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A R T I C L E I N F O A B S T R A C T
Keywords: A highly sensitive trapezium-shaped groove photonic crystal fiber (TSG-PCF) sensor based on surface plasmon
Surface plasmon resonance (SPR) is proposed and investigated numerically in low refractive index (RI) detection range of
trapezium-shaped groove 1.181.30 by the finite element method (FEM). The trapezoidal groove is introduced, this sensor is simple in
Photonic crystal fiber sensor
structure and manufactured easily. Indium tin oxide (ITO) is set as the sensing layer for the reaction between the
Sensitivity
Resolution
core and the plasma. The influences of the structural parameters such as the holes parameters, the geometric
parameters of the trapezium-shaped groove, the ITO layer thickness and other performance parameters on the
design and sensing features of the proposed sensor are discussed comprehensively. The results show that for the
proposed TSG-PCF, the maximum wavelength and amplitude sensitivities can arrive at 9100 nm/RIU and 99
RIU− 1, the corresponding resolutions are 1.10 × 10− 5 RIU and 1.01 × 10− 4 RIU respectively in the analyte RI
from 1.18 to 1.30. Moreover, the average sensitivity of 3429 nm/RIU can be realized for the appropriate pa
rameters. The highly sensitive sensor makes the wide potential development for low RI detection in biological
and chemical sensing.
1. Introduction improved.
Some PCF-SPR sensors have been presented and designed to form the
Photonic crystal fibers (PCFs), as a kind of dielectric cylindrical op internal or external coated structures. For the internal coated structure,
tical waveguide, are composed of the air-holes and adulterated areas the film layer is coated on part of the area or the surface of the holes, and
arranged regularly in a substrate material of different refractive indexes the analyte is inside the air hole. Rifat et al. [16] proposed a structure
(RIs). PCFs have many unique properties such as wide-range tunable with the gold coated on the inside of the core and the outside of the
dispersion characteristic, very high nonlinear coefficient, and hollow larger air hole, this structure achieved a bigger birefringence and better
waveguide transmission [1–5]. Compared with the traditional fibers, sensing ability owing to the air holes of different sizes. Shui et al. [17]
PCFs have been widely applied to supercontinuum broadband light designed a special structure in which the liquid detection was intro
source, fiber laser, optical amplifier, gas and liquid sensing, etc. [6–10]. duced in the core, the silver and TiO2 films were deposited externally in
Recently, surface plasmon resonance (SPR) technology has appeared one of the two air holes in the cladding, and the TiO2 film was on the
and excited increasing attention in biological, medical, physical, and outer side of the silver film. Sharma et al. [18] demonstrated a PCF-SPR
chemical sensing due to its unique and superior characteristics, such as structure filled with the magnetic fluid and covered with the gold at the
high and easily detectable sensitivity, remote, online, and real-time air hole in the core. Moreover, the different properties of different
measurement. Sensors based on SPR stand out among multitudinous temperatures and magnetic fluid compositions were mainly analyzed
sensors, and their applications become broader, such as the measure and discussed. For the external coating structure, the sensing layer is
ment of RI range and concentration in the liquid detection [11,12], the deposited in the cladding, i.e., the analyte is outside of the cladding and
determination of gas concentration and the identification of gas types in inside of the perfect matching layer (PML). Shakya et al. [19] reported
the gas detection [13,14], the detection of biomolecules in the medical PCF-SPR with an external coating structure, the fiber was covered by the
tests [15]. Up to now, various kinds of PCF-SPR sensors have been re gold, TiO2 and analytes from the inside to the outside. Islam et al. [20]
ported, some different sensing properties have been obtained and offered an ultra-sensitive biochemical sensor only consisting of simple
* Corresponding author at: School of Measuring and Optical Engineering, Nanchang Hangkong University, Nanchang 330063, China.
