natytioal smen ripen OC TION Analytical Chemin, ane = Module #9 Student Activily Sheet soos dal 0 Regie ac < igll 5 We Stay yuk mar Precipitation Titrations : ye been used for very many years Titrations employing “Tenmetnc reactions in which the product is of low solubity have curt enc ae trewn as preaptaion ttraions.athough not of widespread importance, for @ kmited number of purposes, suchas the detorminaton of halides, these methods are invaluable. Silver nitrate isthe most widely used caer Sep rae to civer sas which are characterstcaly sparingly soluble. The end points of precipitation trations can be Sort Je eteced An indicator extibting a pronounced color change with the fist excess of the tdrant may be used. The Moxemetnod invowing the formation of red siver chromate with the appearance of an excess of siver ions. isan important Sennnte of ins procedure. whist the Volhard method. which uses the ferric thiocyanate color as an indication of the Gresence of excess thiocyanate ons. is another A series of indicators known as adsorption indicators have also Deen Stazed, These consist of orpanic dyes such as fluorescein which are used in iver nitrate titrations, When the equivalence: ate fo give a positively charged surface which attracts pont is passed the excess siver ions are adsorbed on the precipi Sad adsorbs fuoresceinate fons. This adsorption is accompanied by the appearance of ared color on the precipitate surface, (CHECK FOR UNDERSTANDING ‘The students will draw a figure of tration on t ‘application, disadvantage of the method. This wi (1) point per steps (total of 5 points) one (1) point Gisadvantage of method. Superimpositions or erasures. their own, they should indicate the steps and give the principle, apparatus, il be recorded as their quiz. One (1) point wil be given to the drawing, one or principle, one (1) for apparatus, one (1) for application and one (1) for in answerfratio is not alowed ‘Method Analysis Draw 2 figure of batch method of solvent extraction, indicate the steps and give the principle. apparatus. application, Geadvantage of the method. One (1) point will be given to the drawing. one (1) point per steps (total of 5 points), one (1) pont for principle, one (1) for apparatus, one (1) for application and one (1) for disadvantage of method. RATIONALIZATION ACTIVITY (DURING THE FACE TO FACE INTERACTION WITH THE STUDENTS) ‘The instructor will now rationalize the answers to the students and will encourage them to ask questions and 1o ‘Gecuss among their Glassmates for 20 minutes. 4. MER Bincple: gation ae calle Hihow or sslard solution RATIO, wv 2. ANSWER RATIO: 3. ANSWER sr nthe property of PHINMA EDUCATIONWy Analytical Chemistry ae i h 4 a Module #9 Student Activity Sheet ee Csasag pe MAS RATIO, Apu 4 fitdte - a _ 4. ANSWER RATIO. Dw 4 yeal uri nbical 5. ANSWER: RATIO. Visahaohes Hoch Vale, Other huran Eiiop 6 ANSWER: RATIO. 7 Ao — Png I + Exhochiy the wlult_ jeninibldoys im I ae R A ip 8. ANSWER: Ratio ————_Mhpwalys fay shank eins bop Type Slant Leber 9. ANSWER RATION Kaplan Commonly wird to the seal yale in eical Laetabries 10. ANSWER, : L yale can Lu ben ANOS cara Jaana : evayne ime He solan} om yes Toscneimnent i ie pepe oy PHINMIA EDUCATION k 3$4) ndajog ; py Auriglou ou he nba re ay Maan Prieap And me hi ” i 4 ise apt Pl 0 HO PAY NL (P44 Pe Pl) (pundw2) oo yum Waly m)2%5