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Original Content:
My research and interest focus on the study of the coupling between mechanics,
transport and chemistry in porous media (THMC behavior). In, these phenomena are
ubiquitous in nature and are of paramount importance in hot topics like CCS (Carbon
Capture and storage), EOR (Enhanced Oil Recovery) , in the development of
geothermal applications, or in the shaping of a natural landscapes like karsts.
Research statement
PhD Research
I did my PhD in Laboratoire Navier about the coupling between evaporation,
precipitation and mechanics during CCS in a deep saline aquifer? Indeed, it has
been shown several times that injectionof CO2 in a saline aquifer triggers a strong
evaporation of the brine which is initially saturating the aquifer. This
evaporation leads to a strong precipitation of the salts initially dissolved in the
brine. The main consequence of this precipitation is the clogging of the porosity
and the sharp consecutive decrease of the permeability and injectivity, by blocking
the percolation path of CO2. However, in the civil engineering area , precipitation
of salts in a porous matrix is known to create stresses (called crystallization
pressure), high enough to fracture the material. This phenomenon is particularly
visible in buildings subjected to slat sprays or capillary rise of salty water. The
main idea was then to adapt the knowledge of crystallization pressure from civil
engineering and apply it to CCS.
To do so, we have used a semi-analytical approach combining simulations and
modeling of the flow-through drying of a porous medium and the consecutive
precipitation; with an experimental study on a new reactive percolation prototype
designed within the framework of the project. The conception has been made with
Sanchez Technologies, and the set-up is now one of the main equipment of
Laboratoire Navier. It is able to inject simultaneously two fluids with a constant
pressure or flow rate in a sample within a triaxial cell, with a control on
temperature. Temperature and pressure can be set as high as 150° and 300 bars which
allows in particular to use supercritical CO2 which is the most probable state for
CCS. Thanks to the triaxial cell, the system is able to apply and measure stresses,
and thus measure the mechanical effects associated with the injection.
The combination of modeling and experiments allowed us to estimated the
crystallization pressure which can be created during CCS and to differentiate two
time scales depending on the considered pore size : at short times is created a
transient and intense crystallization pressure, while at longer times the
crystallization pressure is lower and is created by a thermodynamic equilibrium
(Osselin et al. - Env. Geotech. 2014 - Osselin et al. - EPJ-AP 2013, Osselin et al.
Vth Biot conf. 2013). Thanks to the experimental set-up, we have also measured the
relative permeability curves for sample of Vosges sandstone with the fluid pairs
water/gaseous CO2, and water supercritical CO2. Surprisingly, we observed only a
very small difference between the two curves, confirming the hypothesis that
relative permeability and capillary pressure are intrinsic characteristics of a
core and do not depend on the fluids considered (Osselin et al. submitted to CRAS
Geotechnique).
Future Research
Current Research
As underlined by my different researches, my interest is on coupled processes in
porous media. I wish to dig further in the coupling between reactive transport and
mechanics, especially in hot topics like CCS, EOR, or civil engineering
(particularly concrete whose chemistry is particularly challenging). I am
especially interesting in bringin more microfluidics into this research areas, and
go beyond the pore networks. Microfluidics is a very powerful tool which can
provide numerous invaluable results.
I am currently at the University of Warsaw as a postdoctoral researcher in Piotr
Szymczak's team. The goal of my research is to develop and use an experiment
allowing to observe the dissolution phenomena in fractures, with a controlled and
reproducible manner; and to compare results with the models and simulations done in
the team. Indeed, the theoretical part and numerical part of the study of the
dissolution instability are relatively well developed and known, but the
experimental part is lacking a good control of the experimental parameters and
repeatability. Indeed, most of the experiments in the literature where proceeded
with natural cores (Hoefner and Fogler 88, Fredd and Fogler 98, or more recently
Menke et al. 2015), which along with the already mentioned shortcomings, present a
real issue of the observation (even if the development of 4D X-ray tomography tends
to solve the problem). Other experiments, among which the famous experiments from
Daccord (Nature 87) use a 2D geometry but without real control of the paths
followed by the fluid.
