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    ASTM D 2000-06a

    Copyright:

    © All Rights Reserved
    Download as PDF or read online from Scribd
    Flag for inappropriate content
    75 views53 pages

    ASTM D 2000-06a

    Uploaded by

    Felipeandres Lizana Bastias
    ASTM D 2000-06a

    Copyright:

    © All Rights Reserved
    Download as PDF or read online from Scribd
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    of 53
    Designation: D 2000 ~ 06a"? Aly Standard Clas: ication System for Rubber Products in Automotive Applications’ “Tis sandr lsd under the fed designation 12000; the number immedsy folowing the designation indicts the yer of crignal adoption on the eke of revision, the yar of revision. A number in parentheses indicts the year ls apo Supersrigepilon (indies an eit chnge since te lst visio er eappeoval, ‘his specification has been approved for use by agencies ofthe Deparment of Deen er able 6 edtoialy erected in May 2007, 1. Scope L.1 This classification system covers the properties of vul canized rubber materials (natural rubber, reclaimed rubber, synthetic rubbers, alone or in combination) that are intended for, but not limited to, use in rubber products for automotive applications. Nore [This classification system may serve many ofthe needs of other industries in much the same manner as SAE numbered secs Itmust be remembered, howover, that this sysiem is subject fo revision when required by automotive needs is recommended that the latest revision always be used. 1.2 This classification system is based on the premise that the properties of all rubber products can be arranged into characteristic material designations. These designations are determined by types, based on resistance to heat aging, and ‘lasses, based on resistance to swelling in oil. Basic levels are thus established which, together with values describing addi tional requirements, permit complete description of the qué of all elastomeric materials, 13 In all cases where the provisions of this classification system would conflict with those of the detailed specifications for 2 particular product, the latter shall take precedence. [Nore 2—When the rubber products tobe used for purposes where the requirements are too specific to be completely prescribed by this clasi- fication system, iis necessary forthe purchaser to consul the supplier in ‘advance, to establish the appropriate properties, test methods, and sp fication test ini 1.4 The values stated in SI units are to be regarded as standard. "This lation prem is under the nition of ASTM Commitee DIL on Rubber an is th det espnsility of Sobemmmidee D110 on Casio of Riber Compounds ‘Carat efitonepproved Oct. 1, 2005, Pubithed November 2006 Oily approved in 1962 Last previous eon approved in 2006 a © 200006. 2, Referenced Documents 2.1 ASTM Standards: * 1D 395 Test Methods for Rubber Property—Compress Set D412 Test Methods for Valeanized Rubber and Them plastic Elastomers—Tension D429 Test Methods for Rubber Property—Adhesion Rigid Substrates D430 Test Methods for Rubber Deteioration—Dy Fatigue D471 Test Method for Rubber Property—Eifect of Liqui D573 Test Method for Rubber—Deteriortion in an & Oven 1D 575 Test Methods for Rubber Properties in Compress D624 Test Method for Tear Strength of Convention ‘Vuleanized Rubber and Thermoplastic Elastomers 1D 865 Test Method for Rubber—Deterioration by Hea in Ait (Test Tube Enclosure) D925 Test Methods for Rubber Property—Staining of Si faces (Contact, Migration, and Diffusion) D945 Test Methods for Rubber Properties in Compresi or Shear (Mechanical Oscillograph) D 1053 ‘est Methods for Rubber Property—Stiffening Low Temperatures: Flexible Polymers and Coated Fab DIITI Test Method for Rubber Deterioration—Surfs ‘Ozone Cracking Outdoors or Chamber (Triangular Spx mens) 1D 1320 Test Method for Evaluating Rubber Propet: Retraction at Lower Temperatures (TR Test) D 1349 Practice for Rubber—Standard ‘Temperatures f ‘Testing 2 For eferenced ASTM standans, vist the ASTM webs, wows ertset ASTM Customer Service st service@asim rg, For Arial Boot of St ‘Standards volun nfrmmton refer othe standard’ Documest Saenz 108 the ASTM website, cent © AST waters, 180 Bar Hater Di, PO Bat C70, Wes Carson, PA 1042-205, Und Sas 64 fiir D 2000 = 06a Practice for Rubber and Rubber Latices— TABLE 2 Basle Requirements for Establishing Class by Volume ‘Swell jure pesaboadiacaibunchecneniti ~~ eepinuiineeiy i aaniie MTest, Methods for Rubber Propesty—Britileness case aa Flexible Polymers and Coated Fabrics * st Method for Rubber Property—Durometer i ti TABLE 3 Meaning of Sutfic Letters fi engineer