always proposed when starting a new test. If
this parameter is set to “Yes”, the sample number is automatically
incremented avoiding to have the same sample number in the result
database. If the sample ID is selected in the list stored in the Opti-
Dist™, the ID will be incremented when selected
Autoclear sample no.: Sample number field will be cleared at test start
Check cond. cleaning: Checking or not of the condenser cleaning before test starting (part of
the test starting conditions)
Scan charge volume: Measuring of the charge volume in the receiver before test starting
Product modif. by operator: • If this parameter is set to “No”, the operator cannot modify pro-
ducts
• If this parameter is set to “Yes”, the operator can modify products
with the following limitations:
- Product modifications are only effective for one test
- Product modifications will not be stored in the product data-

base
- The operator cannot create new products to be stored in the

database
- The operator cannot delete prestored products from the

database
Temp. unit: Selection of the temperature measurement unit used by default by the
OptiDist™
UM_2.00A_EN 143
Unit parameters on the first page of the Parameter main menu display
Touch beep: Beep when a button is pressed
Lanuage: Selection of the language for the user interface of the OptiDist™ (Eng-
lish, German or French)
Screen saver: Screen saver on or off
S. Saver time: Time before the Screen saver starts
NOTE
From each page of the Parameter main menu it is always possible
to return to the Run / Start & Display screen by pressing the Exit
button.
page with further parameter setting options for the OptiDist™.
The second page of the Parameter main menu
144 UM_2.00A_EN
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Unit parameters on the second page of the Parameter main menu display
Access level reset time: Set-up of the time during which the Supervisor or the Service access
level is active. If the touch screen does not detect any contact up to
the end of this time, the access level is reset to the Operator level (this
time is not taken into account in Diagnostic mode, during a test or dur-
ing calibration). The countdown is reset at each contact.
Startup access level: Selection of the access level activated at the analyzer switching-on.
Supervisor password: Set-up of the password of the Supervisor access level – 5 characters
minimum.
Maintenance password: Set-up of the password of the Maintenance access level – 5 charac-
ters minimum.
The third page of the Parameter main menu
UM_2.00A_EN 145
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Unit parameters on the third page of the Parameter main menu display
Unitname: Set-up of the unit name which is shown on start screen and print out.
Serial No.: Displaying of the unit serial number.
Network configuration: Set-up of the network used
• Stand alone unit: Use of the unit as an independent OptiDist™
• PC controlled: Networking of the unit with the new PC software
• ALAN controlled: Networking of the unit with Alan
• HLIS controlled: Networking of the unit with HLIS
Unit Id: Id of the unit in the network
The fourth page of the Parameter main menu

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Unit parameters on the fourth page of the Parameter main menu display
Printer: Selection of the printer used
• Internal: Printing of data with the built-in printer
• External: Printing of data with an external printer connected to
the USB A connector (located at the rear of the unit).
Lines per page: Set-up of the number of lines per page.
146 UM_2.00A_EN
The fifth page of the Parameter main menu

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Unit parameters on the fifth page of the Parameter main menu display
Ethernet settings
Server IP address: Set-up of the Server IP address to which the OptiDist™ is connected.
Contact your network administrator (requires level 2 access)
Unit IP-Address: Set-up of the unit IP address. Contact your network administrator
(requires level 2 access)
automatic / manual: Set-up of the address manually / automatically (provided by the sys-
tem)
RS232 settings
Baudrate: Set-up of the rate of transfer
Data bit: Set-up of the data bit
Parity bid: Set-up of the parity bit
Stop bit: Set-up of the stop bit
Protocol: Set-up of the communication protocol used (xon-xoff, hardware or
none)
UM_2.00A_EN 147
7.6 The service functions of the Parameter database

The Parameter main menu contains a sixth page, which is only accessible at
Maintenance level. Access to these menus requires having a level 2-access
(Maintenance) authorization.
1. To open the Parameter main menu, press the More button on the Run / Start &
Display screen and then press the Param. button.
The first page of the Parameter main menu opens.
The Parameter main menu - page 1

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Buttons of the Parameter main menu display

Print button: Printing of the parameter settings displayed
Left/right arrow buttons to scroll through the five pages with all internal parameter
settings for the OptiDist™.
2. If not logged in with level 2 access, press on the dedicated field to enter the
maintenance password. The virtual keypad appears.
3. Use the right arrow button to scroll trough the pages until the sixth page
appears:
148 UM_2.00A_EN
The service screen of the Parameter main menu - page 6

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Buttons on the service screen of the Parameter main menu

Store button: Storing of the modified parameters
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The service screen of the Parameter main menu contains the following menus:
Reset calibration Left and right arrow keys allowing scrolling through the set-up
pages of OptiDist™ internal parameters
Delete all products Return to the Run / Start & Display screen
Delete all reports Removal of pre stored report profile list
Delete all operators Removal of the pre stored operator name list
Delete all standards Removal of the pre stored standard method list
Delete all compounds 850 Removal of all D850 compound list
Delete all compounds 1078 Removal of all D1078 compound list
Delete all results Removal of all results stored in the OptiDist™ memory
Delete all QC results Removal of all results stored in the Quality Control database
Reset supervisor password Removal of the supervisor password entered and replacement
by the factory set password
Reset maintenance password Removal of the maintenance password entered and replacement
by the factory set password
UM_2.00A_EN 149
The service screen of the Parameter main menu contains the following menus:
Reset unit parameters Initialization of internal parameters with factory set parameters
Up/Download mode Preparation of the OptiDist™ for the uploading of data (controlled
from the PC) and OptiDist™ software update.
Print Setup of control parameters to be transmitted to the RS 232C
serial port during a test. Code numbers from 1 to 6 are specifying
the range of the control parameters to be transmitted. For details
about the code numbers refer to the Service Manual.
150 UM_2.00A_EN
7.7 The Reports profile database

The Reports main menu allows accessing to a database stored in the OptiDist™
in which all preset reports are stored. Reports are part of the product parameters
and define data to be displayed on the screen, printed, transmitted to a LIMS and
the presentation format.
The PAC1 and PAC2 report profiles are factory set. PAC 2 and other reports can
be modified by pressing on the desired parameter field (the virtual keypad or the
virtual keyboard will automatically appear) or they can be deleted by pressing on
the Removal button.
NOTE
• To modify and create new report profiles, a level 1 access
(Supervisor) or level 2 access (Maintenance) is required.
• With level 0 access, the operator can only view the report pro-
files.
Open the Reports main menu:

Reports button.
The first page of the Reports main menu opens.
The first page of the Reports main menu
The OptiDist™ can store up to 40 report profiles displayed in a list located on the
left of the screen:
UM_2.00A_EN 151
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Buttons on the first page of the Reports main menu display

Remove button: Removal of the report profile displayed
Copy button: Creation of a new report by making a copy of the one displayed
Left/right arrow buttons to scroll through the six pages with all parameter settings
for each report.
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Display settings on the first page of the Reports main menu

Report Name: The name of the report profile (permanent field) – a maximum of 20
characters can be used.
Temp. unit: Selection of the unit of temperature readings (°C or °F).
Vapor Temp. Res.: Resolution of the temperature readings displayed (to the nearest 0,1
°C or 0,01 °C).
Press. Unit: Unit: Selection of the atmospheric pressure measurement unit dis-
played (hPa, kPa, mBar, Bar, mmHg or psi).
Barom. Corr.: Displaying of temperature readings corrected for barometric pressure.
Evap. Corr.: Displaying of percent evaporated corrected for barometric pressure.
Table format: Displaying of volumetric readings following requirements of the
desired standard test method or following the operator needs (every
1%, 5% or 10%).
Test end screen: Displaying format of the result at the end of test:
• Table: Displaying of the result under spreadsheet form
• Graphic: Displaying of the result under graphic form
• Specific limit: Displaying of comparison with specific limits set in
the product
• Method limit: Displaying of comparison wth method limits set in
the product
NOTE
From each page of the Reports main menu it is always possible to
return to the Run / Start & Display screen by pressing the Exit but-
ton.
page with further report profile settings.
152 UM_2.00A_EN
The second page of the Reports main menu

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Display settings on the second page of the Reports main menu

Rounding: Adjust the precision of nearest temperature or volume rounding.
DI Value: Driveability Index calculation
CI Value: Cetane Index calculation
Graphic Temperature Set-up of the result graphic displayed:
Axis: • Mini: Minimum temperature displayed on the graphic temperature axis
• Maxi: Maximum temperature displayed on the graphic temperature
axis
• Step: Values for the scale
UM_2.00A_EN 153
The third page of the Reports main menu

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Printer settings on the third page of the Reports main menu

Printing: • Automatic: Automatic printing of the result at the end of test.
• Manually: Printing of the result on the operator request.
Product: Printing of the product parameters with the result.
Table: Result printing under spreadsheet form.
Spec. limits: Printing of specifications set in the product.
Stand. limits: Printing of standard test method limits set in the product.
Boiling range: Printing of the difference between the IBP and the FBP (in Kelvin).
DI Value: Printing of the Driveability Index value with the result.
Driveability (or Distillation) Index (DI) is a function of distillation tempera-
tures of gasoline and the oxygen content contributed by alcohols (e.g. etha-
nol). It is expressed by the formula:
DI = (1.5*T10) + (3.0*T50) + (T90) + (33*EtOHvol%)
where T10, T50 and T90 (in degrees Celsius) are the distillation tempera-
tures where 10%, 50% and 90% of the gasoline is evaporated.
The DI is a part of CGSB (US) World Wide Fuel Gasoline specifications. By
DI, gasolines are classified in 6 classes of volatility: AA, A, B, C, D and E.
CI Value: Printing of the calculated Cetan Index value with the result.
Graphic: Result printing under graphic form.
154 UM_2.00A_EN
The fourth page of the Reports main menu

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Printer settings on the fourth page of the Reports main menu

Temp. unit: Selection of the unit of temperature readings printed (°C or °F).
Vapor Temp. Res.: Resolution of the temperature readings printed (to the nearest 0,1 °C or
0,01 °C).
Press. unit: Selection of the unit of atmospheric pressure measures printed (hPa, kPa,
mBar, Bar, mmHg or psi).
Barom. corr.: Printing of temperature readings corrected for barometric pressure.
Evap. corr.: Printing of percent evaporated corrected for barometric pressure.
Table format: Printing of the spreadsheet following requirements of the desired standard
test method (ASTM D86 only) or following the operator needs (every 1%,
5% or 10%).
Rounding: Adjust the precision of nearest temperature or volume rounding.
UM_2.00A_EN 155
The fifth page of the Reports main menu

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Settings for LIMS transfer on the fifth page of the Reports main menu
Transfer: Selection of the type of transfer to the LIMS:
• Automatic: Automatic transfer of the result at the end of test.
• Transfer of the result on request of the operator.
Protocol name: Keying of the name of the communication protocol (LIMS header).
Separator: Selection of the character dividing each group of data.
End: Selection of the character sent at each end of string:
• CR: Carriage return
• CR + LF: Carriage return + line feed
• LF + CR: Line feed then carriage return
Product: Transfer of the product parameters.
Spec. limits: Transfer of limit values set in the specification pages of the product.
Table: Sending of the spreadsheet following requirements of the desired standard
test method (ASTM D86 only or following the operator needs (every 1%,
5% or 10%).
Boiling range: Transfer of the difference between the IBP and the FBP (in Kelvin).
Stand. limits: Transfer of limit values set in the standard specification page of the product.
Dist. rate: Transfer of the distillation rate.
Heating: Transfer of the heating temperature.
Computation: Transfer of the DI, CI and TVL20 value.
156 UM_2.00A_EN
The sixth page of the Reports main menu

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Settings for LIMS transfer on the sixth page of the Reports main menu
Temp. unit: Selection of the unit of temperature readings transferred (°C or °F).
Press. Unit: Selection of the unit of atmospheric pressure measures transferred (hPa,
kPa, mBar, Bar, mmHg or psi).
Barom. corr.: Transfer of temperature readings corrected for barometric pressure.
Evap. corr.: Transfer of percent evaporated.
Table format: Transfer of volumetric readings following requirements of the desired stand-
ard test method or following the operator needs (every 1%, 5% or 10%).
Rounding: Adjust the precision of nearest vapor temperature.
UM_2.00A_EN 157
7.8 The Operator database

The operator main menu allows accessing to the operator data base where the
operator names are prestored. The OptiDist™ can store up to 50 operator profiles.
Operators can call up the list of operator names and select their names from the
prestored list during a test start procedure.
NOTE
• To add, remove or modify operator names in the list of
prestored operators, a level 1 access (Supervisor) or level 2
access (Maintenance) is required.
• With level 0 access, the operator can only view the list of
prestored operators.
7.8.1 Displaying the list of prestored Operator names
Open the Operator main menu:

1. Press the More button of the Run / Start & Display screen and then press the
Operator button.
The Operator main menu with the list of prestored operator names opens.
The Operator main menu
158 UM_2.00A_EN
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Buttons on the Operator main menu display

Remove button: Removal of the operator name selected
Add button: Addition of a new operator
Store button: Storing the new operator name
7.8.2 Add a new operator name to the list of prestored operators
1. Press the Add button to add a new operator name to the list.
2. Press on the Operator name field to display the virtual keyboard, enter the
new operator name and then press the ENTER button.
The Operator main menu - add a new name to the operator list
No Store button.
If the Store button was pressed, the new name appears on the operator list.
UM_2.00A_EN 159
The Operator main menu - new name added to the operator list
7.8.3 Remove an operator name from the list of prestored operators
1. Select the operator name to be removed from the operator list.