Numerical simulations show the strong sensitivity of the patterns created by the
dissolution with parameters such as flow rate, porosity (or fracture aperture),
sample size... Patterns can go from homogeneous dissolution, to a flat front, with
a whole range of fingering and fingering competition in between. One of the major
goal of this research is for example EOR and oil reservoir stimulation by the
injection of dissolving fluid. The precise knowledge of the flow rate and the
reactant quantity in order to get the most optimized permeability increase is
obviously extremely important. Other applications can be found in the shaping of
natural landscapes, such as karsts, or at a smaller scale dissolution pipes, or
even the petrified forest in Victoria, Australia, which is actually not a petrified
forest but a combination of precipitation and dissolution in a limestone landscape.
During the conception of the experiment, emphasis has been put on the control of
parameters and repeatability. We have then decided to use the power of
microfluidics and use a Hele-Shaw cell, which allows to simulate the behavior of a
fracture but also a direct observation of the process : the bottom part consists of
the soluble material while the top part consists in transparent polycarbonate. The
soluble material chosen is gypsum (plaster of Paris) which has the double advantage
of being soluble in pure water, and can also be molded in every wanted geometry.
Experiments has been carried out in Piotr Garstecki lab and have given very
interesting results : obtained patterns are very similar to the numerical
simulations, and in particular, there is a very good match between the theoretical
prediction of the initial instability and the experimental measure (results will be
soon submitted).
For the following, we wish to broaden the experiments, adding obstacles with the
plaster, creating layers of different thickness to investigate the effect of a
porosity change, or complexifying the chemistry by adding a precipitation reaction
triggers by the dissolution in order to study the competition between he positive
feedback of dissolution and negative feedback of precipitation.

Rewritten Content:
My studies and interest consciousness on the observe of the coupling among
mechanics, transport and chemistry in porous media (THMC conduct). In, those
phenomena are ubiquitous in nature and are of paramount significance in hot topics
like CCS (Carbon capture and storage), EOR (more suitable Oil recuperation) , in
the development of geothermal packages, or in the shaping of a herbal landscapes
like karsts.
research declaration
PhD studies
I did my PhD in Laboratoire Navier approximately the coupling among evaporation,
precipitation and mechanics all through CCS in a deep saline aquifer? indeed, it
has been shown numerous times that injectionof CO2 in a saline aquifer triggers a
robust evaporation of the brine that is to begin with saturating the aquifer. This
evaporation results in a sturdy precipitation of the salts to begin with dissolved
in the brine. the primary effect of this precipitation is the clogging of the
porosity and the sharp consecutive decrease of the permeability and injectivity,
via blockading the percolation route of CO2. but, within the civil engineering
vicinity , precipitation of salts in a porous matrix is known to create stresses
(called crystallization pressure), excessive sufficient to fracture the fabric.
This phenomenon is especially seen in buildings subjected to slat sprays or
capillary rise of salty water. the main concept was then to adapt the knowledge of
crystallization strain from civil engineering and apply it to CCS.
To do so, we've got used a semi-analytical method combining simulations and
modeling of the float-thru drying of a porous medium and the consecutive
precipitation; with an experimental observe on a new reactive percolation prototype
designed within the framework of the challenge. The concept has been made with
Sanchez technology, and the set-up is now one of the fundamental equipment of
Laboratoire Navier. it may inject simultaneously fluids with a constant stress or
glide charge in a sample inside a triaxial cell, with a control on temperature.
Temperature and stress may be set as excessive as 150° and 300 bars which lets in
in particular to apply supercritical CO2 that's the maximum probable state for CCS.
way to the triaxial cell, the machine is able to practice and measure stresses, and
for that reason measure the mechanical effects associated with the injection.
