Professional Documents
Culture Documents
Izod impact measures energy required to break a specimen by striking a specific size
bar with a pendulum.
Related terms:
Glass Fibre, Lexan, Mols, Monomers, Tensile Strength, Tensiles, Tensile Bar, Poly-
etheretherketone
Testing Properties
John R. WagnerJr., ... Harold F. GilesJr., in Extrusion (Second Edition), 2014
If the Izod bar is cut from a 5-in. (128-mm) long molded bar, either the gate end or
dead end are compared and reported as a group. Different ends of the bars are not
mixed in a sample group. If both ends are tested in the same group and compared,
the standard deviation and the measurement precision suffer due to potentially
different injection molding and packing conditions during specimen formation.
Izod is designated as an impact measurement, since the energy to break a bar is
determined. In reality, Izod measures the notch sensitivity rather than being a true
impact measurement. The notch acts as a stress concentrator and simulates what
occurs if a part is scratched or cut in a specific application, making it easier to break
the product. Figure 21.13 shows an Izod test machine, and Figure 21.14 shows the
notcher.
Composites that are prepared with LDPE have greater impact strength among
unoccupied samples, but the brittleness will increase as loading of filler increases
due to the growing size of the poor interaction between the hydrophilic filler and the
hydrophobic polymer matrix (Yang et al., 2006). For PP/HA/LLDPE ternary biocom-
posites, the impact strength increases as content of LLDPE and impact resistance
increases with temperature (Younesi and Bahrololoom, 2009).
> Read full chapter
Figure 2.9. An illustrative view of the notched izod test set-up, showing the pendu-
lum striker path and the test specimen held with the notch facing the pendulum.The
distance from the notch to the striker impact line is defined within the test specif-
ication.
> Read full chapter
While there are many measurements listed, the measurements use test apparatus
that fall into two types: based on a pendulum or a falling object. The main differences
are sample preparation and measurement units.
• ASTM D256-06a Standard Test Methods for Determining the Izod Pendulum
Impact Resistance of Plastics
Both Izod and Charpy tests are based upon a swinging pendulum, such as that
shown in Figure 1.27.
Figure 1.27. Pendulum-type impact strength tester.
Basically, the pendulum is raised to a measured point, and it is then released. The
weighted end of the pendulum gains speed as it swings toward a mounted molded
bar of the test plastic. It strikes the bar, breaks it, and the pendulum loses energy
while breaking the plastic bar. Therefore it does not swing as high. The energy lost
by the pendulum is equated with the energy absorbed by the test specimen during
the breaking process.
There are different ways to mount the test specimen, and there are different speci-
men sizes and preparation methods. The different sample mounting configurations
for the Izod and Charpy tests are shown in Figure 1.28. Figure 1.29 shows the details
of the notch. The sharpness of the bottom of the notch affects the test result. Table
1.11 shows the different notch radii possible.
Figure 1.28. Izod and Charpy impact test sample configurations.
The impact resistance is usually reported as energy per unit length or per unit area.
• D5420-04 Standard Test Method for Impact Resistance of Flat, Rigid Plastic
Specimen by Means of a Striker Impacted by a Falling Weight (Gardner Impact)
• D5628-06 Standard Test Method for Impact Resistance of Flat, Rigid Plastic
Specimens by Means of a Falling Dart (Tup or Falling Mass)
•
D3763-06 Standard Test Method for High Speed Puncture Properties of Plas-
tics Using Load and Displacement Sensors
• ISO 7765-2:1994 Plastics film and sheeting—Determination of impact resis-
tance by the free-falling Dart method—Part 2: Instrumented puncture test
The Gardner test uses a piece of equipment like that shown in Figure 1.30. A weight
is lifted to a given height and it is dropped onto a test plaque. The Falling Dart is
based on the same principle, but the weight is free falling rather than guided through
a tube as in the Gardner equipment.
9.5. (a) Set-up of Izod test; (b) Model B; (c) hammer–specimen interaction; (d)
meshing of hammer and specimen (specimen is shown larger).
In Abaqus 6.10 (Abaqus, 2010), a kinematic coupling constraint is used to transmit
rotation to a structure while permitting a radial motion. Hence, this feature was
employed to constrain the rotational and translational degrees of freedom of the
hammer except around one axis only; it is z-axis in this case (see Fig. 9.5). To get the
exact movement of the hammer as happens in real tests, all the nodes of the inner
cylinder surface of the upper block of the hammer were kinematically coupled to a
reference point at the middle of the cylinder, then the reference point was restrained
to translate along x, y, and z and to rotate around the x or y axes (Fig. 9.5b). The
reference point was only free to rotate around the z-axis. Using Abaqus/Complete
Abaqus Environment (CAE), two sets were defined: the reference point (set1) and the
inner surface (set2). The following equation was used to define the coupling between
those sets:
[9.1]
where ur1 and ur2 are the rotational degrees of freedom for set1 and set2, respectively.
To compare the force–time history data of experiments and simulations, the force
due to contact pressure between the piezoelectric force sensor and counterpart of the
specimen elements was recorded in the history output of the finite-element software
Abaqus/Standard. Also, the status of the X-FEM that shows the crack path was used
as an output along with the distributions of stress and strain components and their
principal values. In order to compare the fracture behaviour of the cortical bone
specimen under quasi-static and impact loading, Model C (Fig. 9.6) was developed.
It consists of a cantilever-beam specimen of cortical bone with the same geometry,
mesh and material properties as in Model B. In Model C, the hammer was excluded
from the analysis and a displacement of 2 mm was applied instead at the same
position of the hammer–specimen interaction, see Fig. 9.6b.
