Data File H:\CHEM32\2\DATA\JULY 2013\PME DUMAI 17072013 PAGI.D Sample Name: PME MT_SINAR JOHOR CMPSIT ‘Acq. Operator: JHON Acq. Instrument : Instrument 2 Location : Vial 201 Injection Date : 7/17/2013 1:48:30 AM Inj Volume : External Method : E:\CHEM32\2\METHODS\GLY.M Last changed _: 7/9/2013 10:29:48 AM by LETTA ™ igines fc} 4 OR a4 cn ele \O%Ub Wi + a 2004 | | de | i}] face | 4G sae Q 8 fr e-s eo 3 a 2ggee gabe 22/8 “| peeigite g/ Area Percent Report Sorted By Signal Calib. Data Modified 2/13/2013 10:20:04 AM Multiplier 1.0000, Dilution : 1.0000 Use Multiplier & Dilution Factor with ISTDs Signal 1: FID1 A, Front Signal Peak RetTime Type Width Area Area Name 4 [min] [min] [pA*s] a 1 2.285 BB 0.0349 31.66527 0.00493 2 2 2.482 BV 0.0415 188.34572 0.02932 2 3 2.570 W 0.0368 328.51202 0.05115 2 4 2.711 Ww 0.0418 359.99707 0.05605 2 5 4.631 0.0000 0.00000 0.00000 stp x 6 4.803 BB 0.1146 100.14893 0.01559 2 7 6.456 BV 0.0803 803.4157 0.12509 2 8 6.498 W 0.0510 522.80035 0.08140 ? 9 6.550 Ww 0.0232 221.55756 0.03450 2 10 6.578 VB 0.0597 618.01251 0.09622 2 117.984 BV 0.0748 1498.02100 0.23324 2 Instrument 2 7/22/2013 4:07:50 PM LETTA Page 1 of 3Data File B:\CHEM32\2\DATA\JULY 2013\PME DUMAI 17072013 PAGI.D Sample Name: PME MT SINAR JOHOR CMPSIT Peak RetTime Type Width Area Area Name # [min] [min] [pats] 8 12 8.045 W 0.0482 979.41290 0.15249 2 13 8.094 W 0.0445 958.65350 0.14926 7 148.161 W 0.0385 840.40460 0.13085 7 15 8.194 W 0.0155 311.18463 0.04845 7 16 8.214 W 0.0274 579.09778 0.09016 2 17 8.264 VB 0.0691 1492.89355 0.23244 2 18 8.683 BB 0.0762 31.56209 0.00491 2 19 9.162 BV 0.0756 9.07567 0.01387 ? 20 9.682 WW 0.1390 7.03584e4 10.95456 ? 21 9.765 W 0.0549 3.378784 5.26064 2 22 9.782 W 0.0128 6549.71191 1.01977 2 23° 9.808 vv 0.0267 1.30925e4 2.03845 ? 24 9.853 WW 0.0421 2.58520e4 4.02508 ? 25 9.928 vv 0.0530 3.44293e4 5.36052 ? 26 9.957 Ww 0.0161 9442.33105 1.47014 2 27° 9,981 Ww 0.0202 1.06019e4 1.65069 2 28 10.015 WW 0.0407 2.43456e4 3.79053 ? 29 10.052 Ww 0.0188 1.05139e4 1.63699 ? 30 10.086 Ww 0.0396 2.79983e4 4.35924 2 31 10.120 VB 0.0128 6725.84131 1.04719 2 32 10.352 BV 0.1628 352.31607 0.05485 2 33 10.912 W 0.1150 2.70910e4 4.21798 ? 34 11.024 W 0.0697 2.17268e4 3.38279 ? 35° 11.048 w 0.0181 5316.36670 0.82774 2 36 11.119 w 0.0506 1.78550e4 2.77997 2 37 11.154 W 0.0271 9565.74023 1.48935 2 38 11.192 W 0.0300 1.20324e4 1.87341 ? 39 11.339 W 0.0980 5.141744 8.00551 ? 40 11.420 W 0.0591 3.32502e4 5.17695 ? 41 11.458 W 0.0313 1.64856e4 2.56675 7 42 11.484 W 0.0199 1.16238e4 1.80979 2 43° 11.530 W 0.0432 2,53335e4 3.94435 ? 