Is 248-1987 Ra 2021

e Standard provided by BIS via BSB Edge Private Limited to Hind Heat Treatment & Testing Hou
Kota(gcb629@gmail.com) 157.38.136.101 [for non-commercial use only].

IS : 248 - 1987
xxxx)
( Reaffirmed 2003
Indian Standard 2010
(Reaffirmed!2015)!
SPECIFICATION FOR (Reaffirmed 2020)
SODIUM BISULPHITE,' TECHNICAL (Reaffirmed 2021)
(SODIUM METABISULPHITE)
(FourJh Revision)
First Reprint SEPTEMBER 1991
UDe 661'833'523
@ Copyright 1988
BUREAU OF INDIAN STANDARDS

MANAK BHAVAN, 9 BAHADUR SHAH ZAFAR MARG
NEW DELHI 11 0002
Gr 3 January 1988
IS : 248 - 1987
Indian Standard
SPECIFICATION FOR
SODIUM BISULPHITE, TECHNICAL
( SODIUM METABISULPHITE )
(Fourth Revision)
Inorganic Chemicals ( Misc ) Sectional Committee, CDC 3
Chairman Representing
DR M. S. VAlDYA Dharamsi Morarji Chemical Co Ltd, Bombay
M.mbers
SHRI R. S. Vy A8 ( AIllTllate to
Dr M. S. Vaidya )
Dn A. N. BHAT Hindu5tan Lever Ltd, Bombay
DR B. S. MOULIK ( Alt,rnat, )
DR R. M. BHATNAGAR Projects &. Development India Ltd, Sindri
SHRI R. C. BHATTACHARYA Directorate General of Technical Development,
New Delhi
SHRr KULTAR SINGH ( Alt(rnate )
SHRI S. N. BHATTACHARYA Tala Chemicals Ltd, Bombay
SHRr S. GANAPATlIY ( Alternate)
SHRI]. C. BOSE Indian Oxygen Ltd, Calcutta
SHRI A. K. DAB ( Alt.rnall)
CONTROLLEH GENERAL Indian Bureau of Mines, Dhanbad
SHIn V. K. ] AIN ( Alt.rna/,)
SHRT S. DAB Geological Survey of India, Calcutta
SItRr YUDlIISTlJIR ( Alternate)
DR A. V. DEO Associated Cement Companies LId, Ecmbay
SlIRI C. H. PAGE ( Alterllate )
DR S. GHOSH In personal capacity ( 17-A, 'F' Block, Sak,t, Malviyo
Nagar Extellsioll, New Dtlhi )
DR S. H. IQBAL National Chemical Laboratory ( CSIR ), Pune
SlIRI V. B. KBA~A Directorate General of Supplies & Disposals,
New Delhi
SHRI N. K. KAUSHAL (Alternat, )
SlIRI N. J. KJKANI Sarabhai M. Chemicals, Vadodara
SHRI H. H. KAVARANA ( Alternate)
SHRI P. R. MALHAN Development Commissioner, Small Scale Industries,
New Delhi
SHRl R. MUKHOP.~DHYAY (Alternate)
( COlltinued on page 2 )
© CO/Jyrighl 1988
BUREAU OF INDIAN STANDARDS
This publication is protected under the Indiall Copyright Act (XIV of 195i ) and
reproduction in whole or in part by anv means el'cept with written permission of the
publisher shall be deemed to be an infringement of copyright under the said Act.
IS : 248 • 1987
( Continued from pagl 1 )
M",w,rs ReprlSenting
Dn ANIL PANDIT Deepak Nitrite Ltd, Vadodara
SHKI C. S. NAGAR ( Alternate)
Da P. G . PruDHAN Golden Chemicals FVI Ltd, Bombay
SHnI T. S. KALAHASTY ( Alt,rnate )
SIlRI A . K. RAO Shriram Foods & Fertiliser Induotries, New Delhi
SHRI A. K. MEHRA ( Alternate)
Dn S. B. RAY Ministry of Defence ( DGI )
SHRI P. DAS ( Alternate)
SIlal B. K. SACHAR Ministry of Defence ( R&D)
SHRI A. D. GUPTA ( Alternate)
SHRI C. R. SANTHANAKltISIlNAN Travancore Chemical & Manufacturing Co Ltd,
Mettur Dam
SHRI K . V. MAN! ( Alternate)
SHRI C. P . SKARDA Shri Ram Institute for Industrial Research. Delhi
SHR! L . B. SRIVASTAVA ( Alternate)
Dn V . S. SUBRAMANIAN R egional Research Laboratory ( CSIR ), Hyderabad
DR MORl) ZAFAR JAf.lIL ( Alternate)
SHR! N. C. THAKKAR Indian Chemical Manufacturers' Association,
Calcutta
SHm S. C. THAKUR Indian Oil Corporation Ltd ( Refineries & Pipelines
Division ), New.Delhi
SHIt} M USAFIR SINOH ( Alternate)
Sum SATISEI CHANDER, Director General, BIS (Ex-officio Member )
Director ( Chern )
S'efetary
SHaI M. BAKSHI GUPTA
Deputy Director ( Chern), BIS
Auxiliary Chemicals Subcommittee, CDC 3 18

