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 Date
Expt. No. Page No.

ExPERIMENT-9
AIrt- Ts detesnine Chmical Oxygen Deman8 (Co D)
a isluten.
APPARATO5 REGUIRED:
Diaetien Vessela,_
)Bleck heater Opexate at 150t'c],
d)Phmpole -eales,
e)Besesilieate cultoal tobes(lmmlo0 mm
0mm 150 mm ith TFE tinal-CYAa Capi.
REAGENTS:
o)Stondord pslatiom dichyomate digeslon Sslfionlo-01659M
Sulphusic oacid yeagentg
Fesrainîndiatss eution,
STandasd erreus ommenium &uate tityant (Fas) 0-loM
Solfamic Reid
Peta&tiom hdrsqen phthalate standas
THEORY:
Chemical Oxygen Demand (CoD) rs the amsunt qf a dpece
OxTdginq aget that Jeat LTh Sample watey undex
Centrslles Cenditionl an 1 expreed a oxtn equivaleno
T 3 ed ts indcate oxqai mattes Certaminahis and A helpa
inknswing eveyall o4oriclsad t te 3eceiving edy.
-WRITO-LINE- Teacher's Signature:
oure

3 Apparetg ldup

/o o obo
oo00 CoD die fo
 Date

Expt. No. Page No.

Reacien with Drchrernte sslufion_ ample

CH.ON +d CO"+88+cdH
nlo,o+3d-58| H,0 +CNH28 C

hee
- (2n13)+(/6)-(W3)-(cla)

Doina expeñnentexceg dich/ernate (onc. 3 determined by

ttotiq
t t h e i s Omnenium 4ulteFHS),ea tion 13 gven by:

6Fe ACT04H 6F+C5"+24,0

PRoCEDURE:

l. wWash coltose tubes an Capt h 207 H S0,, befot ufina to psevent

Ce-nTaminotien.
39lulion.
. Place 3omple in cuHose tube or anpule and add dietion an
Cascully n 3ulthuac acið_xeaqent down înaide ovesiel Se
5slffon fayey
acdLayer 3 ovmed under the 5omple-drqegtion
Cap tubes or eal Ampules, an înveit each Beveral
and fgntly
Firmes t ix Cemlélely.
block dígestey prcheatad to 150'c and
3, Place tobes e rampules in

ox o Ihvs bekínd a preteivehteld.

V/DITOJ I N E
Teacher's Signature:.
Observon Table

Valume FAS 6elut

Bopette P.dngCn )
Somple Enal CPinal- 1nsal) (m)

2210-

TL
 Date

Expt. No. Page No.

4ss fo 768m Ternpesatose an place veßels in tut tube sack.

Soe mtsuñc Sulpháte may prCcip tate o.t but thg ul not ofet
the analy8is.
15. Renovecultuoe tube Cap? and add mall TEG-cowe ged maqnetic
stfsin baz:Omgula axe ued, tanfer cerntont to a largez
(ontaintyioy itsating.
6. AJJ O-05 to O«lo mL(1 2Jrept) fenoin indKator and a
Topdly orm magntic 3tssts wkle htrating_wth 3tandaz diaed
O10MFAS. The end poit a shavp relar chare tn buc
qsen tosedrgh bseun ,alheugh the bloe qyren may 3eapptag
wthin instes. Ta the Same anney dux and htte a blank
Centaining the Teaqest and a velume e drhlled wáler equal to
that othe dample.
COD' auen by
Chen+cal Oxgen Dernand -((-B)x Mx900o
ng)Ca/L Vsanple
whese
A-Vslume FAS U3ed fer blank(m
B:valame Fasusedeslomplel.
M melat o FAS
Bo00mdreqsvalest ut.y lo00mL
e6xgen

WRITO-LINE- Teacher's Signature:

 Date
Page No.-
Ept No

RESULTS:

he ChenicalOxugen DCenand ethe giuen angle

feund ot te be fng1)ro.l).

PRECAUToNS:

(auie_e tre potiklt e leakingJarnple

De nst u an svon be
(ezrelfue and expleive atmspheye,
gentyating

Thestealed vesselk may be undey pe 34uBe fon gades

2 hand prstedion when
digertion, kleax face ad
qantrated duñn
dangereuse38u3eS will be aentyated at 150C.
handling and

Teacher's Signature
WRITO-LINE-
 Date
Expt. No.. Page No.