44 11.572 W 0.0326 2.21719e4 3.45208 2 45° 11.607 W 0.0315 2.00602e4 3.12331 7 46 11.658 W 0.0285 2.03743e4 3.17221 2 47 11.681 W 0.0184 1.26523e4 1.96992 2 \ 4g 11.718 Ww 0.0327 2.29321e4 3.57045 2 49° 11.779 Ww 0.0429 .1.62253e4 2.52622 2 50 11.845 W 0.0258 85.13698 0.01326 2 51 11.894 W 0.0372 45.48355 0.00708 7 52 12.013 vB 0.0430 382.14276 0.05950 7 53 12.196 BV 0.0408 © 42.69639 0.00665 2 54 12.283 W 0.0389 © 13.25283 0.00206 2 95 12.442 W 0.0629 33.84330 0.00527 7 56 12.634 W 0.0516 1044.00232 0.16255 7 57 12.952 vB 0.0619 2440.89380 0.38004 7 58 13.797 BB 0.0800 47.7087 0.00743 2 59 14,492 BB 0.0615 18.40827 0.00287 2 60 14,999 BB 0.0798 433.54910 0.06750 7 61 15.644 BB 0.0670 155.63390 0.02423 MG 62 16.083 BV 0.0737 1633.31567 0.25430 MG 63 16.196 vB 0.0748 86.61605 0.01349 NG 64 16.598 0.0000 0.00000 0.00000 wc 65 17.441 BV 0.0670 412.56421 0.06423 2 66 17.650 VB 0.0869 190.82800 0.02971 NG 67 18.135 BV 0.0928 1858.04504 0.28929 MG Instrument 2 1/22/2013 4:07:50 PM LETTA Page 2 of 3CHEM32\2\DATA\JULY 2013\PME DUMAI 17072013 PAGI.D PME MT SINAR JOHOR CMPSIT Peak RetTime Type Width Area Area Name # [min] [min] [pas] 8 379.50125 0.05909 ° 18.984 0.0000 0.00000 0.00000 uc 19.034 0.0000 0.00000 0.00000 uc 19.229 0.0000 0.00000 0.00000 uc 20.790 BB 0.0694 45.43621 0.00707 NG 21.726 BV 0.0714 182.21257 0.02837 MG 21.929 VB 0.0653 118.92397 0.01952 2 22.608 BB 0.0588 104.02712 0.01620 2 22.897 BB 0.0726 171.91805 0.02677 NG 23.328 BB 0.0600 257.49304 0.04009 NG 23.703 BB 0.0736 28.15822 0.00438 NG 24.863 BB 0.0682 34.24800 0.00533 STD IT 25.849 BB 0.0638 30.3755 0.00473 2 26.232 BB 0.0607 39.09151 0.00609 ? 26.817 BB 0.0550 31.15327 0.00485 ? 27.089 BB 0.0553 84.96598 0.01323 DG 27.277 BB 0.0638 143.85947 0.02240 DG 28.000 BV 0.0659 198.44867 0.03090 Dg 28.204 VB 0.0639 370.91858 0.05775 DG 28.534 0.0000 0.00000 0.00000 ng 28.877 BV 0.0724 72.1504 0.01123 DG 29.069 VB 0.0852 208.55872 0.03247 DG 29.205 0.0000 0.00000 0.00000 Dg 29.398 0.0000 0.00000 0.00000 Dg 29.475 0.0000 0.00000 0.00000 De 29.930 BB 0.0621 15.13516 0.00236 Dg 32.304 BB 0.0853 43.56926v 0.00678 TG 32.395 0.0000 0.00000 0.00000 16 33.121 BB 0.0755 129.51085% 0,02016 16 33.812 BB 0.0673 330.01059v 0,05138 16 34.566 BB 0.0750 212.31049v 0,03306 6 35.030 0.0000 0.00000 0.00000 16 Totals : 6.42275e5 3 Warnings or Errors Warning : Calibration warnings (see calibration table listing) Warning : Calibrated compound(s) not found Warning : Elution order of calibrated compounds may have changed ‘+ End of Report *** Instrument 2 7/22/2013 4:07:50 PM LETTA Page 3 of 3