Cona.ner
SHRI J. C. BOSE Indian Oxygen Ltd, Calcutta
M,mb"s
SHRI S. BALASUBRAMANIAN Tamil Nadu Chemical Products Ltd, Madras
SUIH K. SUBRAMANIAN ( Alternate)
DR R. M . BHATNAGAa Proj ects & Development India Ltd, Sindri
SHRI A. T. BRAHMBHATT Kalali Chemicals L td, Vadodara
SHR! P. M. SAP-AlVA ( Alternate )
SHm P. C. GOPINA1.'H Travancore-Cochin Che micals Ltd, Udyogamandal
SHRI C . N. G. NAIR ( Alternale )
SHRI A. R. J A'l'AN!A All India Cast Iron Powder Manufacturers
Association, Ahmadabad
Da ANIL PANDIT Deepak Nitrite Ltd, Vadodara
SHmC. S. NAGAR ( Alternate)
Dn P. G. PRADHAN Golden Chemicals PVI Ltd, Bombay
SHRI T. S. KALAHASTY ( Alternate)
( ContinUld on pag, 12 )
2
Standard provided by BIS via BSB Edge Private Limited to Hind Heat Treatment & Testing Hou
IS : 248 - 1987
Indian Standard
·SPECIFICATION FOR
SODIUM BISULPHITE, TECHNICAL
( SODIUM METABISULPHITE)
( Fourth Revision)
o. FOR EWOR D
0.1 This Indian Standard ( Fourth Revision) was adopted by the Bureau
of Indian Standards on 28 May 1987, after the draft finalized by the
Inorganic Chemicals ( Mise) Sectional Committee had been approved by
the Chemical Division Council.
0.2 Sodium bisulphite ( sodium metabisulphite ) is used in the prepara-
tion of dyes, intermediates, organic chemicals, perfumery; in the digestion
of wood pulp, in leather tanning, as an antichlor and mordant in textile
industry. It is also used as food preservative, in photography as reducing
agent, in copper and brass plating, as colour preservative for pale crepe
rubber, general antiseptic, as pesticides and a source of sulphur dioxide.
0.3 This standard was first issued in 1954 and subsequently revised in
1961, 1971 and 1978.
0.4 This stand~rd has been revised again deleting the photographic
grade as a separate Indian Standard On this item is being formulated by
Photographic Materials Sectional Committee. A new spectrophotometric
method has been prescribed as an alternate method for the determination
of iron.
0.4.1 This standard, however, does not cover its application as food
preservative and pesticides.
0.5 For the purpose of deciding whether a particular requirement of this
standard is complied with, the final value, observed or calculated,
expressing the result of a test or analysis, shall be rounded off in accor-
dance ,,·itl! IS : 2-1 <160*. The number of significant places retained in
the rounded off value should be the same as that of the specified value
in this standard.
-Rules for rounding off numerical values ( revised ).