ExPERIMENT-10
AI- To detesmine tstal3d7ds,drssalved sol and TBtal Sutpedd
Soli in Natex

APPARATOS REQUIRED: Balance Beakes, Meduning ylnder Frte

Papey-latrnann Funneland Dreppe,
Mole husnalCe.
THEORY:
he meagOKenent 30lids by meank_e the qsavime
prscedosehe varibus sYns o3eLidsaye defemimeby ahing
oftes The appreprfate handlinq preceduse he Tatal el+ds cex
adomple_can be und drectiy by lawesahing the gample jease
and otey dring at l03C, Heuever the rennin smmi, IDS a
T55 xeise totion ahe Somple. Fsy Luid JampleS all fhese
Selid levely ase tpssted tnma.

Althsuh he nause The varieus fonf thetr zelative concetvatiens

ans the kene +conic Strenath ethe water otect th meadunenet
the drgalved mineral
Such meaU Cntnt Can give_pradtical efmste ot
Cerntent e w he DS tet Con be appyeKkinstal b nhpin
the Speck CenduTaoce fn micro-Siemen per cmLSlon)by an
expeñmental actoy vnpoq atm 0:55-0-90 depennq n the
Chenical cempefon e the TDS

WRITO-LINE-
Teacher's Signature:-
Froute

a1. ghing
Cale
(Balonce)

2 rHr Papey-wahoann

PLTER PRPER

MOECLE
FURNACe
 Date
Expt. No. Page No.

PROCEQURE:

Measusenest e Te 16tal Solrd (TS):

ake a cleax da alalk beakes (which wa kept at 103cin an Gven
o 1heu) e l5ont iapatity and pst appropiste rdenlhsrshfon
marK en it. Wegkt the beaker and nste the weaqht.
2, Pan l00 mt o the treughly mixtomple,meodvsel by The
easu in eulindez in the beakez.

3. Place the beakes ina vn maistained at i0%cos 24houds,

Ates4 hsus Ceel the beakey ond weqht.ind o te wéght
eeldsintke beahes by_3ubtsacioq the waht ef the clean
beaker deteswined în sted).
4.Calcolete Ttal 3otd (TS) slleul
Tetal Solrd mq. oSolkds in the beakarx lO000
Cng/) Sarmple
Measu enet oTtal Drsoked Sekd, (TDS)
Same a abeve (ep 11e total solidg)

a. Takea lo0molample _and fltey

i tthrsugh adouble layered
WRITO-LINE- Teacher'sSignature:
Obtorun Table

Sarnple Valent wCaht e beaKeg

Semgle'm Talnal DAeence

2)Tott 0ssaled Satd LDoble-layereder popes

Wsght o beakey
omple Valume e
Somple(m) TLFfnal DHerxt
 Date
Expt. No.
Page No.

es paper ond colled the ltrate in a beaker

3. Then epest the dome precelse agin sp(3) and (4) of the
atalasld deteyminatfonand detemlne the dolued 1elida
Cetent a ollsw
lstal DrRIalued Sold! (TOS)= mg. 3eld inthe beakey x1000
(rng/0) VAomple

4 Als calcolete the tstal u1pended 30l7d:

Tstl Surpended Sslrds:Ttal Sakds(TS) - Total Disaked akd,(TOS)

(ng/) (ngl)
(15),)
RESULTS:
The total 30kd_psexatin the ample_m

ssleol elrds_pre nt în the Sample: /

The tstal
uspended 3elrdy_poejtnt in the Jample
The ttal
ng

Teacher's Signature
 Date
Expt. No. Page No..

PRECAUTONS:

We Sheds be auase_þselenqed dzyia may esut in loss o

Cen Tueat sPayticulaxy ntates and chleridB,

2. watey Sample ahich Contain kigh Cecetrotion e calkiumgcHeide

maane om 07 3ulphaTe Can ya+dly absarb masueenthe a
Such Sanpla may need t be dfes or a lenaer_peñod e Hne
cseled un der preper dessicanennd whed apidly in ordes to
acheve a seadenable cenatant weaht,
3 Volune omple neuld be adusted to have TeTdue let oter
drying aj100 to o0 nq T+i mînl to preveit loqe Omaunt
Terdue in esisappioq_woter dasinq evapayatfien.