2. Press the Remove button.
160 UM_2.00A_EN
The Operator main menu - delete a name from the operator list
3. Validate by pressing the Yes button or quit without validating by pressing the
No button.
7.9 The Standard test methods database

The standard main menu allows accessing to a database stored in the OptiDist™,
in which all preset standard test methods are stored. The standard test methods
include settings and limit values used by products to monitor the distillation test.
Standard test methods factory set comply with international standard test
methods. With a level 1-access authorization (Supervisor), these standard test
methods can be displayed and copied for creation of a new standard.
Other standard test methods can be modified by pressing on the desired
parameter field (the virtual keypad or the virtual keyboard will automatically
appear) or they can be deleted by pressing on the Removal button.
NOTE
Should the parameters of an existing standard test method be offi-
cially modified, the software should be updated.
UM_2.00A_EN 161
NOTE
• To add, remove or modify standard test methods in the list, a
level 1 access (Supervisor) or level 2 access (Maintenance) is
required.
• With level 0 access, the operator can only view and print the list
of standard test methods.
7.9.1 List of standard test methods

The OptiDist™ can store up to 100 standard profiles.
Open the Standard main menu:

ISO Standard button.
The Standard main menu opens.
The Standard main menu - List of standard test methods
162 UM_2.00A_EN
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Buttons on the Standard main menu display

Remove button: Removal of the standard test method displayed
Copy button: Creation of a new standard test method by making a copy of the
one displayed
Print button: Printing of the parameters of the standard test method displayed
Only appears when a D1078 standard test method is selected – Access to the
list and set-up menu of D1078 compounds
Only appears when a D850 standard test method is selected – Access to the list
and setup menu of D850 compounds
/i
A standard test method consists of the following parameters

Standard: The name of the standard test method (permanent field) – a maximum
of 20 characters can be used.
Thermometer: Selection of the simulated thermometer to be used:
• 7C/7F: Temperature readings according to 7C / 7F mercury ther-
mometer
• 8C/8F: Temperature readings according to 8C / 8F mercury ther-
mometer
• ABSOLUTE C/F: Temperature readings according to a total
immersion mercury-in-glass thermometer (without emergent
stem correction)
• C-8C/8F: For future applications
• x-7C/7F: For future applications
Dist. -group: Group in which the sample falls in accordance with standard test
methods. This parameter defines limit values for concerned parame-
ters
Plate: Diameter of the base plate to be used according to the sample group
for ASTM D86 and similar
Temperatures: • Condenser: Set-up of the minimum and the maximum set point
temperature of the condenser bath (from 0 °C to 65 °C)
• Receiver: Set-up of the minimum and the maximum set point
temperature in the receiving chamber (from 0 °C to 40 °C)
Distillation rate: Set-up of the minimum and maximum uniform average rate of con-
densation between the 5% or 10% recovered to the 5 ml of liquid resi-
due in the flask in ml/min (from 2 to 10ml/min)
Timing: • IBP-time: Set-up of the minimum and maximum time between
the first application of heat and IBP (from 0 to 60 min)
• 5%-time: Set-up of the minimum and maximum time between the
IBP and the 5% recovered (for group1 and 2)
• 10%-time: Set-up of the minimum and maximum time between
the IBP and the 10% recovered (for group 0)
• FBP-time: Set-up of the minimum and maximum time between
the 5 ml of liquid residue in the flask and the FBP
UM_2.00A_EN 163

164 UM_2.00A_EN
7.9.2 List of ASDM D1078 / D850 compounds

To perform a test according to ASTM D1078 or D850 standard test methods, a
compound must be set by the Supervisor in the product parameters. This
compound is selected in the list prestored in the OptiDist™.
Compounds can be accessed through the Standard main menu when an ASTM
D1078 / D850 standard is selected.
Compounds include the constants to be applied for barometric pressure correction
and the adjustment parameters of the heating (the Optimizer cannot be used with
these standard test methods).
Compounds factory set comply with international standard test methods.
The OptiDist™ can store up to 100 compounds (50 compounds for ASTM D1078
and 50 compounds for ASTM D850) displayed in a list located on the left of the
screen:
NOTE
• To modify or remove compounds, a level 1 access (Supervisor)
or level 2 access (Maintenance) is required.
parameters of compounds.
Open the Standard main menu:

ISO Standard button.
The Standard main menu opens.
2. Select an ASTM D1078 or D850 standard test method in the list according to
the standard selected, the button D1078 or the button D850 appears at the
bottom of the screen.
3. Press the appropriate button to access to the list of D1078 compounds or to
the list of D850 compounds and the corresponding setup screens.
The appropriate list of compounds opens.
UM_2.00A_EN 165
List of ASTM D1078 compounds
List of ASTM D850 compounds
166 UM_2.00A_EN
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The setup screens of the prestored compounds lists contain the following buttons:
Removal of the compound displayed / selected
Addition of a new compound
Printing of the compound displayed / selected
Return to the Run / Start & Display screen
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A compound contains the following parameters

For D1078 compounds: • Change of boiling point
Correction = K (1013 - P)
- per mBar: rate of change of boiling point with pressure in

degree Celsius per millibar
- per mmHg: rate of change of boiling point with pressure in

degree Celsius per millimeters of mercury
For D850 compounds: The constants A and B for barometric pressure correction
Correction = [A + {B x (760 - P)}] x (760 - P)
Supported heating mode • Heater Temp.1: Temperature of the heating element during the
settings: first heating level
• Duration: Duration of the first heating level
• Heater Temp.2: Temperature of the heating element for the
second heating level

UM_2.00A_EN 167
7.10 The Calibration database
7.10.1 Introduction
The OptiDist™ measurement instrumentation requires regular verification. How
often depends on the user, but it is recommended that vapor temperature and
volume measurement system are verified at least once a year.
This section includes instructions for calibration of measurement circuits and
component parameters of your OptiDist™, which are critical to distillation
accuracy.
These circuits and parameters were calibrated prior to shipment from the factory,
but must be checked at regular intervals (see 8.1. Frequency of measurement
checks) and readjusted if necessary.
Calibration of the OptiDist™ is in great part dedicated to the supervisor and
service staff.
NOTE
• To calibrate the measurement circuits and components of the
OptiDist™, a level 1 access (Supervisor) is required.
• With level 2 access (Maintenance) the following additional
functions are available:
- the Service buttons
- the Temperature Correction Table submenu
• An Operator with level 0 access can only:
- calibrate the cursor sensivity of the touch panel
- calibrate the backlight of the screen
- view and print information which is displayed on the Cali-
bration main menu
Open the Calibration main menu:

1. Press successively the buttons More > More > Calib. in the Run / Start &
Display screen.
The Calibration menu comprises a series of sub-menus, grouped in the
following screens:
168 UM_2.00A_EN
The Calibration main menu with level 1 access (Supervisor)
The Calibration main menu with level 2 access (Maintenance)
UM_2.00A_EN 169
7.10.2 Calibration of the barometric pressure
NOTE
For the calibration of the barometric pressure sensor, a reference
barometer indicating absolute pressure values (not values cor-
rected to sea level) is required.
Only absolute values are acceptable for the barometric pressure
calibration.
1. Press the Barometric Pressure button of the Calibration main menu. The
following screen appears:
Barometric Pressure Calibration
2. Press the Modif button to unlock the setting: the Modif button turns into Save
button allowing registering modifications.
3. Select the desired pressure unit by pressing on the entry field corresponding
to Barometric Pressure Unit to scroll through the various possibilities (Pa,
hPa, kPa, mBar, Bar, HG, PSI or Torr).
4. Enter the reference barometer identity by pressing on the entry field
corresponding to Reference Barometer ID. This calls up the virtual keyboard
allowing to enter a name or a serial number.
• Press the ENTER button to validate the entry;
• or press the ESC button to abort the modification and to go back to the
previous screen.
170 UM_2.00A_EN
5. Enter the actual ambient barometric pressure by pressing on the entry field
corresponding to Reference Read. This calls up the virtual keypad allowing to
enter the barometric pressure reading from the reference barometer.
• Press the ENTER button to validate the new value;
previous screen.
6. Enter the calibration frequency of the barometric pressure sensor by pressing

on the entry field corresponding to Freq. This calls up the virtual keypad.
previous screen.
7. Configure the OptiDist™ to refuse or allow a test start when the calibration is
overdue by pressing on the entry field corresponding to Refuse test:
• Yes: the test start is refused
• No: the test can be started
8. Press the Save button to register the new settings or the Exit button to abort
and to go back to the Calibration main menu.
7.10.3 Vapor probe calibration

The vapor temperature is measured with a PT100 probe, which uses the physical
property of certain metals, wherein the resistance depends on the temperature. A
PT100 probe has a resistance of 100 ohms at 0 °C/ 32 °F. The exact resistance is
different for each device and can change over time. Therefore, it is essential to
monitor the probe deviation:
• At regular intervals
• Each time the probe is changed
The OptiDist™ corrects this deviation using the "Vapor Probe Calibration Table".
The vapor temperature probe supplied with the OptiDist™ is equipped with a built-
in memory circuit that can store up to 10 calibration points, the probe identity and
its serial number. The probe correction values are signed (+/-) and rounded to the
nearest 0,01 °C.
The OptiDist™ detects the probe at plug-in and automatically downloads these
calibration parameters into the instrument memory. This guarantees the correct
calibration values for each instrument even if the vapor temperature probe is
replaced or exchanged between different units.
NOTE
A PAC probe with memory for calibration data is required to start a
test.
The Vapor Probe menu enables the display of these values and the user can
modify them if needed.
UM_2.00A_EN 171
1. Press the Vapor Probe button of the Calibration main menu. The following
screen appears:
First screen of the Vapor Probe calibration submenu
NOTE
The Init button allows the initialization of the vapor probe table with
the factory set of correction values (correction values correspond-
ing to the first probe supplied with the OptiDist™).
172 UM_2.00A_EN
Second screen of the Vapor Probe calibration submenu
3. Select the entry field to modify the calibration frequency of the probe on the
entry field corresponding to Freq. This calls up the virtual keypad.
previous screen.
4. Configure the OptiDist™ to refuse or allow a test start when the calibration of
the probe is overdue by pressing on the entry field corresponding to Refuse:
5. To add a correction point, press on the entry field corresponding to Rt

(Reference temperature) on the left bottom of the screen. This calls up the
virtual keypad. Enter the reference temperature and then:
• press the ENTER button to validate the new value;
previous screen.
6. Then press the entry field corresponding to Mv (Measured value). This calls
up again the virtual keypad. Enter the temperature measured by the probe for
the given reference temperature.
UM_2.00A_EN 173
You get these values from the calibration certificate delivered with your probe
or from another calibration service. Press the ENTER button to validate it. The
correction is automatically transferred into the memory and displayed in the
vapor probe table.
7. To delete a correction point, press on the entry field corresponding to Item on
the right bottom of the screen. This calls up the virtual keypad. Enter the
number of the line to be deleted and then:
• press the ENTER button to validate the new value;
previous screen.
8. To choose another temperature unit and to convert the values entered in the
vapor probe table, press on the box indicating the temperature unit used
above the table (scroll selection: °C/ °F).
7.10.4 Vapor probe circuit calibration

Calibration of the vapor probe temperature measurement circuit is done through
the Vapor Probe Circuit Calibration menu. To do this, the optional available PAC
PS400 probe simulator is required (Part no.: 1000-004-001, see spare part list).
1. Press the Vapor Probe Circuit button of the Calibration main menu. The
First screen of the Vapor Probe Circuit Calibration submenu
174 UM_2.00A_EN
2. Press the Modif button to unlock the setting.
Second screen of the Vapor Probe Circuit Calibration submenu
3. To keep the present values press the Save button or continue with entering of
new values.
4. Enter the identity of the PS400 probe simulator used by pressing on the entry
field corresponding to "Probe simulator". This calls up the virtual keyboard
allowing to enter a name.
previous screen.
5. Enter the serial number of the PS400 probe simulator used by pressing on the
entry field corresponding to S/N. This calls up the virtual keypad.
previous screen.
6. Enter the calibration frequency of the vapor temperature measurement circuit

by pressing on the entry field corresponding to Freq. This calls up the virtual
keypad.
previous screen.
UM_2.00A_EN 175
7. Configure the OptiDist™ to refuse or allow a test start when the calibration is
overdue by pressing on the entry field corresponding to Refuse test:
8. Having filled these 4 fields, disconnect the vapor temperature probe on the
front of the OptiDist™ and replace it by the PS400 probe simulator as
described on the screen then press the Continue button to start the
calibration. The following screen appears:
Third screen of the Vapor Probe Circuit Calibration submenu
9. Position the rotary switch of the PS400 probe simulator on 0 °C / 32 °F

position.
10. Press on the entry field corresponding to Resistance. This calls up the virtual
keypad.
11. Enter the resistance value corresponding to this temperature position on your
PS400 probe simulator (you get these values from the Quality Control
Certificate delivered with the PS400 probe simulator).
12. Press the Next button to go to the next step.
13. Position the rotary switch of the PS400 probe simulator on the 400 °C / 752 °F
position.
14. Press again on the entry field corresponding to Resistance. This calls up the
virtual keypad.
176 UM_2.00A_EN
15. Enter the resistance value corresponding to this temperature position on your
PS400 probe simulator (you get these values from the Quality Control
Certificate delivered with the PS400 probe simulator).
16. Press the Next button to go to the next step.
7.10.5 The service button of the vapor probe circuit calibration

The Service button of the vapor probe circuit calibration submenu allows direct
entry of calibration settings into the dedicated entry fields.
NOTE
For access to the service buttons, level 2 access (Maintenance) is
required.
Display screen.
The Calibration main menu opens (see 7.10. The Calibration database).
3. On the Calibration main menu screen, press the Service button next to the
Vapor Probe circuit button.The following screen appears:
Service screen of the Vapor Probe Circuit submenu
UM_2.00A_EN 177
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Entry fields on the service screen of the Vapor Probe Circuit submenu
Freq Calibration frequency of the vapor temperature measurement circuit
Refuse test Refuse or allow a test start when the calibration frequency is overdue
Resistance Information about the resistance value corresponding to 0 °C/32 °F on the
PS400 probe simulator used for last calibration
AD Points Information about calculated AD points corresponding to 0 °C/32 °F on the
Resistance Information about the resistance value corresponding to 400 °C/752 °F on the
AD Points Information about calculated AD points corresponding to 400 °C/752 °F on the
4. Check values and modify settings if neccessary.