E-mail address: jgy579@nchu.edu.cn (G. Jiang).
https://doi.org/10.1016/j.sbsr.2021.100452
Received 8 July 2021; Received in revised form 14 September 2021; Accepted 21 September 2021
Available online 29 September 2021
2214-1804/© 2021 Published by Elsevier B.V. This is an open access article under the CC BY-NC-ND license (http://creativecommons.org/licenses/by-nc-nd/4.0/).
Y. Wang et al. Sensing and Bio-Sensing Research 34 (2021) 100452
circular holes, using either gold or AZO (ZnO doped with 2% Al) as the allows quicker and easier placement of the analyte, facilitates replace
plasma material. In this sensor, the common materials such as the silver ment and cleaning, and the inclinations enlarge the contact area for
and graphene were not employed, but AZO, which is much rarer. faster reaction. The wavelength sensitivity, the resolution and the
Meanwhile, by comparing the two materials, the results showed that the average sensitivity of the TSG-PCF sensor are investigated and analyzed.
sensitivity, resolution and other characteristics obtained by using AZO Additionally, the confinement loss, amplitude sensitivity, and amplitude
as the plasma material were not as good as those obtained by using the resolution are also carefully studied. This will be helpful for under
gold as the plasma material. By analyzing the external coating is obvi standing and exploring the sensing performances of PCF-SPR sensors.
ously more popular than the internal coating. On the one hand, the
former is more convenient and simple, and there is no need to inject the 2. Design and theoretical model
analyte to be tested into the air holes in a complicated way, especially
for the detection of different analytes in a single channel. On the other The model was created through five steps: geometric parameters
hand, it is easier to control the thickness, length and sensing area of the setting, geometric figures creation, materials setting, PML creating, and
sensing layers, which will not only be more uniform, but also reduce the mesh setting. Based on the finite element method (FEM), the charac
difficulty of manufacturing. teristics can be calculated and relevant parameters are optimized to
In addition, the D-type and slotted structure belong to the external obtain the better results. The TSG-PCF sensor structure is shown in
coating structure. The D-type structure is derived from the partial pol Fig. 1. The PML is wrapped around the outermost part of the fiber to
ishing of the PCF structure, which is named because the remaining part absorb the radiation waves, while inside the PML, in order, are the silica-
is shaped like the capital letter D. In general, the plasma film is coated on based background material, air holes, and TSG for the analyte. Specif
the polishing plane and the tested analyte directly contacts with the ically, the circular holes of two different sizes are designed and arranged
plasma film surface, or can be injected into the holes nearest to the film in a hexagon, and the TSG is embedded below the arched hole to place
[21–23]. According to the depth and angle of polishing, the structure the analyte. In order to achieve the goal of increased sensitivity, except
can be further subdivided into the partial polishing, full polishing, single for the TSG structure, the larger size air holes are designed in the core
D-type polishing, double D-type polishing and other structures. Rela region. The diameters of the two kinds of air holes are respectively
tively speaking, the D-type structure has a greater advantage in coating, expressed by dc (= 0.8Λ) and da (= 0.5Λ), in which Λ (= 2 μm) is the
but the polishing is susceptible to problems such as the roughness and spacing between adjacent holes. For the TSG, h represents the depth of
uneven of polishing surface. For the slotted structures, the large-size the groove and td denotes the thickness of the ITO layer. The difference
outer coating channels are transformed into microfluidic channels of between the top and bottom of the TSG is represented by 2a, and its
various shapes for the better light-matter interaction. Liu et al. [24] inclination is 120◦ . In addition, dp (= 1.1Λ) is the polished depth, which
described a sensor with the U-shaped microfluidic channel (for storing can be obtained by polishing a large arched hole in the background
analytes), in which the bottom of the U-shaped groove was coated with material at the top of the fiber.
the indium tin oxide (ITO), two sides and the lower part of the U-shaped The RI of the silica is demonstrated by Sellmeier's equation [24]:
groove were covered with circular holes of different sizes.
