NAME -M € OHAMMAD ASAD KUURSHID SHEIKY Roll Now IF! 1205] Expert 4 Cuplaljle. solid) and. inorganic AIM - To determyny fob! organic fixed solid) solicts n_tusgivan sasple——— —— THERY - Th teva olal ola solo nef? In raatiryot tod oue completely clalized pom. wal gt higher benyporadiovs __Thase solic ay oftin vefewed bo Nu ovgonic orn bat of Ha etn ancl Mu tum bola! fired solide con be reecred ho material tabi ave nob volaliliged prom watts od laghus binpevalory __Cesorc). the sols au offen veered fo Mu inorgarte- cottunk 4 We wats. ovated ina uulglud oth ona ag in an oun ati “PRINCIPLE - The ample is evap __sleom baby one alvied Jo 4 constant m iguiked fo contlath uxrig 103-105 C. The _vesidun oblaimed isi at 550%, Tha vemaltlig spliols nvepretend hue holed fired soli and Ha _usight lost devin ta ignihon wepreserl ttn bled —volefile solids EQUEMENTS - Evaparaling ish, water Galt, Quen dry and —- _ Moffle fornace , Pesicaloy , waghinag balana, Dh hon —_ aver, Wesh boifte. oe a Mapas hie sh le ancl fied Jolie, faler To mepsure Mle! uolah! q chen silica crvdbl etiich hos been vssshed and ded. ing hob oly oven af 108% jor ont hour ond yuked dt Gore PROCE PURE 4be vem -ell ovgamic motevials presentin it. _ a) Se Weigh My emyply ilca erueibl. y_analy olaFical balonee wt) 4 3) Using pipette trawler Sout of onfi ered Boupl in pordladn disl, A) Swikdh on pu own and allow be veach 105% 9) Place Wu silica —evveble ib Hy bakeiy ovws ————— Rep es sawp to get covsland moth Duyiey pov lony devohion __ts dow Jp ited necesily Be dadsiey of wntboot mos 7) Gel Hy conkeiny in g clessica by. 8) atch Hu obith od soon, at Ht bos csoled te ausid phsovplion of weishve due be it hy greswpla pdbuve _ —Neke He weight wile resid as Ww, —— = 19) Sutil on Me fernau. end allow ib. reads Ssa% 2) Place bu silica crucible in Met [penece 2) Alipas ik le ignitt fox 20 min Foget cout may 1) Geol silica evucibl ino elessicalor fy veo Ganperabyre _4) ubsigle Mu clish assoon aa it is cooled bo guoid absorp lion f— i mais hyve _ _15)_Node Ms weight wil westda O46 We oe ~~ ALCULATION _ © Told volatily solicle ot of empl porcelain cish = 46-5859 _ a ~—"_affit_eeporaliow of 1wowl yroste wot (Wn) = or. 31g fier evapavation of volahle soles (us) = 49.2955 of wolahile cybslony (w= wr-Ws = 4h34I- 47.257 ° not) ual ot somcpl © Gantt pan etly bs lolal volohle lid ln sangle * » ein . : = 0.064 x (coo) a Sp : Fak na TL Otol jined “oli , _ : _ ut 9 renvolahle “solid = Wee Ws 0.692 Auoutt of doled fixed. ashy ® si) : _ Os any : "Rad - - Tolal wala ls Solids = 1280 my le - _ __Tolal fixed solids = 1364 0my Je = 44.2979 — 46.585 oo