in the selection of practical, commer- 2 fable rubber materials, and further © provide « —Seetsiw __Tet Rome specifying these materials by the use of a simple i © Gamr Nese Resse Classification system was developed to permit the B_ Somes tas ensance Of descriptive. values for future rubber materials Ell Rete Acc) Teorganization of the classification systom fb Fad Renros On avian © crenperte Rese & Tarratanoe fn Recrasttance Sas sane i) Formby Reserce ‘prefix letter “M” shall be used to indicate that the ‘ =a ‘system is based on SI units. e ‘Staining Resistance: helene Cot ous not prefised by the Kier M refer a8 eae F_ Revered eqdremer wih sa be seed nt h-pound unit. This was published in ber matsials shall be designated on the basisof ype _TABLE 4 Sufix Numbers to inacateTempersture of Test ) and class (oil resistance), Type and clsss are Second Su ys phate Suh: Regurements ene Temps 18.0, BR ER EO.G, * a K %0 250 ° Bs ‘more than +15 points after heat aging for 70 h at 8 = te temperature. The temperatures at which these % ta lr shall be tested for determining type are listed in Table 5 5 ‘0 3 70 2 a in IRM 903 Oil (most tables were originally devel- 1 3 ASTM Oil No. 3) after 70-h immersion at a F c = wre determined from Table 1, except that a maximum 2 rl cof 150°C (the upper limit of oil stability) shall be 3 =a ‘of swelling for each class are shown in Table 2 4 = é os BLE 1 Basic Requirements for Establishing Type by 3 3 ‘Temperature ° os 0 os " a 2 =o hee wat 8 pmblent temperature nto coc of olor testing. 44.1 ASTM No. 1, No. 2, and No. 3 Oils have been replaced by IRM 901, 902, and 903 Oils, respectively, under Practice D 5964. These oils are similar but not identical to ASTM No. 1, No. 2, and No. 3 Oils. nexommooa> ily b 2000 - o62* 44.2 Substiwability of IRM 901, 902, and 903 Oils for ASTM No. 1, No. 2, and No. 3 Oils has not been established, as their swelling characteristics are different and may affect compound classification, Nore 4—The selection of type based on eat resistance is undestond to ‘be indicative ofthe inherent heat resistance that ean be normally expected {rom commercial compositions. Likewise, choice of class is based on the ‘ange of volume swell nonmally expected from such commercial compo- sitions as established by type. The fact tha a type and class of material is listed in Table 6, under Basic Requirements, indicaes that materials that ‘meet these requirements for heat and ofl resistance are commercially availabe. 45 The letter designations shall always be followed by a three-digit number to specify the hardness and the tensile sirength—for example, 505. The firs digit indicates durometer hardness, Type A, for example, 5 for 50 * 5, 6 for 60 + 5. The next two digits indicate the minimum tensile strength—for example, 05 for 5 MPa, 14 for 14 MPa. Correlation of available materials for desired harness and tensile strength is obtained through the elongation values in Table 6. See 7.2. 5. Grade Numbers, Suffix Letters, and Number 5.1 Grade Numbers—Since the basic requirements do not always describe sufficiently all the necessary qualities, provi- sion is made for deviation or adding requirements through a system of prefix grade numbers. Grade No, 1 indicates thet only the basic requirements are compulsory, and no suslix requirements are permitted, Grades other than No. 1 are used for expressing deviation or additional requirements and are listed as “Available Suffix Grade Numbers” in the last column under Basic Requirements in Table 6. A grade number is, written as a material prefix number preceding the letters for type and class (see 9.1). Grade No. 1 is always an available suffix grade number, and thus is not referenced in the last column of each basic requirement table, 5.2 Sufix Letters—The suffix letters that may be used, together with their meaning, appear in Table 3. 5.3 Sufix Numbers—Each suffix letter should preferably be followed by two suffix numbers (see Note 6 in 8.1). The frst suffox number always indicates the test method; time of test is part ofthe method and is taken from the listings in Table 5. The second sufi number, if used, always indicates the temperature of test and is taken from Table 4, Where three-digit numbers are required, they are separated by a dash—for example: —1 B410; FI-I1 6. Composition and Manufacture 6.1 This classification system is predicated upon mate furnished under a specification based thereon being manu tured from natural rubber, reclaimed rubber, synthetic rub alone or in combination, together with added compound ingredients of such nature and quantity as to produce Vules zales that comply with the specified requirements. All mater and workmanship shall be in accordance with good comm cial practice, and the resulting product shall be free of por. areas, weak sections, bubbles, foreign matter, or other defe affecting serviceability 6.2. Color—With the exception of FC, FE, FK, snd « ‘materials, the values in the material (ables are based on ble compounds and comparable values may not be availeble color. 