IS • 248 - 1987
1. SCOPE
1.1 This standard prescribes the requirements and the methods of sampl-
ing and test for sqdium bisulphite ( sodium metabisulphite ),
2. REQ.UIREMENTS
2.1 Description - The material shaH be dry, white or cream coloured
powder, free from extraneous matter and having a faint smell of sulphur
dioxide gas.
2.2 The material shall also conform to the requirements laid down in
Table I, when tested in accordance with the methods prescribed in
Appendix A,
TABLE 1 REQUIREMENTS FOR SODIUM BISULPHITE
SL CHAR ACTERISTIO REQUIREMENT METHOD OJ!' TEST
No, ( REF TO CLAUSE No,
IN ApPENDIX A )
(1) (2) (3) (4)
i)Purity ( as SO. content), percent by 60'0 A-2
mass, Min
ii) pH of 5-percent solution 4'5 to 5'5 A-3
iii) Matter insoluble in water, percent 0'1 A-4
by mass, Max
iv) Iron ( as Fe ), percent by mass, Max 0'02 A-5
v) Heavy metals ( as Pb), percent by 0'1 A-6
mass, Max
vi) Appearance of solution To pass test A-7
3. PAC~ING AND MARKING

3.1 Packing - The material shall be suitably packed taking care that
it does not come in direct contact with iron container either during
storage or in transit.
3.2 Marking -:- The containers shall be marked with the name of the
material; name of the manufacturer and recognized trade-mark, if any;
net mass and the year of manufacture.
3.2.1 The containers may also be marked with the Standard Mark.
NOTE - The use of the Standard Mark is governed by the provisions of the Bureau
of Indian Standards Act, 1986 and the Rules and Regulations made thereunder. The
Standard Mark on products covered by an Indian Standard conveys the assurance
that they have been produced to comply with the requirements of that standard under
a well-defined system of inspection, testing and quality control which is devised and
supervised by BIS and operated by the producer. Standard marked products are
also continuously checked by BIS for conformity to that standard as a further
safeguard. Details of conditions under which a licence for the use of the Standard
Mark may be granted to manufacturers or producers, may be obtained from the
Bureau of Indian Standards.
IS : 248 - 1987
4. SCALE OF SAMPLING AND CRITERIA FOR CONFORMI1'Y
4.1 The scale of sampling and criteria for conformity of the material to
the standard shall be as prescribed in Appendix B.
APPENDIX A
( Clause 2.2 and Tab/, 1 )
METHODS OF TEST FOR SODIUM BISULPHITE
A-I. Q.UALITY OF REAGENTS
A-l.l Unless specified otherwise, pure chemicals and distilled water
( see IS : 1070-1977* ) shall be used in tests.
NOTE - 'Pure chrmicals' shall mean chemicals that do not contain infuri"ties
which affect the results of anal} sis.
A-2. DETERMINATION OF PURITY OF SODIUM BISULPHITE

A-2.l Realents
A-2.1.l Starch Solution - Take 3 g of starch and make a paste with
cold water. Pour the paste into I litre of boiling water and add 10 ml of
one percent salicylic acid.
A-2.1.'Z Potassium Iodide - crystals.
A-2.1.3 Iodine Solution - approximately 0'1 r\. Dissolve in a 1 000 ml
volumetric flask about 12'5 g of resublimed iodine in a concentrated
SQlution of ~5 g of potassium iodide. Make up the solution to 1 COO mI.
A-2.1.4 Standard Sodium Tlziosulphale SolutioT! - 0·1~. Dissolve about
25 g of crystallized sodium thioslIlphate in I 000 1111 of recently boiled
water in a volumetric flask. Standardize the solution against standard
potassium dichromate or freshly standardized iodine solution, using
towards the end of the reaction, starch solution as indicator. The solut;on
shall be prepared freshly.
A-2.2 Procedure - Weigh accurately about 0'2 g of the material and
add it to exactly 50 ml of standard iodine solution. Allow to stand for 5
minutes, ad d I ml of hydrochloric acid and titrate the excess of iodine
with standard sodium thiosulphate solution I using starch solution as
indicator. The end point of the reaction being indicated by the disappear-
ance of blue colour. Carry out a blank titration with same amounts of
reagents but without sample .
• Specification for water for general laboratory use ( set."d r.,·is;on ).
5
IS : 248 • 1987
A-2.3 Calculation - Calculate the percentage of sulphur dioxide