On the other hand, to obtain various kinds of excellent sensing per A1 λ 2 A2 λ2 A3 λ2
n2 (λ) = 1 + + 2 + 2 (1)
formances, except for changing the structures to enrich the structural
2
λ − B1 λ − B2 λ − B3
diversity, the changes can also be made in plasma materials, such as the
gold, silver, copper, aluminum and other metals. Sarker et al. [25] where n is the RI of fused silica, and λ is the wavelength in μm. The
discovered a kind of slotted PCF-SPR in which the gold was applied and parameters A1, A2, A3, B1, B2, and B3 are the Sellmeier constants, which
covered on the outside of the cladding, analyzed the influences of the are 0.69616300, 0.407942600, 0.897479400, 0.00467914826,
parameters such as the wavelength, analyte RI, and slotted inclination 0.0135120631, and 97.9340025, respectively.
angle on the characteristics such as the confinement loss, sensitivity, and The frequency-dependent complex relative permittivity of ITO is
resolution. Liu et al. [26] demonstrated a partially polished D-type expressed by the Drude model [24]:
sensor in which the gold, silver, and ITO in the selection of the plasma ω2p
materials were employed and researched the effects of plasma materials εm = ε∞ − (2)
ω(ω + iγ)
contrastively, found that the gold had a higher confinement loss and was
more suitable for the further research. In addition, the researchers also where ε∞ (= 3.9) denotes the dielectric constant at infinite angular
explore other sensing materials, such as oxides, oxide-compounds, frequency, γ (= 0.111 eV) is the damping frequency of the oscillations, ω
metal-nonmetallic multilayered structures [27–30] as the sensing me presents the angular frequency, and ωp (= 2.39 eV) is the bulk plasma
diums, which not only enrich the diversity of sensing materials, but also
produce more and better performances.
Very recently, ITO as a new exciting medium has caught more and
more attention on numerous special and attractive characteristics.
Rahman et al. [31] achieved a hexagonal SPR sensor with the silicon as
the background material and ITO as the sensing layer. By comparing
three different structures, the optimal structure was determined and the
corresponding relationships between each parameter and the sensing
performances were studied. Kaur et al. [32] designed a double-coated D-
type sensor with the metal oxide ZnO added on the surface of the ITO to
achieve higher sensitivity and resolution than the single-layer ITO.
Compared with the gold, silver, and other materials, some performances
of ITO are more superior. For example, ITO can avoid the oxidation of
the silver layer, have a lower plasma frequency, and increase the
penetration depth of the plasma waves [31].
Despite the above progress, the PCF-SPR sensors are still poorly
explored for low RI detection. We present a highly sensitive trapezium-
shaped groove photonic crystal fiber (TSG-PCF) sensor. The sensor takes
on simple construction, the trapezium-shaped groove (TSG) design Fig. 1. The cross section of the proposed TSG-PCF sensor.
