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Shlotermuller&al
Shlotermuller&al
INTRODUCTION
processing values and the measured residual stress values were determined
and how well they correspond with the results of the theoretical model.
The thermoplastic winding process is commonly known and here the
method described by Funck [10] was applied using a hydrogen-oxygen flame
as heat source and in this case a consolidation roller that applies pressure at
the nip-point. The residual stress, and the strain, can be determined in
several different ways. Knight [11] used orthotropic photoelastic analysis to
determine the residual stresses. White [12] presented measurement by special
strain gauges for the hole drilling method and the layer removal procedure.
Ersoy and Vardar [13] slitted metal and composite specimens to measure the
residual stress and showed that this method also complies to composite
materials. All these methods are less suitable for ring samples whereas the
method of Funck [14] matches the requirements of filament wound test
samples and guarantees a high grade of reproducibility and accuracy. Strain
gauges measured the restoring strain when the ring was cut open. From this
strain the residual stress can be calculated.
Temperature measurement
VW
Measurement of tape
tension and velocity
Brake Mandrel
Flame
Due to the relatively low viscosity of the melted matrix during the winding
process, the fiber will sink under the tension force applied to the tapes. Such
a microphenomenon can be described partially by the radial displacement
of every layer. The fiber motion submodel describes the position, displace-
ment and instantaneous tension of the fibers, the thickness of each layer and
of the whole composite as well as the fiber volume fraction. Input data for
this submodel are the physical and mechanical properties of the fiber and
matrix materials, the geometrical dimensions of the mandrel and the
composite, and the processing parameters such as winding angle and tape
tension force. Other data includes the actual temperature, the degree of
solidification and the viscosity of the matrix and is provided by other
submodels.
The radial component of the fiber tension produces a radial displacement
wfðjÞ , where the index j indicates the jth layer of the composite. After reaching
the glass transition temperature of the matrix the fibers are locked in their
position and no more displacements occur.
The radial displacement wðjÞf depends on the balance between the radial
component of the fiber tension and the resistance that the viscous matrix
presents to fiber movement. Radial tension is a function of the fiber
modulus Ef, whereas the viscous resistance follows Darcy’s law [15] of flows
through porous media and is a function of the permeability S of the fibers.
Considering the two contributions, the displacement of a fiber layer during
a short time interval t is given by the following expression:
SfðjÞ
wfðjÞ ¼ t sin2 ðjÞ ð1Þ
ðjÞ rfðjÞ
where m(j) is the matrix viscosity, rðjÞf the radial coordinate indicating the
position of the jth layer and fðjÞ the stress in the fiber due to the force of the
tape F. The effective force F applied to the fiber is continuously changing
from its initial value F0 during the winding process. The permeability S of a
porous medium for a Newtonian fluid may be obtained by the Carman–
Kozeny equation [16] as
R2 ð1 f Þ3
S¼ ð2Þ
4kzz 2f
where R is the fiber radius, f the fiber volume fraction and kzz the Carman–
Kozeny constant in the transverse direction of the fiber bundle. The
Carman–Kozeny equation is based on the capillary model of a granular bed
as a bundle of tortuous channels and appears to hold true for isotropic
porous media. However, several authors reported less satisfactory results for
transverse flow through anisotropic porous media [17,18]. This was often
compensated by adjusting the Carman–Kozeny constant to fit the data.
Usually, the Carman–Kozeny constant kzz ¼ 50,000.
An example of fiber layer displacement of the first layer during the whole
process is shown in Figure 2. The displacement changes of other layers are
similar. The outer radius of the mandrel ¼ 0.073 m. With the temperature
decrease, the fiber movements also decrease and stop after the part is totally
consolidated.