( S02 ) on the basis that 1 ml of 0'1 N iodine solution is equivalent to
0'003 203 g of sulphur dioxide ( S02 ).
Purity ( as S02 content ), ( VI _ V) ]I
percent by mass = 3'203 X M
VI = volume in ml of standard thiosulphate required for blank,

V = volume in ml of standard thiosulphate required for test,
N = normality of standard thiosulphate solution, and
M = mass in g .ofthe material taken for the test.
A-3. DETERMINATION OF pH
A-3.1 Apparatus
A-3.1.1 pH Meter - Equipped with a standard calomel electrode and
a glass electrode.
A-3.2 Procedure - Dissolve 5 g of the material in 100 ml of carbon-
dioxide-free wafer. Determine the pH by pH meter.
A-4. DETERMINATION OF MATTER INSOLUBLE IN WATER
A-4.1 Apparatus
A-4.l.l Gooch Crucible or Sintered Glass Crucible - Porosity No.4.
A-4.2 Procedure - Weigh accurately about 50 g of the material and
dissolvd in 300 ml of water. Filter through the tared Gooch crucible or
tared sintered glass crucible and wash well with water. Dry at
105 ± 2°C to constant mass.
A-4.3 Calculation
~atterinsoluble in water, 100 x m
percent by mass
M
where
m = mass in g of the residue.obtaineci, and
M = mass in g of the sample taken for the test.
A-5. TEST FOR IRON

A-5.0 The following two methods are prescribed:
a) Colorimetric method, and
b) Spectrophotometric method.
6
IS : 248 - 1987
A-5.1 Colorimetric Method
A-5.1.1 Principle - Iron is determined colorimetrically by visual com-
parison of the colour in Nessler cylinders using potassium thiocyanate.
A-!j.l.l.1 Nessler cylinders - 50 ml capacity.
A-5.1.2 Reagents
A-S.1.2.1 Ammonium persulphate - solid.
A-S.l.2.2 Concentrated hydrochloric acid - See IS : 265-1976*.
A-S.l.2.3 Butanolic potassium thiocyanate solution -- Dissolve 10 g of
potassium thiocy;mate in 10 mlof water. Add sufficient n-butanol to
make 100 ml and shake vigorously until solution is clear.
A-S.1.2.4 Standard. iron solution - Dissolve 0'702 g of ferrous
ammonium sulphate [ FeS04' ( NH')2 S04.6H20 ] in water containing
10 ml of dilute sulphuric acid ( 10 percent) and dilute to one litre in a
volumetric flask. One millilitre of the solution contains 0'] rug of iron
(as Fe). Further dilute 100 rul of the solution to 1 000 m!. One millilitre
of the diluted solution contains 0'01 mg of iron ( as Fe ).
A-5.1.3 Procedure - Dissolve 1'00 g of the sample in 30 ml of hot
water, add 5 ml of hydrochloric acid and evaporate to dryness on a steam
bath. Add 15 ml of hot water and 2 ml of hydrochloric acid and
evaporate again to complete dryness. Dissolve the residue in 10 ml of
water and transfer to a beaker. Add) ml of hydrochloric acid, about
30 mg of ammonium persulphate, heat to hoiling, cool and transfer to a
Nessler cylinder. Add 15 ml of butanolic potassium thiocyanate. Shake
vigorously for 30 seconds and allow the two layers to separate. For
control test, take 2 ml of standard iron solution and repeat the test as
above.
A-5.1.3.1 The limit prescribed in TabJe 1 shall be taken as not hav-
ing been exceeded, if the red colour produced in the butanolic layer of
the sample solution is not more intense than that produced in the control
test.
A-5.2 Spectrophotometric Method
A-S.2.0 Outline of the Method - Iron is re:luced to ferrous state by
thioglycollic acid and then trea~ed with excess of ~mm?nium hydro:cide.
The intensity of the resultant pINk coloured complex IS measured III a
spectrophotometer at 535 nm at pH 10.
A-5.2.1 Apparatus
A-S.2.1.1 Any suitable spectrophotometer .
• Specification for hydrochloric acid ( second rlvision ).
7
IS : 2flS • 1987
A-5.2.2 Reagtnts
A~5.2.2.l Dilute sulphuric acid - 10 percent ( viI) ).
A~S.2.2.2 Standard iron solution - Weigh 0'702 g of ferrous ammonium
sulphate [FeS04' ( NH4 )2 S04· 6H 20] and dissolve in 10 ml of dilute
sulphuric acid. Dilute with water to make up the volume to I 000 ml.
Transfer 10 ml of this solution and again dilute with water 10 make up
the volume to 100 m\. One ml of this solution is equivalent to 0'01 mg
of iron ( as Fe ).
A-S.2.2.3 Concentrated hydrochloric acid - See IS : 265-1976*.
A~S.2.2.4 Dilute ammonium hydroxide - Approx 6 N.
A-S.2.2.S Thioglycollic acid AR (SH.CH2COOH) - 10 percent
( V/l 1 ).
A·5.3 Procedure - Weigh about 10 g of the sample, dissolve in about