The mixture of modeling and experiments allowed us to predicted the crystallization
pressure which may be created throughout CCS and to distinguish two time scales
depending on the considered pore size : at brief instances is created a temporary
and severe crystallization strain, at the same time as at longer instances the
crystallization strain is decrease and is created by using a thermodynamic
equilibrium (Osselin et al. - Env. Geotech. 2014 - Osselin et al. - EPJ-AP 2013,
Osselin et al. Vth Biot conf. 2013). way to the experimental set-up, we've got also
measured the relative permeability curves for sample of Vosges sandstone with the
fluid pairs water/gaseous CO2, and water supercritical CO2. fairly, we determined
simplest a very small difference among the two curves, confirming the speculation
that relative permeability and capillary pressure are intrinsic traits of a middle
and do now not rely upon the fluids considered (Osselin et al. submitted to CRAS
Geotechnique).
future studies
modern-day research
As underlined with the aid of my distinctive researches, my hobby is on coupled
approaches in porous media. I want to dig further within the coupling between
reactive delivery and mechanics, especially in warm topics like CCS, EOR, or civil
engineering (mainly concrete whose chemistry is specifically hard). i'm specially
interesting in bringin greater microfluidics into this research regions, and cross
past the pore networks. Microfluidics is a completely powerful device that could
offer numerous helpful outcomes.
i am currently on the university of Warsaw as a postdoctoral researcher in Piotr
Szymczak's crew. The intention of my studies is to broaden and use an test
permitting to take a look at the dissolution phenomena in fractures, with a
controlled and reproducible way; and to evaluate results with the models and
simulations finished inside the group. certainly, the theoretical element and
numerical a part of the take a look at of the dissolution instability are rather
nicely advanced and recognized, however the experimental component is lacking an
amazing control of the experimental parameters and repeatability. indeed, most of
the experiments within the literature wherein proceeded with herbal cores (Hoefner
and Fogler 88, Fredd and Fogler ninety eight, or extra these days Menke et al.
2015), which in conjunction with the already stated shortcomings, present a real
difficulty of the statement (even supposing the improvement of 4D X-ray tomography
tends to solve the hassle). different experiments, amongst which the well-known
experiments from Daccord (Nature 87) use a 2d geometry but without real manage of
the trails followed by means of the fluid.
Numerical simulations show the sturdy sensitivity of the patterns created by using
the dissolution with parameters consisting of go with the flow rate, porosity (or
fracture aperture), sample size... styles can pass from homogeneous dissolution, to
a flat the front, with a whole variety of fingering and fingering opposition in
among. one of the major aim of this research is for instance EOR and oil reservoir
stimulation via the injection of dissolving fluid. the ideal expertise of the go
with the flow rate and the reactant amount so one can get the most optimized
permeability boom is manifestly extraordinarily vital. other programs may be
observed within the shaping of natural landscapes, consisting of karsts, or at a
smaller scale dissolution pipes, or even the petrified wooded area in Victoria,
Australia, which is simply no longer a petrified wooded area but a aggregate of
precipitation and dissolution in a limestone landscape.
at some stage in the theory of the experiment, emphasis has been placed on the
manage of parameters and repeatability. we've got then decided to use the
electricity of microfluidics and use a Hele-Shaw mobile, which lets in to simulate
the conduct of a fracture but also an immediate commentary of the manner : the
lowest component consists of the soluble material while the top element is composed
in transparent polycarbonate. The soluble cloth chosen is gypsum (plaster of Paris)
which has the double benefit of being soluble in natural water, and also can be
molded in every wanted geometry. Experiments has been done in Piotr Garstecki lab
and feature given very thrilling outcomes : obtained patterns are very similar to
the numerical simulations, and specifically, there may be a excellent match among
the theoretical prediction of the initial instability and the experimental degree
(effects may be soon submitted).
For the following, we wish to broaden the experiments, adding barriers with the
plaster, growing layers of different thickness to investigate the impact of a
porosity change, or complexifying the chemistry with the aid of including a
precipitation response triggers by using the dissolution with a purpose to have a
look at the opposition between he nice remarks of dissolution and terrible comments
of precipitation.

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