5. Press the Save button to save the settings or press the Exit button to cancel
the action and to return to the Calibration main menu.
7.10.6 Calibration of the volume measurement system

Calibration of the volume measurement system is done trough the Volume
Measurement Calibration menu. For the calibration, you need a clean, dry PAC
receiver cylinder and the optional available PAC volume calibration gauge (Part
no.: 5202-004-003).
The volume measurement system of the OptiDist™ is based on a height
measurement of the liquid level in a glass cylinder with precise inner diameter.
180 mm in height correspond to 100 volume %.
With the PAC volume calibration gauge we calibrate the height at 5 and 94
volume %.
For the automatic calibration, the PAC receiver cylinder with the gauge inside has
to be installed in the receiver chamber of the unit and the user has just to follow
the instructions on the screen.
NOTE
Use only standard OptiDist™ PAC receiver cylinders. If it is not the
case, the OptiDist™ does not detect the receiver cylinder and the
alarm “No receiver detected” is triggered.
1. Press the Volume measurement button of the Calibration main menu. The first
screen of the Volume Measurement Calibration submenu appears.
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First screen of the Volume Measurement Calibration submenu
2. Press the Modif button to unlock the setting.
Second screen of the Volume Measurement Calibration menu
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3. To keep the present values press the Save button or continue with entering of
new values.
4. Enter the identity of the gauge used: press on the entry field corresponding to
Receiver, this calls up the virtual keyboard allowing keying a name or a
number.
previous screen.
5. Enter the serial number of the gauge used: press on the entry field
corresponding to S/N, this calls up the virtual keypad.
previous screen.
6. Enter or modify the calibration/verification frequency of the Volume

Measurement System by pressing on the entry field corresponding to Freq,
this calls up the virtual keypad.
previous screen.
7. Configure the OptiDist™ to refuse or allow a test start when the calibration/
verification is overdue by pressing on the entry field corresponding to Refuse
test:
8. Press the Continue button to perform the volume calibration or the Exit button
to abort and to go back to the Calibration main menu.
9. If you press the Continue button, the next screen of the Volume Measurement
Calibration menu appears:
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Third screen of the Volume Measurement Calibration submenu
10. As explained in the display, place a standard OptiDist™ PAC receiver cylinder
containing the volume calibration gauge in the receiving chamber.
NOTE
The slots of the volume calibration gauge need to show to the rear
of the receiving chamber.
11. Close the receiving chamber door, then press the Continue button.
12. If you press the Continue button, the next screen of the Volume Measurement
Calibration menu appears and the OptiDist™ is now calibrating the volume
measurement system by scanning the volume calibration gauge:
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Fourth screen of the Volume Measurement Calibration submenu
13. As soon as the calibration is completed, the next screen appears:
Fifth screen of the Volume Measurement Calibration submenu
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7.10.7 The service button of the volume measurement calibration

The Service button of the volume measurement calibration submenue allows
direct entry of calibration settings into the dedicated entry fields.
NOTE
required.
Display screen.
Volume measurement button.
Service screen of the Volume measurement submenu
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/i
Entry fields on the service screen of the Volume measurement submenu

Freq: Calibration frequency of the volume measurement system
Refuse test: Refuse or allow a test start when the calibration frequency is overdue
Steps at 94% Digital coded steps for the step motor of the level follower:
• E: Excentric value at 94 % volume
• C: Centric value at 94 % volume
These values are factory calibrated with the PAC volume calibration
gauge and written down in the factory test certificate prior to shipment.
Steps at 5% Digital coded steps for the step motor of the level follower:
• E: Excentric value at 5 % volume
• C: Centric value at 5 % volume
These values are factory calibrated with the PAC volume calibration
gauge and written down in the factory test certificate prior to shipment.

7.10.8 Temperature correction table

The Electronic Circuit Correction Table allows linearization of the temperature
measurement system.
The Temperature Correction Table submenu enables the display of these values
and the modification if needed.
NOTE
For access to the temperature correction table, level 2 access
(Maintenance) is required.
Display screen.
3. On the Calibration main menu screen, press the Tmp Correction Table button.
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First screen of the Temperature Correction Table submenu
Second screen of the Temperature Correction Table submenu
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NOTE
Pushing the Save button will update the calibration date, even if
nothing was changed.
NOTE
The Init button allows the initialization of the temperature correction
table with the factory set of correction values.
5. Press the Init button in order to delete all values in the Temperature Correction
Table.
6. After the values in the Temperature Correction Table are deleted, press the
Save button to save the changes.
7. Press the Exit button to go back to the Calibration main menu, then press
again the Exit button to go back to the Run / Start & Display screen.
8. Press successively the buttons More > More > Diag. on the Run / Start &
Display screen to open the Diagnostic main menu (see 8.2. Displaying current
readings).
9. Disconnect the vapor temperature probe on the front of the OptiDist™ and
replace it by the PS400 probe simulator.
10. Set the rotary switch of the PS400 probe simulator to the 50 °C (122 °F)
position.
11. Check the measured temperature value displayed next to Vapor Tmp (first
box on top left of the Diagnostic screen).
12. Wait a few seconds until the temperature reading has stabilized and write
down the measured temperature value displayed next to Vapor Tmp.
13. Then set the rotary switch of the PS400 probe simulator successively to the
positions 100 °C (212 °F), 200 °C (392 °F), 300 °C (572 °F) and 400 °C (752
°F) and write down the displayed corresponding measured temperature value
for each of the rotary switch positions.
14. Press the Exit button of the Diagnostic screen to go back to the Run / Start &
Display screen.
Display screen to return to the Calibration main menu.
16. Press the Tmp Correction Table button and then press the Modif button to
unlock the setting: the Modif button turns into Save button allowing registering
modifications.
17. Enter or modify the name of the temperature correction table by pressing on
the entry field corresponding to Table Name. This calls up the virtual keyboard
allowing keying a name or a number.
186 UM_2.00A_EN

previous screen.
18. To add a correction, press on the entry field corresponding to Rt (Reference

temperature) under Add a Correction on the left bottom of the screen. This
calls up the virtual keypad.
19. Enter the reference temperature. You get these values from the Quality
Control Certificate delivered with the PS400 probe simulator (listed under
column “Temp. simulated”).
previous screen.
20. Then press on the entry field corresponding to Mv (Measured value). This
calls up again the virtual keypad.
21. Enter the previously written down temperature values measured by the unit
for the given reference temperature.
• Press the ENTER button to validate the entry (the correction is
automatically transferred in internal parameters of the OptiDist™ and
displayed in the Temperature Correction Table);
previous screen.
22. Repeat the above steps until all values in lines 1 to 5 of the Temperature
Correction Table are entered: reference temperature values (Rt) and
corresponding measured values (Mv) according to the PS400 probe simulator
rotary switch positions: 50 °C (122 °F), 100 °C (212 °F), 200 °C (392 °F), 300
°C (572 °F) and 400 °C (752 °F).
23. To delete a correction, press on the entry field corresponding to Item under
Delete a Correction on the right bottom of the screen. This calls up the virtual
keypad. Enter the number of the line to be deleted and then:
• press the ENTER button to validate the entry;
previous screen.
24. To choose another temperature unit and to convert the values entered in the
unit correction table, press on the box indicating the unit used above the table
(scroll selection: °C / °F).
25. After all values are correctly entered, press the Save button to save the
settings or press the Exit button to cancel the action and to return to the
Calibration main menu.
Checking of the modified values:

1. Exit the Calibration main menu and go back to the Run / Start & Display
screen.
UM_2.00A_EN 187
Display screen to open the Diagnostic main menu (see 8.2. Displaying current
readings).
3. Make sure that the PS400 probe simulator is still connected.
4. Set the rotary switch of the PS400 probe simulator to the 50 °C (122 °F)
position.
5. Wait a few seconds until the temperature reading has stabilized and check the
measured temperature value displayed next to Vapor Tmp (first box on top left
of the Diagnostic screen).
NOTE
In comparison with the stated temperature values in the Quality
Control Certificate (delivered with the PS400 probe simulator), the
deviation of the corresponding measured temperature values must
be less than 0,2 °C (0.36 °F).
6. Then set the rotary switch of the PS400 probe simulator successively to the
positions 100 °C (212 °F), 200 °C (392 °F), 300 °C (572 °F) and 400 °C (752
°F) and check the corresponding measured temperature value for each of the
rotary switch positions.
7. If one of the measured temperature values is out of the allowable tolerance,
repeat the calibration of the temperature correction table.
8. To go back to the Run / Start & Display screen, press the Exit button of the
Diagnostic screen.
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7.10.9 Calibration of the heater temperature
NOTE
For the calibration of the measurement circuit of the heating ele-
ment temperature a reference thermometer is required.
CAUTION
The flask heater temperature must be calibrated when not ener-
gized.
1. Press the Heater Temperature button of the Calibration main menu. The
Heater Temperature Calibration menu
3. Select the temperature unit by pressing on the entry field corresponding to
Temperature Unit to scroll through the various possibilities (scroll selection: °C
or °F).
4. Enter the reference thermometer identity by pressing on the entry field
corresponding to Reference Thermometer ID. This calls up the virtual
keyboard allowing to enter a name or a number.
UM_2.00A_EN 189

previous screen.
5. Position the bulb of the reference thermometer in the center of the heating
element next to the temperature measurement thermocouple.
6. Once the temperature reading on the reference thermometer is stable, enter it
by pressing on the entry field corresponding to Reference Read. This calls up
the virtual keypad allowing keying the heating element temperature read on
the reference thermometer.
previous screen.
7. Press the Save button to register the settings or the Exit button to abort and to
go back to the Calibration main menu.
7.10.10 The service button of the heater temperature calibration

The Service button of the heater temperature calibration submenue allows direct
entry of calibration settings into the dedicated entry fields.
NOTE
required.
Display screen.
Heater Temperature button.
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Service screen of the Heater Temperature Calibration submenu

/i
Entry fields on the service screen of the Heater Temperature Calibration submenu
Reference Tmp: Entry field for the reference temperature measured by a reference thermome-
ter. The bulb of the reference thermometer must be placed in the center of the
heating element next to the temperature measurement thermocouple.
Correction: Correction of the temperature will be calculated automatically.
4. Check values and modify settings if neccessary..

7.10.11 Calibration of the optimizer
Calibration of the optimizer is performed by distilling two pure compounds (only

accessible at the Supervisor level):
• Distillation of Toluene or ISO-Octane for the calibration at low temperature
with the prestored product “OPTIMIZER CAL 1”.
• Then distillation of Hexadecane for the calibration at high temperature with the
prestored product "OPTIMIZER CAL 2".
UM_2.00A_EN 191
CAUTION
Use pure Toluene or ISO-Octane and pure Hexadecane
(purity > 95% minimum).
NOTE
The optimizer calibration is not performed from the Calibration
main menu.
If you activate the optimizer menu, a screen appears indicating that
the optimizer calibration is done by distilling two pure samples and
these distillations must be started from the Run / Start & Display
screen.
1. Press the Exit button to go back to the Calibration main menu then press
again the Exit button to go back to the Run / Start & Display screen.
2. Prepare a sample of Toluene and then prepare the OptiDist™.
3. Press the New Test button then parameterize the test: select the product
OPTIMIZER CAL 1 for the distillation of the Toluene or ISO-Octane sample.
NOTE
When the OPTIMIZER CAL product is validated, the Start button
turns into Calibration button indicating the following distillation is a
calibration run.
4. Insert the sample and the receiver cylinder then press the Calibration button
to start the distillation run.
When the test is completed, calibration parameters of the optimizer are

automatically updated.
5. Follow the same procedure for the optimizer calibration at high temperature
with the Hexadecane.
7.10.12 The service button of the optimizer calibration

The Service button of the optimizer calibration submenue allows direct entry of
calibration settings into the dedicated entry fields.
NOTE
required.
Display screen.
192 UM_2.00A_EN
Optimizer button.
Service screen of the Optimizer Calibration submenu

/i
Entry fields on the service screen of the Optimizer Calibration submenu

Product used: • Calibration 1: The min./max. temperature values for Isooctane are factory
Isooctane calibrated and written down in the factory test certificate prior to shipment.
• New Temp: Entry field for a new temperature measured during a calibration
test run.
• K: The min/max K values are calculated automatically.
• KCoeff: The min./max KCoeff values are factory calibrated and written down
in the factory test certificate prior to shipment.
Product used: • Calibration 2: The min./max. temperature values for Hexadecane are factory
Hexadecane calibrated and written down in the factory test certificate prior to shipment.
• New Temp: Entry field for a new temperature measured during a calibration
test run.
• K: The min/max K values are calculated automatically.
• KCoeff: The min./max KCoeff values are factory calibrated and written down
in the factory test certificate prior to shipment.