9.6. (a) Meshed 3D quasi-static specimen; (b) applied displacement and boundary
conditions of 3D quasi-static model (Model C).
Material properties
The Resil Impactor hammer used in this study was made of carbon steel. Its elastic
material properties are given in Table 9.3. These data were obtained directly from
the manufacturer.
For numerical analysis of the cortical bone tissue, two important conclusions
based on our experimental studies were recalled: (1) experimental Izod impact tests
demonstrated that the studied bovine femoral cortical bone tissue had a nearly
uniform character of fracture energy for different cortex positions and was not
sensitive to the notch depth within the physiologically pertinent range (Abdel-Wahab
and Silberschmidt, 2011); (2) quasi-static tests provided a low level of anisotropy
(between 1.2 and 2) compared to structural composites (Abdel-Wahab et al., 2010a).
Taking this into account, it is reasonable to consider only specimens cut from the
anterior longitudinal cortex position when dealing with fracture – for Models A, B
and C.
The elastic, plastic and viscoelastic data of cortical bone tissue were quantified by
the authors experimentally (Abdel-Wahab and Silberschmidt, 2011). The average
elastic modulus and Poisson ratio of anterior longitudinal specimens are given in
Table 9.1. The average true stress-plastic strain behaviour of the latter specimens is
given in Table 9.4. Density of the cortical bone tissue was measured as 1860 kg/m3.
The viscous behaviour of bones was introduced into the FEMs A and B in terms of
the Prony series expansion of the dimensionless relaxation modulus. These material
constants are the shear relaxation modulus ratios ei = 0.1346, bulk relaxation ratios ki
= 0 and relaxation time = 117.85. Only the linear-elastic material model was used
for Model C for quasi-static loading.
Table 9.4. True stress–plastic strain data for anterior longitudinal cortical bone tissue
specimen
Figure 11.17. Izod impact strength of polyamide 11 plasticized with variable quanti-
ties of p-methylbenzene sulfonamide, A, and p-butyl hydroxybenzoate, B.[Data from
Li Q F; Tian M; Kim D G; Wu D Z; Jin R G J. Appl. Polym. Sci., 83, No.7, 14th Feb.
2002, p.1600–7.]Copyright © 2002
Figure 11.19 shows that even small additions of plasticizer increase rapidly fatigue
life of monofilaments obtained from plasticized polyamide-6,6. Considering that the
minimum fatigue life required by commercial product is 50 minutes, at least 3 wt%
plasticizer is needed to make product useful in practical applications.203
Figure 11.19. Effect of N-methylbenzene sulfonamide on fatigue life of
polyamide-6,6.[Data from US Patent 6,249,928.]
Figure 11.19 shows that even small additions of plasticizer increase rapidly fatigue
life of monofilaments obtained from plasticized polyamide-6,6. Considering that the
minimum fatigue life required by commercial product is 50 minutes, at least 3 wt%
plasticizer is needed to make product useful in practical applications.14
Figure 11.19. Effect of N-methylbenzene sulfonamide on fatigue life of
polyamide-6,6.[Data from US Patent 6,249,928.]
The numerical results of the plastic strain distribution within the undamaged spec-
imens at different mold temperatures are presented in Figure 4.13. The greatest
straining occurs at the notch, and there is also a high-strain region opposite to the
notch where the bending strains are concentrated. The plastic strain is always higher
for the specimen with lower mold temperature than with the opposite. This is due
to the processing-affected yield stress of polycarbonate. Since the yield stress of
polycarbonate is reduced as the mold temperature decreases, plastic deformation
will be more easily developed and the plastic strain will be accumulated to a higher
level in the specimen with lower mold temperature.
Figure 4.13. Plastic strain distribution within the undamaged specimens
at different mold temperatures. For a color version of this figure, see
www.iste.co.uk/zhang/polycarbonate.zip
Figure 4.14 presents the variation of internal energy, i.e. the total energy absorbed by
the specimens at different mold temperatures during the impact. Internal energies
can be found to vary in a similar way at different mold temperatures. The energies
gradually increase with time and suddenly decrease at the final stage, which means
that the specimens are fractured. Since the elastic properties of polycarbonate
specimens at different mold temperatures are assumed to be constant, the variations
of the energy with time are exactly the same before the yielding of polycarbonate.
Thus, the energy variation curves of the specimens at different mold temperatures
are overlapping by up to nearly 3 ms. However, distinct separations of the energy
curves are found after yielding, especially in the fracture process.
Figure 4.14. Internal energy variation of impacted specimens at different mold
temperatures. For a color version of this figure, see www.iste.co.uk/zhang/polycar-
bonate.zip
Figure 4.15. shows the detailed fracture process of the specimen at the mold
temperature of 60°C.
Figure 4.15. Fracture process of the specimen at the mold temperature of 60°C. For
a color version of this figure, see www.iste.co.uk/zhang/polycarbonate.zip
Table 4.1 lists the fracture energies obtained by numerical simulations and exper-
imental tests. The fracture energy is measured by dividing the total lost energy by
the cross-sectional area at the notch (ISO 180 2000).
As shown in Table 4.1, both experimental and numerical results clearly indicate that
the fracture energy increases as the mold temperature increases. Since the increase
in the mold temperature leads to the increase in the yield stress of polycarbonate,
more energy of the striker will be consumed for the plastic deformation and fracture
of the polycarbonate specimen. The predicted fracture energies of the polycarbonate
specimens at 60, 80 and 120°C mold temperatures are shown to be in good agree-
ment with the experimental data, indicating the predictive ability of the proposed
integrated simulation framework.