7. Basic Requirements 7.1. The basic requirements for physical properties specif in Table 6 are based on values obtained from stand laboratory test specimens prepared and tested in accord with the applicable ASTM test methods. Test results fn specimens prepared from finished products may not dupic, values obtained from standard test specimens. Nore 5—When standard test specimens ae cut from fished pa accordance with Practice D 3183, a deviation tothe extent of 105% tem strength snd elongation values only) is permisble when ago upon bythe purchaser andthe supple. This deviton is perisile because of the recognized eels of kiting, esi, and bung 02 material whes test specimens ae prepare from ithe ps ads forteasileseengh and elongation. When diferences dus tothe mato: processing ort the dificult in obtaining suitable test specinens fron finished part ars, the purchaser andthe supplier may agree on ce deviations. This ean be done by comparing resus of sania specimens with those obtained on seta pat 7.2 The available materials are listed in the appropi material section of the table, giving each hardness and tens strongth with its appropriate elongation value. Also, these i repetition of the values for the basic heat and cil as requirements for the material resulting from the assignment type and class. In addition, values for compression set, n mally a basic requirement to ensure proper vulcanization, specified. 73 Unless a sullix requirement is used 10 override existing basic requirement, the basic requirement applies. * Tens values ar shown as pounds per squelch in Tle 6 fo infor ony, ‘TABLE 5 ASTM Tost Methods Basie Requtements ‘Fie Sule No, ‘Sue Ltr “enste Srengin, Elongaton| Durometr Horne “ype Sut A, Host Raster dec" e210 573,708 Dees, 70m | 66s, 168n ava, 168 | D573, 1000h | D285, 1000 n Ap D 2000 = 062" TABLE 5 Continued i ee sae] 1 2 3 ‘ 5 . 7 e fo ‘ba06, 22h, |0306, 70h, | D305,22n, | 0508, 70m, | 0205, 100, | O3B5, 1000 Maed 8, |Maods,” | Metres,” | Weihos 8,” | Memos 8, "|r, Mehed 8 Pao} le pled ples id led pum, | osm pa - 4 oxne* | woater zone ‘exposure, exposure, ated Nathod bers, |osis, Mabe A | Hatred 8 parti |oariime —foarsig |osritea | 0471, eae sor = Joo2ci.e® — | aosone* | ooror,2 | a2 oi," mn 70h mr wah ‘ean pari, | Dart, Service | Oise Frid | spectay | Ne | dosnt toi" | ntabee, on |70n art, Refer | D471, Rot | 0471, Rote | D471, Rater | 0471, 85 Vol |. ‘ence FuBlA, | ence Fusl8, | onea Feat C, | ence Feel D, | une ercent 70h. on mn mn Felerence Fuel Pius 45 volume Denatured Ethan, 70% ~ |oars.o% |oarteqa |. : tea Wate, | Pans by Tone | Volume Dismed Wotar Reagent Grade Etytone ial, 70 peter, | D1068,smin, [ozts7, |v sa29,381 | 01920, 304 | 0 1088, 5 min, : Matned A | TTs. Tye Ton | Moted A | mm co, 69% | mm do, 50% 932,3min | oT 332,22 | elongation, | elongeten, rovacion” | ravacson Soxmn — |so%mn = |osraon [e,coe |. a es = [pase | 0420, ba, = 7 fi Matoss [Matos | Method e az, | Das, ond mado |. etal 5 MatesA | Netoan | ater ‘wulesrizaten! Chamber expobus mathod 6 Tesi Method D 17%, ed 0 1171, Weather Test, 6 wooka duration Tot rea and tine of ear ob egred upen by the purchaser and the menutactrer Stone charter exposure method of Test Mebiod D 1171, Method B, out of supply of Ill S01, FM 802, en FM C3 Ol onto he come at this ime Is Penreco, 4426 East Washington Bie, Los Angles, CA 76 (Sette by, . Caro ne, PO. Boe $805, Teron, NI O8686-0008), ‘aro ef cematve suppl, poate provide inarnatio fo AST Inematonal Heacquavter. Your comments wl resive crt consdoratin at 2 Teaponsie tecnica commie,” which yeu may ater. ‘cure of suns of Serco Fhid 101 (vein as Andersol 74) known tothe commits st his time is Hills AG Divison, PO. Box 2, Tuner Plco, 08854, te she be usd. Voume increas by vale splcemant mathe, cop aohal dp ote. When detemiring changes in ens eng, lonaton, ht ube fo bo hl ster specimens ere mmessd. Osterman tobe fade silt 30 in. Cec a sled watar, acetone ep tobe omits. by volume of dtilodwstr and reagent grado ebvlano ea. Vole Increase by cspacomont method, except coh ap emit. When dering rls etrength, elongation, endharenes, et ube bo cul ator epcimone are inveresd.Dotrminatin tebe made ster $0 rin. Coon ilo wate, emits values used fo dfn @ curve for Cami cal mates, See example n 82. a Af]. 