Suggested Problem (LLE)

An aqueous feed solution of 1000 kg/h containing 23.5 wt % acetone and 76.5 wt % water is being
extracted in a countercurrent multistage extraction system using pure Methyl-isobutyl ketone
(MIK) solvent at 298-299K. The outlet water raffinate is to contain 2.5 wt % acetone. The
equilibrium data is given below.

a. Calculate the minimum solvent that can be used.

b. Using a solvent rate of 1.5 times the minimum, calculate the number of theoretical
stages.

Composition Data Acetone distribution data

wt % wt %
MIK Acetone Water Water Phase MIK
phase
98 0 2 2.5 4.5
93.2 4.6 2.2 5.5 10
77.3 18.95 3.75 7.5 13.5
71 24.4 4.6 10 17.5
65.5 28.9 5.6 12.5 21.3
54.7 37.6 7.7 15.5 25.5
46.2 43.2 10.6 17.5 28.2
12.4 42.7 44.9 20 31.2
5.01 30.9 64.09 22.5 34
3.23 20.9 75.87 25 36.5
2.12 3.73 94.15 26 37.5
2.2 0 97.8