UM_2.00A_EN 193
7.10.13 Calibration of the touch screen
7.10.13.1 Adjustment of the touch panel

The touch panel is factory adjusted but in case of problems the cursor sensivity
area can be adjusted according to the position of buttons on the screen.
1. Press the Touch Panel button of the Calibration main menu.
The Touch Panel adjustment screen opens.
Three yellow spots will appear successively on the screen.
Touch panel adjustment screen

2. Follow the instructions on the screen:
• To adjust the cursor, press on each yellow spot until it becomes green (for
a better precision, use a sharp opject to press on the center of the spots)
• To cancel the calibration and to go back to the Calibration main menu,
press on the text window
7.10.13.2 Adjustment of the screen backlight

The brightness of the screen backlight can change according to the ambient
temperature and may need to be adjusted.
1. Press the BackLight button of the Calibration main menu.

The Backlight submenu opens:
194 UM_2.00A_EN
Backlight adjustment screen
2. To adjust the brightness of the screen:

• Press the Plus button to increase the brightness.
• Press the Minus button to decrease the brightness.
UM_2.00A_EN 195
7.10.14 Refuse the test start
The laboratory supervisor has the possibility to configure the calibration frequency
of the following measurement circuits and devices:
• The vapor temperature measurement circuit:
• The vapor temperature probe correction values
• The receiving chamber volume measurement circuit
It is possible to configure the OptiDist™ to deny a test start if the date set for the
calibration is passed if the customer’s Quality Assurance Program requires it.
For this, indicate a calibration date in the corresponding calibration menu and set
the field Refus (test refusal) on Yes.
7.10.15 Calibration ticket printing

The calibration ticket includes the date of all calibrations with the corresponding
conversion counts, the calibration frequencies required and if the test is denied
when date set for calibration is passed.
1. Press the Print button in the Calibration main menu.
196 UM_2.00A_EN
7.11 Diagnostic functions
The Diagnostic main menu is in great part dedicated to the OptiDist™ service and
maintenance. With this menu, it is possible to:
• Display current readings
• In Diagnostic mode: Control the main parts of the analyzer to check for their
proper operation.
NOTE
• The diagnostic functions of the OptiDist™ are mainly dedicated
to service and maintenance staff. Using of the dignostic func-
tions needs having a level 2 access (Maintenance).
• With level 0 access, the operator can only view the current
readings on the Diagnostic main menu screen.
Open the Diagnostic main menu:
Display screen.
The Diagnostic main menu opens.
The Diagnostic main menu
UM_2.00A_EN 197
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Buttons on the Diagnostic main menu screen:

EXIT Return to the Run / Start & Display screen
Measure - The active mode is the “Measure mode”. In Measure mode, the measurement-
Command parameter screen allows checking all current readings and the corresponding
Analog / Digital conversion counts.
This enables the ability to quickly check for abnormal data, which may be due to
a faulty sensor or a faulty electrical component.
Pressing the Measure button activates the “diagnostic mode”. The Measure but-
ton turns into Command button indicating, that the main parts of the OptiDist™
can be controlled.
Activation of the “diagnostic mode” needs having a level 2 access (Maintenance).
/i
The Diagnostic main menu screen gives access to the following information:
The flask heater assembly • Vapor Tmp:
(first box on top left) Temperature given by the vapor temperature probe with the
resistance value of the temperature probe (Res:) and the corre-
sponding conversion count (A/D)
• Optimizer:
Value given by the Optimizer and the corresponding conversion
count (A/D)
• Dry Point:
Temperature given by the thermocouple (if connected)
• Heating Tmp:
Temperature of the heating element with the corresponding con-
version count (A/D)
The volume measurement • Volume:
(second box on center left) Volume measured with the level follower optical fork
• Follower Back:
Conversion counts of the reception light signal of the level fol-
lower 1
• Follower Central:
lower 2
Ambient conditions • Bar. Pressure:
(third box on bottom left) Volume measured with the level follower optical fork
• Ambient Tmp:
lower 1
The condenser bath • Condenser:
(first box on top right) Temperature given by the condenser bath temperature probe
The receiving chamber • Receiver:
(second box on center right) Temperature given by the receiving chamber temperature probe
The cooling system • Exchanger:
(third box on bottom right) Temperature of the heat exchanging liquid in the cooling circuit

198 UM_2.00A_EN
7.12 The About main menu

The About main menu gives access to information about firmware version, serial
numbers of electronic boards and the MMI (Man Machine Interface).
Open the About main menu:

1. Press successively the buttons More > More > About on the Run / Start &
Display screen.
The About main menu opens.
Screen of the About main menu

/i
Buttons on the Standard main menu display

Print button: Printing of the detailed report of firmware and hardware versions of
the OptiDist™.
Copyright Access to copyright information
/i
Information provided on the About main menu screen:

Serial No.: The serial no. of the OptiDist™
Firmware Revision The unit firmware revision
Boot V The boot firmware revision
UM_2.00A_EN 199
Information provided on the About main menu screen:

FPGA revision The FPGA version (version of the logic system of the integrated circuit)
MAC Address Medium Access Control: Identifying address of the network interface
CPU Board The part number of the Control Processing Unit board, revision and date
Test bench ID The name of the test bench used to test the CPU board and the version
Control Board The part number of the control board and the version
MMI Interface Board The part number of the MMI interface board and the version
Heating Control Board The part number of the heating control board and the version

200 UM_2.00A_EN
7.13 Backup and Restore

The content of the OptiDist™ internal memory can be saved on an USB memory
stick and restored agein later, such as:
• Internal parameters
• Calibration values
• Distillation products
• Test results
• or all of the above
NOTE
• To restore data and to update the firmware on the OptiDist™
needs having a level 1 access (Supervisor) or level 2 access
(Maintenance).
• The operator can perform a Backup only, which needs having a
level 0 access (Operator).
Open the Backup and Restore main menu:

1. Press successively the buttons More > More > Backup on the Run / Start &
Display screen.
The Backup and Restore menu opens.
Screen of the Backup and Restore main menu
UM_2.00A_EN 201
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Elements on the Backup and Restore main menu display

Firmware • Firmware revision no. used on the OptiDist™
• Firmware revision no. saved on the USB memory stick
Backup All, Parameters, Calibrations, Products, Results (ASCII)
Restore All, Parameters, Calibrations, Products
Upload Firmware Upload Firmware button; only active with level 1 access (Supervisor) or level 2
access (Maintenance)
Backup button
Restore button; only active with level 1 access (Supervisor) or level 2 access
(Maintenance)
Exit button, return to Run / Start & Display screen
1. Insert the USB memory stick into the USB A port on the right side of the
OptiDist™ or into the USB A port at the rear.
2. Select the data to be saved or restored from the pull down list in the Backup
field or from the pull down list in the Restore field.
Backup and Restore main menu - pull down list
3. Press the Backup button to perform a backup or the Restore button to restore
data from the USB memory stick to the internal memory of the OptiDist™.
202 UM_2.00A_EN
4. After the data transfer is completed,

a. either remove the USB stick to return to the Run / Start & Display screen,
b. or press the Exit button to return to the Run / Start & Display screen.
NOTE
According to the data transferred, the OptiDist™ might need to be
switched off for the new data to be taken into account. If it is
needed, it will be indicated in the status bar. The OptiDist™ takeoff
is automatically done when the USB stick is removed.
7.14 Firmware update
NOTE
To update the firmware on the OptiDist™ needs having a level 1
access (Supervisor) or level 2 access (Maintenance).
1. Insert the USB memory stick into the USB A port on the right side of the
OptiDist™ or into the USB A port at the rear.
NOTE
The USB stick is not considered as a valid, if it does not contain all
files needed. In this case an alarm message appears.
2. In the Backup and Restore main menu press the Upload Firmware button to
start the transfer of the new firmware to the internal memory of the OptiDist™.
3. After the data transfer is completed,
a. either remove the USB stick to return to the Run / Start & Display screen,
b. or press the Exit button to return to the Run / Start & Display screen.
NOTE
According to the data transferred, the OptiDist™ might need to be
switched off for the new data to be taken into account. If it is
needed, it will be indicated in the status bar. The OptiDist™ takeoff
is automatically done when the USB stick is removed.
UM_2.00A_EN 203
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Diagnostic functions OptiDist™
8 Diagnostic functions
UM_2.00A_EN 205
OptiDist™ Diagnostic functions
This section includes instructions for measurement checks and testing procedures
of the instrument’s major parts using diagnostic functions and the Doctor Box.
NOTE
The diagnostic functions are mainly dedicated to service and main-
tenance of the OptiDist™. It requires having a level 2-access
authorization (maintenance).
8.1 Frequency of measurement checks

Before starting your first test run or periodically thereafter, check the volume and
temperature measurements. Measurement checks are part of routine
maintenance. The minimum checks to perform are in particular, the volume and
the vapor temperature measurement.
It is best that the measurement checks should be performed by the operator. In
this way, the operator will better understand the operation of the OptiDist™ and
will be more apt to notice any anomalies as regards the measurement circuits.
The following checks can be done:
• Barometric pressure measurement

• Vapor temperature measurement
• Heater temperature measurement
• Condenser bath temperature measurement
• Receiving chamber temperature measurement
• Volume measured in the receiver
The OptiDist™ distillation analyzer needs to be verified at intervals of not more

than six months or after one of the elements of a measuring circuit has been
replaced or repaired but the ideal time interval for the frequency of controls is to be
determined by the user according to the OptiDist™ environment, its frequency
of use and the customer’s Quality Assurance Program.
The conditions listed below increase the frequency of measurement checks:

• Ambient temperature above 25 °C (77 °F).
• The number of distillation unit operators.
• Dirty or dusty ambient air.
• The distillation unit is operated during multiple shifts each day.
Having completed these operations (calibrations if necessary), you can have

confidence in your OptiDist™ readings. You will also have acquired a solid
working knowledge of the OptiDist™ and the self-confidence to start your first test.
206 UM_2.00A_EN
NOTE
For the corresponding calibarations of these circuits refer to section
7.10. The Calibration database.
8.2 Displaying current readings
The Diagnostic main menu is in great part dedicated to the OptiDist™ service and
maintenance. With this menu, it is possible to:
• Display current readings
• In Diagnostic mode: Control the main parts of the analyzer to check for their
proper operation, see chapter 8.4. Various individual component diagnostic
functions.
To display all current readings, activate the Diagnostic main menu:

Display screen.
The measurement-parameters screen appears thus:
The Diagnostic main menu – Current readings
UM_2.00A_EN 207
/i
Buttons on the Diagnostic main menu screen:

EXIT Return to the Run / Start & Display screen
Measure - The active mode is the “Measure mode”. In Measure mode, the measurement-
Command parameter screen allows checking all current readings and the corresponding
Analog / Digital conversion counts.
This enables the ability to quickly check for abnormal data, which may be due to
a faulty sensor or a faulty electrical component.
Pressing the Measure button activates the “diagnostic mode”. The Measure but-
ton turns into Command button indicating, that the main parts of the OptiDist™
can be controlled, see 8.4.1. Activate the diagnostic mode.
Activation of the “diagnostic mode” needs having a level 2 access (Maintenance).
/i
The Diagnostic main menu screen gives access to the following information:
The flask heater assembly • Vapor Tmp:
(first box on top left) Temperature given by the vapor temperature probe with the
resistance value of the temperature probe (Res:) and the corre-
sponding conversion count (A/D)
• Optimizer:
Value given by the Optimizer and the corresponding conversion
count (A/D)
• Dry Point:
Temperature given by the thermocouple (if connected)
• Heating Tmp:
Temperature of the heating element with the corresponding con-
version count (A/D)
The volume measurement • Volume:
(second box on center left) Volume measured with the level follower optical fork
• Follower Back:
lower 1
• Follower Central:
lower 2
Ambient conditions • Bar. Pressure:
(third box on bottom left) Volume measured with the level follower optical fork
• Ambient Tmp:
lower 1
The condenser bath • Condenser:
(first box on top right) Temperature given by the condenser bath temperature probe
The receiving chamber • Receiver:
(second box on center right) Temperature given by the receiving chamber temperature probe
The cooling system • Exchanger:
(third box on bottom right) Temperature of the heat exchanging liquid in the cooling circuit
208 UM_2.00A_EN
8.3 Measurement checking procedures
8.3.1 Barometric pressure measurement

To check the barometric pressure measurement the operator needs a reference
barometer indicating absolute values (not values corrected to sea level).
Only absolute values are acceptable for the atmospheric pressure calibration.
1. Activate the Diagnostic main menu to display the measurement-parameters
screen.
2. Check that the reading opposite "Bar. Pressure" in the display, verifying that it
is the same as that on the reference barometer reading.
If the deviation is greater than ±3 mbar carry out the calibration of the atmospheric
pressure measurement.
If there is an abnormal reading displayed, the atmospheric pressure sensor may
be disconnected or faulty. Call for a qualified technician.
8.3.2 Vapor temperature measurement circuit

To check the vapor temperature measurement circuit, the operator needs the PAC
PS400 probe simulator (Part no.: 1000-004-001, available as optional accessory
in the spare part list).
1. Activate the Diagnostic main menu to display the measurement parameter
screen.
2. Disconnect the vapor temperature probe on the front of the OptiDist™.
3. Replace it by the PS400 probe simulator.
4. Set the rotary switch of the PS400 probe simulator on 0 °C (32 °F) position.
5. Once the temperature reading has stabilized, check that the reading in front of
"Vapor Tmp" is 0 °C (32 °F).
6. Then position the PS400 probe simulator rotary switch on 400 °C (752 °F).
7. Once the temperature reading has stabilized, check that the reading in front of
"Vapor Tmp" is 400 °C (752 °F).
If the OptiDist™ does not indicate the expected value, calibrate the vapor
temperature measurement circuit, see 7.10.4. Vapor probe circuit calibration.
UM_2.00A_EN 209
8.3.3 Heating element temperature measurement

To carry out a quick check on the heating element temperature measurement, use
a reference thermometer.
CAUTION
The heating element temperature must be checked when the heat-
ing block is at ambient temperature, either before a test or at least
ten minutes after the end of a test and the heater must not be ener-
gized.
1. Activate the Diagnostic main menu to

display the measurement parameters
screen. A
2. Position the bulb of the reference
thermometer in the center of the heating
element next to the temperature
measurement thermocouple (A).
3. Once the temperature reading in front of
"Heating Tmp" has stabilized, check it is
the same as the temperature indicated
by the reference thermometer.
If calibration is necessary, see 7.10.9.