75 ml of water. Add one millilitre of concentrated hydrochloric acid and
boil for two minutes. Cool to 15°C and add 10 ml of 10 percent thioglycollic
acid solution. Add dilute ammonium hydroxide solution drop by drop
till pale pink colour appears keeping the tern perature of the solution below
15°C. Add one millilitre more of dilute ammonium hydroxide solution to
bring to pH about 10. Dilute to 100 ml in a standard volumetric flask.
Read the intensity of the colour in a spectrophotometer using 535 nm
wavelength. Note down the reading. Run a blank on all the reagent~
following the above procedure, Subtract this reading from the reading
obtained with the sample. Let this be A.
A-5.3.l Prepare a series of standard iron solution by taking 2, 5,7, 10,
15 and 20 ml of standard iron solution. Subject them to above procedure
and note down the readings. Plot a standard curve for readings obtained
against concentration of iron ( as Fe ).
A·5A Calculation
Iron ( as Fe ), percent by
mass
where
A = mg of Fe from the calibration curve, and
M = mass in g of prepared sample taken for test .
·Specification for hydrochloric acid ( se&ond rez-iJiDn ).
8
IS. 248·1917
A-6. TEST FOR REAVY METALS

A-6.1 Apparatu.
A-6.1.1 Nessler Cylinders - 50 ml capacity.
A-6.2 Reagent.
A-6.2.1 Acetic Acid - approximately 33 percent (mlv ).
A-6.2.2 Dilute Ammonium Hydro~ide Solution - approximately 10 percent
( plv ).
A-6.2.3 C01/£enJrated H)'droch/oric Acid - See IS: 265-1976*.
A-6.2.4 Standard Lead Solution - Dissolve 1'60 g oflead nitrate 1n water
and make up the solution to 2 litres in a volumetric fla.sk. One milliIitre
of the solution contains 0'5 mg of It;ad (as Pb). Further dilute 100 ml of
the solution to I 000 ml. One milliIitre of the diluted solution contains
0 '05 mg of lead ( as Pb ).
A-6.2.5 Sodium Sulphide Solution - 10 percent ( m/p ), freshly prepared.
A-6.3 Procedure - Dissolve 4'00 g of the sample in 20 ml of hot water.
Add 6 ml of hydrochloric acid and evaporate the contents nearly to
dryness on a water bath. Add 15 ml 01 hot water, 3 ml of hydrochloric
acid and evaporate again on the water bath. Finally heat for '1 hour at
150°C. Dissolve the residue in water, filter and make up the filtrate to
50 ml in a volumetric flaSk.
A-6.3 .1 Pipette into a Nessler cylinder 12'5 ml of the sample solution,
.. ml of standard lead solution and I ml of acetic . acid. Add 2 drops of
sodium sulphide solution and make up to the mark with water. Mix well.
A-6.3.1~1 To another Nessler cylinder add the remaining 37'5 ml of
the sample solution and 1 ml of acetic acid. Add 2 drops of sodium