2
Y. Wang et al. Sensing and Bio-Sensing Research 34 (2021) 100452
where k0 indicates the wave number and can be computed by k0 = 2π/λ, The mode field properties in the TSG-PCF are investigated and
Im(neff) symbolizes the imaginary part of the index. calculated by the FEM. In simulation, we select the generic case for the
There are two conventional methods, called the wavelength inter set of the structure parameters: Λ = 2 μm, dc = Λ, da = 0.6Λ, dp = 1.1Λ, θ
rogation and amplitude interrogation methods, can be adopted for = 120◦ , h = 2.55 μm, td = 100 nm, and na = 1.22, except where
calculating sensing performance and detecting the RI range. The otherwise noted. Based on these values, the corresponding relationship
wavelength interrogation is frequently used and can be described by between the wavelength and index, as well as the electric field distri
[20]: butions of the core mode (TE and TM modes) and the surface plasmon
/ polarization (SPP) mode are emphatically investigated in Fig. 2(a), (b)
Sλ (nm/RIU) = Δλpeak Δna (4) respectively. In Fig. 2(a), as the wavelength enhances to 1480 nm from
1180 nm, the variation curve of Re(nTE) keeps decreasing monotonously
where Δλpeak and Δna stand for the difference of the adjacent resonance and slowly, while those of Re(nTM) and Re(nSPP) reduce at first, then
wavelengths and analyte RIs, respectively. In addition, the resolution is happen to change up and down at the specific point where the Re(neff) of
also a very important parameter to evaluate the performance of sensor, the TM and SPP modes intersect at the wavelength 1311 nm, and then
which can be expressed by [20]: separate and reduce accordingly again. In addition, for the Im(nTM), it
/ rapidly augments and arrives a peak value at the wavelength 1311 nm,
R(RIU) = Δna Δλmin Δλpeak (5)
and then steeply declines with the variation of wavelength. However for
where Δλmin (= 0.1 nm) depicts the minimum resolution of the the Im(nTE), it is very small and nearly keeps unchanged for the whole
spectrometer. wavelength. The reasons for these variations can be explained and
The amplitude sensitivity can be usually adopted for evaluating verified in Fig. 2(a) and (b). The Fig. 2(b) depicts the E-field distribu
effectively the sensing proprieties at a single wavelength which can be tions of three modes at the wavelengths 1260 nm, 1311 nm, and 1460
calculated by [20]: nm respectively from left to right. The E-field distributions of the TE
mode mainly concentrate on the core and there is almost no coupling
( ) 1 ∂α(λ, na ) between TE mode and SPP mode, which is why Im(nTE) barely changes.
SA RIU − 1 = − (6)
α(λ, na ) ∂na The E-field distributions of the TM and SPP modes will couple mutually,
especially at the wavelength 1311 nm most field intensity will permeate
where Δα(λ, na) stands for the difference of two adjacent losses, α(λ, na) from the TM mode to the ITO layer. According to Fig. 2(a), the
1.46 0.012
Re(nTE)
(d) Re(nTM )
0.01
1.44 Re(nspp)
Im(nTE)
0.008
Im(nTM )
1.42
Re(n eff)
Im (neff)
0.006
1.4
0.004
1.38
0.002
1.36 0
1160 1200 1240 1280 1320 1360 1400 1440 1480
Wavelength(nm)
(a)
(b)
Fig. 2. (a) The correlation between the wavelength and neff of the TE, TM, and SPP modes. (b) The electric field distributions at the wavelengths 1260 nm, 1311 nm,
and 1460 nm respectively from left to right.
3
Y. Wang et al. Sensing and Bio-Sensing Research 34 (2021) 100452
enlarges the difficulty of the interaction between the ITO and the analyte
but reduces the sensitivity. On the other hand, seen from Fig. 5, the loss
is higher at na = 1.22, td = 100 nm and the loss peak is sharper, i.e., the
full width at half maximum (FWHM) is smaller which means more ac
curate detection of the peak locations and better sensing accuracy.
The influence of the parameter a on the loss is obtained in Fig. 6. The
loss peak happens to shift but only a little when the parameter a is set to
different values for a fixed na. On the other hand, with the increase of
either of the two parameters na and a, the resonance peak always moves
towards the direction of the longer wavelength. For na = 1.22, the loss
has the variation tendency of falling after rising when the parameter a
increases from 1.0 μm to 1.1 μm and then to 1.2 μm. For na = 1.23 and
1.24, the loss spectrum constantly declines with the a varying in 1.0
μm–1.2 μm. Therefore, a = 1.1 μm is adopted for the optimized results.
For the TSG, the effect of the open-TSG depth h on the loss needs to
be considered. As the na enhances in Fig. 7, the loss lessens and the
resonance wavelength has a noticeable red shift. For na = 1.22, the loss
spectrum will decrease with the increasing h, but for h = 2.65 μm and
2.75 μm, the extent of the reduction is negligible. As the na enhances to
Fig. 3. The change between the loss and the smaller hole-diameter da for na 1.23 and 1.24, the loss increases with h, but the alteration is also
= 1.22–1.24.