Calibration of the heater temperature for the calibration procedure of the
heating element temperature measurement circuit.
8.3.4 Condenser bath temperature measurement

To carry out a quick check on the condenser bath temperature probe
measurement, use a control thermometer (e.g.: the vapor temperature probe,
having reconnected it on the front of the OptiDist™).
screen..
2. Pour a little heat exchanging liquid into the temperature check well, provided
for the verification of the condenser bath temperature on the top of the
OptiDist™.
3. Place the vapor temperature probe in the check well.
4. Wait until the "Vapor Tmp": and the "Condenser" temperature readings have
stabilized. These two readings should be the same ± 0.5 °C.
If the two readings are not the same, the temperature probe of the condenser bath
can be faulty or disconnected. Call for a qualified technician.
210 UM_2.00A_EN
8.3.5 Receiving chamber temperature measurement

To carry out a quick check on the receiving chamber temperature probe
measurement, use a control thermometer.
screen.
2. Place a thermometer in the receiving chamber with the bulb halfway up the
compartment.
3. Wait until the “Receiver” temperature and the thermometer readings have
stabilized. These two readings should be the same ± 0.5 °C.
If the two temperatures are not identical, the receiving chamber temperature
probe can be faulty or disconnected. Call for a qualified technician.
8.3.6 Volume measurement of the receiver cylinder

To carry out a quick check on the volume measurement, use the command 4 of
the diagnostic commands of the level follower motor, see 8.4.3. Diagnostic of the
volume measurement.
UM_2.00A_EN 211
8.4 Various individual component diagnostic functions
The Diagnostic main menu is in great part dedicated to mainenance of the

OptiDist™. With this menu, it is possible to:
• Display measures in real time
• Control the main parts of the OptiDist™ to check their good operation
NOTE
Be aware that an OptiDist™ that is running a test cannot carry out
any diagnostics and an OptiDist™ in diagnostic mode cannot start
a test.
8.4.1 Activate the diagnostic mode
Display screen.
The diagnostic main menu opens.
Diagnostic main menu – Current Readings
2. Press the Measure button in the right bottom of the screen to activate the
diagnostic mode.
212 UM_2.00A_EN
NOTE
The diagnostic function is mainly dedicated to service and mainte-
nance of the OptiDist™. It requires having a level 2-access author-
ization (maintenance).
If entry to a protected level is attempted, a warning message is dis-
played, indicating the current level and the access level requested.
3. Press on the password entry field to display the virtual keyboard and enter the
maintenance password.
The Measure button turns into Command button indicating the OptiDist™ is in
diagnostic mode. From now on, each part can be controlled separately.
Diagnostic main menu – Diagnostic mode
Diagnostics can be performed on all power-consuming devices:

• The flask heater assembly :
- lift (descent motion of the heating block)
- fan
- heating element
• The volume measurement :
- up-and-down cycles
- volume measurement
- level follower detector (back and central)
UM_2.00A_EN 213
• The condenser bath circuit

- solenoid valve
- heater
- boost heater (if present)
• The receiving chamber and receiving chamber circuit :
- heater
- pump
- fan
- VOC pump
- drop detection optical fork
• The cooling system:
- The cooling unit
Commands remain active until they are disabled and as long as the OptiDist™ is
in diagnostic mode.
4. To disable the diagnostic mode, press the Command button or press the Exit
button and confirm that you want to quit the diagnostic mode.
NOTE
When a problem is identified on a specific element, its supply cir-
cuit can be quickly tested with the optional Doctor Box, see 8.5.
Connection and use of the “Doctor Box”.
8.4.2 Diagnostic of the distillation flask heating block

Commands for heating block elements are located in the top left box of the
diagnostic screen, see 8.4.1. Activate the diagnostic mode.
1. Activate the diagnostic mode.
8.4.2.1 Down solenoid of the flask heating block

1. Lower the heating block positioning lever: the heating block comes in contact
with the distillation flask bottom (high or run position).
2. Press on the Lift button to release the heating block to the low position
The platform of the heating block should lower. If not, a faulty component or a
faulty connection in the command circuit is likely: the down solenoid valve
activating the electromagnet at the rear of the heating block to release it in low
position or its supply circuit is failing.
3. Check the supply circuit of the heating block down solenoid using the Doctor
Box or call for a qualified technician to check the supply circuit and the down
solenoid operation.
214 UM_2.00A_EN
8.4.2.2 Cooling fan of the flask heating block

1. Press on the Fan button to start the cooling fan of the heating block.
You should hear the heating block fan starting up and the heating element
temperature indicated opposite Heating Tmp should decrease. If not, this fan
or its supply circuit is failing.
2. Check the supply circuit of the fan using the Doctor Box or call for a qualified
technician to check the supply circuit and fan operation.
3. To stop the command, press on the Fan button again or press on the
Command button to quit the diagnostic mode.
8.4.2.3 Flask heating element

1. Press on one of the two entry fields opposite the Heater command and enter
either the temperature desired in degree Celsius or the power to be applied to
the heating element in percent.
The heating element temperature indicated opposite Heating Tmp should rise
after a few seconds. If not, the heating element or its supply circuit is failing.
2. Check the supply circuit of the heating element using the Doctor Box or call for
a qualified technician to check the supply circuit and heating element
operation.
3. Press again on the entry field modified and stop the heating command or
press on the Command button to quit the diagnostic mode.
8.4.3 Diagnostic of the volume measurement

Commands for the volume measurement elements are located in the middle left
box of the diagnostic screen, see 8.4.1. Activate the diagnostic mode.
8.4.3.1 Level follower motor

1. Press on the entry field opposite the Motor command and enter a number
from 1 to 4:
/i
0 Stop the level follower

1 Ascent of the level follower up to its standby position
2 Descent of the level follower up to its zero position (at the bottom of the receiving chamber)
3 Up-and-down cycles
4 Volume measurement
You should observe:

• The level follower detector starts its movement
• The Volume reading and corresponding Steps change progressively from
the values at activation.
UM_2.00A_EN 215
2. If the level follower does not move, call for a qualified technician to check:
• the condition of the drive belt
• the motor operation
• the motor supply circuit
3. Press on the Command button to quit the diagnostic mode and for the level
follower detector returns to its standby position.
8.4.3.2 Optical detectors for volume measurement (level follower fork)

1. Remove the receiver cylinder from the receiving chamber.
2. Press on the entry field opposite Transm (transmitter) of the Follower Back or
of the Follower Central and enter the maximum number of points which are
commanding the transmitter (see table below).
/i
Conversion counts on the optical receptors according conversion count of the optical trans-
mitter:
Conversion count on the transmitter Conversion count on the receptor
0 points > 4000 points (provided the OptiDist™ is away
from direct sunlight)
4095 points (maximum) < 1500 points
3. Press again on the entry field and stop the transmitter.

4. If the conversion count of the receptor is out of the boundary, first clean the
optical detector concerned (back or central).
5. Restart the test. If the problem persists, call for a qualified technician to
replace the level follower optical fork.
8.4.4 Diagnostic of the condenser bath circuit

Commands for condenser bath elements are located in the top right box of the
diagnostic screen, see 8.4.1. Activate the diagnostic mode.
8.4.4.1 Condenser heating

1. Press on the entry field opposite Heater and enter the heating power desired
in percent.
NOTE
Power on the pump to flow the heat exchanging liquid in the con-
denser bath (see 8.4.4.4. Condenser bath pump). Thus, the raising
of temperature of the condenser bath will be more rapid and homo-
geneous.
216 UM_2.00A_EN
The condenser bath temperature indicated just above should begin to rise
after few seconds. If not, the condenser heating element or its supply circuit is
failing.
2. Check the supply circuit of the condenser heating element using the Doctor
Box or call for a qualified technician to check the supply circuit and heating
element operation.
8.4.4.2 Cooling solenoid valve

1. Press on the entry field opposite SV and enter the cooling power desired in
percent (for example: 80%).
NOTE
denser bath (see 8.4.4.4. Condenser bath pump). Thus, the drop
(assuming the exchanger temperature is < 0 °C) of temperature of
the condenser bath will be more rapid and homogeneous.
The condenser bath temperature indicated just above should begin to

decrease after a few seconds. If not, the condenser solenoid valve or its
supply circuit is failing.
2. Check the supply circuit of the solenoid valve using the Doctor Box or call for
a qualified technician to check the supply circuit and solenoid valve operation.
3. Press again on the entry field modified and stop the solenoid valve command
or press on the Command button to quit the diagnostic mode.
8.4.4.3 Optional condenser boost heating
NOTE
Note: This command is only available if the optional condenser
boost heating is installed.
1. Press on the entry field opposite Boost and enter the additional heating power
desired in percent.
NOTE
denser bath (see 8.4.4.4. Condenser bath pump). Thus, the raising
of temperature of the condenser bath will be more rapid and homo-
geneous.
The condenser bath temperature indicated just above should begin to rise
after a few seconds. If not, the optional condenser boost heating element or its
UM_2.00A_EN 217
2. Check the supply circuit of the boost heating element using the Doctor Box or
call for a qualified technician to check the supply circuit and boost heating
element operation.
3. Press again on the entry field modified and stop the boost heating command
or press on the Command button to quit the diagnostic mode.
8.4.4.4 Condenser bath pump

1. Press on the entry field opposite Pump to start the condenser bath pump.
The condenser pump allows the heat exchanging liquid flowing in the
condenser bath. If this pump is not powered on during heating or cooling of
the condenser bath, the temperature will not be homogeneous and the
temperature indicated opposite Condenser will not evolve in linear way.
2. Check the supply circuit of the condenser bath pump using the Doctor Box or
call for a qualified technician to check the supply circuit and the condenser
bath pump operation.
3. Press again on the entry field to stop the pump command or press on the
8.4.5 Diagnostic of the receiving chamber

Commands for receiving chamber elements are located in the middle right box of
the diagnostic screen, see 8.4.1. Activate the diagnostic mode.
8.4.5.1 Receiving chamber heating

1. Press on the entry field opposite Heater.
2. Enter the heating power desired in percent.
NOTE
To detect an immediate raising of temperature in the receiving
chamber, power on the fan (see 8.4.5.3. Receiving chamber fan).
The receiving chamber temperature indicated just above should begin to rise
after few seconds. If not, the heating element or its supply circuit is failing.
3. Check the supply circuit of the heating element of the receiving chamber using
the Doctor Box or call for a qualified technician to check the supply circuit and
heating element operation.
218 UM_2.00A_EN
8.4.5.2 Receiving chamber cooling pump

1. Press on the entry field opposite Pump and enter the cooling power desired in
percent.
NOTE
To detect an immediate drop of temperature (assuming the
exchanger temperature is < 0 °C) in the receiving chamber, power
on the fan, see 8.4.5.3. Receiving chamber fan.
The receiving chamber temperature indicated just above should begin to

decrease after few seconds. If not, the pump or its supply circuit is failing.
2. Check the supply circuit of the receiving chamber pump using the Doctor Box
or call for a qualified technician to check the supply circuit and receiving
chamber pump operation.
3. Press again on the entry field modified and stop the pump command or press
on the Command button to quit the diagnostic mode.
8.4.5.3 Receiving chamber fan

1. Press on the Fan button to start the receiving chamber fan.
NOTE
The receiving chamber fan allows the air flowing in the receiving
chamber during heating or cooling. If this fan is not powered on, the
temperature of the receiving chamber will not be homogeneous
and the temperature indicated opposite Receiver will not evolve in
linear way.
2. Check the supply circuit of the receiving chamber fan using the Doctor Box or
call for a qualified technician to check the supply circuit and the fan operation.
3. To stop the command, press on the Fan button again or press on the
UM_2.00A_EN 219
8.4.5.4 VOC pump (optional)
NOTE
Note: This command is only available if the VOC control option is
installed.
1. Press on the VOC pump button to start the extraction pump of the volatile
organic components.
The VOC Pump should start up: disconnect the exhaust pipe at the rear of the
OptiDist™, to check the air in the receiving chamber is being moved at a rapid
rate. If not, the VOC pump or its supply circuit is failing.
2. Check the supply circuit of the VOC pump using the Doctor Box or call for a
qualified technician to check the supply circuit and the VOC pump operation.
3. To stop the command, press on the VOC pump button again or press on the
8.4.5.5 Drop detection optical fork