Thermal Submodel
This submodel, based on the solution of the energy balance, provides the
temperature distribution in the filament wound composite as a function of
1,00686
1,00684
1,00682
1,00680
r1/r0
1,00678
1,00676
1,00674
1,00672
1,00670
0 50 100 150 200
Time (min)
Figure 2. Radial position changes of layers during filament winding process (GF/PP, steel
mandrel).
time. Input data include the thermal properties of the raw material and the
thermal boundary conditions. The geometry and the instantaneous position
of the fibers are given by the fiber motion submodel. Unlike thermoset
matrix materials, the energy balance equation is less complicated as there is
no chemical reaction occurring and no heat generated in thermoplastic
matrix materials. For this cylindrical geometry it can be written in the
following form:
@T 1 @ @T
C ¼ rKr ð3Þ
@t r @r @r
T
R¼ ð4Þ
q
Rradiation
Tcomponent T∞
Rconvection
where q is the heat flux. If the total thermal resistivity of all heat transfer
types is attained, the temperature change of the composite component is
obtainable.
The heat transfer from the component to the air through convection and
radiation is considered as a parallel model (Figure 4), where Rradiation and
Rconvection are the thermal radiation and convection resistivities of the air,
Tcomponent the surface temperature of the component and T1 the ambient
temperature. The thermal resistivities that are encountered in the filament
winding process are discussed below. The thermal radiation resistivity can
be determined by the following equation [19]:
Tcomponent T1 Tcomponent T1
Rradiation ¼ ¼ ð5Þ
q "b ðT 4 T1
4 Þ
where " is the hemispherical emissivity of the component and b the universal
constant for black-body radiation.
For natural convective flows and a component which is placed
horizontally, the Nusselt number can be calculated by the correlating
equation proposed by Churchill [20]:
d
Rconvection ¼ ð8Þ
Nu
1 1 1
0
¼ þ ð9Þ
R Rconvection Rradiation
with the activation energy E0, the gas constant R (8.314 103 kg mol1
K1) and the Newtonian viscosity 0 of the polymer melt at a certain
temperature Tn.
However, the generalized Newtonian models discussed above do not
attempt to relate the polymer viscosity to its chemical and physical
properties. Williams et al. [22] conjectured that the mobility of the polymer
at temperatures above Tg should be a function of the amount of free volume
in the melt. This concept had been used to describe the viscosity of simple
liquids. The logarithm of the viscosity is taken to be proportional to the
fractional change in the free volume. Other theories of the liquid state
propose a temperature dependence of viscosity that is an Arrhenius-type
formulation. This seems to be a good physical picture of polymer liquids at
temperatures much higher than Tg. The following equation is suggested to
express the viscosity of many polymer systems if more specific values are
unknown:
AðT Tg Þ 17:44ðT Tg Þ
ln ¼ ¼ ð11Þ
0 B þ ðT Tg Þ 51:6 þ ðT Tg Þ
In [23] Williams–Landel–Ferry ‘‘(WLF)’’ constants for specific polymers
are listed.
Stress–Strain Submodel
1 r
"r ¼ r þ
r T ð14Þ
Er E
r 1
" ¼ r þ þ
T ð15Þ
Er E
where Ei and ij are the corresponding direction Young’s modulus and
Poisson’s ratios,
i the thermal expansion coefficients, r and the radial
and circumferential stress and T is the temperature change. To account for
general conditions, both the mechanical and thermal properties may vary
from layer to layer according to the fiber orientation.
The equilibrium equation in the radial direction is:
dr r
þ ¼0 ð16Þ
dr r
d 2u du
r2 þ r k2 u ¼ C1 rT ð17Þ
dr2 dr
Figure 6. Internal stress changes during filament winding process: (a) t; (b) r t.
(a) 8
σθ (MPa) 2
-2
-4
-6
-8
0,074 0,076 0,078 0,080 0,082
Radius (m)
(b) 0,18
0,16
0,14
0,12
0,10
σr (MPa)
0,08
0,06
0,04
0,02
0,00
0,074 0,076 0,078 0,080 0,082
Radius (m)
Figure 7. Radial and circumferential residual stress distributions after mandrel removed
(a) circumferential residual stress ; (b) radial residual stress r .
the internal stress changes of every layer during the filament winding
process. After the mandrel is removed at t ¼ 14,000 s, the radial and
circumferential stress distributions are shown in Figure 7. The measured
experimental data are also shown in it. Larger winding angle generates
larger residual stresses.