sulphide solution and make up to the mark with water. Mix well.
A-6.3.2 The limits prescribed in Table I shall be taken as not having
been exceeded if the colour produced in the second cylinder is not more
intense than that produced in the first.
A-7. APPEARANCE OF SOLUTION
A·7.1 Dissolve 20 g of the material in a little quantity of water and make
up the volume. to 100 ml. The solution shall not have more than a pale
yellow colour and shall be free from extraneous impurities other than
slight flocculence.
·SyecificatioD for hydrochloric acid ( ,u"nd,.1fIisiora ).
9
IS I 248 - 1987
APPENDIX B
(ClauSt 4:1 )
SAMPLING OF SODIUM BISULPHITE
B-1. GENERAL REQUIREMENTS OF SAMPLING
B-I.O In drawing, preparing, storing and handling test samples, the
precautions given in B-l.l to B-1.7 shall be observed .
B-l.l Samples shall not be taken at a place exposed to weather.
B-l.2 Precautions shall be taken to protect the samples, the material
being sampled, the sampling instrument and the containers for samples
frOm adventitious contamination. .
B-I.3 To draw a representative sample, the contents of each container
selected for sampling shall be mixed thoroughly by suitable means .
B-l.4 The samples shall be placed in suitable, clean, dry and air-tight
opaque glass or plastics containers.
B~I.5 The sample containers shali be of such a size that they are almost
completelY filled by the sample.
D-l.6 Each sample container shall be sealed air-tight afl'er filling and
marked with full details of sampling, the date of sampling and the year
of manufacture.
B-l_7 Samples shaH be stored in such a manner that the temperature of
the material does not vary unduly from the normal temperature.
B-2. SCALE OF SAMPLING

B-2.1 Lot - All the containers in a single consignment of the material
drawn from a single batch of manufacture shall constitute a lot.
D-7.1.1 Samples shall be tested from each lot for ascertaining the
conformity of t he material to the requirements of the specification.
B-2.2 The number ( n ) of containers to be chosen from a lot depends on
the size of the lot ( N) and shall be · in accordance with coli and 2 of
Table 2.
B-2_3 The containers to be selected for sampling shall be dra \\'n at
random from the lot. For randdm sampling procedures, guidance may
be obtained from IS : 4905-1968·
·Methods for random sampling.
10
IS t 241 .. 1987
TABLE 2 SCALE OF SAMPLING OF CONTAINERS

( C1Qru, B-2.2 )
LOT SIZE NUMBER OF CONTAINERS

TO BE SELECTED IX THB
SAMPLE
(N) (II)
0) (2)
Up to 50 3
51 to 100 4-
101 to 300 5
301 and above 7
B-3. PREPARATION OF TEST SAMPLES