4
Y. Wang et al. Sensing and Bio-Sensing Research 34 (2021) 100452
Fig. 6. The influence of the parameter a on the loss for na = 1.22, 1.23, 1.24. Fig. 8. The variation tendency of the loss with the wavelength as the RI goes
from 1.18 to 1.30.
5
Y. Wang et al. Sensing and Bio-Sensing Research 34 (2021) 100452
design, the wheel polishing technique is more widely used. After the side
polishing, the fiber needs to be coated with a thin film before the SPR
sensor can be fabricated completely. The main coating techniques
mainly include the chemical vapor deposition (CVD) and the physical
vapor deposition (including the sputtering coating and the thermal
evaporation coating) [34,36]. Each of these techniques has its own ad
vantages, for example, CVD can be used to coat on complex shapes and
can be used repeatably, the sputtering coating technique has strong film
adhesion, the thermal evaporation coating technique is easy to operate
and the film thickness can be accurately controlled. All of these tech
niques can be used for the coating of the proposed sensor.
4. Conclusions
Table 1
Performances of the TSG-PCF sensor.
Analyte RI Resonant wavelength Resonant peak shift (nm) Wavelength sensitivity (nm/ Resolution Amplitude sensitivity Resolution
(nm) RIU) (RIU) (RIU− 1) (RIU)
5 4
1.18 1244 16 1600 6.25 × 10− 24.33 4.11 × 10−
5 4
1.19 1260 16 1600 6.25 × 10− 28.11 3.56 × 10−
5 4
1.20 1276 17 1700 5.88 × 10− 34.80 2.87 × 10−
5 4
1.21 1293 18 1800 5.56 × 10− 47.78 2.09 × 10−
5 4
1.22 1311 27 2700 3.70 × 10− 99.01 1.01 × 10−
5 4
1.23 1338 28 2800 3.57 × 10− 71.76 1.39 × 10−
5 4
1.24 1366 32 3200 3.13 × 10− 60.04 1.67 × 10−
5 4
1.25 1398 38 3800 2.63 × 10− 53.26 1.88 × 10−
5 4
1.26 1436 43 4300 2.33 × 10− 48.63 2.06 × 10−
5 4
1.27 1479 50 5000 2.00 × 10− 45.39 2.20 × 10−
5 4
1.28 1529 69 6900 1.45 × 10− 42.91 2.33 × 10−
5 4
1.29 1598 91 9100 1.10 × 10− 41.00 2.44 × 10−
1.30 1689 N/A N/A N/A N/A N/A
6
Y. Wang et al. Sensing and Bio-Sensing Research 34 (2021) 100452
reported in the manuscript and have given their written permission to be [17] X. Shui, Q. Gu, X. Jiang, G. Si, Surface plasmon resonance sensor based on polymer
liquid-core fiber for refractive index detection, Photonics 7 (4) (2020) 123.
named.
[18] A.K. Sharma, V. Popescu, Magnetic field sensor with truncated honeycomb
photonic crystal fiber: analysis under the variations in magnetic fluid composition
Declaration of Competing Interest and temperature for high performance in near infrared, Opt. Quant. Electron. 53
(3) (2021) 1–14.
[19] A.K. Shakya, S. Singh, Design and analysis of dual polarized Au and TiO2-coated
The authors declare that they have no known competing financial photonic crystal fiber surface plasmon resonance refractive index sensor: an
interests or personal relationships that could have appeared to influence extraneous sensing approach, J. Nanophot. 15 (1) (2021).
the work reported in this paper. [20] M.R. Islam, A.N.M. Iftekher, K.R. Hasan, J. Nayen, S.B. Islam, M.M. Islam Khan, J.
A. Chowdhury, F. Mehjabin, M. Islam, M.S. Islam, Design and analysis of a
biochemical sensor based on surface plasmon resonance with ultra-high sensitivity,
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