1. Remove the receiver from the receiving chamber.
2. Press on the entry field opposite Transm: (transmitter) of the Drop detector
and enter the maximum number of points to command the transmitter of the
drop detection optical fork (see table below).
/i
Conversion counts on the optical receptors according conversion count of the optical trans-
mitter:
Conversion count on the transmitter Conversion count on the receptor
0 points > 4000 points (provided the OptiDist™ is away
from direct sunlight)
4095 points (maximum) < 1500 points
3. Pass an object, e.g. a pencil, between the emitter and the receiver of the first
drop optical detector. The indicator lamp opposite the entry field Transm:
should light.
4. Press again on the entry field and stop the transmitter.
5. If the conversion count of the receptor is out of the boundary, first clean the
drop detection optical fork.
6. Restart the test. If the problem persists, call for a qualified technician to
replace the drop detection optical fork.
220 UM_2.00A_EN
8.4.6 Diagnostic of the cooling unit: the exchanger
1. Activate the diagnostic mode (see 8.4.1. Activate the diagnostic mode).
2. Press on the CoolSyst button to start the cooling unit of the OptiDist™
(provided the OptiDist™ has been switched on for 2 min)
You should hear the cooling unit starting up and the temperature of the
exchanger of the cooling system should decrease. If not, the cooling unit or its
3. Check the supply circuit of the cooling unit using the Doctor Box or call for a
qualified technician to check the supply circuit and cooling unit operation.
4. Press on the CoolSyst button again to stop the command or press on the
8.4.7 End of diagnostic
1. After terminating diagnostics, press again the Command button.
NOTE
If the Command button is not pressed, the OptiDist™ remains in
diagnostic mode, all regulations are switched off and a test run can-
not be started.
2. Press the Exit button and confirm that you want to quit the diagnostic mode
and to return to the Run / Start & Display screen.
8.5 Connection and use of the “Doctor Box”
8.5.1 Introduction
The optional available Doctor Box allows rapid diagnostics of the OptiDist™
components and electronic boards without need for OptiDist™ disassembly.
The Doctor Box connects to the 25-pin connector on the right side of the
OptiDist™.
A F
F F1 F2 30A
U BIP 24V FLASK HT
S VOLTMETER
E F3 F4 F5 F6 OUTPUT
S 24V
12V 12V
5V
T
R
5V 3.3V
A RED COND. HT BOOST HT REC . FAN LED
F
F
I 3.3V
C COOL . UNITT COOL . SV
ORANGE
L ADA DOCTOR BOX
I
G DOWN SOL. COND. REC.
H
T
GREEN
FLASK FAN REC . HT VOC PUMP
B C D E
The Doctor Box
UM_2.00A_EN 221
When the Doctor Box is connected, it supplies information on the operation of the
following components (when they are energized):
• The fuses (A)
• The status indicator beacon (B)
• The heating elements (C, D, E)
• The fans (C, E)
• The cooling unit (C)
• The pumps (E)
• The heating block solenoid (C)
• The cooling unit solenoid valve (C)
Moreover the Doctor Box allows:

• Checking voltages (F)
• Measuring voltages (F)
8.5.2 Checking of the operation of supply circuits

OptiDist™ components are controlled by electronic boards. Each supply circuit is
protected by a fuse. In case of failure, with the Doctor Box it is easy for the
operator to know if the problem comes from the supply circuit controlling elements
or from the fuse protecting the concerned supply circuit (and thus from one
element).
Moreover, it is easy to check the supply voltage of the electronic board concerned.
8.5.2.1 Checking the fuses

1. Connect the Doctor Box to the 25-pin connector on the right side of the
OptiDist™.
Fuses are located on the electronic boards. If fuses are operable, the LED
corresponding to each fuse in box (A) of the figure above should light up
(except fuse F1).
NOTE
If installed, the optional built-in printer should be activated to check
the fuse F1.
A lighted LED indicates an open or failed fuse. Thus, it is easy to identify

which fuse has failed.
222 UM_2.00A_EN
/i
Fuses Location Supply Function

circuit
concerned
F1 Control Board Protects the built-in printer 24V supply circuit
F2 Control Board Protects the 24V supply circuit
F3 Control Board B Protects the supply circuit of the status indicator
beacon
F4 Control board C Protects the supply circuit of the following ele-
ments:
• Condenser heating element
• Cooling unit
• Down Solenoid: control of the heating

block position to the bottom
• Distillation flask fan

F5 Control board D Protects the supply circuit of the additional heating
cartridge of the condenser tube included in the
optional boost heating function
F6 Control board E Protects the supply circuit of the following ele-
ments:
• Receiver fan
• Cooling solenoid valve (cooling of the

condenser tube)
• Condenser pump
• Receiver pump
• Receiver heating element
• VOC pump
30A Heating control Protects the supply circuit of the distillation flask
FLASK HT board heating element
If one fuse is failing, call for a qualified technician to verify the various elements
controlled by the concerned circuit (see table above) before replacing it with a fuse
of the specified type and current ratings.
WARNING
Switch off the OptiDist™ and disconnect it from the mains before
removing the housing.
If the service operations, to be carried out by a qualified technician,
require you to switch on the OptiDist™, switch it off again before
disconnecting or removing any electrically powered components.
UM_2.00A_EN 223
8.5.2.2 Rapid diagnostic

OptiDist™.
2. First, confirm that the fuse protecting the supply circuit of the concerned
element has not failed (see table above).
3. Using the diagnostic mode, control the element to be checked: The LED
corresponding to the concerned supply circuit should light up (for modulated
control, the LED blinks according to the control duration).
NOTE
The Doctor Box checks the powered output of electronic boards.
Consequently, the LED corresponding to the supply circuit of a con-
trolled part lights up even if the part is failing.
If a LED does not light up and the fuse corresponding to the concerned supply
circuit is ok, the concerned electronic component(s) on board is(are) failing. The
electronic board has to be replaced.
8.5.3 Checking and measuring voltages
8.5.3.1 Checking voltages

OptiDist™.
2. Position the commutator switch to the “LED” position.
If all fuses are operational and one LED does not light up, the corresponding
power supply has failed and needs to be replaced.
NOTE
These checked voltages are generated by the control electronic
board.
8.5.3.2 Measuring voltages

OptiDist™.
2. Connect a voltmeter to the connector on the front side of the Doctor Box.
3. Position the commutator switch to each voltage position to measure the actual
values with the voltmeter.
224 UM_2.00A_EN
Maintenance OptiDist™
9 Maintenance
UM_2.00A_EN 225
OptiDist™ Maintenance
9.1 Reminder on frequency of measurement checks and

calibration
The OptiDist™ distillation analyzer needs to be verified at intervals of not more
than six months or after one of the elements of a measuring circuit has been
replaced or repaired but the ideal time interval for the frequency of measurement
checks is to be determined by the user according to the OptiDist™ environment,
its frequency of use and the customer’s Quality Assurance Program, see 8.1.
Frequency of measurement checks.
9.2 Routine maintenance

Maintenance checks should be performed regularly. Generally speaking, the
frequency depends on the tested products. The ideal time interval for the
frequency of controls and preventive maintenance on the OptiDist™ listed below
is to be determined by the user according to the OptiDist™ environment, its
frequency of use and the customer’s Quality Assurance Program. The optimal
time intervals of maintenance and check come from experience.
The conditions listed below may involve closer time intervals:

• Ambient temperature above 25 °C (77 °F).
• The number of distillation unit operators.
• Dirty or dusty ambient air.
• The distillation unit is operated during multiple shifts each day.
It is best that the maintenance checks and operations explained in this manual
should be performed by the operator. In this way, the operator will better
understand the operation of the OptiDist™ and will be more apt to notice any
anomalies as regards the measurement circuits.
Here is a list of checks and recurring maintenance operations:

/i
Timing Action
Daily Check the state of the distillation flask
Check the state of the vapor tube
Check the state of the condenser tube - distillation flask silicone tube
Check the state of the stopper seals
Check the state of the stopper tip
Check the state of the receiver rubber cap
Weekly Execute the measurement checks
Carry out a cleaning destillation:
Depending on the nature of the material being distilled and on the frequency of
distillations, a cleaning distillation should be performed at regular intervals (e.g.
weekly or monthly) to remove wax crystals that deposit in the condenser tube.
This is best done with a mixture of 50% toluene and 50% methanol/ethanol
226 UM_2.00A_EN
Timing Action
Once a year Calibrate the measurement circuits and elements
Control the working condition of the flame extinguisher device
Control the heating element coil
Clean all vent holes and protection bars of the extinguisher injection slopes
Clean the condenser of the cooling unit
Control of heat exchanging liquid coolant level in the cooling system
As required Replace the printer paper (see the printer manual).
Replace the printer ink ribbon (see the printer manual)
Replace the condenser tube
Replace the distillation flask silicone tube
Replace the receiver rubber cap
Replace the stopper seals
Replace the stopper tip
Drain the receiving chamber spillage trap
UM_2.00A_EN 227
9.3 Disassembling/Reassembling of the OptiDist™ housing
9.3.1 Disassemble/Reassemble the housing of the distillation flask heater

assembly
WARNING
removing a housing.
If the service operations (carried out by a qualified technician)
1. Disconnect the vapor temperature probe from the OptiDist™.

2. Remove the distillation flask stopper and its holder.
3. Remove the base plate installed.
4. Grip the housing between both hands and lift up to remove it.
5. Proceed in reverse order to reassemble the housing of the distillation flask
heater assembly.
WARNING
Replace the housing cover before switching on the OptiDist™.
Ascertain that the distillation flask heater assembly housing is prop-
erly seated: Openings provided for the fire sensors and the opti-
mizer must face the sensors).
9.3.2 Disassembe/Reassemble the main housing of the OptiDist™
WARNING
removing a housing.
1. Remove the 2 screws (A) on the top of the OptiDist™ main housing.
2. Remove the 3 screws (A) on the left hand side of the OptiDist™ main housing.
3. Remove the left part (B) of the OptiDist™ main housing by pulling it to the rear
and then to the left.
4. Remove the 3 screws (A) on the right hand side of the OptiDist™ housing.
5. Remove the right part (C) of the OptiDist™ main housing by pulling it to the
rear and then to the right.
228 UM_2.00A_EN
A C
B
A
A
Disassembling/Reassembling the main housing of the OptiDist™
6. Proceed in reverse order to reassemble the main housing of the OptiDist™.
9.4 Check and replace wear and tear parts
9.4.1 Check the coils of the heating element
WARNING
1. To control the heating element coil, remove the distillation flask heater
assembly housing.
2. Control, that the coils of the heating element do not touch each other to avoid
a hot spot.
3. If the coils touch each other, separate the coils with a flat-bladed screwdriver.
If this is not sufficient, replace the heating element.
4. Reassemble the base plate and the distillation flask heater assembly housing.
UM_2.00A_EN 229
9.4.2 Replace the heating element
WARNING
1. To replace the heating element, remove

the distillation flask heater assembly
E
housing.
D
2. Loosen the 4 screws (A).
C
3. Loosen the 4 screws (B) (accessible from C D
the left).
4. Pull the heating element (E) upward to
remove it.
B
5. Install the new heating element: A
a. Insert completely the connection lugs
in the ceramic tubes (D) provided for this.
b. Tighten the 4 screws (A).
c. Check that the coils do not touch each other.
d. Check that the heating element (E) leans on the four ceramic tubes (C)
positioned under the heating element.
e. Tighten the 4 screws (B).
6. Proceed in the reverse order to reassemble the distillation flask heater
assembly housing.
7. Calibrate the optimizer following the procedure explained in the calibration
section, see 7.10.11. Calibration of the optimizer.
9.4.3 Check and replace the condenser/distillation flask silicone tube

The silicone tube (A) fixed at the entrance
opening of the condenser tube ensures an
easily installed and secure connection
between the distillation flask vapor tube and
condenser. After a time (depending on the
A
products tested), this silicone tube can
become discolored and less pliable and do
not ensure any more the tightness between
the distillation flask vapor tube and the
condenser tube.
If this tightness is no longer ensured,
dangerous vapors escape from the
condensate recovery area. The condenser/
distillation flask silicone tube can be replaced
rapidly (see list of spare parts).
230 UM_2.00A_EN
CAUTION
Wear protective cloves if you have to cut off the distillation flask sili-
cone tube to avoid all cut and burn hazards .
1. Pull-off the condenser/distillation flask silicone tube (A) carefully or cut it off
with caution if it is stuck to the condenser tube.
2. Attach a new condenser/distillation flask silicone tube to the condenser tube.
9.4.4 Check and replace the receiver cylinder rubber cap

To reduce evaporation loss of the distillate
while it flows down the wall of the receiver,
the receiver cylinder is covered with a rubber
cap (A). This rubber cap is slipped on the
lower end of the condenser tube. It A
automatically goes down onto the top of the
receiver when the cylinder is inserted. After a
certain time (depending on the products
tested), this rubber cap can become
discolored and less pliable and does not
ensure its function any more. It can be easily
replaced (see list of spare parts).
CAUTION
When replacing the rubber cap, wear protective gloves to avoid all
cut and burn hazards .
1. Pull-off the the rubber cap (A) carefully to slide it over the drip tip.
2. Attach a new rubber cap to the condenser tube.
9.4.5 Check and replace the stopper seals

After a few months of use with certain sample
types, the seals of the stopper (A) ensuring
tightness between the stopper and the
distillation flask neck can become dark and
less pliable.
Just as for the silicone tube, if this tightness is A
no longer ensured, dangerous vapors can
escape from the condensate recovery area.
These stopper seals (A) can be easily B
replaced (see list of spare parts):
1. Remove the stopper tip (B) just by pulling
on the tip.
2. Replace the stopper seals (A) and push back the stopper tip (B) in its position.
UM_2.00A_EN 231
9.4.6 Check and replace the stopper tip