MANUFACTURING CONDITIONS
Here, in the practical part, the same conditions are used as in the model.
From this it is clear that the process of filament winding itself has to be
SENSITIVITY STUDY
The aim of the present sensitivity study was to determine the relevant
process parameters that should be investigated more closely and their
influence on the residual stress state. 16 process parameters were identified
in the beginning. This would mean a number of 216 experiments in a full
factorial DOE (design of experiments) multiplied by the number of samples
per experiment. Regarding the time and the material that was used it was
clearly better to effect the study in a fractional factorial concept as proposed
for example by Taguchi [25]. With this design all processing parameters were
respected but only the relevant ones were selected for the further proceeding.
The reduction of parameters is in this case from 16 to 8. In terms of
experiments this means a reduction from 128 to 8. The chosen parameters
have to be varied. Fractional factorial concepts normally operate with two
to four variations of one parameter. In this case, each parameter applies to
two different values. They are assigned to the orthogonal array (Table 3)
that gives the combinations for the tests that have to be performed. If more
values for one parameter should be investigated, the number of parameters
The samples produced with the winding machine have a geometry derived
from the NOL tensile strength ring test samples. This means that the
diameter is the same as for NOL rings, but the width has to be different to
avoid the influence of boundary conditions in the area of residual stress
measurement. Gould [29], for example, showed how to determine the
minimum axial length of the test samples that is required to avoid boundary
influence. From the equation
3ð1 2 Þ Eh
k4 ¼ 2 2
¼ ð19Þ
a h 4Da2
it is easy to determine the k and with the condition that the length L of the
sample must be greater than 6/k. For two open boundaries of a tube, the
noncritical length of the samples can be calculated. As there are strain
gauges being applied, the length of the samples must be increased by the
width of the gauges. The strain was measured simultaneously on the inner
and outer diameter.
The residual stress measuring device consists of a support and diamond
sawing blade for cutting the test rings. The support is designed to prevent
the cut samples from snapping in either an opening or closing direction. The
strain release is affected by slowly opening the support. The strain
measurement is continued during the cutting process, so that any potential
influence of the cutting on the strain measurement is immediately revealed.
Figure 10 shows a picture of the test device designed at IVW.
TEST RESULTS
30
20
90°
10
σθ (MPa)
60°
0
-10
-20
1 2 3 4 5 6 7 8 9 10
Layer
60° Experimental results
90° Experimental results
Theoretical results
Figure 11. Residual stress of test samples and prediction model.
other parameters were the same for both samples: GF/PP material, no
liner, 110 C mandrel temperature, free cooling, 10 layers, and a winding
force of 5 N.
The results are agreeable for the sample with 60 winding angle. They are
within the range of 8–15%. The difference between model and test values,
especially for the 90 version, is most likely caused by the creep occurring
during the production process itself. It is to be underlined that in the present
paper not only is a new model of residual stress presented, but also the
authors showed its application towards a production process that runs on
an industrial scale.
CONCLUSION
A model for the thermoplastic matrix filament winding process and its
implementation in a simulation of the internal residual stresses was
presented. The utilization of the model requires the solution of a system
of coupled differential equations describing the different phenomena. This
solution can be obtained by applying a number of numerical techniques.
Some relevant results are reported in this paper. The model is validated
through experiments. Furthermore, a sensitivity study under production
conditions has shown that the potential of residual stresses can only be
exploited when the temperatures during production are sufficiently
controlled. The necessary equipment has been identified and the imple-
mentation of theoretical knowledge was successfully demonstrated.
ACKNOWLEDGMENT
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