2000 = 06a"* 8, Suffix Requirements 8.1 Suffix requirements shall be specified only as needed to define qualities necessary to meet service requirements. These suffix requirements are set forth forthe various grade numbers, ‘Sufix letters and suffix numbers describing these suffix re- ‘quirements may be used singly or in combination, but not all sufi values available for a given material need be specified. [Nore 6—Examples of the se of sufix letters and numbers would be |Al4 and BOS. Sufix A (Table 3) stands for heat resistance, Suix 1 (Table) specifies thet the test be run in accordance with Test Method 1575 for 70h, and Sufix 4 (Table 4 indicates the temperature of test as 100°C. Similarly, Sufix EO34 indicates resistance in TRM 903 Oil in accordance with Test Method D471 for 70 hat 100°C. 8.2 Basic requirements are always in effect, unless super seded by specific suffix requirements in the “line call-out.” 83 Use of Test Methods D 1053 as a Suffix Requirement: When specifying an F2 or F6 requirement, the line specifica- tion must define which T-values are required, along with the ‘maximum allowed temperature. Test Methods D 1053 proper- ties must then be less than or equal to the specified temperature for the corresponding T-valve. 9, Line Call-Outs 9.1 Aline call-out," which is a specification, shall contain: the document's names, the prefix letter M, the grade number, the material designation (type and class), and the hardness and tensile strength, followed by the appropriate suffix require- ments. Following is an example of a “line call-out” or specification: ASTI 02000 M28C 507 At4 EOS |ASTHD 2000 « Stands Cxgeizaton and Document Number asic Requirements: quirements are in St Unis plebla Sut Grace. stra Typ based on Terpertue Resistance. star Class based on IAM 903 Ol lure Swe NOs Typo A Hardness (.e, 5 neat rqurerent fs $0. (7= Tonle Seng (Hin ne call out cates wns rein MPa) os Sue Atte A= Heat Rastanes; 1 - 0573, 70 £004 - EO ~ Fuld Ractnce in Ois and Lubin; 3 7, IR 203 04, 70% 4 100" In this example, basic requirements for heat resistance anj fiuid resistance are superseded by suffix requirements, Ho, ‘ever, the basic requirement of 80 % for compression set, vic is not included as a suffix requirement, is not superseded ay, therefore shall be met as specified in Table 6. 9.2 Incorporation of Test Methods D 1053 F2 of F6 su into a Tine call out. ‘ASTI D 2000 MSHKBIO A1-10 B97 EO78 24; 21 ‘10:28, 7100-37), In this example the numbers following F2 represent the vs, desired T-values (12, TS, THO, T50, and T100 are typical). y this case TS, THO, and TI00 are the desired “T's” to b reported, This example has an “IV denoting that all data is metric, so the T-values are represented in degrees Centigrae (maximum temperature), ASTM D 2000 NGHKBIO AI-10 B37 EOTG 21:21 = FS (12-142) In this example the numbers following F6 represent TS, Ti ‘and the maximum degrees of separation allowed between T and TS. This example has an “M" denoting that all data is in metric, so the T-values are represented in degrees Centigate (maximum temperature). 10, Test Methods 10.1 The applicable test methods are listed in Table 5. 111, Sampling and Inspection TIAL A lot, unless otherwise specified, shall consist ofall products of the same material submitted for inspection atte same time. 11.2 When proof of conformance with a specification bas! con this classification system is required, the supplier shl upon request of the purchaser atthe time of ordering, furisha sufficient number of samples to permit the performance of it required tests, Test specimens shall be prepared as prescil in 71. The samples shall be warranted to have equivalent cue and to be from the same run or batch of compound used in he Jot 25, Gly b 2000 - 06a" TABLE 6 Basic and Supplementary (Suffix) Requirements for Classification of Elastomarie Matoriale arenas Sa egulenanie Tiras Sree mn Wile Fat ga Tet ‘Ol Foran, Tot Conpeain Sa, Tea Alans Se rareahmh_ ofmen, —MehovOG,Tohat shes Dere mses on Meteo Sue rue wa fore Tonio meena tes Neve Ame eo ae y es at = oer eo i 7 we 0 a4 ote fe at Qe a re es sc HaEECt ee tte oe Et 3 oa 2 : mo 2 a ee) be ee es ois £8 ua am eS oes a8 Xe ae a 3 owe 2 $0 oe i oo a 8 180 ‘300 Grange nuts elonge- ‘Compreseion set, 33 10 1450, 350 “tion 50 %6 max - No requirement 50% max 2.3): HB hte ameter 286. wv ja = ‘ness, +18 points. a x = @ 1 23. a Moa 2 fee oe = om i See 2 Me oe oo ae mat So 4 @ & Re 3 tw + st ow fe oo ae dee ee fee 3 7 2 + oe : 2 a 2 Ally D 2000 - 06a" TABLE 6 Continued BA WATER Grage Grade Gade ~——

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