After a few months of use with certain sample types, the plastic part of the stopper
tip inserted in the distillation flask neck can be slightly distorted (see previous
section). This tip can affect the vapor temperature probe positioning and thus
results.
This part can be easily replaced (see list of spare parts): .
1. Remove the stopper tip (B) just by pulling on the tip.
2. Replace the stopper seals too, see 9.4.5. Check and replace the stopper
seals.
3. Push the new stopper tip in its position.
9.4.7 Replace the vapor temperature probe

If you have to replace the vapor temperature probe, unplug the old probe and
replace it with a new one. Adjust the position of the new probe through the stopper
assembly using the stopper assembly holder: read the vapor temperature probe
adjustment procedure, 4.3.9. Vapor temperature probe or 5.9.2. Adjustment of the
vapor probe in the dry point stopper.
NOTE
The distillation flask stopper assembly is specially designed for the
precise adjustment of the probe positioning in the stopper and so,
in the distillation flask.
The vapor temperature probe is equipped with a built-in memory circuit including
up to 10 correction values, the probe identity and its serial number. Thus, no
adjustment is necessary: the OptiDist™ automatically recognizes the probe and
imports data at plug-in avoiding manual entry of probe correction values and
probe ID.
NOTE
PAC probe is required. If another probe is used, a new test will not
be able to start.
To display these correction values and adjust the calibration frequency of the
vapor temperature probe, see 7.10.3. Vapor probe calibration.
To order a new probe, please see spare part list for the item (the probe, wiring and
connector cannot be dismantled).
9.4.8 Replace the dry point thermocouple

If the thermocouple is found to be faulty, replacement does not pose any particular
problem as the connector is on the front of the OptiDist™, see 4.1.1. Front view
left.
232 UM_2.00A_EN
9.5 Drain the receiving chamber spillage trap

If some liquid was spilled into the receiving chamber, it will be recovered into a
liquid spillage trap protecting instrument components from damage. This trap is
located under the receiver stand.
The liquid spillage trap must be regularly checked and emptied, especially if the
OptiDist™ needs to be transported.
WARNING
Take care of hot or acid liquids!
To drain the spillage trap:

1. Press the door latch to open the receiving chamber door.
2. Pull on the spillage trap to extract it.
3. Empty the spillage trap and put it back in place.
9.6 Servicing the cooling system
9.6.1 Check the coolant level - filling

The heat exchanging liquid (coolant) level of the cooling system may have to be
serviced about once a year.
The level sensor in the coolant filling reservoir located in the OptiDist™ behind the
distillation flask heater assembly will trigger the failure alarm “Low cooling liquid
level” if the coolant level in the reservoir is too low.
NOTE
The heat exchanging liquid must be ordered at PAC (see the spare
part list). It is important to use coolant provided by PAC for correct
operation of your OptiDist™, as its properties are particularly com-
patible with the application.
CAUTION
removing a housing.
UM_2.00A_EN 233
1. Switch off the OptiDist™ and disconnect

B
it from the mains.
2. Remove the left housing cover of the
OptiDist™.
3. Remove the stopper from the reservoir
(A) located on the top of the OptiDist™
behind the heating block.
4. Remove the stoppers from the two
draining tubes (B) located to the left of
the coolant reservoir.
A
5. Use a funnel to complete the coolant

level of the cooling system circuit up to
the level mark (A) inside the reservoir.
Do not lift up the funnel during filling. A
Fill the reservoir slowly so as to avoid
back-up due to trapped air.
Wait for a few minutes at the end to
make sure that all the air bubbles are
expelled.
6. Remove the funnel and replace the
stoppers of the reservoir and the
draining tubes.
7. Reassemble the housing cover of the
OptiDist™ .
8. Switch on the OptiDist™ and wait for a few minutes to allow the coolant to
circulate in the closed circuits. At this stage, if you hear a noise from the
pumps, caused by the circulation of air pockets, wait for more time, the air
pockets will be eliminated but the coolant level may have to be completed
again.
9. Check the coolant level in the reservoir and complete it again if it is necessary.
234 UM_2.00A_EN
9.6.2 Clean the condenser of the cooling unit
NOTE
To obtain accurate and repeatable results, prepare the samples
and OptiDist™ with particular care as described in the following
sections.
CAUTION
removing a housing.
1. Switch off the OptiDist™.

2. Remove the left housing cover of the
OptiDist™.
3. Clean the condenser (A) of the cooling
unit using a vacuum cleaner.
A
9.7 Testing the fire extinguisher solenoid valve and flame

detector
9.7.1 Frequency of tests

The time interval between each test depends on the OptiDist™ environment and
its frequency of use. The experience of the operator and the personnel charged
with servicing of the equipment will help to determine an optimal time interval.
This test should, in any case, be scheduled at short time intervals, the detector
has not however been designed for prolonged and repeated tests. This will only
result in the reduction of the efficiency of the detector.
9.7.2 Test procedure
1. Shut off the external gas supply and disconnect it from the fire extinguisher
gas inlet at the rear of the OptiDist™.
2. Approach a naked flame (e.g. a cigarette lighter flame) to the vicinity of the
flame detector, located on the right side of the distillation flask heater
assembly.
UM_2.00A_EN 235
The solenoid valve makes a “clicking” sound when it is opened.

The flame detection alarm should be triggered and the power consuming
devices switch to safety mode power supply cut-off.
3. Activate the Messages main menu of the Run / Start & Display screen and the
following failure alarm will appear: Fire.
4. Switch off the unit to acquit the alarm.
NOTE
The flame detection audio alarm remains active until the OptiDist™
is switched off, even if the fault has been acquitted and the flame
has been extinguished.
CAUTION
If a real fire detection and extinction operation is performed, should
it be after an accident or during testing by setting fire to a sample in
the distillation flask compartment, then the test described in this
section should be used to verify that the flame detector works cor-
rectly.
When a real fire has been extinguished, it is strongly advised to
open windows in order to air the laboratory (extinction gas being
CO2).
9.8 Connection of an external fire alarm device

It is possible to connect an external fire alarm device onto the OptiDist™ (the user
must provide the power supply for his alarm device).
The series contact provided for the connection of the user’s external alarm device
functions as an ON/OFF switch for the user’s device: this series contact has 2
connection positions such that when a fire is detected:
• 1-2 normally closed
• 2-3 normally opened
Characteristics: Contact ratings 230V AC 3A - 110V DC 3A
NOTE
To stop the alarm, the OptiDist™ must be switched off
CAUTION
Caution! Switch off the OptiDist™ and disconnect it from the mains
before removing the housing.
236 UM_2.00A_EN
1. To connect an external fire alarm device,

remove the main housing cover of the
OptiDist™.
2. Connect the external fire alarm device on
the J4 connector (B) on the fire safety
board (A):
The fire safety board (A) is located on the
A
left side of the OptiDist™ when you are
facing the OptiDist™:
3. Locate the grommet (D) above the power

supply (mains) cable at the rear of the
OptiDist™.
D
4. Pass the wiring of the external fire alarm
device through this opening (D).
5. Connect the wiring to the J4 connector of the fire safety board (connection
made by screw).
J1 J5
J4 connector
J6
NO Com NC
J2
J3 Fire Safety Board
J4
6. Reassemble the main housing cover of the OptiDist™.
UM_2.00A_EN 237
238 UM_2.00A_EN
Alarm treatment OptiDist™
10 Alarm treatment
UM_2.00A_EN 239
OptiDist™ Alarm treatment
10.1 Alarm processing

Certain alarm cases present a danger. This is why certain failures switch the
analyzer into idle status, for example the pump feed is cut out and the heating is
stopped
However, this is not to say that this type of apparatus is hazard-free or that if the
analyzer fails to go into idle status the operator and/or analyzer are not in danger.
It is important always to verify what is going on whenever an alarm is triggered.
CAUTION
Generally when the alarm buzzer is triggered, the operator must
display the cause and ensure that everything is working correctly.
For example, owing to a faulty component an alarm that normally should place the
OptiDist™ in idle mode fails to do so. In that case, the operator must switch off the
OptiDist™.
10.2 Alarm displaying and stopping

When a default occurs, a red box appears indicating the alarm code and
message:
1. Press the OK button to acquit the alarm and stop the buzzer.
2. Check causes of alarm setting of: see 10.4. List of alarm messages and
troubleshooting.
10.3 Alarm review

The OptiDist™ can register up to 48 different alarm messages. These alarm
messages can be displayed in the alarm review screen, see 7.4. The Messages
database.
1. Activate the Messages main manu of the Run / Start & Display Screen.
The alarm review is displayed with the list of alarms eventually occurred.
240 UM_2.00A_EN
10.4 List of alarm messages and troubleshooting

/i
Code Alarm message Causes Actions

0 “Fire” Fire detected in the distillation • Deactivate the alarm:
flask heating area. switch off and switch on the
• Fire automatically extin- OptiDist™.
guished if CO2 gas is sup- • If the distillation flask
plied to the unit. broke, clean the sample
• Stops a test in progress heating area.
and prevent from starting a • Clean CO2 injections slots
new test and optimizer opening.
1 “Power On Test One of the power on current test • Switch off then switch the
Failure” performed and displayed at the OptiDist™ on again to dis-
OptiDist™ switching on fails: play the checklist of ele-
• Lift coil ment supply circuits.
• Distillation flask fan • Check the element impli-
• Receiver fan cated in diagnostic mode
• VOC or using the Doctor Box.
• Receiver pump
• Condenser pump
• Condenser solenoid valve
• Receiver heater
• Boost heater
• Condenser heater
2 "AD7794 ADC Analog/Digital conversion fault • Switch off then switch on
Error" • Stop the test and prevent the OptiDist™ to reinitialize
from starting a new test the memory.
• If the problem persists,
download the firmware
using the specific PAC soft-
ware supplied.
• If the problem persists, call
for a qualified technician to
replace the CPU Board
3 "Program flash Stop the test and prevent from • Switch off then switch on
memory" starting a new test the OptiDist™ to reinitialize
• Stop the test and prevent the memory.
from starting a new test If the problem persists,
download the firmware
using the specific PAC soft-
ware supplied.
replace the CPU Board.
UM_2.00A_EN 241

4 "Data flash mem- Non volatile memory corrupted • Download the OptiDist™
ory" (only tested at switching on) factory internal parameters
• Prevent from starting a from a PC using the spe-
new test cific PAC software sup-
plied.
• Then perform all calibra-
tions.
for a qualified technlcian to
5 “RAM” Memory corrupted (only tested • Switch off then switch on
at switching on). the OptiDist™ to initialize
• Prevent from starting a the RAM memory.
new test. • If the problem persists, call
6 "Heater power" Heater power above the given • In run: verify OptiDist™
security limits: application limits are com-
In run: P>70% patible with the product
In diagnostic mode: P>100 tested (20°C (68 °F) to 400
°C (752 °F).
7 "Heater in standby'' Increasing of the sample tem- • Switch off then switch on
perature more than 1°C/s in idle the OptiDist™.
mode. • If the problem persists, use
the Doctor Box to check
the heating element sup-
ply circuit and voltages in
diagnostic mode or call for
a qualified technician to
check the operation of the
heating element and
replace it if needed.
8 "Low temperature Temperature of the heating ele- • Check the heating element
when heating" ment is <150 °C whereas the operation in diagnostic
command is >30% during 60s mode.
• Stop a test in progress and • Using the Doctor Box,
prevent from starting a new check the heating element
test power supply circuit and
voltages in diagnostic
mode or call for a qualified
technician to check the
operation of the heating
element and replace it if
needed.
9 "Heater tempera- Temperature of the heating ele- • Wait till the heating ele-
ture" ment is out of the given security ment gets cold and check
limits: its operation in diagnostic
< -50 °C or > 1000 °C during 5 mode.
sec • Restart the test
242 UM_2.00A_EN

10 "Low cooling liquid Liquid level in the cooling sys- Fill the reservoir of the cooling
level" tem under the minimum level system.
• Stop all temperature regu-
lations
• Stop a test in progress and
prevent from starting a new
test
11 "Vapor temperature" Vapor temperature is out the • Verify the vapor tempera-
given security limits: Vapor T°<- ture probe is correctly con-
50 °C (58 °F) or vapor T°> 420 nected to the OptiDist™
°C (788 °F) during 10s and inserted in the distilla-
• Stop heating tion flask..
• Stop a test in progress and • Verify OptiDist™ applica-
prevent from starting a new tion limits are compatible
test with the product tested (20
°C (68 °F) to 400 °C (752
°F)).
• Verify the vapor tempera-
ture measurement and per-
form the calibration if
needed.
• Verify the probe correction
table has not been modi-
fied (compare with the
probe test certificate).
• If calibrations are correct,
evaluate the reason of
abnormal vapor tempera-
ture readings or verify the
operation of the vapor tem-
perature measurement
thermocouple by distillation
of a pure product if need
be.
• Replace the probe if
needed.
12 "Optimizer" Values out of the given security • Verify OptiDist™ applica-
limits tion limits are compatible
with the product tested (20
°C (68 °F) to 400 °C (752
°F).
• Calibrate the optimizer.
13 "Optimizer internal Temperature of the optimizer is Verify the ambient temperature
value”" out of the security limits: <1 °C is compatible with the operating
or >80 °C for greater than 10s temperatures of the OptiDist™.
UM_2.00A_EN 243

14 "Condenser temper- Temperature of the condenser • Verify the temperature
ature" bath is out of the security lim- measurement of the con-
its:< -20 °C or > 8 °C during 5s denser bath.
• Stop the temperature regu- • Using the Doctor Box and
lation of the condenser the diagnostic mode or
bath calling for a qualified tech-
• Stop a test in progress and nician, check the power
prevent from starting a new supply circuit and voltages
test of following elements: the
cooling unit, the cooling
unit solenoid valve, the
condenser heater, the
boost heater (if installed),
the condenser pump.
• Call for a qualified techni-
cian to check the operation
of these elements and
replace the one failinq if
needed.
15 “Condenser regula- Temperature setpoint of the con- • Verify the temperature
tion" denser bath can not be reached measurement of the con-
denser bath.
• Using the Doctor Box and
the diagnostic mode or
calling for a qualified tech-
nician, check the power
supply circuit and voltages
of following elements: the
condenser heater, the
boost heater (if installed),
the condenser pump.
replace the one failinq if
needed.
244 UM_2.00A_EN