B-3.l Draw, with an appropriate sampling instrument, 50 g of sodium
bisulphite from different parts of each container selected. This portion
shall be transferred to suitable sample container. From each of the
sample containers approximately equal quantities of the material shall be
taken and mixed together to give a composite sample weighing about
100 g. The remaining material in each of the sample container is termed
as individual sample.
8-4. CRITERIA FOR CONFORMITY
B-4.l Test for purity of the material shall be conducted on individual
samples. The lot shall be considered as conforming to the specification
if all the individual samples pass the test.
B-4.2 Tests for all other characteristics shall be carried out on composite
sample. The lot shall be declared as conforming to the specification
if the test results on the composite sample satisfy the corresponding
requirem~nts.
11
IS : 2<18 • 1987
( Continrml from ~a" 2 )
M,mbrrs R'i"'sInti"g
SHIn R. R. R .w Waldies Ltd, Calcutta
SHRI S. K. BARAT ( Alllrnat, )
DR H. C. SHAH :3 K Chemical Co, Thane
SHRIMATI K. H. SHAH ( Allernal,)
SHRI S. R. SINGH Development Commissioner, Small Scale Industries.
New Delhi
SHRI J. C . PASRIJA ( Alternale)
SIIRI S. S. SINGHANIA Forum of Small Scale Entrepreneurs, Calcutta
SHRI B. L. KANOD!A ( Alternate )
DR J. K. SINHA Central Mining Research Station (CSIR), Dhanbad
SHRI V. B. SONI Electrolytic Manganese Co ( Division of Union
Carbide India Ltd ), Thane
SHR! D. GaosH ( Alllrnal, )
DR M. S. VAIDYA Dbaramsi Morarji Chemical Co Ltd, Bombay
SHIU R. S. V Y AS ( Allerrl4/' )
12
BUREAU OF IN D I AN STANDARDS
Headquarters:
Manak Bhavan, 9 Bahadur Shah Zatar Marg, NEW DELHI 110002
. 331 01 31 Telegrams: Manaksanstha
Telephones. 331 1375 (Common to all Offices)
Regionill Offices: Telephone
Central : Manak Bhavan, 9, Bahadur Shah Zafar Marg, {331 01 31
NEW DELHI 110002 331 1375
*Eastern : 1/14 C.I. T. Scheme VII M, 3786 62
V.I.P. Road, Maniktola, CALCUTT A 700054
Northern : SCO 445-446, Sector 35-C, CHANDIGARH 160036 533843
Southern : C.!.T. Campus, IV Cross Road, MADRAS 600113 2350216
tWestern : Manakalaya, E9 MIOC, Marol, Andheri (East), 6329295
BOMBAY 400093
Branch Offices:
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:!:Peenya Industrial Area, 1 st Stage, Bangalore-Tumkur Road, 394955
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117/418 B Sarvodaya Nagar, KANPUR 208005 216876
Plot No. A-9, House No. 561/63, Sindhu Nagar, Kanpur Road, 55507
luCKNOW 226005
Patliputra Industrial Estate, PATNA 800013 62305
District Industries Centre Complex, Bagh-e-Ali Maidan,
S RINAGAR 190011
T.C. No. 14/1421. University p.O., Palayam, 621 04
THIRUVANANTHAPURAM 695034
Inspection Office (With Sale Point)
Pushpanjali, First Floor, 205-A, West Hig:-' Court Road. 52 51 71
Shankar Nagar Square, NAGPUR 440010
Institution of Engineers (India) Building, 1332 Shivaii Nagar, 52435
PUNE 411005 .
*Sales Ottice Calcutta is at 5 Chowringhee Approach, 276800

P.O. Princep Street, CALCUTTA
tSales Office is at Novelty Chambers, Grant Road, BOMBA)' 896528
tSales Office is at Unity Building, Narasimharaja Square, 223971
BANGALORE
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e Standard provided by BIS via BSB Edge Private Limited to Hind Heat Treatment & Testing Hou

Kota(gcb629@gmail.com) 157.38.136.101 [for non-commercial use only].

BUREAU OF INDIAN STANDARDS

Auxiliary Chemicals Subcommittee, CDC 3 18

-Rules for rounding off numerical values ( revised ).

3. PAC~ING AND MARKING

A-2. DETERMINATION OF PURITY OF SODIUM BISULPHITE

A-2.3 Calculation - Calculate the percentage of sulphur dioxide

VI = volume in ml of standard thiosulphate required for blank,

A-5. TEST FOR IRON

A·5.3 Procedure - Weigh about 10 g of the sample, dissolve in about

A-6. TEST FOR REAVY METALS

·SyecificatioD for hydrochloric acid ( ,u"nd,.1fIisiora ).

B-2. SCALE OF SAMPLING

TABLE 2 SCALE OF SAMPLING OF CONTAINERS

LOT SIZE NUMBER OF CONTAINERS

B-3. PREPARATION OF TEST SAMPLES

*Sales Ottice Calcutta is at 5 Chowringhee Approach, 276800

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