16 "Receiver tempera- Temperature of the receiving • If the problem persists, use
ture" chamber is out the security lim- the Doctor Box to check
its: <-5 °C or >45 °C during 5s the heating element sup-
• Stop the temperature regu- ply circuit and voltages in
lation of the receiving diagnostic mode or call for
chamber a qualified technician to
• Stop a test in progress and check the operation of the
prevent from starting a new heating element and
test replace it if needed.
receiver heater, the
receiver pump.
replace the one failing if
needed.
17 "Receiver regula- Temperature setpoint of the • Verify the temperature
tion" receiving chamber can not be measurement of the receiv-
reached ing chamber.
receiver heater, the
receiver pump.
replace the one failing if
needed.
UM_2.00A_EN 245

18 "Exchanger temper- Temperature of the exchanger is • Using the Doctor Box and
ature" > 6 °C during 5min for the the diagnostic mode or
15 min following the OptiDist™ calling for a qualified tech-
switching on and after, the tem- nician, check the power
perature <40 °C or >40 °C supply circuit and voltages
• Stop the temperature regu- (see of the cooling unit and
lation of the receiving the cooling unit solenoid
chamber and condenser valve.
bath • Call for a qualified techni-
• Stop a test in progress and cian to check the operation
prevent from starting a new of these elements and
test replace the one failing if
needed.
19 "Exchanger regula- Temperature setpoint of the • Switch off then switch on
tion" exchanger can not be reached the OptiDist™.
• If the problem persists, use
the Doctor Box to check
the heating element sup-
ply circuit and voltages in
diagnostic mode or call for
a qualified technician to
check the operation of the
heating element and
replace it if needed.
20 "Drop light barrier' Conversion counts of the emitter • Clean the drop detection
light signal of the drop barrier is optical fork.
out the limits: <100 pts or > • In diagnostic mode, test
3500 pts the drop detection.
21 "Drops per volume" Number of drops per volume is • Perform a volume calibra-
<10 drops/ ml during 30s (failure tion.
detected from the IBP to 5 ml
residue) In diagnostic mode:
1st case: The volume does not • Check the drop detection
increase while drops are operation.
detected • Check the level follower
2nd case: The volume increases motor operation.
while drops are not all detected • Test the operation of the
level follower optical fork .
22 "Follower1 light bar- After automatic adjustment at • Clean the back optical
rier' test starting, counts of the back transmitter and receptor of
emitter light signal of the level the level follower optical
follower optical fork are out of fork.
the limits: <100 or 3500 pts • In diagnostic mode, test
• Stop a test in progress and the back optical detector of
prevent from startinq a new the level follower optical
test fork (. There is only one fol-
lower fork.
246 UM_2.00A_EN

23 "Follower2 light bar- After automatic adjustment at • Clean the central optical
rier' test starting, conversion counts transmitter and receptor of
of the central emitter light signal the level follower optical
of the level follower optical fork fork.
are out of the limits: <100 or > • In diagnostic mode, test
3500 pts the central optical detector
• Stop a test in progress and of the level follower optical
prevent from starting a new fork.
test
24 "Follower" Blocking of the level follower • Call for a qualified techni-
• Stop a test in progress and cian to check the level fol-
prevent from startinq a new lower operation.
test
25 "Dry point sensor' Temperature measured out of • Check the thermocouple
the security limits: <-40 °C or connection on the front of
>1000 °C the OptiDist™.
• Stop a test in progress and • Check that the thermocou-
prevent from starting a new ple is not damaged.
test • Replace it if needed.
26 "lnitial boiling point" The test starts for a certain time • Verify OptiDist™ applica-
and the IBP has not been found tion limits are compatible
(time is different or each stand- with the product tested.
ard method) • Repeat the test watching
the distillation progress to
detect unusual events.
for a qualified technician.
27 "Program error" Verification of the product
parameters before test starting
28 “Door open for 2 The door was opened for more • Close the door.
min. during test” than 2min during a run • Repeat the test to be sure
• Do not stop a test in the result is not affected.
progress
29 "Door" The door was opened for more • Close the door.
than 5s during a test run or for • Repeat the test to be sure
more than 2min in idle mode the result is not affected.
• Do not stop a test in
progress
30 "Distillation rate" The distillation rate is out the • Repeat the test watching
limits: <25% or > 15O% of the the distillation progress to
setpoint for at least 60s detect unusual events.
• Do not stop a test in
progress
31 “Ambient Tempera- The ambient temperature is out • Check the probe position-
ture” of the given limits: <-50 °C or ing.
>100 °C • If the problem persists,
replace the ambient tem-
perature probe by a new
one.
UM_2.00A_EN 247

32 "Barometric pres- The atmospheric pressure is out • Verify ambient conditions
sure" of the given limits: <73,3 kPa or around the OptiDist™ (con-
>106.7 kPa stant pressure).
• Proceed with the baromet-
ric pressure calibration
replace the Control Board.
33 "Check the heating During the distillation run the • Check the base plate
block position" base plate switches are tested, switches operation.
if no base plate is detected the
test is stopped with the mes-
sage above. The switches are
sampled each 5 ms and 8 read-
ings must be stable to take into
account the switch value. The
switch value can be checked in
the diagnostic screen.
34 "Receiver seems At the beginning of the distilla- Empty the receiver in the distil-
not to be empty, tion, the level follower goes lation flask and restart the test.
Check it" down and the volume is meas-
ured, when the reading is stable
it is checked and if it is >3% the
run is cancelled with the mes-
sage above. The heating is not
started until his first measure-
ment is done.
35 "Calibration is The next calibration date for the • Check the calibration fre-
needed to start a volume or the temperature quency recommended for
test" measurement is over but the the vapor temperature
test starting is not denied. measurement system and
In these conditions, the result the vapor temperature
could not be reliable. probe
• Check the calibration fre-
quency recommended for
the volume measurement
system
• Perform automatic calibra-
tion needed
• Repeat the test
248 UM_2.00A_EN

36 "Calibration is out of The next calibration date for the • Check the calibration fre-
date" volume or the temperature quency recommended for
measurement is over and the the vapor temperature
test starting is denied in this measurement system and
case. the vapor temperature
In these conditions, the result probe
could not be reliable. • Check the calibration fre-
quency recommended for
the volume measurement
system
• Perform automatic calibra-
tion needed
• Repeat the test
37 “Optimizer calibra- Optimizer calibration is not cor- Calibrate the optimizer
tion error” rect • Distillation of a pure sam-
ple of Isooctane or Toluene
for the calibration at low
temperature
• Then distillation of a pure
sample of Hexadecane for
the calibration at high tem-
perature
38 “Vapor probe mem- The vapor probe offset read or Call for a qualified technician.
ory Error” write failed.
39 “Max heating temp. Max. heating temperature is Adjust set-point temperature
reached” reached during a distillation run parameter setting
40 “Max heating temp. Max. heating temperature is Adjust set-point temperature
reached during fin. reached at the end of a distilla- parameter setting
heating” tion run
41 “Condenser temper- Set-point temperature regulation • Check parameter settings
ature error” of the condenser failed • Call for a qualified techni-
cian.
42 “Receiver tempera- Set-point temperature regulation • Check parameter settings
ture error” of the receiver failed • Call for a qualified techni-
cian.
43-50 - Used for internal firmware -
51 “Please detect man- Parameter setting option for Confirm button exactly when the
ually the dry point.” manual dry point detection is set bottom of the flask gets dry
52 “New CPU board New CPU board is installed Confirm OK button
detected”
53 “New CTRL board New CTR board is installed Confirm OK button
detected”
54 “New MMI board New MMI board is installed Confirm OK button
detected”
55 “New heating board New heating board is installed Confirm OK button
detected”
56-57 - Used for internal firmware -
UM_2.00A_EN 249
250 UM_2.00A_EN
List of accessories OptiDist™
11 List of accessories
UM_2.00A_EN 251
OptiDist™ List of accessories
OptiDist™ List of accessories

/i
Quantity P/N Description

1 8013-004-00x Documentation CD
1 2002-004-001 OptiDist™ Measuring Cylinder 100ml with brass base
1 2201-004-001 OptiDist™ Flask 125ml
1 2001-004-008 OptiDist™ Vapor Probe Stopper for 100ml, 125ml and
250ml flask
1 3801-110-001 OptiDist™ Vapor Probe with calibration certificate cali-
brated at 50°C and 250°C
1 3002-004-1031 OptiDist™ Vapor Probe wire guide
1 3003-004-1007 OptiDist™ Vapor Probe holder
1 3002-004-1013 OptiDist™ Heater Base Plate 50 mm
1 3002-004-1014 OptiDist™ Heater Base Plate 38 mm
1 2007-004-009 OptiDist™ Silicone hose for flask connection
1 3004-004-1002 Rubber Cap for Measuring Cylinder
1 2000-004-002 OptiDist™ Condenser Cleaner
1 3001-004-1065 OptiDist™ Receiver Chamber Liquid Vessel
1 1700-000-007 Ethernet Cable 3 m
1 3002-000-1002 Hose connection piece
1 5201-000-001 Set of hexagonal wrenches
1 - Packing List
1 - Additional information for Documentation on CD
Only for Unit Type 0101-004-003 and 0101-004-004
1 2201-004-005 OptiDist™ Flask 250ml
252 UM_2.00A_EN
OptiDist™
/i
NOTES
UM_2.00A_EN 253
OptiDist™
Web site: http://www.paclp.com

/i
PAC Companies
Address: PAC L.P.
PAC Corporate Headquarters
8824 Fallbrook Drive
Houston, Texas 77064
USA
Phone: +1 (0) 281 580 0339
Fax: +1 (0) 281 580 0719
Sales: sales@paclp.com
Service: service@paclp.com
Address: PAC ISL
BP 70285 - Verson
Parc d’Activités de la Mesnillière
14653 Carpiquet Cedex
France
Phone: +33 (0) 231 264 300
Fax: +33 (0) 231 266 293
Sales: salessupport.france@paclp.com
Service: service.france@paclp.com
Address: PAC Herzog
Badstrasse 3 - 5
P.O. Box 1241
DE-97912 Lauda-Königshofen
Germany
Phone: +49 (0) 9343 640 0
Fax: +49 (0) 9343 640 101
Sales: sales.germany@paclp.com
Service: service.germany@paclp.com
Address: PAC Rotterdam
Innsbruckweg 35
3047 AG Rotterdam
The Netherlands
Phone: +31 (0) 10 462 4811
Fax: +31 (0) 10 462 6330
Sales: sales.netherlands2@paclp.com
Service: service.netherlands@paclp.com
254 UM_2.00A_EN

OptiDist User Manual

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OptiDist™

Document number 8001-004-01E

Table 1.1 Revision History

This manual contains confidential and proprietary information. The information

3.9 Nameplate ............................................................................................................................ 28

7.2 The Products database....................................................................................................... 123

8.4 Various individual component diagnostic functions ............................................................ 212

1.1 Policy statement

1.2 Standard limited warranty of PAC

1.2.1 Limited warranty

whichever is less (the "Initial Warranty"). If a failure to conform to specifications or

1.2.1.3 Limited warranty exclusions

PAC makes no warranty, express or implied, as to the design, sale, installation or

There is no warranty by PAC with respect to any product’s:

There is no warranty for products determined to be, in PAC’s sole discretion,

D operation outside of the published environmental specification;

1.2.1.4 Resale products

1.2.1.5 Expenses on non-warranty work

1.2.1.6 Exclusive remedy

1.2.1.7 Procedure and costs

1.2.1.8 Terms and conditions

1.2.2 Limitations on PAC liability

1.2.2.2 Buyer Data

1.2.2.3 Force majeure

1.2.2.4 Limitation on warranty claims

1.3 Software license

The SOFTWARE PRODUCT is protected by copyright laws and international

1.3.1 Grant of license

This EULA grants you the following rights:

1.3.2 Description of other rights and limitations

1.3.5 Dual-media software

1.3.6 U.S. Government restricted rights

1.4.1 Good Laboratory Practice

1.4.2 The standards of laboratory safety

1.4.3 Electronic device

1.5 Return policy

1.5.1 Returned product warranty determination

1.5.2 On-site repair

1.5.3.1 Visible loss or damage

1.5.3.2 Concealed loss or damage

This product is designed for exclusive professional use by commercial

1.7.1 Document validity

1.7.2 Document storage

1.7.4 Typographical and authoring conventions

For a copy of the corresponding declarations, please consult the Service

During performance or routine maintenance, the system operator may be exposed

2.2 Warning pictograms

2.3 Caution pictograms

2.4 Note pictograms

2.5 Tip pictograms

2.6 Environmental protection

3.1 Intended use

3.2 Intended audience

3.3 Product overview

According to strict guidelines and protocols described in these standard test

touch screen interface provides guidance regarding instrument set up and

Simple, straightforward operation involves selecting a sample ID or a product from

The OptiDist™ can be operated as a stand-alone distillation unit. lt also can be

Sophisticated safety features include a built-in fire extinguisher system, traceable

3.4 Applicable standard methods

Table 3.1 Applicable methods

Standard method Remark

3.5 Benefits and features